APPENDIX B Laboratory Chemical Analysis
Transcript of APPENDIX B Laboratory Chemical Analysis
Phase 2 Ground Investigation Poundstretchers, Gorseinon Rd, Gorseinon
795.02.01, November 2020
36
APPENDIX B Laboratory Chemical Analysis
Eurofins Chemtest Ltd
Depot Road
Newmarket
CB8 0AL
Tel: 01638 606070
Email: [email protected]
Report No.: 20-28339-1
Initial Date of Issue: 22-Oct-2020
Client Remada Ltd
Client Address: Forward House
17 High Street
Henley in Arden
B95 5AA
Contact(s): Greg Jones
Peter Dickinson
Project 795.01 Gorseinon
Quotation No.: Date Received: 21-Oct-2020
Order No.: 795.01 Date Instructed: 21-Oct-2020
No. of Samples: 2
Turnaround (Wkdays): 5 Results Due: 27-Oct-2020
Date Approved: 22-Oct-2020
Approved By:
Details: Glynn Harvey, Technical Manager
Final Report
Page 1 of 4
Results - Soil
Client: Remada Ltd 20-28339 20-28339
Quotation No.: 1083733 1083734
Order No.: 795.01 801.01 801.01
BH1 BH2
BH1 BH1
SOIL SOIL
0.00 0.00
0.05 0.05
19-Oct-2020 20-Oct-2020
Determinand Accred. SOP Units LOD
Moisture N 2030 % 0.020 < 0.020 < 0.020
Soil Colour N 2040 N/A Black Black
Other Material N 2040 N/A None None
Soil Texture N 2040 N/A Tarmac Tarmac
Naphthalene M 2700 mg/kg 0.10 < 0.10 < 0.10
Acenaphthylene M 2700 mg/kg 0.10 < 0.10 < 0.10
Acenaphthene M 2700 mg/kg 0.10 < 0.10 < 0.10
Fluorene M 2700 mg/kg 0.10 < 0.10 < 0.10
Phenanthrene M 2700 mg/kg 0.10 < 0.10 < 0.10
Anthracene M 2700 mg/kg 0.10 < 0.10 < 0.10
Fluoranthene M 2700 mg/kg 0.10 < 0.10 < 0.10
Pyrene M 2700 mg/kg 0.10 < 0.10 < 0.10
Benzo[a]anthracene M 2700 mg/kg 0.10 < 0.10 < 0.10
Chrysene M 2700 mg/kg 0.10 < 0.10 < 0.10
Benzo[b]fluoranthene M 2700 mg/kg 0.10 < 0.10 < 0.10
Benzo[k]fluoranthene M 2700 mg/kg 0.10 < 0.10 < 0.10
Benzo[a]pyrene M 2700 mg/kg 0.10 < 0.10 < 0.10
Indeno(1,2,3-c,d)Pyrene M 2700 mg/kg 0.10 < 0.10 < 0.10
Dibenz(a,h)Anthracene M 2700 mg/kg 0.10 < 0.10 < 0.10
Benzo[g,h,i]perylene M 2700 mg/kg 0.10 < 0.10 < 0.10
Coronene N 2700 mg/kg 0.10 < 0.10 < 0.10
Total Of 17 PAH's N 2700 mg/kg 2.0 < 2.0 < 2.0
Project: 795.01 Gorseinon
Top Depth (m):
Bottom Depth (m):
Chemtest Job No.:
Chemtest Sample ID.:
Client Sample Ref.:
Client Sample ID.:
Sample Type:
Date Sampled:
Sample Location:
Page 2 of 4
Test Methods
SOP Title Parameters included Method summary
2030
Moisture and Stone Content of
Soils(Requirement of
MCERTS)
Moisture content
Determination of moisture content of soil as a
percentage of its as received mass obtained at
<37°C.
2040Soil Description(Requirement of
MCERTS)Soil description
As received soil is described based upon
BS5930
2700
Speciated Polynuclear
Aromatic Hydrocarbons (PAH)
in Soil by GC-FID
Acenaphthene; Acenaphthylene; Anthracene;
Benzo[a]Anthracene; Benzo[a]Pyrene;
Benzo[b]Fluoranthene; Benzo[ghi]Perylene;
Benzo[k]Fluoranthene; Chrysene;
Dibenz[ah]Anthracene; Fluoranthene; Fluorene;
Indeno[123cd]Pyrene; Naphthalene;
Phenanthrene; Pyrene
Dichloromethane extraction / GC-FID (GC-FID
detection is non-selective and can be subject to
interference from co-eluting compounds)
Page 3 of 4
Report Information
Key
U UKAS accredited
M MCERTS and UKAS accredited
N Unaccredited
SThis analysis has been subcontracted to a UKAS accredited laboratory that is accredited for
this analysis
SNThis analysis has been subcontracted to a UKAS accredited laboratory that is not accredited
for this analysis
T This analysis has been subcontracted to an unaccredited laboratory
I/S Insufficient Sample
U/S Unsuitable Sample
N/E not evaluated
< "less than"
> "greater than"
Comments or interpretations are beyond the scope of UKAS accreditation
The results relate only to the items tested
Uncertainty of measurement for the determinands tested are available upon request
None of the results in this report have been recovery corrected
All results are expressed on a dry weight basis
The following tests were analysed on samples as received and the results subsequently
corrected to a dry weight basis TPH, BTEX, VOCs, SVOCs, PCBs, Phenols
For all other tests the samples were dried at < 37°C prior to analysis
All Asbestos testing is performed at the indicated laboratory
Issue numbers are sequential starting with 1 all subsequent reports are incremented by 1
Sample Deviation Codes
A - Date of sampling not supplied
B - Sample age exceeds stability time (sampling to extraction)
C - Sample not received in appropriate containers
D - Broken Container
E - Insufficient Sample (Applies to LOI in Trommel Fines Only)
Sample Retention and Disposal
All soil samples will be retained for a period of 45 days from the date of receipt
All water samples will be retained for 14 days from the date of receipt
Charges may apply to extended sample storage
If you require extended retention of samples, please email your requirements to:
Page 4 of 4
Eurofins Chemtest Ltd
Depot Road
Newmarket
CB8 0AL
Tel: 01638 606070
Email: [email protected]
Report No.: 20-27828-1
Initial Date of Issue: 21-Oct-2020
Client Remada Ltd
Client Address: Forward House
17 High Street
Henley in Arden
B95 5AA
Contact(s): Peter Dickinson
Greg Jones
Project 795.02 Gorseinon
Quotation No.: Date Received: 15-Oct-2020
Order No.: Date Instructed: 15-Oct-2020
No. of Samples: 5
Turnaround (Wkdays): 5 Results Due: 21-Oct-2020
Date Approved: 21-Oct-2020
Approved By:
Details: Glynn Harvey, Technical Manager
Final Report
Page 1 of 10
Results - Soil
Client: Remada Ltd 20-27828 20-27828 20-27828 20-27828 20-27828
Quotation No.: 1081041 1081042 1081043 1081044 1081045
1 2 3 4 5
WS1 WS2 WS3 WS4 WS5
SOIL SOIL SOIL SOIL SOIL
0.15 1.10 0.40 0.80 0.80
0.35 1.40 0.60 1.00 0.90
13-Oct-2020 13-Oct-2020 13-Oct-2020 13-Oct-2020 13-Oct-2020
LIVERPOOL LIVERPOOL LIVERPOOL LIVERPOOL LIVERPOOL
Determinand Accred. SOP Units LOD
ACM Type U 2192 N/A - - - - -
Asbestos Identification U 2192 N/ANo Asbestos
Detected
No Asbestos
Detected
No Asbestos
Detected
No Asbestos
Detected
No Asbestos
Detected
ACM Detection Stage U 2192 N/A - - - - -
Moisture N 2030 % 0.020 9.4 15 7.3 10 < 0.020
Soil Colour N 2040 N/A Brown Brown Brown Brown Black
Other Material N 2040 N/A Stones Stones Stones Stones None
Soil Texture N 2040 N/A Sand Sand Sand Clay Tarmac
Chromatogram (TPH) N N/A See Attached See Attached See Attached See Attached See Attached
pH M 2010 4.0 8.6 8.6 9.5 8.8 8.7
Boron (Hot Water Soluble) M 2120 mg/kg 0.40 0.74 0.67 < 0.40 < 0.40 0.60
Arsenic M 2450 mg/kg 1.0 21 21 22 26 120
Beryllium U 2450 mg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Cadmium M 2450 mg/kg 0.10 0.35 0.43 0.34 0.42 2.5
Copper M 2450 mg/kg 0.50 52 46 37 46 580
Mercury M 2450 mg/kg 0.10 0.14 0.15 < 0.10 0.14 0.29
Nickel M 2450 mg/kg 0.50 34 23 12 25 31
Lead M 2450 mg/kg 0.50 58 59 47 90 830
Selenium M 2450 mg/kg 0.20 0.53 0.50 < 0.20 0.32 0.41
Vanadium U 2450 mg/kg 5.0 75 18 15 49 31
Zinc M 2450 mg/kg 0.50 130 110 77 160 2500
Chromium (Trivalent) N 2490 mg/kg 1.0 67 16 17 68 53
Chromium (Hexavalent) N 2490 mg/kg 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50
Fraction of Organic Carbon M 2625 0.0010 0.036 0.082 0.024 0.029 0.10
Aliphatic TPH >C5-C6 N 2680 mg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Aliphatic TPH >C6-C8 N 2680 mg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Aliphatic TPH >C8-C10 M 2680 mg/kg 1.0 < 1.0 < 1.0 35 5.6 < 1.0
Aliphatic TPH >C10-C12 M 2680 mg/kg 1.0 < 1.0 < 1.0 12 21 < 1.0
Aliphatic TPH >C12-C16 M 2680 mg/kg 1.0 < 1.0 < 1.0 7.3 15 < 1.0
Aliphatic TPH >C16-C21 M 2680 mg/kg 1.0 < 1.0 < 1.0 5.2 19 < 1.0
Aliphatic TPH >C21-C35 M 2680 mg/kg 1.0 15 14 30 93 < 1.0
Aliphatic TPH >C35-C44 N 2680 mg/kg 1.0 < 1.0 < 1.0 8.6 30 < 1.0
Total Aliphatic Hydrocarbons N 2680 mg/kg 5.0 15 14 99 180 < 5.0
Aromatic TPH >C5-C7 N 2680 mg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Aromatic TPH >C7-C8 N 2680 mg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Aromatic TPH >C8-C10 M 2680 mg/kg 1.0 < 1.0 < 1.0 97 160 < 1.0
Aromatic TPH >C10-C12 M 2680 mg/kg 1.0 < 1.0 < 1.0 34 59 < 1.0
Project: 795.02 Gorseinon
Top Depth (m):
Bottom Depth (m):
Asbestos Lab:
Chemtest Job No.:
Chemtest Sample ID.:
Client Sample ID.:
Sample Type:
Date Sampled:
Sample Location:
Page 2 of 10
Results - Soil
Client: Remada Ltd 20-27828 20-27828 20-27828 20-27828 20-27828
Quotation No.: 1081041 1081042 1081043 1081044 1081045
1 2 3 4 5
WS1 WS2 WS3 WS4 WS5
SOIL SOIL SOIL SOIL SOIL
0.15 1.10 0.40 0.80 0.80
0.35 1.40 0.60 1.00 0.90
13-Oct-2020 13-Oct-2020 13-Oct-2020 13-Oct-2020 13-Oct-2020
LIVERPOOL LIVERPOOL LIVERPOOL LIVERPOOL LIVERPOOL
Determinand Accred. SOP Units LOD
Project: 795.02 Gorseinon
Top Depth (m):
Bottom Depth (m):
Asbestos Lab:
Chemtest Job No.:
Chemtest Sample ID.:
Client Sample ID.:
Sample Type:
Date Sampled:
Sample Location:
Aromatic TPH >C12-C16 M 2680 mg/kg 1.0 < 1.0 < 1.0 35 85 < 1.0
Aromatic TPH >C16-C21 U 2680 mg/kg 1.0 4.1 3.8 100 270 < 1.0
Aromatic TPH >C21-C35 M 2680 mg/kg 1.0 64 79 340 1700 < 1.0
Aromatic TPH >C35-C44 N 2680 mg/kg 1.0 < 1.0 < 1.0 29 180 < 1.0
Total Aromatic Hydrocarbons N 2680 mg/kg 5.0 69 83 630 2500 < 5.0
Total Petroleum Hydrocarbons N 2680 mg/kg 10.0 83 97 730 2700 < 10
Naphthalene M 2700 mg/kg 0.10 < 0.10 2.0 0.60 0.72 < 0.10
Acenaphthylene M 2700 mg/kg 0.10 < 0.10 0.50 0.30 0.78 < 0.10
Acenaphthene M 2700 mg/kg 0.10 < 0.10 3.6 0.39 1.3 < 0.10
Fluorene M 2700 mg/kg 0.10 < 0.10 4.0 0.45 1.2 < 0.10
Phenanthrene M 2700 mg/kg 0.10 < 0.10 7.9 3.1 7.1 < 0.10
Anthracene M 2700 mg/kg 0.10 < 0.10 2.8 1.1 2.8 < 0.10
Fluoranthene M 2700 mg/kg 0.10 < 0.10 12 7.4 20 < 0.10
Pyrene M 2700 mg/kg 0.10 < 0.10 11 6.8 20 < 0.10
Benzo[a]anthracene M 2700 mg/kg 0.10 < 0.10 4.6 5.0 13 < 0.10
Chrysene M 2700 mg/kg 0.10 < 0.10 5.3 4.7 11 < 0.10
Benzo[b]fluoranthene M 2700 mg/kg 0.10 < 0.10 7.8 7.0 17 < 0.10
Benzo[k]fluoranthene M 2700 mg/kg 0.10 < 0.10 3.3 2.5 6.6 < 0.10
Benzo[a]pyrene M 2700 mg/kg 0.10 < 0.10 5.8 5.3 14 < 0.10
Indeno(1,2,3-c,d)Pyrene M 2700 mg/kg 0.10 < 0.10 3.6 3.6 9.1 < 0.10
Dibenz(a,h)Anthracene M 2700 mg/kg 0.10 < 0.10 1.5 1.3 2.7 < 0.10
Benzo[g,h,i]perylene M 2700 mg/kg 0.10 < 0.10 3.6 3.4 9.3 < 0.10
Total Of 16 PAH's M 2700 mg/kg 2.0 < 2.0 79 53 140 < 2.0
Benzene M 2760 µg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Toluene M 2760 µg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Ethylbenzene M 2760 µg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
m & p-Xylene M 2760 µg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
o-Xylene M 2760 µg/kg 1.0 < 1.0 < 1.0 < 1.0 < 1.0 < 1.0
Total Phenols M 2920 mg/kg 0.30 < 0.30 < 0.30 < 0.30 < 0.30 < 0.30
Page 3 of 10
TPH Chromatogram on Soil Sample: 1081041
Page 4 of 10
TPH Chromatogram on Soil Sample: 1081042
Page 5 of 10
TPH Chromatogram on Soil Sample: 1081043
Page 6 of 10
TPH Chromatogram on Soil Sample: 1081044
Page 7 of 10
TPH Chromatogram on Soil Sample: 1081045
Page 8 of 10
Test Methods
SOP Title Parameters included Method summary
2010 pH Value of Soils pH pH Meter
2030
Moisture and Stone Content of
Soils(Requirement of
MCERTS)
Moisture content
Determination of moisture content of soil as a
percentage of its as received mass obtained at
<37°C.
2040Soil Description(Requirement of
MCERTS)Soil description
As received soil is described based upon
BS5930
2120Water Soluble Boron, Sulphate,
Magnesium & ChromiumBoron; Sulphate; Magnesium; Chromium Aqueous extraction / ICP-OES
2192 Asbestos Asbestos Polarised light microscopy / Gravimetry
2450 Acid Soluble Metals in Soils
Metals, including: Arsenic; Barium; Beryllium;
Cadmium; Chromium; Cobalt; Copper; Lead;
Manganese; Mercury; Molybdenum; Nickel;
Selenium; Vanadium; Zinc
Acid digestion followed by determination of
metals in extract by ICP-MS.
2490 Hexavalent Chromium in Soils Chromium [VI]
Soil extracts are prepared by extracting dried
and ground soil samples into boiling water.
Chromium [VI] is determined by ‘Aquakem 600’
Discrete Analyser using 1,5-diphenylcarbazide.
2625 Total Organic Carbon in Soils Total organic Carbon (TOC)
Determined by high temperature combustion
under oxygen, using an Eltra elemental
analyser.
2680 TPH A/A Split
Aliphatics: >C5–C6, >C6–C8,>C8–C10,
>C10–C12, >C12–C16, >C16–C21, >C21–
C35, >C35– C44Aromatics: >C5–C7, >C7–C8,
>C8– C10, >C10–C12, >C12–C16, >C16– C21,
>C21– C35, >C35– C44
Dichloromethane extraction / GCxGC FID
detection
2700
Speciated Polynuclear
Aromatic Hydrocarbons (PAH)
in Soil by GC-FID
Acenaphthene; Acenaphthylene; Anthracene;
Benzo[a]Anthracene; Benzo[a]Pyrene;
Benzo[b]Fluoranthene; Benzo[ghi]Perylene;
Benzo[k]Fluoranthene; Chrysene;
Dibenz[ah]Anthracene; Fluoranthene; Fluorene;
Indeno[123cd]Pyrene; Naphthalene;
Phenanthrene; Pyrene
Dichloromethane extraction / GC-FID (GC-FID
detection is non-selective and can be subject to
interference from co-eluting compounds)
2760
Volatile Organic Compounds
(VOCs) in Soils by Headspace
GC-MS
Volatile organic compounds, including BTEX
and halogenated Aliphatic/Aromatics.(cf.
USEPA Method 8260)*please refer to UKAS
schedule
Automated headspace gas chromatographic
(GC) analysis of a soil sample, as received,
with mass spectrometric (MS) detection of
volatile organic compounds.
2920 Phenols in Soils by HPLC
Phenolic compounds including Resorcinol,
Phenol, Methylphenols, Dimethylphenols, 1-
Naphthol and TrimethylphenolsNote:
chlorophenols are excluded.
60:40 methanol/water mixture extraction,
followed by HPLC determination using
electrochemical detection.
Page 9 of 10
Report Information
Key
U UKAS accredited
M MCERTS and UKAS accredited
N Unaccredited
SThis analysis has been subcontracted to a UKAS accredited laboratory that is accredited for
this analysis
SNThis analysis has been subcontracted to a UKAS accredited laboratory that is not accredited
for this analysis
T This analysis has been subcontracted to an unaccredited laboratory
I/S Insufficient Sample
U/S Unsuitable Sample
N/E not evaluated
< "less than"
> "greater than"
Comments or interpretations are beyond the scope of UKAS accreditation
The results relate only to the items tested
Uncertainty of measurement for the determinands tested are available upon request
None of the results in this report have been recovery corrected
All results are expressed on a dry weight basis
The following tests were analysed on samples as received and the results subsequently
corrected to a dry weight basis TPH, BTEX, VOCs, SVOCs, PCBs, Phenols
For all other tests the samples were dried at < 37°C prior to analysis
All Asbestos testing is performed at the indicated laboratory
Issue numbers are sequential starting with 1 all subsequent reports are incremented by 1
Sample Deviation Codes
A - Date of sampling not supplied
B - Sample age exceeds stability time (sampling to extraction)
C - Sample not received in appropriate containers
D - Broken Container
E - Insufficient Sample (Applies to LOI in Trommel Fines Only)
Sample Retention and Disposal
All soil samples will be retained for a period of 45 days from the date of receipt
All water samples will be retained for 14 days from the date of receipt
Charges may apply to extended sample storage
If you require extended retention of samples, please email your requirements to:
Page 10 of 10