AP42 Section: 9.10.1.2 Background Chapter · P42 chapter and section. The file name...

AP42 Section:

Background Chapter Reference:

Title:

9.10.1.2

16

Results of the February 22-24, 1994, Air Emission Compliance Testing of Process Sources at the American Crystal Sugar East Grand Forks Plant, Interpoll Laboratories, Inc., Circle Pines, MN,

March 21, 1994.

EPA

Text Box

Note: This is a reference cited in AP 42, Compilation of Air Pollutant Emission Factors, Volume I Stationary Point and Area Sources. AP42 is located on the EPA web site at www.epa.gov/ttn/chief/ap42/ The file name refers to the reference number, the AP42 chapter and section. The file name "ref02_c01s02.pdf" would mean the reference is from AP42 chapter 1 section 2. The reference may be from a previous version of the section and no longer cited. The primary source should always be checked.

Interpoll Laboratories, Inc. 4500 Ball Road N.E.

Circle Pines, Minnesota 55014-1819

TEL: (612) 786-6020 FAX: (612) 786-7854

RESULTS OF THE FEBRUARY 22 - 24, 1994 AIR EMISSION COMPLIANCE TESTING

OF PROCESS SOURCES AT THE AMERICAN CRYSTAL SUGAR

EAST GRAND FORKS PLANT

Submitted to:

AMERICAN CRYSTAL SUGAR COMPANY Business Highway 220

P.O. Box 357 East Grand Forks, Minnesota 56721

Attention:

Bruce Keifenheim

Approved by:

Report Number 4-2326 March 21, 1994 SP/slp

Daniel Desgn /

Manager Stationary Source Testing Department

INTRODUCTION

24, 1994 Interpol1 Laboratories Personnel conductedState Air

EMISSION

POLLUTANT

"A" Pulp Dryer Stack

"B" Pulp Dryer Stack

"C" Pulp Dryer Stack

No. 1 Boiler Stack

No. 2 Boiler Stack

n Nuessmeier performed

ities and plant operation

dell of ACS. A member

PA Methods 1 - 5, CFR

terminations of the gas

on at each site to allow

sample withdrawal. An

ns in the abovecited

ed probe. Wet catch

?

E

0 m

c L W E

W 4 . c , m m -c 0 3 Y VI o w

-4.8 c L c Y ~ S

m x x n u

m m x m L

m - U Y V I

- L O W l L

- a O L U N O C

m % P L L - 0 m 3 3 a u

n a m L V I

W W U W c c

W Y . - c 4A c u

O W L 1

V I 0 w w o 0 c - l

O Y m

* l

e

P

I

0

c

c 0

S Y I- b

w

I O N I N 0

m

O

I O N I N 0

m

U

I O N I N 0

m

Y YI W I.,

L 0

al 4A m 0

m N w rl \ m N O rl

m 0 O 4 \ 0 0 N - O m 4 4 x

rn 0

m

rn X a - W C 0 U

W L W 3 VI S II L

W E

+ 7

W Y

L m

VI VI

W 0 0 L a c

O N m N 0 0 0 N m m w m w 0 4 m o r - . w m m ~

4 U N f . . . m N u -. m m 0 u w m m 0 0 m P N m -if. . .

m o u r- 0 0 0 N - m m - m o m m o r - . m w m O P N . . . . * N O . rnm 0 u w m m 0 0 m U N m - 4 - . .

m N m w 0 0 0 m N N m O N 0 m w m p . . m m rl UY) N f . . . m Nul . O m .-I o m m m 0 0 - O N m - h . . ,4

w

- U I 0 W 0 -

W L II Y

L al P E 0) Y

w

m

m c3

- x 0 - - u s

C W

. - O W 0 Y.0 D L - L a+ w m x - o u o c P E 0

o c c m

0

VI

m 0

..?

C 0

cl c

m

m

-?

L

> 0

Y W C

Y 0 VI

U

r

E + .r

> VI VI W

L U 0 0 L .. a L 0

0 LL z *

W 0

I

2 SUMMARY AND DISCUSSION

POINT SOU

1 No. 1 Boiler

2 No. 2 Boiler

EMISSION

POINT SOURCE Emission Rate

Note that the avera

samples each as an error i Id resulted in double sampling of lasks 43-48, which

the basis of these fac

at the time the test was performed.

4

K

0

L W E

w a f u m m w u

m - - z 0 3 u m o w .-e c L . - u m c m x z n o

m - ourn m m x m L - L o

w u -=. o iu

m >,PL

m z s i p &

o a m

N O c

L F ( 3

L m

w w u w

.Kr w u - .K c c 3

O W L *

m o

)

o u m

3 m u _ - m o r w s m rx m -

a o - L - m m m u E m m E - 5, 3 E L m w u

0

I U N I N 0

m

U

I U N I N 0

m

U

I U N

I N 0

m

u m W u

e 0

W 4J

0 m

m N W 4 . m N v 4

m 0 U 4 . 0 0 N 4

U m 4 4 . m 0 m

- m

I a - W C 0 U

W L W 3

m K 3 L

W E

c -

W 4

L m

In m W o 0 L

.li

a

U N 07 N 0 0 0 N w m 4 m w 0 d m o r - . m m m -4U N . . . . m N U . m m 0 o w m m 00 w U N m 4 - . .

m o w r- 0 0 0 N or- m d m o m m o r - . N O - - W U N . . . . N e . P N m dr- . . m m 0 ~ w m m 0 0 m

m N w w 0 0 0 m o w 0 . . . m N U *

O N 0 m o m N .

d o m m m 00 0 W N m 4 - . . d

~ m r - . w m o

W

-- T I u u u u -0 a m -

U 3 L 0 - m

L 3 C u m

o o u - m r n L Y W E 3

0 > F

- U

I (3 W 0 -

W L 2 Y

m L W a E W Y

m m (3

c

U K 8 W o c c m c o w 0 u n m ~ .- L au m m x - O V O S a E 0 0

VI m (3

-- u u v u

0.0

uorx L - u S W o u C L

r a m -a. m - ( 3

0 - m v m u w w m m m m

3 s Y o u 7

3 o - u L m a

- a

m I \

-1

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K 0 7

m m c E W

L L m a

X

-0 c W c c a

.r

0) W VI

6

c

W

R

c

c

m

- I

m N I N 0

m

U

I m N I N 0

m

v

I m N I N 0

m

U VI W U

e 0

W U

0 m

0 0 r- d \ m v LO d

m 0 LO .-(

\ 0 0 m 4

LO N N d \

N 0 d

- m CT X - W c 0 u W L W 3

VI c S L

W E

I- 7

W U

L

VI VI W 0 0 L

*

m

n

w m w 0 0 0 0 (0 m v l - m o m d mLOw . r - - 4 U L O N N . . . . m Nul . m r - m u m m 0 0 10 w m N dr- . . d

o m r- m 0 0 0 m m m u N U m 4 m m a . m m m o m N . . . . 10 N L O . m a I. m w m m 0 0 (D w m N - r - . . d

m m m PI 0 0 0 m w m m w P I m m m m w - o w m NPI N . . . . d mLO . m w r- m u m m 00 r- (Dm N -I. . . d

W

x

- U I 0 W 0 -

W L 3 U

L W P E W U

VI

m

m U

- > \ > * -

U

W U c 0 0

W L 3 U ln - 0 z

u c W

o c c m - o w 0 ~ n m ~ 7 L > U VI m x - o o o c c E 0 0

m m 0

K X \

J m - W U m L

c 0 - VI VI - E W

U L m n

.- = u

m a 0 4

0 K U W c

U W W W 3 v)

I o K

C 0 7

.r

L 0 E

0 (c C

+ =. .- .. L v) 0 v)

W u L

W c I 0

o L

O o = L L

S

0 m - L

: w a . m W Y o m

-.s 0 3 o VI o w - r s r m s I.- m x x n o

m - uoVI m m x m L - L O

w u .

L V I

w w L L W 1 s

w u - 1 o S J

o w e o

V I 0 V I W O Y C J

a m m

o o m

f.

I

c

r

i I

I

i

L t b

0

I m N I N 0

m

. o m I

m N I N 0

U

I m N I N 0

m

U VI

W I.'

IL 0

01 I.' m a

0 0 r-

\ m 0 m 4

4

m 0 m 4 . 0 0 m r(

m N N 4 . 4 N 0 d

- m IT I I

W C 0 -0

0 L W 3

VI S 3 L

W E + .-

W Y

L m

VI VI W 0 0 L a U

w m w u 0 0 0 w w - u m o m rl m m w . w m w VIN N . . . . m N D . m p . I. m w m m 0 0 VI a m N 4- . . rl

vu7 I. m 0 0 0 m m u m

o m N . . . . w N(O . m a p. m u m m 0 0 v1 a m N - I . . . 4 N(O m 4 m m w . r -o m

m m cn I- 0 0 0 m o m m m m m wr- m m G l m w .

N h N . . . . rl N L O * m w p. m w m m 0 0 w w m N - p . . . 4

- L I U W 0 -

W L 3 4.8

L W a E W o

VI

m

m U

8

> . > I

c) S W o C 0 0

W L 3 Y VI 7

0 r

- u c

S W 0 r c D l - o w 0 o n O I L .- L a o VI m x - 0 0 0 c

. 0

VI

m U

*. -

S 0 - Y m

m

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> 0

+I

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Y 0 VI

H

.-

-

-- Uu. v u

c < m

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o x o - a x

m -u

o r m v m u

W Y m

m m m

3 c Y 0 o

7

3 0

o L m a

IT r . m

W S 4 2 0 m L 1

0 S o

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0 m

r W L o m 0 a z

Y

X

J C a, c

.-

2 a, W 111

I

C 0 .r u !I f 0 L C .r

VI VI W u 0 L c L 0 L

U

a m

U

I N N I N 0

m

U 01 I N N I N 0

U

I

N I N 0

m N

o VI W o

e 0

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O m

W U 4 N . 0 U 0, 4

rl 4

m + . v) 0 l- 4

N N W 4 . 4 U 4

m

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W L al 3

VI C 3 L

W E - c

W o

L m

111 VI W 0 0 L n c

w w u t o w Lo o, 0 0 0 l- m m rl m m u m PIN m mr( N . . . . 0, NLo . * L o N u m m m 0 0 4 W N m -I. . . 4

o m m LD o o o m P - w 4 to- 4 w NO^ - w o o, m W N * . . . 0 mp. p.u m Lorno, 0 0 0 u O N m - I f - 4 . . 4

1-(0 N l- 0 0 0 N N W U m - 4 N m m p . . N - m u m N . . . . N -m w . tou m u m m o 0 0 N U N m dl- 4 . . 4

I-

T I ULL 0 0

-0 a m -

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o m 0 0 o - m V I L * W E 3

0 > 7

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W L 3 Y

L 01 P E W o

VI

m

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I

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I

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> \ W > U

. + ? - - x

0

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c

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L

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m

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0 '

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o L W E

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m -

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1110 V I W O ol-2 r 3 w o V I 0 c w c m t z m - -a

w - L Q L U E ~

o m e 0 1 o m

C > O F L - m m V I - E W * E - > 3 E L r n w v

n m

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I N N I N 0

m

O

I N N I N 0

m

0

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m

U VI W U

e 0

W o m n

W O 3 N . 0 O m 4

4 d

3 . m

VI 0 r- 4

N N W 4 . co O 3

4

- m I a

W C 0 U

W L W 3

VI C 3 L

W E

l- -

W c)

m L

* VI W 0 0 L 0. *

w w VI m 0 0 0 P. VIP. m m m 3 m m o m . m m o m - l N . . . . 0) N O . * V I N ~ m m m 0 0 0 O N m - 4 - . . 4

o m m m o o o m m m m W - l 3 a NO^ . W W 4 m a N . . . . 0 m a .

m VIVIm 0 0 0 O P.O O N m -I. -l . . 3

b W N r- 0 0 0 N - V I m m 4 d N m m r - . or- m O m N . . . . N m y 1 . W O m o m m 0 0 0 O N m 3 r - 4 . . 3

W

LL I 0 W 0 -

W L 3 U

L W c E W o VI

m

m (3

I

> > . * -

U K W U C 0 0

W L 3 o VI ?-

0 z

U K K W o c c m - o w 0 U R D L 7 L > u VI m x - 0 0 0 s Q E 0 0

VI m (3

E -

S 0

U m

m

- L

> 0

o W C

Y 0 * I+

7

7

a

m = . -I

W U m L

K 0 - VI VI - E W

U L m n

x U C aJ c c 4

.r

aJ al VI

10

I n t e r p o l 1 Labs R e p o r t No . 4-2326 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s . MN

T e s t No . 1 C P u l p D r y e r S t a c k

R e s u l t s o f V o l u m e t r i c Flow R a t e Determination....... M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . T i m e o f D e t e r m i n a t i o n . . . . . . . (HRS) B a r o m e t r i c p r e s s u r e . ...... ( 1 N . H G )

P i t o t t u b e c o e f f i c i e n t . . . . . . . . . . .

Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l n u m b e r o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . (SQ.FT)

D i r e c t i o n o f f l o w . . . . . . . . . . . . . . . .

S t a t i c p r e s s u r e . . . . . . . . . . . ( 1 N . W C )

A v g . g a s t e m p ............. (DEG-F)

M o i s t u r e c o n t e n t . . ........ ( % V / V )

A v g . l i n e a r v e l o c i t y . . . . . ( F T / S E C )

Gas d e n s i t y . . . . . . . . . . . . . . ( L B / A C F )

M o l e c u l a r w e i g h t . . . . . . (LB/LBMOLE)

Mass f l o w o f g a s . ......... ( L B / H R )

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . . ( D S C F M )

19

02-22-94

1250

29.94

.04

2

24

Round

48

12.57

UP

.. 95 210

33.27

61.4

. 05230 29.39

145175

46262 24288

- _ _-

I n t e r p o l 1 L a b s R e p o r t No. 4-2326 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , MN

T e s t No. 1 C P u l p D r y e r S t a c k

r R e s u l t s o f P a r t i c u l a t e L o a d i n g D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

)

D a t e o f r un

T i m e run s t a r t / e n d . . . . S t a t i c p r e s s u r e . . . . . . C r o s s s e c t i o n a l a r e a P i t o t t u b e c o e f f i c i e n

W a t e r i n s a m p l e g a s

Run 1 02-22-94

. ( H R S ) 1418/1622

1 N . W C ) SQ.FT) . .....

c o n d e n s e r . . . . . . . . . . . . . ( M L ) i m p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . ........ (GRAMS) t o t a l . . . . . . . . . . . . . . ( GRAMS)

T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . c o l l e c t e d ( g r a m s )

Gas m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( 1 N . H G ) Avg . o r i f . p r e s . d r o p . . ( I N . W C ) A v g . g a s m e t e r t e m p . . ( D E F - F )

Vo lume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e .... ( M I N ) N o z z l e d i a m e t e r . . ....... ( I N ) A v g . s t a c k g a s t e m p . . (DEG-F)

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . ...... (DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( % )

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . (GR/ACF) d r y s t a n d a r d . . . . . (GR/DSCF)

P a r t i c l e mass r a t e . . . ( L B / H R )

-0.95 12.57 .840

0.0 452.0 11.0

463.0

0.1748

0.9976 29.94 0.47 85.0

45.24 43.79

120.00 .184 212

46487 24316

102.2 I

0.03221 0.06160

12.839

Run 2 02-22-94

1705/1911

-0.95 12.57 .840

0.0 461.0 10.0

471.0

0.2005

0.9976 29.94 0.47 85.0

45.25 43.80

120.00 .184 213

47360 24619

100.9

0.03671 0.07064

14.907

Run 3 02-22-94

1940/2146

-0.95 12.57 .840

0.0 454.0

5.0 459.0

0.1507

0.9976 29.94 0.48 84.6

45.60 44.17

120.00 .184 215

47936 25136

99.7

0.02760 0.05265

11.343

32

1 -..


E a s t G r a n d F o r k s , MN I


o f V o l u m e t r i c F low R a t e D e t e r m i n a t i o n - - - - - - -

T i m e o f D e t e a t i o n . . . . . . . ( H R S )

B a r o m e t r i c p r e s ....... ( I N . H G )

. a4

2

24

Round

S t a c k d i a m e t e r . . . . . . . . . . . . . . . 48

12.57

D i r e c t i o n o f f l o w . . . . . . . . . . U P

-1.2

A v g . g a s temp . . . . . . . 214

Mol s t u r e c o n t e n t . . . . . . . ( s V / V ) 2 8 . 6 7

61.1

. 0 4 9 a 9

28.00

u a l . . . . . . . . . . . . . . . . . . . (ACFM) s t a n d a r d . . . . . . . . . . . . (DSCFM)

22

I n t e r p o l 1 Labs R e p o r t No. 4-2326 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , MN

T e s t No. 2 B P u l p D r y e r S t a c k

R e s u l t s o f P a r t i c u l a t e Loading D e t e r m i n a t i o n s - - - - - - - M e t h o d 5

D a t e o f r u n Run 1 Run 2

02-23-94 02-23-94

T i m e run s t a r t / e n d . . . . . ( H R S ) 1021/1225 1300/1503

S t a t i c p r e s s u r e . C r o s s s e c t i o n a l P i t o t t u b e c o e f

W a t e r i n s a m p l e c o n d e n s e r . . .. i m p i n g e r s . . . . . d e s i c c a n t . . . .. t o t a l . . . . . . . . .

. . . . . (1N.WC) a r e a ( S Q . F T ) i c i e n t . . . . . .

g a s . . . . . . . . ( M L ) . . . . . (GRAMS) . . . . . (GRAMS) . . . . . (GRAMS)


Gas m e t e r c o e f f i c i e n t . B a r o m e t r i c p r e s s u r e . . A v g . o r i f . p r e s . d r o p . . A v g . g a s m e t e r t e m p . .

. . .... 1N.HG) IN.WC) DEF-F)

Volume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( CF) s t a n d a r d c o n d i t i o n s . ( D S C F )

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . . . . . . . . . ( I N ) A v g . s t a c k g a s t e m p . . DEG-F)

V o l u m e t r i c f l o w r a t e . a c t u a l . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . .

I s o k i n e t i c v a r i a t i o n . .

. . . . . . ( A C F M ) DSCFM)

. . . ( % )


P a r t i c l e m a s s r a t e . . . ( L B / H R )

-0.79 18.99 .840

0.0 305.0 8.0

313.0

0.1444

0.9976 29.43 0.43 85.3

41.20 39.17

120.00 .184 239

68268 36779

91.3

0.03063 0.05688

17.931

-0.79 18.99 .840

0.0 322.0

5.0 327.0

0.1430

0.9976 29.43 0.43 85.3

43.55 41.41

120.00 .184 237

68024 36865

96.3

0.02887 0.05329

16.839

Run 3 02-23-94

1543/1744

-0.79 18.99 .840

0.0 331.0

7 .O 338.0

0.1427

0.9976 29.43 0.46 84.3

44.91 42.78

120.00 .184 236

68536 37205

98.6

0.02793 0.05147

16.413

34

I n t e r p o l 1 L a b s R e p o r t No. 4-2.326 A m e r i c a n C r y s t a l S u g a r


T e s t No. 4 A P u l p D r y e r S t a c k

R e s u l t s o f P a r t i c u l a t e Loading D e t e r m i n a t i o n s - - - - - - - H e t h o d 5

D a t e o f r un

T i m e run s t a r t / e n d . . . . . (HRS)

S t a t i c p r e s s u r e . . . . .. (1N.WC) C r o s s s e c t i o n a l a r e a ( S Q . F T ) P i t o t t u b e c o e f f i c i e n t . . . . . . W a t e r i n s a m p l e g a s

c o n d e n s e r . . . . . . . . . . . . . ( M L ) i r n p i n g e r s . . . . . . . . . . (GRAMS) d e s i c c a n t . . . . . . . . . . (GRAMS) t o t a l . . . . . . . . . . . . . . (GRAMS)


G a s m e t e r c o e f f i c i e n t . . . . . . . B a r o m e t r i c p r e s s u r e . . ( I N . H G ) A v g . o r i f . p r e s . d r o p . . (1N.WC) Avg . g a s m e t e r t e m p . . ( D E F - F )

Vo lume t h r o u g h g a s m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( C F ) s t a n d a r d c o n d i t i o n s . (DSCF)

T o t a l s a m p l i n g t i m e . . . . ( M I N ) N o z z l e d i a m e t e r . ........ ( I N ) A v g . s t a c k g a s t e m p . . ( D E G - F )

V o l u m e t r i c f l o w r a t e . . . . . . . . a c t u a l . . . . . . . . . . . . . . (ACFM) d r y s t a n d a r d . . . . . . . (DSCFM)

I s o k i n e t i c v a r i a t i o n . . . . . ( % )


P a r t i c l e mass r a t e . . . ( LB /HR)

35

Run 1 0 2 - 2 4 - 9 4

9 3 0 / 1 1 3 4

- 0 . 7 8 1 2 . 0 5

. 8 4 0

0.0 4 0 3 . 0

1 3 . 0 4 1 6 . 0

0 . 1 5 3 6

1 . 0 0 2 7 2 9 . 2 8

0 . 4 1 6 9 . 7

4 3 . 8 6 4 2 . 9 3

1 2 0 . 0 0 .184 2 0 8

4 4 4 0 9 2 3 5 2 2

9 9 . 3

0 . 0 2 9 2 3 0 . 0 5 5 2 1

1 1 . 1 3 2

Run 2 0 2 -'2 4 - 9 4

1 2 0 0 / 1 4 0 5

- 0 . 7 8 1 2 . 0 5

. E 4 0

0 . 0 3 8 0 . 0

1 2 . 0 3 9 2 . 0

0 . 1 2 7 6

1 . 0 0 2 7 2 9 . 2 8

0 . 4 1 7 3 . 8

4 3 . 6 4 4 2 . 3 8

1 2 0 . 0 0 . 1 8 4 2 0 4

4 3 4 1 5 2 3 4 9 0

9 8 . 2

0 . 0 2 5 1 2 0 . 0 4 6 4 5

9 . 3 5 3

Run 3 0 2 - 2 4 - 9 4

1 4 2 5 / 1 6 2 5

- 0 . 7 8 1 2 . 0 5

. 8 4 0

0 .0 3 8 0 . 0

11.0 3 9 1 . 0

0 . 1 3 7 2

1 . 0 0 2 7 2 9 . 2 8

0 . 4 2 7 4 . 4

4 4 . 0 8 4 2 . 7 6

1 2 0 . 0 0 . 1 8 4 2 0 3

4 3 1 5 4 2 3 4 6 2

9 9 . 2

0 . 0 2 6 9 0 0 . 0 4 9 5 0

9 . 9 5 6

Interpoll Labs Report No. 3-1 638 American Crystal Suger

East Grand Forks, Minnesota Test No. 3

Results of the Particle Size Distribution Determination

Sample Identification: B Pulp Dyrer Stack - February 23, 1994 Cascade Impactor Sampling

Assigned Density: 1.00 g/cc

Run 1 Stage um Yo 2

Preimpactor 1 2 3 4 5 6 7

10.0 6.1 4.0 2.5 1.5

0.98 0.61 0.35

10.9 18.0 23.0 29.8 33.2 36.0 39.5 45.6

urn 010 2

'Aerodynamic equivalent diameter in microns Relative cumulative frequency - percent by mass of aerosol with diameters greater than stated size

I n t e r p o l 1 L a b s R e p o r t No. 4 - 2 3 2 6 A m e r i c a n C r y s t a l S u g a r


T e s t No. 3 8 P u l p D r y e r S t a c k

(CASCACE IMPACTOR)

R e s u l t s o f P a r t i c u l a t e Loading'Determinations------- M e t h o d 5

D a t e o f run Run 1

0 2 - 2 3 - 9 4

T i m e run s t a r t / e n d . .... ( H R S ) 1 8 3 3 / 1 9 4 0

S t a t i c p r e s s u r e . C r o s s s e c t i o n a l P i t o t t u b e c o e f

W a t e r i n s a m p l e c o n d e n s e r . . . . i m p i n g e r s . . . . d e s i c c a n t . . . .

. . . . . ( I N . W C ) -0 .79 a r e a ( S Q . F T ) 18 .99 i c i e n t . . . . . . . E 4 0

g a s . ....... ( M L ) 0.0 ( G R A M S ) 201 .0

. . . . . ( GRAMS) 5.0 t o t a l . . . . . . . . . . . . . . (GRAMS) 2 0 6 . 0

. . . . .

T o t a l p a r t i c u l a t e m a t e r i a l . . . . . . . . . . . . . c o l l e c t e d ( g r a i n s ) 0. a 6 9 7

Gas m e t e r c o e f f i c i e n t . . . . . . . 0 . 9 9 7 6 B a r o m e t r i c p r e s s u r e . . ( 1 N . H G ) 2 9 . 4 3 A v g . o r i f . p r e s . d r o p . . ( I N . W C ) 0 . 7 1 A v g . g a s m e t e r t e m p . . ( D E F - F ) 8 2 . 0

V o l u m e t h r o u g h gas m e t e r . . . . a t m e t e r c o n d i t i o n s . . . ( CF) 2 8 . 0 5 s t a n d a r d c o n d i t i o n s . ( D S C F ) 26.8.5

T o t a l s a m p l i n g t i m e . . . N o z z l e d i a m e t e r . . . . ... A v g . s t a c k g a s temp . . V o l u m e t r i c f 1 ow r a t e .

a c t u a l . . . . . . . . . . . . . d r y s t a n d a r d . . . . . . .

. ( M I N ) 6 0 . 0 0

. . ( I N ) . 2 0 6 D E G - F ) 236

. . . . . . (ACFM) 68604 DSCFM) 3 7 5 1 0

I s o k i n e t i c v a r i a t i o n . . . . . ( % ) 9 7 . 9

P a r t i c u l a t e c o n c e n t r a t i o n . . . a c t u a l . . . . . . . . . . . . ( G R / A C F ) 0 . 0 2 1 8 9 d r y s t a n d a r d . . . . . (GR/DSCF) 0 . 0 4 0 0 4

P a r t i c l e mass r a t e . . . ( L B / H R ) 12 .87

1 1

L

'" N i' m

- P-

I n t e r p o l 1 Labora t - r i es ( b i z ) 796-5320

EPFI Method 5 Data R e p o r t i n g Sheet Impinger Catch/Mlnnesota P ro toco l

sourcz C dww Taam Leader - ni Test 5 i t e 54, !/L Job k.5-/fcF Date Submit ted 2 - 25- ?Y t a t = of T e s t 1 ‘ 2 2 - S y

Dste of C)nalysis I -6 -SY Techn ic ian k.P[OE& Test PJo- I P ~ O . of H u n s Completod 7

~~

0.0 t i 6

Test-Run 0 D i s h No. 12 F i e l d Blank D1-h Tare U t . yk.14?0 9 Log Number 13% ’ d 5 Z Dish+Sample W t . %-lr4-/ 9

Log Number - dD I: D i s h Tare U t . Y R . Y 5 & 1 9 Comment 5 DishcSample W t . . Y b . 9 6 f I 9

Sample U t . Q . o t t o 9

9 0. Odd, Comtnen t s Sample W t .

Tes t -Run- D i sh No. 1 8

T e s t I R u n 2 Dish No. 20 Log Number -07 r D i s h Tare W t . Comments Dish+Sample W t . ? Y ! E i 2 4

Sample U t . 0 . d l O Y 9

T e s t l R u n l D i s h No. z / Log Number - 0 S f D i s h Tare W t . 47 ‘ 5 ? 1 i 9 Comments Dish+Sample W t . Y?. 53 % f 9

Sample U t . 0.0 I17 9

Log Number D ish Tare W t . 9 Comments Dish+Samole W t . 9

Sample W t . 9

Test- R u n - D i s h No.

-12 LSC-03 m 0 . d I O S 0 . 0 1 I 3

Tes t - Run - Dish No. Log Numter. D ish Tare W t . 9 Comment-, D i sh+Sampl e !dt. 9

Sample W t . 9

B l a n k So lvent Wt.U.d&Yg

Results: F i e l d B lk . R u n 1 R u n 2 R u n 3 R u n 4 Run 5

I n t e r p o l l Lakcrstories ( 5 1 2 ) 7SA-&2ZO

Epfi Method 5 D a t a R e p o r t i n g S h e e t P r o b e / C y c l o n e Wash

o

- T e s t - R u n Q 0 1 s h NO. 502 F i e l d S l a n k D r s h T a r e a t . 9 03Y 9 Log :lumber 2 3 z L 4 0 5 9 D i s h t S a m p l e Wt.Yb.403F 9 'Jol. of S o l v e n t / 6 3 m l S a m p l e W t . 6 . c m 3 9 + S o l v e n t Resi due&uq/ml

1 T e s t ! Run- D i s h N o . .foY vol . of S o l v e n t 225 m l D i s h T a r e W t . .TO * O U C '3 Log Number - 0 C f D i s h + S a m p l e WtSO.ObL(~ 9 C o m m e n t s S a m p l e W t . Q.ocl rq 9

2

D i s h No. T e s t Run __ Val. of S o l v e n t m l D i s h T a r e U t . 9 Log N u m b e r D i s h c S a m p l e W t . 4 C o m m e n t s S a m p l e U t . 9

'Jol. of Solven t m l D i s h T a r e W t . 9

Csmmen t s S a m p l e U t . 3

D i s h No. T e s t Run - Log Number D i sh+Sampl e U t -

+ S o l v e n t R a s i d u e ~ u g / m l = C ( S a m p l e Wk.u&g) ( I O p ) I /Vol . o f Sol . e m : EPG-MS A c e t o n e R e s i d u e B l a n k Spac. - (7.8 u y / m l

D i s h N o . ,722 '.'ol. of i o l v e n t & m l D i s h T a r e U t . '17.0022. Q Log ?!umber - 0 7 9 D i s h t S a m p l e U t y 7 . @ 8 I G 3 Comnen t z S a m p l e W t . 0.0 1 S 4 9

T e s t I R u n k

- R e s u l t s : F i e l d E l k . Run 1 Hun 2 Run 5 Run 4

3

Run 5

v o l . of S o l v e n t 150 m l D i s h T a r e W t . W.. f6C19 9 Log Number -0Y P D i s h t S a m p l e Ut -yS.5828 r.

S a m p l e W t . 0.02 I9 Comment=

.Interpoll Laboratories (612) 7Sb-bQZQ

EPA Method 5 Data Reporting Sheet Fi 1 ter Gravimetric5

0

1

2 )

3

4

5

Fi 1 ter No. 6 2 6 3 Fi 1 ter Type q"G C

T e s t l R u n h Field Blank

.Log Number ZL3r6 -056 Filter Tare Wt. ,8703 9 Comments Filter+Sample Wt. 46703 9

Sample W t . 9

Filter No. b 13Lj

Filter+Sample Wt. /,0L,k? 9

c1 'Gf= T e s t - R u n I Log Number - 0 6 6 Fi 1 ter Type Comments 9 Filter Tare Ut. ~ k & k O

Sample Wt. o . / P q g . .

Test I R u n A Fi 1 ter No. 6 l U f Log Number -07F Filter Type Y"GF Comments Filter Tare Wt. , &7k6 9

Filter+Sample Wt. + 4 ? q y 9 Sample Wt. O . l ( It 9

Test R u n 3 Fi 1 ter No. &%5S 6 - F -6 %F Fi 1 ter Type

Fi 1 ter Tare Wt. Filter+Sample Wt

Log Number Comments vg

Sample Wt. r 7 , I l

Run - Filter No. Test - Log Number Fi 1 ter Type Comments Filter Tare Wt. 9

Filter+Sample Wt. 9 Sample Wt. 9

Test Run Fi 1 ter No. Log Number Fi 1 ter Type Comments Fi 1 ter Tare Wt. 9


Resu I t s :

- Field E l k . Run 1 Run 2 Run 3 Run 4 Run 5

# I

I n t e r p o l 1 L a b o r a t c r L e s (612) 7S6-5JZQ

€PA M e t h o d 5 D a t a R e p o r t i n g S h e e t I m p i n g e r C a t c h / M i n n e s o t a P r o t o c o l

Sourca T e s t 5-

Job ~ L S / E ~ F Tsam Lead& DU i i

D s t e o f A n a l y s i s . . T e c h n i c i an R.EllrEH4

D a t e Submi t t e d 2 - 2 5 - 9 i / Cat= o f T e s t 2-2 -c/ T e s t KO. 2- NO. of H u n s C o m p l e t e d 1

Tes t A R u n D i s h No. 2 F i e l d B l a n k D i s h T a r e W t . % ,22L7 9 Lo9 Number Z 3 2 - I D i s h + S a m p l e W t . Y b . tz7 I 9 Comments Sample W t . 0.oad.l 9

Log N u m b e r c 1 3 1 D i s h T a r e W t . <2./230 9 Comments D i s h + S a m p l e W t . 51. 1316 9

Sample W t . U.LIU%d 9

Log Number - 141 D i s h T a r e W t . Y 7 , 7 5 7 7 9 Comments Di sh+Sampl e W t . 4 7 . 7 b 7 b 9

Sample W t . O..adG I 9

Log Number - f 51 D i s h T a r e W t . 4 8 . 393 I 9 Comment s D i sh+Sampl e W t . Yk. Y O 0 2 9

Sample U t . D.dd 7 I 9

T e s t A R u n I D i s h No. 3

T e s t R u n x D i s h No. I /

T e s t A R u n - D i s h NO. /7

Test- Run - D i s h No. Log N u m b s r D i s h T a r e W t . 9 Comments D i s h + S a m p l e U t . 9

Sample W t . 9

D i s h No. T e s t - Run - Log rkmber D i s h T a r e U t . 9 Commen t s D i s h + S a m p l e X t . 9

Sample W t . 9

Blank S o l v e n t W t . d . & Y g

R e s u l t s : F i e l d B l k . Run 1 R u n 2 Hun 3 R u n 4 R u n 5

I

~~~ ~ ~~

~~ ~~

7

I n t e r p o l l L a b u r s t o r i e s (512) 70,&-h.J"-0

EPQ Method 5 D a t a R e p o r t i n g Sheet P r o b o / C y c l o n e Wash

3

AC.5 - EGF Source R O r b et*

nutt SCb L/C Job T e a m Leader D a t e S u b m i t t e d l - L C - ? ; / Data of T e s t 2 - 2 3 - g j T e s t No. z No. of R u n s C o m p l e t e d 3 D a t a of C n a l y s i s 3-3-5'Y T e c h n i c i a n fl.a;'/ow T r a n s p o r t L e a k a s e 0 @ & n l S o l v e n t (iCe+n*,.

T e s t S i t e

D i s h T a r s W t . u o l . of s o l v e n t l2< m l Log F!umber - D i s h c S a m p l e W t . q . e l @ r; C o m m a n t s S a m p l e U t . 0 . 0 2 8 5 q l

0

1

2

D- 1 0.0305 O.QJ78 0 . c" 2.6- 1

9 T e s t L R u n Q f i s h r40. F i e l d B l a n k D i s h T a r e U t . 47. b+q 4 Log Xumber 3 ?2b 'a ' DishcSamp1.e W t . q 7 . ( 9 ' 4 3 3 9

yo -

vol. of S o l v e n t LOU m i S a m p l e W t . 0 . B O O 3 9

SC-OIYR

T e s t Z R u n / ~ o l . of S o l v e n t . a ~ m 1 Loq Number -I3 P - Cctnments Sample W t .

D i s h NO. W ,

G i s h c S a n p l e Ldt.$:;y;; q

T e s t &Run 1201. of S o l v e n t I66 m l D i s h T a r e U t . Lcq Number - 1 - P - - Comment s ~ S a m p l e Ut. O . O h S 3

Results: F i e l d E l k . Run 1 Run 2 Run 3 Run 4 Run 5

Interpol1 Laboratories (612) 796-0020

€PA Method 5 Data Reporting Sheet Filter Gravimetric5

0

1

2 .I

3

4

5

Job hS/L&t Source B b r y f " Team Leader O V M Test Site i& Gk

Date of Analysis 7~ 3-$ Y Technician _ I

Date Submitted 2- 2l--qq Date of Test Z - L 3 3 + T e s t No. 2- No. of Runs Compl te 3

A 2 L . L T e s t L R u n L Fi 1 ter No. 6 ~ 7 - Field Blank Fi 1 ter Type 4'' ,-v Comments Fi 1 ter+Sampl e Wt -, & b o 8 9

Sample Wt. 0-00s I 9

9 Log Number 7-6- J Zc Filter Tare Wt. , 86 b l

Test L R u n I Fi 1 ter No. g t < ?

Comments Filter Tare Wt. .?LbqI 9 FiltertSample Wt. .'I160 9 Sample Wt. 0- lob7 9

Log Number -13F Filter Type Y'* f&

Test Z R u n A Filter No. 6L6 I Log Numbfr -IVF Fi 1 ter Type - 1 ' 6 - f

Comment s Filter Tare Wt. f872-3 9 FiltercSample Wt. .919 B 9 Sample Wt. 0. I075 9

T e s t A R u n 3 - Log Number -15- G Comments

Fi 1 ter Fi 1 ter Fi 1 ter Fi 1 ter+ Samp 1 e

~~

Test - Run - Filter No. Log Number Filter Type Comments Fi 1 ter Tare Wt . 9

Filter+Sample Wt. 9 Sample Wt. 9 .

Test - Run - Fi 1 ter No. Log Number Fi 1 ter Type Comments Filter Tare Wt. 9


?e+ul t s : Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5

10.10ca3 10. 1015 10. lo79 - )

Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5 I I d-1 Y q q I D , i Y 3 0 I d , . I Y r 7 I

I -. I I I I I LSC-02PR D- 20

- )I 4

5

D i s h NO. D i s h T a r e Ut. D i sh+Samp 1 e U t . Sample W t .

D i s h No.

01 sh+Sampl e U t SI I . W O 9 Sample U t .

R u n L 9 Test-

Loq Number Comments

9 T e s t R u n L * D ~ s h T a r e U t . '-t1.%qiq 9

Comments

9 9

(3 F i e l d B l a n k

3 28 1 Log Number 2 ? 7 ( - i r a T

0.0 \SS 9

D i s h No. 3 q O T e s t R u n 2 .4136 9

-\If 9 ~1 sh+Sampl e W t ql.C1ZT9

0. 01 b-7 S a m p l e U t - -

371 D i s h No. D i s h T a r e U t . 41. D i s h + S a m p l e W t H 7 .(a751 Sample W t -

D i s h No.

n l s h c s a m p l e W t .

D i s h T a r e U t . '(7 2 Log Number

9 Comments

r c.5 8'7 9 T e s t R u n 3 Log N u m b e r Comments 9

q

- 0 . 0 I 6 2

T e s t R u n - 9 Log Number D i s h T a r e W t .

9

€PA Nethod 5 D a t a R e p o r t i n g S h e e t Imp inger C a t c h / M i n n e s o t a P r O t O C O l

-

D i s h No. D i s h T a r e U t . D i s h c S a m p l e ut. S a m p l e U t .

T e s t R u n - 9

9 Log N u m b e r Comments 9

R u n 4 R u n 5 R u n 3 Results: F i e l d B l k . Run 1 R u n 2

0.OlSI 1 &1.0159 I LS(

IntErpoll L a k u r z t o r l e s (512) ?C&-k*JXl

EPCI tfethod 5 D a t a Repor t ing Sheet P r o b o / C y c l o n e Wash

0

1

2

- ;i

4

5

S o u r c e A ~ n v $ . r . Job A c S - E G F

D a t e S u b n i t t a d 2 - z r - ? C / D a t e O C T e s t 2 - 2 Y - P Y Taa.n Laadar nv i f T e s t ita 5ra:k

C a t s o f C n a l y k i s 3 - ? - 9 Y Technician A ElOEM7 T r a n s p o r t Leakage a None m l So lven t U&nC

No. of R u n s C o m p l e t e d ? T e s t r.10.

- T e s t - R u n 8 G ~ s h NO.

F i a l d Y l a n k D:sh T x e U t . 9 Log N u m b e r D i sh+Sampl e Wt . 9 ‘ do l . of S o l v e n t m l S a m p l e W t . 9 +Solvent R e s l d u e 3 . 0 u q / m l

D i s h No. 16 D i s h Tare W t . 4 ? . / 3 8 4 ‘3

T e r t x R u n 1 VOI. of S o l v e n t / 2 5 m l

Ccinmen t 7 Sample U t . O.OL(7b 5 Log Number 2 7 . ~ - 16 P D i s h + S a m p l e Wt.L(?.IX 6 0 9

v D i s h No. 175 , , T e s t L R u n 2

‘dol. o f S o l v e n t / 9 0 m l D i s h T a r e U t . 5 ’ 2 . 30 9 Log :Jumber - D i s h + S a m p l e W t . 5 3 . (s, 600 3

V C L . o f S o l v e n t / m m l ish T a r a W t . 47.4 214 ‘3 Log ?!umber -18 t‘ D i s h + S a m p l e kJt.Yl. IS 0 b G

Conmen t E S a m p l e W t . O.OL4’1 9

D i sh No.. 50 9 T e s t R u n 3

Comments S a m p l e W t . 0.oze.b q

Vol. of Solvent m l D i s h T a r e W t - 9

Comments S a m p l e Ut . 9

‘Jol - o f S o l v e n t m l D i s h T a r e W t . 9 Log Number D i sh+Sampl e W t . ci Csmmen t 5 S a m p l e U t . 9

+Sol%,ent fiasidue-ug/ml=C ( S a m p l e Ut.- g 1 ( 1 w ) 3 / C O l . o f Sol . -

T e s t R u n - D i s h No.

Log Numba- D i s h + S a m p l e W t . 9

D i s h No. T e s t R u n

Eps-MS A c e t o n e R e s i d u e B l a n k Spec. (7.8 U g / m l - R e s u l t s : F i e l d B lk . Run 1 R u n 2 R u n 3 R u n 4 R u n 5

Interpol1 Laboratories (512) 755-5CI20

EPCI Method S Data Reporting Sheet Fil'ter Gravimetric5

I 6. I 2 7 6 0 . 1 3 7 2

- Source A. D r s . t r

OUH Test Site C C U " I < c Job ,/k- S C G r Date Submitted 2-ZS-qV Date of Test 2 . 2 Y -4 Test NO. 'I No. o f Runs Completed ? Date of Analysis 7-3-911 Techn i c i an 6. D

Team Leader

L3

1

2

3

4

5

Run 0 Fi 1 ter No. Test - Field Blank Fi 1 ter Type Log Number 9 Filter Tare Wt. Comments Filter+Sample Wt. 9

Sample Wt. 9

Fi 1 ter No. 611 I I. (r ,=

Comments Filter Tare Wt. I kbb 7 9 Filter+Sample Wt. . '?Sf3 9 Sample Wt. 0.OSIL 9

Test Run Log Number 1 3 2 b - Iu F Fi 1 ter Type

Test Y Run 2- Fi 1 t er No. b27L

Comments Filter Tare Wt. .Lbll 9 Filter+Sample Wt. qY3J- 9

Log Number . I= Filter Type V " & F

Sample Ut. .m82< 9

Test '\ Run 3 Filter No. 6 2 7 3

Comments Filter Tare Wt. . b L q f 9 Log Number - ( e (Z Fi 1 ter Type Y " G f

Fi 1 ter+Sampl e Wt . , q S 7 V 4 Sample Wt. . 0 4 ~ 3 3

~~ ~

Test Run Filter No. Log Number Fi 1 ter Type Comments Filter Tare Wt. 9


Fi 1 ter No. Test Run - Log Number Fi 1 ter Type Comments Filter Tare Wt. 9


Rerul ts: Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5

F ' Field Elk. Run 1 Run 2 Run 3 Run 4 Run 5

0- 23 -

.... . . :. .. . ". . , ..; . . .

. . . . . . . . . . . . . . . : i . '.. .... . >: . .....

. .

..; . . . . .>P. ......... . . . . . . . -... . ... . ........ L :

, .I .> ..-

: .. I.. . . . q . , . : . ... . . .. a - . . .

8'. - . (,'; . . 1 . .... ;.,<' .. .:

. . . . . .: ~ . . . . I : . . . , ..

I . . . . . - ,.. . . . . ... . . . . . . . . ' _ . . .(" , . . . . !

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E- 3

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E a s t G r a n d F o r k s . M i n n e s o t a


R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

Run 1 A Run 18 Run 1C Run 1 D

D a t e o f r u n . . . . . . . . . . . . . . . . 02-24-94 02-24-94 02-24-94 02-24-94 T ime o f r u n . . ; . . . . . . . . . ( H R S ) 930 945 1000 1015

F l a s k n u m b e r . . . . . . . . . . . . . . . . 61 62 63 64 Volume o f f l a s k . ........ ( M L ) 2100 2079 2067 2087

D a t a : t i m e o f s a m p l i n g

f l a s k t e m p e r a t u r e . . (DEG-F) 60.00 60.00 60.00 60.00 b a r . p r e s s . . . . . . . . . (1N.HG) 29.28 29.28 29.28 29.28 f l a s k vacuum . . . . . . . (1N.HG) 26.55 26.60 26.60 26.55 f l a s k a b s . p r e s s . . . (1N.HG) 2.73 2.68 2.68 2.73

D a t a : T i m e o f F l a s k O p e n i n g

f l a s k t e m p e r a t u r e . . (DEG-F) 70.00 70.00 70.00 70.00 ) l a b . b a r . p r e s s . . . . (1N.HG) 29.10 29.10 29.10 29.10

f l a s k s t a t i c p r e s s . ( I N . H G ) -0.25 -0.10 -0 .70 0.90 f l a s k a b s . p r e s s . .. ( IN .HG) 28.85 29.00 28.40 30.00

Volume g a s s a m p l e d . . . . (DSML) 1800 1796 1745 1868

M o i s t u r e c o n t e n t . . . . .. ( % V / V ) 30.55 30.55 30.55 30.55

N i t r a t e I n g a s s a m p l e ... ( J G ) 284.0 273.0 318.0 350.0 NO2 i n g a s s a m p l e . . ..... ( J G ) 210.7 202.6 235.9 259.7

NOx C o n c e n t r a t i o n

(GR/DSCF) . . . . . . . . . . . . . . . . . 0.0512 0.0493 0.0591 0.0608 (MG/DSCM).. . . . . . . . . . . . . . . . 117 113 135 139 (PPM-DRY). . . . . . . . . . . . . . . . . 61 5 9 71 73 "

(PPM-WET) . ................ 43 41 49 50

NOX E m i s s i o n r a t e . . . . (LB/HR) 10.30 9.93 11.91 12.24

37

I n t e r p o l 1 L a b s R e p o r t No . 4-2326 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s , M i n n e s o t a


!

R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - H e t h o d 7

Run 2A

D a t e o f r u n . ............... 02-24-94 T i m e o f run . . . . . . . . . . . . (HRS) 1030

F l a s k n u m b e r . . . . . . . . . . . . . . . . 65 Volume o f f l a s k . . ....... ( M L ) 2068


f l a s k t e m p e r a t u r e . . (DEG-F) 60.00 b a r . p r e s s . . . . . . . . . (1N.HG) 29.28 f l a s k vacuum . . . . . . . (1N.HG) 26.65 f l a s k a b s . p r e s s . . . (1N.HG) 2.63


f l a s k t e m p e r a t u r e . . (DEG-F) 70.00 l a b . b a r . p r e s s . . . . (1N.HG) 29.10 f l a s k s t a t i c p r e s s . ( 1 N . H G ) -0.30 f l a s k a b s . p r e s s . . . ( I N . H G ) 28.80

Volume g a s s a m p l e d . ... (DSML) 1776

M o i s t u r e c o n t e n t . . . . . . ( % V / V ) 30.55

N i t r a t e i n g a s s a m p l e . . . ( J G ) 324.0 NO2 i n gas s a m p l e . . . . . . . ( J G ) 240.4


(GR/DSCF) . . . . . . . . . . . . . . . . . 0.0592 (MG/DSCM) . . . . . . . . . . . . . . . . . 135 (PPM-DRY).. . . .............. 71 (PPM-WET) . . . . . . . . . . . . . . . . . 49

NOX E m i s s i o n r a t e . . . . (LB /HR) 11.91

Run 28

02-24-94 1045

66 2096

60.00 29.28 26.65 2.63

70.00 29.10 -0.90 28.20

1759

30.55

274.0 203.3

0.0505 116 60 42

10.17 '

Run 2C

02-24-94 1100

19 2069

60.00 29.28 26.65 2.63

70.00 29.10 0.70

29.80

1845

30.55

251.0 186.2

0.0441 101 53 37

8.89

Run 2 0

02-24-94 1115

20 2060

60.00 29.28 26.60 2.68

70.00 29.10 -1.00 28.10

1718

30.55

261.0 193.7

0.0493 1 1 3 596' 41

9.92

38

I n t e r p o l 1 L a b s R e p o r t N o . 4-2326 A m e r i c a n C r y s t a l S u g a r


T e s t NO. 4 A P u l p D r y e r S t a c k

R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

Run 3 A Run 3 8 Run 3 C Run 3 D

D a t e o f run . . . . . . . . . . . . . . . . 02-24-94 02-24-94 02-24-94 02-24-94 T i m e o f run. . . . . . . . . . . . (HRS) 1200 1215 1230 1245

F l a s k number . . . . . . . . . . . . . . . . 21 22 23 24 Volume o f f l a s k . . . . . . . . . ( M L ) 2068 2031 2056 2031


f l a s k t e m p e r a t u r e . . ( D E G - F ) 60.00 60.00 60.00 60.00 b a r . p r e s s . . . . . . . . . (1N.HG) 29.28 29.28 29.28 29.28 f l a s k vacuum . . . . . . . ( I N . H G ) 26.70 26.70 26.70 26.70 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 2.58 2.58 2.58 2.58

D a t a : T l m e o f F l a s k O p e n i n g

f l a s k t e m p e r a t u r e . . (DEG-F) 70.00 70.00 70.00 70.00 l a b . b a r . p r e s s . . . . ( I N . H G ) 29.10 29.10 29.10 29.10 f l a s k s t a t i c p r e s s . ( I N . H G ) -1.90 -0.30 -1.25 1.70 f l a s k a b s . p r e s s . . . ( 1 N . H G ) 27.20 28.00 27.85 30.80

Volume g a s s a m p l e d . . . . ( DSML) 1671 1747 1705 1881

M o i s t u r e c o n t e n t . . . . . . ( S V / V ) 30.55 30 .55 30 .55 30.55

N i t r a t e i n g a s s a m p l e . . . ( J G ) 368.0 3 3 5 . 0 342.0 349.0 NO2 I n g a s s a m p l e . . . . . . . ( J G ) 273.0 ' 248.6 253.8 259.0'


(GR/DSCF) . . . . . . . . . . . . . . . . . 0.0714 0.0622 0.0650 0.0602 ( M G / D S C M ) . . . . . . . . . . . . . . . . . 163 142 149 138 (PPM-DRY) . . . . . . . . . . . . . . . . . 85 74 78 72 -*' (PPM-WET) . . . . . . . . . . . . . . . . . 59 52 54 50

NOX E m i s s i o n r a t e .... (LB/HR) 14.39 12.52 13.10 12.12

-. __ I n t e r p o l l L a b s R e p o r t No. 4 - 2 3 2 6

A m e r i c a n C r y s t a l S u g a r E a s t G r a n d F o r k s , M i n n e s o t a

T e s t No. 2 8 P u l p D r y e r S t a c k

R e s u l t s o f O x i d e s o f N i t r o g e n ( N O x ) D e t e r m i n a t i o n s - - - - - - - - - Method 7

) I

Run 1 A Run 1 8 Run 1 C Run 1 D

D a t e o f r u n ................ 0 2 - 2 3 - 9 4 0 2 - 2 3 - 9 4 0 2 - 2 3 - 9 4 0 2 - 2 3 - 9 4 T i m e o f run . ........... (HRS) 1 6 4 5 1 7 0 0 1 7 1 5 1 7 3 0

F l a s k n u m b e r . ............... 43 4 4 4 6 45 V o l u m e o f f l a s k ......... ( M L ) 2 0 8 8 2 0 9 0 2 0 9 0 2 0 8 6


f l a s k t e m p e r a t u r e . . ( D E G - F ) 6 0 . 0 0 6 0 . 0 0 60.00 60.00 b a r . p r e s s . . . . . . . . . ( I N . H G ) 2 9 . 4 3 2 9 . 4 3 2 9 . 4 3 2 9 . 4 3 f l a s k vacuum ....... ( IN .HG) 2 6 . 8 0 2 6 . 8 0 2 6 . 8 5 2 6 . 9 0 f l a s k a b s . p r e s s ... ( I N . H G ) 2 . 6 3 2 . 6 3 2 . 5 8 2 . 5 3

D a t a : T i m e o f F l a s k Opening

f l a s k t e m p e r a t u r e . . (DEG-F) 70.00 7 0 . 0 0 7 0 . 0 0 7 0 . 0 0 l a b . b a r . p r e s s . ... ( IN .HG) 2 9 . 1 1 2 9 . 1 1 2 9 . 1 1 2 9 . 1 1 f l a s k s t a t i c p r e s s . ( I N . H G ) - 5 . 6 5 0 . 7 0 -6.00 - 5 . 0 0 f l a s k a b s . p r e s s . . . ( IN.HG) 2 3 . 4 6 2 9 . 8 1 2 3 . 1 1 2 4 . 1 1

V o l u m e g a s s a m p l e d . ...( DSML) 1 4 2 7 1 8 6 4 1 4 0 7 1 4 7 7

M o i s t u r e c o n t e n t . . . . . . ( t V / V ) 2 7 . 6 8 2 7 . 6 8 2 7 . 6 8 2 7 . 6 8

N i t r a t e i n g a s s a m p l e ... ( J G ) ND2 i n g a s s a m p l e ....... ( J G )


(GR/OSCF) . . . . . . . . . . . . . . . . . (MG/OSCM) . . . . . . . . . . . . . . . . . (PPM-DRY) . ................ (PPM-WET) .................

NOX E m i s s i o n r a t e .... (LB/HR)

!

40

I

\

: i

I I I I I 1

1 I i I I I

) i

I

i )

I




R e s u l t s of O x i d e s of N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - M e t h o d 7

Run 2A Run 28 Run 2 C

D a t e of run . . . . . . . . . . . . . . . . 02-23-94 02-23-94 02-23-94 T i m e o f run ............ (HRS) F l a s k n u m b e r . . . . . ........... V o l u m e o f f l a s k . . . . . . . . . ( M L )

D a t a : t i m e of s a m p l i n g

f l a s k t e m p e r a t u r e . . (OEG-F) b a r . p r e s s . . . . . . . . . (1N.HG) f l a s k vacuum . . . . . . . (1N.HG) f l a s k a b s . p r e s s . . . (IN.HG)


f l a s k t e m p e r a t u r e . . ( D E G - F )

f l a s k s t a t i c p r e s s . (1N.HG) l a b . b a r . p r e s s . . . . (1N.HG) f l a s k a b s . p r e s s . . . (1N.HG)

V o l u m e g a s s a m p l e d . . . . ( D S M L )

M o i s t u r e c o n t e n t . . .... ( S V / V )

N i t r a t e i n g a s s a m p l e ... ( J G ) NO2 i n g a s s a m p l e ....... ( J G )


(GR/OSCF) . . . . . . . . . . . . . . . . . (MG/DSCM) . ................ (PPM-DRY) . ................ (PPM-WET) . . . . . . . . . . . . . . . . .

NOX E m i s s i o n r a t e .... (LB/HR)

1745

47 2074

60.00 29.43 26.95 2.48

70.00 29.11 0.50

29.61

1847

27.68

41

1835 1850

48 67 2102 2073

60.00 60.00 29.43 29.43 26.85 26.95 2.58 2.40

70.00 70.00 29.11 29.11 -3.35 0.60 25.76 29.71

1599 1853

27.68 27.68

259.0 192.2

0.0453 104 54 39

14.53

Run 2D

02-23-94 1910

68 2101

60.00 29.43 27.00 2.43

70.00 29.11 0.50

29.61

1875

27.68

243.0 180.3

0.0420 96 50 5 1

36

13.47

~- -~ __ I n t e r p o l 1 L a b s R e p o r t No. 4 - 2 3 2 6

A m e r i c a n C r y s t a l S u g a r E a s t G r a n d F o r k s , M i n n e s o t a


R e s u l t s o f O x i d e s o f N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - H e t h o d 7

)

Run 3A Run 3 8 Run 3C Run 30

D a t e o f run . . . . . . . . . . . . . . . . 02-23 -94 0 2 - 2 3 - 9 4 0 2 - 2 3 - 9 4 0 2 - 2 3 - 9 4 T i m e o f r u n . . . . . . . . . . . . (HRS) 1 9 4 5 2 0 1 3 2 0 2 9 2 0 4 0

F l a s k n u m b e r . . . . . . . . . . . . . . . . 6 9 7 0 7 1 7 2 Vo lume o f f l a s k . . . . . . . . . (ML) 2 0 6 9 2 0 7 1 2 0 3 8 2 0 9 2


f 1 a s k t e m p e r a t u r e . . (OEG-F) 6 0 . 0 0 6 0 . 0 0 6 0 . 0 0 6 0 . 0 0 b a r . p r e s s . . . . . . . . . ( 1 N . H G ) 2 9 . 4 3 2 9 . 4 3 2 9 . 4 3 29 .43 f l a s k vacuum . . . . . . . ( I N . H G ) 2 6 . 8 5 2 6 . 8 0 2 6 . 8 0 2 6 . 8 0 f l a s k a b s . p r e s s . . . (1N.HG) 2 . 5 8 2 . 6 3 2 .63 2 . 6 3


f l a s k t e m p e r a t u r e . . (OEG-F) 7 0 . 0 0 7 0 . 0 0 7 0 . 0 0 7 0 . 0 0

f l a s k s t a t i c p r e s s . (1N.HG) 0.10 -0.10 - 6 . 5 0 - 4 . 3 0 f l a s k a b s . p r e s s . . . ( I N . H G ) 2 9 . 2 1 2 9 . 0 1 2 2 . 6 1 2 4 . 8 1

l a b . b a r . p r e s s . . . . ( 1 N . H G ) 2 9 . 1 1 2 9 . 1 1 2 9 . 1 1 2 9 . 1 1

Vo lume g a s s a m p l e d . . . . (DSML) 1 8 0 8 1 7 9 3 1 3 3 5 1 5 2 2

M o i s t u r e c o n t e n t . . . . . . ( S V / V ) 2 7 . 6 8 2 7 . 6 8 2 7 . 6 8 2 7 . 6 8

NO2 i n g a s s a m p l e . . . . . . . ( J G ) 2 0 4 . 8 2 2 7 . 8 1 8 7 . 7 200 .3 N i t r a t e i n g a s s a m p l e . . . ( J G) 2 7 6 . 0 307 .O 2 5 3 . 0 2 7 0 . 0


(GR/DSCF) . . . . . . . . . . . . . . . . . 0 . 0 4 9 5 0.0555 0 . 0 6 1 4 0 . 0 5 7 5 .(MG/OSCM) . . . . . . . . . . . . . . . . . 1 1 3 1 2 7 1 4 1 1 3 2

(PPM-DRY) . ................ 5 9 6 6 7 4 6 9 c / (PPM-WET) . . . . . . . . . . . . . . . . . 43 48 53 50

NOX E m i s s i o n r a t e . . . . (LB /HR) 1 5 . 8 7 1 7 . 8 0 1 9 . 7 0 1 8 . 4 4

42

~~~ -- ~

I n t e r p o l l L a b s R e p o r t No. 4-2326 A m e r i c a n C r y s t a l S u g a r

E a s t G r a n d F o r k s . M i n n e s o t a

i T e s t No. 5 C P u l p D r y e r S t a c k

R e s u l t s Of O x i d e s of N i t r o g e n (NOx) D e t e r m i n a t i o n s - - - - - - - - - Method 7

Run 1 A

D a t e o f run . . . . . . . . . . . . . . . . 02-24-94 T ime o f r u n . . . . . . . . . . . . ( H R S ) 832

F l a s k n u m b e r . . . . . . . . . . . . . . . . 13 Volume o f f l a s k . ........ (ML) 2060


f l a s k t e m p e r a t u r e . . ( D E G - F ) 50.00 b a r . p r e s s . . . . . . . . . ( 1 N . H G ) 29.24 f l a s k vacuum . . . . . . . ( 1 N . H G ) 26.70 f l a s k a b s . p r e s s . . . ( IN.HG) 2.54

D a t a : T i m e of F l a s k Opening

f l a s k t e m p e r a t u r e . . (DEG-F) 70.00 ) l a b . b a r . p r e s s . . . . ( I N . H G ) 29.10

f l a s k s t a t i c p r e s s . (1N.HG) 1.10 f l a s k a b s . p r e s s . . . (1N.HG) 30.20

Volume g a s s a m p l e d . . . . (DSML) 1867

M o i s t u r e c o n t e n t . . . . . . ( 3 V / V ) 28.69

N i t r a t e i n g a s s a m p l e . . . ( J G ) 525.0 NO2 i n g a s s a m p l e . . . . . . . ( J G ) 389.5


(GR/OSCF) . . . . . . . . . . . . . . . . . 0.0912 (MG/DSCM) . . . . . . . . . . . . . . . . . 209 (PPM-DRY) . . . . . . . . . . . . . . . . . 109 (PPM-WET) . . . . . . . . . . . . . . . . . 78

NOX E m i s s i o n r a t e . . . . ( LE/HR) 19.62

Run 18

02-24-94 847

14 2048

50.00 29.24 26.90 2.34

70.00 29.10 6.35

35.45

2223

28.69

454.0 336.9

0.0662 152 79 56

14.25

Run 1 C

02-24-94 914

15 2045

50.00 29.24 26.80 2.44

70.00 29.10 5.75

34.85

2173

28.69

436.0 323.5

0.0651 149 78 56

14.00

Run 10

02-24-94 929

16 2067

50.00 29.24 26.85 2.39

70.00 29.10 -0.40 28.70

1782

28.69

438.0 325.0

0 ;,<' 0.0797 '.

182 95 . 4 ,

68

17.15

43

1 I I 1 I I 1

I 1 1 1 i I

1 I

I n t e r p o l 1 L a b s R e p o r t No. 4 - 2 3 2 6 A m e r i c a n C r y s t a l S u g a r


T e s t No . 5 C P u l p D r y e r S t a c k

R e s u l t s o f O x i d e s o f M l t r o g e n (NOx) D e t e r m i n a t l o n s - - - - - - - - - Method 1

Run 2A

D a t e o f r u n . . . . . . . . . . . . . . . . 0 2 - 2 4 - 9 4 T i m e o f run . . . . . . . . . . . . (HRS)

F l a s k n u m b e r . . . . . ........... V o l u m e o f f l a s k . . ....... (ML)


f l a s k t e m p e r a t u r e . . (DEG-F) b a r . p r e s s . . . . . . . . . (1N.HG) f l a s k v a c u u m . . . . . . . (1N.HG) f l a s k a b s . p r e s s . . . (1N.HG)

D a t a : T lme o f F l a s k Open ing

f l a s k t e m p e r a t u r e . . (DEG-F) l a b . b a r . p r e s s . . . . ( I N . H G ) f l a s k s t a t l c p r e s s . (1N.HG) f l a s k a b s . p r e s s . . . (1N.HG)

V o l u m e g a s s a m p l e d .... Moi s t u r e c o n t e n t . . . . . . N l t r a t e I n g a s s a m p l e . NO2 i n g a s s a m p l e . . ... NOx C o n c e n t r a t i o n

(GR/DSCF) . . . . . . . . . . . . . . . . . (MG/DSCM) . . . . . . . . . . . . . . . . . ( P P M - D R Y ) . . . . . . . . . . . . . . . . . i PPM-WE

NOX E m i s s

) . . . . . . . . . . . . . . . . . on r a t e .... ( L B / H R )

9 4 5

1 7 2 0 5 4

4 5 . 0 0 2 9 . 2 4 2 6 . 9 0

2 . 3 4

7 0 . 0 0 2 9 . 1 0

1 . 6 0 3 0 . 7 0

1 9 0 7

2 8 . 6 9

3 3 3 . 0 2 4 7 . 1

0 . 0 5 6 6 1 3 0

6 8 4 8

1 2 . 1 8

Run 2 8

0 2 - 2 4 - 9 4 9 5 8

1 8 2 0 4 5

40.00 2 9 . 2 4 2 6 . 6 0

2 . 6 4

7 0 . 0 0 2 9 . 1 0 - 5 . 0 0 2 4 . 1 0

1 4 3 2

2 8 . 6 9

3 2 7 . 0 2 4 2 . 6

0 . 0 7 4 0 1 6 9

8 9 63

1 5 . 9 3

Run 2C

0 2 - 2 4 - 9 4 1 0 1 4

43 2 0 8 8

4 0 . 0 0 2 9 . 2 4 2 7 . 1 0

2 . 1 4

7 0 . 0 0 2 9 . 1 0 - 5 . 6 5 2 3 . 4 5

1 4 5 4

2 8 . 6 9

- ,a

Run 20

0 2 - 2 4-94 1 0 3 0

44 2 0 9 0

4 0 . 0 0 2 9 . 2 4 2 1 . 1 0

2 . 1 4

7 0 . 0 0 2 9 . 1 0

0 . 1 0 2 9 . 8 0

1 8 9 2

2 8 . 6 9

44

I n t e r p o l l L a b s R e p o r t No. 4 - 2 3 2 6 A m e r i c a n C r y s t a l S u g a r



i R e s u l t s o f O x i d e s o f N1 t rogen ( N O x ) D e t e r m i n a t i o n s - - - - - - - - - U e t h o d 7

I 1

1

I I

1 ! I

i

Run 3 A Run 3 8 Run 3C Run 3 D

D a t e o f run . ............... 0 2 - 2 4 - 9 4 0 2 - 2 4 - 9 4 0 2 - 2 4 - 9 4 0 2 - 2 4 - 9 4 T i m e o f run ............ ( H R S ) 1 0 4 8 1108 1 1 2 0 1 1 3 5

F l a s k n u m b e r . ............... 4 5 4 6 4 7 4 8 Vo lume o f f l a s k . . . . . . . . . ( M L ) 2 0 8 6 2 0 9 0 2 0 7 4 2 1 0 2


f l a s k t e m p e r a t u r e . . ( D E G - F ) 4 0 . 0 0 4 0 . 0 0 3 5 . 0 0 3 6 . 0 0 b a r . p r e s s . . . . . . . . . ( I N . H G ) 2 9 . 2 4 2 9 . 2 4 2 9 . 2 4 2 9 . 2 4 f l a s k vacuum . . . . . . . ( I N . H G ) 2 7 . 1 0 2 6 . 9 0 2 7 . 4 0 27 1 a0 f l a s k a b s . p r e s s . . . ( IN .HG) 2 . 1 4 2 . 3 4 1 . 8 4 1 . 4 4

D a t a : T i m e o f F l a s k Opening

f l a s k t e m p e r a t u r e . . (DEG-F) 7 0 . 0 0 7 0 . 0 0 7 0 . 0 0 7 0 . 0 0 l a b . b a r . p r e s s .... ( I N . H G ) 2 9 . 1 0 29.10 - 2 9 . 1 0 2 9 . 1 0 f l a s k s t a t i c p r e s s . (IN.HG) 5 . 0 0 6 .00 0 . 5 0 - 3 . 3 5 f l a s k . a b s . p r e s s . . . ( I N . H G ) 3 4 . 1 0 3 5 . 1 0 2 9 . 6 0 2 5 . 7 5

Vo lume g a s s a m p l e d . . . . ( D S M L ) 2 1 8 4 2 2 4 2 1 8 8 4 1 6 7 4

M o i s t u r e c o n t e n t . . .... ( % V / V ) 2 8 . 6 9 2 8 . 6 9 2 8 . 6 9 2 8 . 6 9

N i t r a t e i n g a s s a m p l e . . . ( J G ) NO2 i n g a s s a m p l e ....... ( J G )

-


(GR/DSCF) . . . . . . . . . . . . . . . . . (MG/DSCM) . . ............... ( P P M - D R Y ) . . . . . . . . . . . . . . . . . (PPM-WET) . . . . . . . . . . . . . . . . .

NOX E m i s s i o n r a t e .... ( L B / H R )

45

Filename: BEET1 6.WQ1 Date: 16-Dec-94

Facility: American Crystal Sugar

Source: Pulp dryer with multiple cyclones Location: East Grand Forks, Minnesota

Test date: 02/24/94

D. Emission Data/Mass Flux Rates/Emission Factors

*DSCFM BASED ON A STANDARD TEMPERATURE OF 68 DEGREES FAHRENHEIT

Filename: BEETI €? WQI Date: 16-Dec-94



Test date: 02/23/94

Filename: BEET1 6B.WQI Date: 16-Dec-94



Test date: 02/23/94

D. Emission DataIMass Flux Rates/Emission Factors

The NO, samples were collected in volume-calibrated two-liter all-glass flasks. An

aliquot of 25 cc of absorbing solution was added to each flask on-site; the flask was closed;

inserted into the sampling train; and evacuated. The probe was then purged and the sample

collected over a 15 second interval. The flask was then closed; the flask removed from the

sampling train; shook for two minutes and then secured for transport to the laboratory.

.

Upon arrival at the laboratory, the NO, samples are logged in, placed in a designated

area and maintained at 72 "F for 24 hours to allow completion of the conversion of NO to

NO, and absorption in the acidified peroxide reagent. The flasks are then shook to complete

absorption; attached to a mercury manometer and the static pressure and temperature

recorded. The samples are then recovered and analyzed by ion chromatography.

An integrated flue gas sample was extracted simultaneously with each particulate

sample using a specially designed gas sampling system. Integrated flue gas samples were

collected in 14-liter Tedlar bags housed in a protective aluminum container. After sampling

was complete, the bags were sealed and returned to the laboratory for Orsat analysis. Prior

to sampling, the Tedlar bags are leak checked at 15 IN.HC. vacuum with an in-line

rotameter. Bags with any detectable inleakage are discarded. The integrated flue gas

samples on the No. 1 and 2 Boilers were also analyzed for carbon monoxide in accordance

with EPA Method 10 (NDIR).

Testing on the "A" Pulp Dryer Stack was conducted from 2 test ports oriented at 90

degrees on the stack. The test ports are located diameters 2 downstream and 5.5 diameters

upstream of the nearest flow disturbances. A 24-point traverse was used to collect

representative particulate samples. Each traverse point was sampled 2.5 minutes to give a

total sampling time of 60 minutes per run. Visible emission determinations were unable to

be performed due to converging plumes.

Testing on the "B" Pulp Dryer Stack was conducted from 2 test ports oriented at 90

degrees on the stack. The test ports are located 2 diameters downstream of a flow

straightener and 2 diameters upstream of the nearest flow disturbances. A 24-point traverse

was used to collect representative particulate samples. Each traverse point was sampled 2.5

minutes to give a total sampling time of 60 minutes per run. Visible emission determinations

were unable to be performed due to converging plumes.

2

Testing on the "C" Pulp Dryer Stack was conducted from 2 test ports oriented at 90 degrees on the stack. The test ports are located 2 diameters downstream and 2 diameters



total sampling time of 60 minutes per run. Visible emission determinations were unable to

be performed due to converging plumes.

Testing on the No. 1 Boiler Stack was conducted from 4 test ports oriented at 90 degrees on the stack. The test ports are located 4.5 diameters downstream and 2.4 diameters



total sampling time of 60 minutes per run.

Testing on the No. 2 Boiler Stack was conducted from 4 test ports oriented at 90 degrees on the stack. The test ports are located 4.5 diameters downstream and 2.4 diameters



total sampling time of 60 minutes per run.

The important results of the test are summarized in Section 2. Detailed results are

presented in Section 3. Field data and all other supporting information are presented in the

appendices.

3



T e s t No . 2 8 P u l p D r y e r S t a c k

R e s u l t s o f V o l u m e t r i c F l o w R a t e Determination....... M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . 02-23-94

T i m e o f D e t e r m i n a t i o n . . . . . . . (HRS)

B a r o m e t r i c p r e s s u r e . . . . . . . (1N.HG)


Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l n u m b e r o f p o i n t s . . . . . . . . . . . Shape o f d u c t .................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

b D u c t a r e a . ................. ( S Q . F T )


S t a t i c p r e s s u r e . . . . . . . . . . . ( 1 N . W C )

Avg . g a s t e m p . . . . . . . . . . . . . ( D E G - F )

M o i s t u r e c o n t e n t . . . . . . . . . . ( S V / V )

Avg . l i n e a r v e l o c i t y . . . . . ( F T / S E C )

G a s d e n s i t y . . . . . . . . . . . . . . ( L B / A C F )


Mass f l o w o f g a s . . . . . . . . . . ( L B / H R )

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . ( D S C F M )

845

29.43

.84

2

24

Round

59

18.99

UP

-.79

231

27.37

60.3

. 05059 29.28

208383

68652 37082

20

.



T e s t No . 4 A P u l p D r y e r S t a c k

R e s u l t s o f V o l u m e t r i c F l o w R a t e Determination... .... M e t h o d 2

D a t e o f D e t e r m i n a t i o n . . . . . . . . . . . . T i m e o f D e t e r m i n a t i o n . ...... (HRS)

B a r o m e t r i c p r e s s u r e . ...... (1N.HG)


Number o f s a m p l i n g p o r t s . . . . . . . . . T o t a l n u m b e r o f p o i n t s . . ......... Shape o f d u c t ..................... S t a c k d i a m e t e r . . . . . . . . . . . . . . . ( I N )

D u c t a r e a . . . . . . . . . . . . . . . . . . ( SQ.FT)


S t a t i c p r e s s u r e . . . . . . . . . . . (1N.WC)

A v g . g a s t e m p . . . . . . . . . . . . . (DEG-F)

M o i s t u r e c o n t e n t . . ........ ( 3 V / V )

A v g . l i n e a r v e l o c i t y . . ... ( F T I S E C )

Gas d e n s i t y . . ............ ( L B / A C F )


Mass f l o w o f g a s . . . . . . . . . . ( L B / H R )

V o l u m e t r i c f l o w r a t e . . . . . . . . . . . . . a c t u a l . . . . . . . . . . . . . . . . . . . ( A C F M ) d r y s t a n d a r d . . . . . . . . . . . . (DSCFM)

02-24-94

749

29.28

.84

2

24

Round

47

12.05

UP

{

.. 78 209

31.36

60.2

. 05161 29.34

134810

43532 23032

21 .

Particulate Loadings and Emission Rates

The particulate emission rates were determined per EPA Methods 1-5, CFR title 40, Part 60, Appendix A (revised July 1, 1987). In this procedure, a preliminary velocity profile of the gases in the flue is obtained by means of a temperature and velocity traverse. On the basis

of these values, sampling nozzles of appropriate diameter are selected to allow isokinetic sampling, a necessary prerequisite for obtaining a representative sample.

The sampling train consists of a heated glass-lined sampling probe equipped with a Type 5 pitot and a thermocouple. The probe is attached to a sampling module which houses the all-glass in line filter holder in a temperature controlled oven. In addition, the sampling module also houses the impinger case and a Drierite drying column. The sampling module is connected by means o f an umbilical cord to the control module which houses the dry test gasmeter, the calibrated orifice, a leakless pump, two inclined manometers. and all controls required f o r operating the sampling train. -

Particulate samples were collected as follows: The sample gas was drawn in through the sampling probe isokinetically and passed through a 4-inch diameter Gelman Type A/E glass fiber filter. . The particulates were removed at this point and collected on the filter. The gases then passed through an ice-cooled impinger train and a desiccant-packed drying column which quantitatively absorb all moisture from the sample gas stream after which the sample gas passes through the pump and the dry test gasmeter which integrates the sample gas flow throughout the course of the test. A calibrated orifice attached to the outlet of the gasmeter provides instantaneous flow rate data..

A representative particulate sample was acquired by sampling for equal periods of time at the centroid of a number of equal area regions in the duct. The sampling rate is adjusted at each site such that an isokinetic sampling condition prevails. Nwnographs are used to aid in the rapid determination of the sampling rate.

I

3a Pl(1-5) F- 1

Particulate loading and Emission Rates

After sampling i s complete, the filter is removed and placed in a clean container. The nozzle and

inlet side of the filter holder are quantitatively washed with acetone and the washings are stored in a second

container. A brush is often used in the cleaning step to help dislodge deposits. The samples are returned

to the laboratory where they are logged in and analyzed. The volume of the acetone rinse ("probe wash")

i s noted and then the rinse i s quantitatively transferred to a tared 120 cc porcelain evaporating dish and the

acetone evaporated off at 97-105 O F . This temperature i s used to prevent condensation of atmospheric

moisture due to the cooling effect induced by the evaporation of acetone. The acetonefree sample is then

transferred to an oven and dried at 105 "C for 30 minutes, cooled in a desiccator over Drierite, and then

weighed to the nearest .01 mg. The filter sample i s quantitatively transferred to a &inch watch glass and

dried in an oven at 105 "C for two hours. The filter and watch glass are then cooled in a desiccator and

the filter weighed to the nearest .01 mg. All weighings are performed in a balance room where the relative

humidity i s hydrostatted to less than 50% relative humidity. Microscopic examination of the samples i s

performed if any unusual characteristics are observed. The weight of the acetone rinse is corrected for the

acetone blank. The Drierite column i s weighed on-site and the water collected by Drierite i s added to the

condensate so that the total amount of absorbed water may be ascertained.

./ Integrated flue gas samples for Orsat analysis were collected simultaneously with each pollutant

sample. The samples were collected in 15-liter gas sampling bags at a constant flow rate throughout each

particulate run. The bags were at a constant flow rate throughout each particulate run. The bags were then

returned to the laboratory and analyzed by Orsat analysis. Standard commercially prepared solutions were

used in the Orsat analyzer (sat. KOH for carbon dioxide and reduced methylene blue for oxygen).

)

F- 2

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