“liL4QLG2g3L44.3%j5421 - Alaska DEC...Whitestone Logging Project: Sortyard cleanup CLUe Sample...

Smith Bayliss LC”esche Inc Environmental Consu’ ts and EngineersRichard Smith FE. (907) 747-5775 ii, Seward Street #10Randolph Bayliss RE. (907) 586-6813 Juneau Alaska 99801

Robert LeResche PhD (907) 586-8338 fax (907) 586-6819

Wayne Valentic by fax to 225-2196Sealaska Timber Corporation2030 Sea Level Drive #202Ketchikan, Alaska 99901

Whitestone Logging Hoonah Sortyard Investigation

On July 1 1999 Jason Ginter and Amy Randolph of Smith Bayliss LeResche Inc directed theexcavation of suspected oily materials at the northwest corner of Whitestone Logging’sHoonah sortyard. Although the materials did have an odor, field screening of the materialsusing the hot water sheen test did not confirm petroleum contamination.

/ Whitestone Logging removed about 100 cu çyardsof shot rock materiaJ from the top foot of

v’’1 ‘ this area and hauled it to their approved stockpile site. The removed material consisted of“

\ oversized (greater than 2”) shot rock fill with some fines. We took six clearance samples fromthe excavation area and two samples from the removed material. We sent the samples to

çj’ ‘5 Analytical Resources, Inc. (ARI) in Seattle for analysis. ARI analyzed the samples for dieselJ’ range organics (DRO), residual (oil) range organics (RRO), and total BTEX (benzene, toluene,

“ < ethylbenzene and xylenes). All clearance samples are below ADEC Method Two action levels

D >r of 230 ppm for DRO and 9,700 ppm for RRO. Sample results are listed in the table below.

Soil sample results in ppm

Sample ID DRO RRO Total BTEXWSYCL01* 78 78 None detectedWSYCL02* 48 61 None detectedWSY-CLO3 27 29 None detectedWSY-CLO4 ‘ 48 30 None detectedWSY-CLO5 94 81 None detectedWSY-CLO6 190 120 None detected

WSYCZ01** 2,200 4,400 None detectedWSYCZ02** 450 280 None detected

*field duplicate samples**these samples characterize removed materials

Although the removed materials exceed Method Two cleanup levels for diesel, laboratoryanalysis does not show a positive pattern match for diesel. ARI’s analysts indicate that thecontaminants more closely resemble hydraulic oil. WSY-CZO1 did contain 0.00454 ppm1,1 ,2,2-tetrachloroethane, which is also below the Method Two cleanup level of 0.01 ppm. Werecommend no further action at this site, and await ADEC’s decision on the status of theremoved materials.

“liL4QLG2g3L44.3%j5421Attachments: ARI lab report

Smith Bavliss LeResehe Inc by site sketchRandolph Bayliss, P. E., Environmental Engineer,Managing Principal9 July 1999

field duplicate samplesthese samples characterize removed

Sample Location

Site sketch7/1/99Contaminatedmaterial removal

Smith Bayliss LeResche Inc.119 Seward Street #10Juneau, Alaska 99801

(907) 586 6813

Client:Whitestone Logging

Project:Sortyard cleanup

CLUe

Sample results in ppm

SampleWSY—CL01WSY—CLO2’WSY-CLU3WSY—CL04WSY—CLO5WSY—CLO6wsY—Cz01..WSY—CZ02t

CLO5

DRO78482748941902,200450

ERa78612930811204,400280

Bedrock.

Total BTEXNDNDNDNDNDNDNDND

0L03

cz01

/NORTh

0

in

toIII’’

Scale in feet

ÂME 7/9/99

Sealaska Timber Corporation

0 a

MAIN HIGHWAY

Icy StraitsMill Sit!

SECTION IC.

VICINITY MAP:Sealaska Corporation and Fluna Totem Corporation Land Ownership

7Pollution Prevention PlanWhilestone Maintenance Facility

Sealaska Timber Corporation

/

Scale: 1 inch = 250 feet

I’

SECTION 3.D.

The Whitestone MaintenanceFacility Drainage Site Plan

S

Port Frederick

LEGEND

-1— “Drainage

Finger’s

Bay

/

Surnp #2/Outfall #2

Sump #1/Outfall #1

Equipment Washwator

Drainage Ditch

0

-a-,

0

-

#4

S*imp #3

aS

0

/

tPollution Prevention PlanWhitestone Maintenance Facility

Sealaska Timber CorporationC)

Fuel Tank FarmCovered Saw Gas Dispensing Shed:

Equipment

Scale: 1 inch = 125 feet

C

Equipment

Parking

9

1-55 gal. Barrel 2-Stroke Oil

3-55 gal. Barrels Saw Gas

2 - 5.000 gal. Gasolinc

1 - 10,000 gaL #1 Diesel

4- 10.000 gal. #2 Die,

OillWater

Separator

Parts

Storage

Non-Operational

Wash Ramp

Upper Shop

Storage

Oil Dispensing

Container

Equipment

Storage

2o q?Ac2.Es

Operational

t SECTION 3.E.

The WhitestoneMaintenance Facility

Site Plan

Pollution Prevention PlanWhitestone Maintenance Facility

,? 0 0P Analytical Resources, Incorporated

Analytical Chemists and Consuftants

9 July 1999

Jason GinterSmith, Bayliss, LaRescheFax: 907-586-6819

RE: Client Project Whitestone BoatyardAR! Project No: AM3I

Dear Jason:

Analytical Resources, Inc. (ARI) received eight soil samples on July 2, 1999. ARI receivedthe samples Intact and there were no discrepancies in the paperwork. The samples wereanalyzed for diesel and motor oil range hydrocarbons.

The analyst who performed this analysis noted that WSY-CLO1, WSY-CLOS, WSYCLO6, wsy-czoi, and WSY-a02 have patterns overlapping In the diesel and motoroil ranges that could possibly be a heavy diesel and/or transformer oil plus a hydraulic oilor lube oil. The analyst also noted that samples WSY-CLO2, WSY-CLO3, and WSYCLO4 could also contain these products In addItion to another organIc’ Interference In themotor oil range.

No analytical complications were noted.

Sincerely,

ANALYTICAL RESOURCES, INC.

Mary Lou FoxProject Manager206-38g-6155e-mail mary1ouCpñIabs.com

MLFJmIf

cc: file #AM31

333 Ninth Avenue North • Seattle WA 98109-5187 • 206-621-6490 • 206-621-7523 fax

C)() ANALYTICAL

40 RESOURCESINCORPORATED

TOTAL DIESEL RANGE HYDROCARBONSAZ102 TPH4 Range 010 to 024 by CC/rIDan4 Motor Oil

LIMS ID: 99-9852 QC Report No; AN31-Smich Baylies LeResche Inc.Matrix; soil Project: Whicescone Boatyard

Data Release Authcrized:,jb, Date Received; 07/02/99Reported; 07/C9/99mI..jYtYWV

Oats Ciltition Diesel ‘Mc Motor oil surrogateLa IC Saeole TO AnayeG Factor Range to Range Recovery

AZI3IMB Method Blank 07/07/99 1:1 5.0 0 --- 10 U 104%AN31A WSY-CLO1 07/07/99 1:1 78 NC 18 135%A2’lJlS WSY-CLO2 07/07/99 1:1 48 NO 61. 93.0%AN31C WSY-CLO3 07/07/99 1:1 27 NO 29 102%A1I31D WST-CL04 07/07/99 1:1 48 NO 30 89.0%flI3IE WSY-CLOS 07/07/99 1:1 94 NO 61 98.0%N’131F wsy-ctos 07/07/99 1:2 190 NO 120 94.0%A1’1310 Wsy.C10l 07/07/99 1:50 2,200 NO 4,400 DAM31H WSY-0Z02 07/07/99 l;10 450 NO 280 90.0%

Velusu reported in ppm (mg/kg) on a dry weight Snig.

Surrogate is Methyl-Arachidate.

• ID indicates, in the opinion of the analyst, the petroleum product with the best patternmatch. ‘NO’ indicates that there was not a good match for any of the requested products.Diesel quancitacion on total peaka in the range from 010 to C24.Motor Ci]. quantitation on total peaks in the ran9e fron 024 to 038.

Data Qualiti•rs

U compound not detected at the given detectier. limit.J Indicates an estimated value below the calculated detecc±on limit.S No value reported due to saturation of the detector. Dilution required.D Indicates the surrogate was not detected because of dilution of the extract.E Indicates a value above the linear range of the detector. Dilution required.Nit Indicates no recovery due to macrix interference.B Indicates compound also detected in the method blank.

TORN-i WA TPED

j’n S $çii import-bi.mp.wit printed: // 8/99

Data Analyst: Jeff RobersonWorkljst created: 7/ 8(99Corirnents:

RUN CODE (null): S

Worklist: 777

ri&lyzed by: LJRnalysis Jots: 7/ 7/99

/Tjine: 7/ 7/99 lStOSL/gni or n/mg): 0.770

Iristrurnant: finnsSmp1e Amt: 0.710

Purge Volt 5.00

SURROGATE RECOVERIES

d—l,—DicIoroethar,ed8—To 1 uene8romotlJornDenzened4—l 2—Diclilorobenzene

Compound -

Chl.o-ometbaneviflyl ChlorIdeS romomethentC h it r oc th at eTrichiorotl;jo-omethaneAcrolein

I, t—OiehloroetheneBrotnoethaneMethyl IodideNethyiene ChlorideCarbor DisulfideAcrylontriletrans—i ,2—DichloroetheneVinyl Acetate1. 1—Dichioroetnane2— Bu tan one2, 2—Dichlcropropanecis—1,2—Dichkroeth.u-ieChlorDforrnBr ornoc bit r orneth are1,1, 1—Trjchl o’oethane1 ,l—DichlorcpropeneCarbon TetrachlorideI .2—Diehiojoetnane

S. 350‘15. 76047. 57047.660

L Rau gmi

o - 000.000 00o -

0 . 000 000 - 000 - 000 - 000 000 - 003.85o . go0 - 000.000 - 000 - 00o -

0 . 00o - 000.000 . 000 000 - 000.00C . 660.000.000 - 00o .eo0.000 - 000 . 000.000 - 00o -

0 - 000 - 000 -000.00

Not RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requestedjqussted

Not RequestedNot RequestecNot RequestedNot RequestedNot RequestedNot Requested

equested000No RequestedNot RequestedNot RequestedNot RequestedNot RequestodNot Requested

C) C

1. Ai’131 A99--9852 -2SV—CL01

Soil

LEVEI(LoLow, M—t’1d, t4’L4ater): LTotal Solids: 92.23

Analysis DateDL or et Wt(

Aiiiount Found tRee

gm—dry—ut

96391595 i95.3

l,1,2—TrichlcrotritlJoroethaneCe to ‘-is

PieAZfltEQJJlifkjot RequestedNot RequestedNot RequestedNQt RequestedNot RequestedNot Requested

.— eflZeneTrichiorcetheneI, D—DicnioropropaneS r o’no d i c h lo rome than eDibromonethane2—Chioroethylviriyls ther4—Msthyi---2—Pentanone (tI8K)cis—1 3—Cichioroprapene

— Toluenetrans—i ,3—Oichloropropene1. 1,2—TrichloroethaneEthylene Dibromide2—i-4exan one1, 3—DIchie r-opropaneTetrachioroethene

>-cc

uJcca-

0

0 C)

Finn S Soil Import OrKli5t: 777F5imp.t.4f printed: 7/ 8/99

Data Analyst: Jeff Roberson analyzed by: LJRL.Jorklist created: 7/ 8/99 Analysis Oats: 7/ 7/99Corrrents:

Dibrornochiorome Chaos 00 Not RequestedChiorobenrene 0.00 Not Requested1,1,1,2—Tetrachioroutharie 0.00 equected

“Ethylbenzene ø.00.—m,p—Xylene 0.00 0.00

o—Xylene 0.00 .00Styreric o .00 No Requestederomoform 1.0 0.00 Nat Requested1 • 1, 2 • 2—Tetrach.Loroethane 0.00 Not Requested1,2,3—Trichioropropane 0.00 Nol: Requestedtrans—i 4—Oichloro—2—butene 0.00 Not Requestedn—Propyibenzene 0.00 Not Requestederoinobenzerie 0.00 Not RequestedIsopropylbenzene 0.00 Not Requested2—Chiorotoluene 0.00 Not Requested4—Crilorotoluene 0.00 Not Requectedtsrt—Sutylbenzene 0.00 Not Requestedi,3,S—Trimethylbenzene 0.00 Not Requestedi,2,—Trirnethylbenzene 0.00 Not Requestedsec—Butyibenzene 0.02 Not RequestedI—IsoprQpyltoiuer-Ie 0.00 Not Requested1,3—Oichlorobenzene 0.00 Not Requested1,4—Dichlorobenzene 0.00 Not equestean—Rutylbenzene 0.00 Not Requested1,2—Dichioroberizene 0.00 Not Requested1,2—Oibromo—3—chloropropane 0.00 Not Requested1 2,4—Trichlorobenzerie (6,00 Not RequestedHexechiorobutadiene 0.00 Not RequestedNaphthalerie 0.00 Not Requestedi2.3—Trichlorobenzene 0.00 Not RequestedDichiorodifluorometharie 0.00 Not Requested

•j Lwa:0-

C C

Finn S Soil Import L.JorIcliSt: 777FSimp.wlf prtnted: 7/ e/99

Data Analyst: Jeff Roberson Analyzed by; LDRL.Jorkliet created: 7/ 8/99 Analysis Date: 7/ 7/99Corrrientsr

LEVEI(LLot.J. M=Med, WrnL4ater): LRUN CODE (null): S Total Solids: 93.05

Analysis Date/Time: 7/ 7/99 18:342. AM31 DL or Wet Wt(L/gm or rn/mg): 1.09

99—9853 USY—CLO2 In,trunpent: finnsSoil Somple Art: 1.01 gm—dry—ut

Purge Vol: s.oeSURROGATE RECOVERIES Amount Found tRec

dA—1.2-.Oichloroethane 8..2i0 96.4dO—Toluerie 6.S80 9.28romofluorooerlene G7540 95.1d4-l .2—Oichlerobenxone 8 .510 97.0

Ccmpound DL Raw Mit Sample_Amount (0)

Chlorometharie 0.00 Not RequestedVinyl Chiorid€ 000 Not RequesteeRornoetiane 0.0 Not RecuestedChloroetnarie 0.00 Not RequestedTrichlorofluorome.thane Q. 00 Not RequestedAcrolein 0.00 Not Requested3. • 1 .2—Trichlorotrifluoroethane 0 00 Not RequestedAcetone 0.00 Not RequestedI, 1—Djchloroethene 0.00 Not Requested8romoethano 0.00 Not RequestedMethyl Iodide 0.00 Not Reqi.iestedMethylene Chloride 3.79 Not RequestedCarbon Cisultide 0.00 Not RequestedAcrylonitrile 0.00 Not Requestedtrns—i.2—Oicl-loroethene 000 Not RequestedVinyl Acetate 0.00 Not Requestedi,1—Dichloroethane 0.0€ Not Requested2—Sutanone 0.00 Not Requested2.2—Dichloropropane 0.00 Not Requestedcis—1 • 2—Dichloroethene 0.00 Not RequestedChloroform ‘.60 Not Requestederomocfllcronwthanp 0 .00 Not Requested:,1,l—Trichloroethane 0.00 Not Requestedi,1—Dichlo’oprope’ie 0.00 Not RequestedCabon et-acloride 0.00 Not RequestedI • 2—Dichlor-oethane quested

—Benzene 0.00 0.00irichi ores there 0.00 o RequestEd1.2—Dichloropropane 0.0€ Not Requestederomodictiloromethane 0.00 Not Requestedflibromomethane 0.20 Not: Requested2—Chloroethylviriylether 0.00 Not Requested4—Methyl2—Pentanone (M18K) 0.00 Not Requestedcis—1 3—oichloroproptne 0.00 quested

._—Toluene 0.00 0.00 1—trans—1,3—Oichloroprnpene 0.00 equested1,1,2—Trichloroethane 0.00 Not Requestedthylsne Dibroirtide 0.00 Not Requested2—knanone 0.00 Not Requested LI)1 .3—Qichlo-opropane 0.00 Not RequestedTetrachioroethene 0.00 Not Requested a

S

Finn S Soil IniortFsinç.wlf printi3d; 7/ 8/99

0

Data Analyst: jeff RobersorWorklist created: 7/ 8/99Coninents:

Dibronochl oromethaneChlorobenzene1,1,1, 2—Tetrachioroethane

rEthylbenzene..—ni,p—Xylene

— o—XyleneS ty r e ci e

Erornotorm1,1.2.2—Tetrachioroethane1,2.3—Trich)or’opropanetrans—i, 4—Ujcnloro—2—tuterien — P r opyl b n I en eB r omo b € n zen eISDO ro py be riz one;—Dnlorotoiuene

—c il Cr etc I se:le

t € r t— S u ty 1 b € n z 0 fl e1 3, S—Trirnethyibenzeni1,2, 4—Trimcchylbenzenesec—Butylben7ene4—Isopropyl toluere1,3—Dic;hlorobenzene3., 4—CichJ.urobenzenen—Sutylbenzene1., 2—Dch1oroberizene1, 2—Dihromo—3—chloropropaneI ,2,4—TrichlorobenzeneHO xac’.lo rob ii tadieNaphthai.anc1 ,2,3—Trichlor-obenzeneIDichic rodi tluoronethane

orklist: 777

Analyzed by: LiRAnalysis Date: 7/ 7/99

7.cc

cc0-

0.000 - 00e.0 - 000 . 000.000 00

1.3 0.000.000 000 - 000.000 - 00

• 00

0.00O 000.000.300 - 000 - 090 .000 - 0$0.000 - 000 . 003 . 000 .000. dO0 .000 - 00

Not RequestedNot ReqUested

Requested

o . go0.00

O equestedNot RequestedNot RequestedNot RequestedNot RequestedNot; RequestedNot RequestedNot RequestedNut RequestedNot RequestedNot RequestedNd: Requested

Not RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

Finn S Soil ImportFSimp..ulf printed: 7/ 8/99

rm

Data Analyst: Jeff Robersont.Jorkljgt created: 7/ 8/99CorTTnents:

Jrklist: 777

Analyzed by: LiPAnalysis Date:

C

7/ 7/99

RUN CODE (null): S

3. AMSI. C99—98S4 LSY—CL03

SURROGATE REDVERILS

• 2—DichloroetianedR—To luete8romotluorohezeneJ4—: • 2—Olchlorobenzene

Compound

ChiorometbaneVinyl ChloriøeBromomethaneChjoroetharieTrjchlorotluorcniethaneAcrolejnI, i,2—TrichlorotritluorosthaneAce tone1, 1—Oichloroethene8romoethancMethyl IodideMethylene Chlor.Lde.Carbon DisulticeAcrylonltriletrans—i .2—O.ichloroetheneVinyl Acetate

• l—Dichlooethane2—utanone2, 2—Oicr.ioropropare(rig—i, 2—Oichlor-n€ttis’r-,eChlorofo-nB romoch lo r orneth a ne1,i.i—Trjchloroethan€1 .l—OichlorcpropeneC.3rbon TetrachlorideI • 2—Dicl,lorcethorieSenzeneI rich 10 roe then o1, 2—DichloropropaneOromodLehiorome thaneDibromomethane2—Chi o roethy liinyl ether4—Methyl—2—Pecitanone (MISK)cis—i .3—CichloropropeneToluerietrans—i ,3—Oichloropropenu1 1,2—Trichloroetbanehy1ene Oibrornide2—Wexanone1, 3—DichloropropaneTetrachioroethene

Amount Pound tRec

60.240 100.48.410 96.l49.450 98.9

98.9

.00o .

0 - 000O00 000.000.000 - 00o . go0.00o .

4 280 . 000.0000Oe -

0.000.000.080 - 000.300 . 000 .000 000 - 00‘1 - 640.000 000 . 000.00O .000 000 00o .geo .oo0 - 000.000 . 000-000.0%O . 00

Not RequestedNot RequestedNot ReqjestedNot RequestedNot: RguestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RecuestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

equested0.00N equestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

eqiiestvd0-00

equestodNot: RequestedNot RequestedNot RequestedNot RequestedNot Requested

LEVEL(LLow. M=Med, L44.4ater); LTotal SolIds: 92.28

Analysis DateDL or et t(

/Tjme: 7/ 7/99 19:00or M/cng): 6.740

Iristrurrient: finnsSample Anit: 0.583

Purqe Vol: 5.00gm— d ry— t

1mPTEEi)

>-ft‘C

iiUift0

‘C

0

0 0

Finn S Soil import L.JorRlist: 777FSimp..uif printed: 7/ 8/99

Data 4nalyst: Jet Robereon fnalyzed by: LJRWor4clist created: ii 8/99 Analysis Date: 7/ 7/99Coments:

Dibromoehlo’oriethane a .oe Not RequestedChloroben2ene ØØg Not Requested1 1,1,2—Tetrachioroethene 0Q,0 equested

—Eb,ylberizene 0.00..—rn,p—Xylene 0.00 0.00_.—o—Xyl€rie 0.00 0.00

Styrene 0.00 No RequestodSromoform 1.0 0.00 Not Requested1,1,2,2—Tetrachioroothane 0.00 Not Requested1,2,3—Trichioropropane 0.00 Not Requestedtrans.—1,4—Oi.chloro—2..butene 0,00 Not Requestedn—Propylbenzene 0O0 Not Requestedlrorobenzene o - Not RequestedIsopropylbenzene 0.00 Not Requested2—Chioroto) uene 000 Not Requested4—Chlorotoluene 0O0 Not Requested

te-t—Butyibernene 0.06 Not RequestedI,3,5—Triiiethylbenzene 0.00 Nd: Requested1,2, 4—Trirnethylbenzer’e 0.00 Not Requestedsec—8uty1benzrie 0.00 Not: equested‘—Isopropy. toluene 0.00 Not Requested:,3—Cicrlorohenzene 0.00 Not RequestedI, S—Dichlo robenzene Not Requestedn—Sutylbenzene 0.00 Not Requested1,2—Dichlorobenzene 0.00 Not Requested1,2—Oibromo--3—chloropropene 000 Not: Requested1, 2,4—Trichlorobenzene 0.00 Not RequestedNexachiorobutadiene 0.00 Not RequestedNaphthaiene 0.00 Not Requested1,2,3—Trichioroberizene 0.00 Not RequestedOichlorodi fluoromettiane 0.00 Not Requested

>-

zoLu

Finn S Soil ImportFSimp.df printed: 7/ sig

Data Analyst: Jeff Rcbersont$or)cjist created: 7/ 6/99Conments:

.Jorklist: 777

Analyzed by: LJRAnalysis Date: 7/ 7/99


d4—l • 2—DichioroethanedB—Tol jgreBromofluoroberizeried4—l, 2—Oichlorobenzene

Compound

ChiorornethaneVinyl ChlorideBromomethaneChic roetbarie

i chic r of luo - one thaneIcrolein1, 1,2—TrichiorotritluoroethaneAcetoneI • 1—Cichioroethene&romoethaneMethyl IodideNethylene ChlorideCarbon DisulfideAcrylonitriletrans—i, 2—DichioroetheneVinyl Acetate1 • 1—Dichioroethane2—Butanone2. 2—Dichloropropaneoie—i, 2—Dichioroet’eneChloroformS romochiorornetfiarie1. 1,1—Trichloroethacie

i—DichloroprepeneCarbon Tetrachioride1 .2—DichiorcethaneBenzeneTrichioroethenca1 • 2—Oichlo ropropaneSroanodjchlorornethnneDibromomethane2—CM o roethylvi nyle ttier4—Methyl--2—Pentanone (MIOK)cis—1 —Vichloropropene

—Toluenetrans—I ,3—Oichloropropene1,1,2—Trichloroethar,eEthylene Dibron!ide2—hiexanone1. 3—DichloropropsneTetrachioroethene

Amount Found tRee

Si.ae0 1’2.49.060 98.949.040 951

100

DL Raw Amt

0 - 000 - 000 . 090 - 00

• goo - ee0 - 000.000090 . 000 .

3 - 5300

O - 000.000.000 039 . 000.000 - 000.000.000.000.00O . 00I . 570.000 - 00e0 - 090 . 09e. 000.000 . 000 . 00a -

0.000.00o - 000.000.00

Q)

Not RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedN1: RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

e quested0-00

equestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

quested9 * 30

questedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

C C)

RUN CODE (null): S

4. AM31 D99—9855 L4SY—CLO4

E’.’1(1.’Low, MeMed, L-4’ater): LTotal Solids: 93.96

Ana1ys Date/Time: 7/ 7/99 19:25DL or Uet L.Jt(Ljgm or M/rng): 0-910

Intrunient: finnsSample Amt: 0.855

Purge Vat: S.0*gm—d ry—i.t

1%

a

a0

7

0 0

Finn S Sofl Import Worklist: 777FSimp.wlt printedt 7/ 8/99

Data Analyst: cleft Roberson Analyzed by: LJRWorklist created: 7/ 8/99 Analysis Date: 7/ 7/99Conirents:

Olbrornnchloromet:hano 09 Not RequestedChiorobenzene 0.00 Not Requested1,1j,2—TetrachiDronthane 0.00 quested

‘‘Ethylbenzene o.oe..—rn.p—Xylene t.oc 0.00,.—o—Xyiene 0.00 0.00

Styrene 0.08 o RequstsidRro,oform 1.0 000 Not: Requested2 ,1,2,2—Tetrachloroethane 0.09 Not Requested1.2,3—Trichloropropne 0.00 Not Requestedtrans—i, A—Oichloro—2—butene 0.00 Not Requestedn-Propy1benzene 0.00 Not RequestedOromobenzeri€ - Not RequestedIsooropylbenzene Not Requestad2—Chiorotoluene 0,00 ot Qequested—Chloroto1LJere 0 .00 Not Requestedtert—ButylLienione 0.00 Not Requested1,3S—Triretfly1benzene 0.00 Not RequestedI • 2, —Trirne thy1benone 0.00 Not Requestedsec—Butylbengene 0.00 Not Requestedi—Isopropy±tctuene Not Requested1.3—Dichlorobenzene 0.00 Not Requested1,4—Dichlorobenzene 000 Not Requectedn—8utyIbenene 0,0 Nd: Requested1, 2—Dchiorohenzene 000 Not Requested1,2—Oibrorno—3—cnloropropar’.e 0.00 Not Reçuestedi,2.4--Trlcnlorobertzer’e 0.00 Not RequestedHexachlcrobutadiene g.oØ Not RequestedNaphthaiene 0.00 Not Requested1 • 2 • 3—Trichlorobenzene 0 .00 Not RequestedDichl o rodiFluorumethanp 0.00 Not Requested

>-‘I

z

D

t

C 4,LL)9-CLDS VO

Finn S Soil Irnpot JonIclist; 1G25

F5imp.wif prjn_@d: 1/ 9/99

Data nalysc: 2eff Robercn nalyzed by: LR

Worklist created: 7/ 9/99 Analysis Gate: 7/ 8/99

Corinents:

LEVEL(LL0w, Med, L.4nUatcsr): LRUN CDDE (null): S Total Solids: 94.70

Analysis Gate/Time: 7/ 699 i6:2DL or t4st Uat(L/gw or ‘i/rnj,: 1.18

Y9—SS6Et_GLOS

tnstrurnent: FinnSSan’ple Amt 1.12 gm—dryt

Purge ‘iol: 5.0%

SURROGATE RECOVERIES Ariount Found %Rec

d4—l ,2•Oichloroethane 51.980 104.d8—Tolugne S0.340 101.Bromofluorobenze,-ie 50.990 102.d4—1 . 2—Qjchjorobenzone Si. 500 103.

____________________________

Comocund DL Rau Amt amount

Chioromethar-is 0.00 Not RequestedVinyl Chloride 0.00 Not Requested8romompthane 0.00 Not RequestedChloroethane L00 Not RequestedTrichloroflucrornethane 0.00 Not RequestedAcrolein 0.00 Not Requested1.1,2—Tnjchlorctrjfluopoer.hane 0.00 Not RequestedAcetone 0.00 Not Requestedi,l—Djchloroechene 000 Not RequestedSroqnoechane 0.00 Nor RequeetedMethyl. Iodide 0.00 Not RequestedMethylene Chloride 0.00 Nd: RequestecCarbon Cisulljoe 0.00 Not RequestedAcrylonitrjle 0.Ø Not Requestedtrans—1,2—Ojchlorogthene 0.00 Not ReQuestedVinyl cetate 0.20 Not Requested1.1—Dichloroethane 0.00 . Not Requested2—Butanone 0.20 Not Requested2.2—Dichloropropane

. 0.00 Not Requestedcis—i • 2—Djch1oroetIen 0.00 Not RequestedChloroform 0.00 Not RequestedBromooblorornethane 0.00 Not Requestedl.i,l—Yrichloraethane 0.30 Not Requestedl,l—Oichioropropens 0.20 Not RequestedCarbon Tetrachlonide 0.00 Not Requestedi,2—Oichloroethane 0.00 quested

0.30 0.00Trichioroethene 0.20 !quested1, 2—Oichloropropane 0.00 Not RequestedBrcmodichlorcme thane 0.00 Not RequestedDibromomethane 0.00 Not Requested 02—Chloroethvlviriylatlier 0-00 Not Requested4—Methvl—2— entanone (I8K) 0.00 Not Requested Liicu—i, —Cichioropropene 9.00

0.00trans—i .3—Oichloropropere 0.00

3uested

quested 0...l,1,2—Trjchloroethane 0.00 Nol: RecuestedEthylene Dibromide 0.09 Not Requested2—Hexanone 0.00 Not Requestedl.3—Dichloropropane 0.00 Not RequestedTetrachloroethene 0.00 Not: Requested

0 0

Firm S Soil Import t.Jrk1ist 1126

FSimp..4f prinfied: 7/ 9/99

Data Analyst: 3eff Roberson na1%y-eed by: LJR -

Workljst created: 7/ 9/q9 na1ysis Oats: 1/ 6/99

Coments:

Qibromochloroinethane 0.00 Not Requested

Ch1orob,nzene 0.00 Not Rqi,ested

1,1,1, 2—Tetrachioron t:hane 0 00 equestcd

€thylbenzene 0.00 0.00m.p—Xylsneo—XyleneStyrene 0.00 . RequestedSromoform 1.0 0.00 Not Requested

t,l.Z.2—Tetrach.oro€R:hane @.00 Not Request€d

l.2,3—Trich)orcprcpane 0.00 Not Requsced

trans—i • 4—Oichlora—2--butene 0.00 Not Request:d

n—Propylbenzene 0.00 No I: Requested

Sromobenzene 0.00 Not RequestedIsopropylbenzane 0 00 Not Requested

2—Chiorotoluens 0.00 Not Requestod4—Chlerotojuane 0.00 Not Recuestedtert—Qutylbeezene 0.00 Not Requested1,3,S—Tri’nethylbenzene 0.00 Not Requested1,2,4Trirnethy1bnzerie 00a Not Rsquastodsec—Butylbanzene 0. 0@ Not Requested4—Isopropy.Itoluene 0.00 Not Requested1,3—Dich1orobsnene 0.00 Not Requested1, 4—Oichlo robenzone 000 Not Request3dr—eutylbenzene 0.00 Not Requested1,2—Oichlorobenzer,e 09B Not Requested1,2—Oibromc--3—chloroproparie 0.00 Not Requested1,2, 4—rich1orobenzer C. 00 ‘4ot Request9dHexac.’,IQrohutieng 0.20 Nol: Requost€dNaphthalene 0. 0 Not Requestedl2,3—Trjch1orobenzene 0.00 Not RequestedDlchlorodj fluorometh3ne 0 00 Not Requested

>-ItcC

—JoLUcc0

Finn S Soil Import51mp.w1f printed: 7/ 8/9

Data Analyst:Woriclist created:Cements:

d4—l • 2—Dicoloroethaned8—ToLueneBromofluorobenzened4—1, 2—Dich 1orobenz,irie

1 .3—Dichlor-opropansTetrachioroethene

52.48.76049 18050.020

DL

Worldist: 777

tnalyzed by: L2RAnai.ysis Date: 7/ 7/99

jTime: 7/ igg 20:15L/gm or N/mg): 0790

instrument: rnnsSampe Anit; 0.751

Purge Vol: 6.00

0 .000 .

0 . 000 - 000.000 . 000.000 - 000.000. 000 . 004 09o .

0 000 000.00O 000.000 .00o . 000 .000 - 000O00 - 000.4 . Sio .

O .000.000.a.0 . 000.00O . 000 . 000.00a . 00c.0.030.000.00

Not RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RaquestdNot: RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestadNot: RequestedNot RequestedNot RequestedNot RequestedNot Requestedot RequestedNot RequestedNor RequestedNot Requested

Io-t_..çequestec

Nta-rieqLestedNot RequestedNot RequestedNot RequestedNot RequestedNot Requested

eq u e ste d.00

— equestedNot RequestedNot RequestedNot RequestocNot RequestedNot Requested

C) C

iett Roberson7/ 8/99

RUN CODE (null) : S

5. AM31 F99—9857 uJsv—cLe6


LEVEI(L-zLow, M=Mc-c. .—mL4atr): LTotal SOlids: 96.09

Analysis DateDL or .Iet -Jt(

knount ‘ourid

Compound

gr’i—e ry—it

tRec

105.97.599.4100.

R au 4mt

ChloromethaneVinyl ChlorideBromomethaneChloroetf,aneTrichlorofluoromethaneAcrolein1,1 2—TrichIorotrifluoroethaneAce one1, 1—Dichloroethenet3roiiioethaneNiethyl IodideMethylene ChlorideCarbçn Qisqjfide4cryionitr- tietrans—i ,2Dichloro€theneVinyl Acetate1. 1—Cichloroethare2—Butanone2, 2—Oichloropropanecig—l , 2—OichlcroethenaChloroformSromochlo’-ometr,jne1, 1, 1—Trichioroethane1.. 1—DichloropropeneCarbon Tetrachioride1. .2—Dichioroethane— SerzeneYr ich i.e roe thene1, 2—DlchloropropaneSron,odichioro,nethaneDibromometh,3ne2—Ch 10 roe thy h-I nyle the4—Met;lyl—2—Pentanone (MISK)cia—i, 3—Dichioropropene

— Toluenetrans—i ,3—Oichloropropene1 1,2—Trlchloroethanecbiyiene Cltbrornide2 —H a x ar one

>-Ix

wcc0

9

C) C

Finn S Soil Import .Jorklisz: 777F5irnp.wlf printed: 7/ 8/99

Data Analyst: Jeff Roberson Analyzed by: LJRork1flt createch 7/ 8/99 ria1ysis Gate: 7/ 7/99Cements:

Cibromochlcromethane O.00 Not RequestedChlorobenzene 0 00 Not Requested1,1,1,2—Tetrachioroethanu Ø.Øg equested

—Ethylbenzene 0.00—m.p—Xy1ee 0_00 0.00

o—Xylerie 0.00 0.0.Styrone 0 00 RequestadSromolorm 1.0 0.00 Not Requested1.1,2,2—Tetrachioroethane 3.00 Not Requestedi.2,3—fliohloropropane 0.00 Net Rsquestedtrans—i 4—Uichiora—2—buteiie 0.00 Not Rsqusst&dn—Proylbenzere 000 Not RsqJest2dRromobenzane .00 Not RequestedIsopropylbenzene 000 Not Requested2—Chlorotoiuer.e 0.00 Not Requested4—Chiorotoluene Ø.aO Not Requestedtert—Sut1benzana 0.00 Not Requested1,3,5—Trxmethylbenzsne 0.00 Not Requested1.2, 4—Trimethylhenzene 0 00 Not Requestedsec—Butylbenzene 0.00 Not Requested4—Isopropyltotuene 0.00 Not Requested1,3—Ojchlorobenzene 0.00 Not Redijested

• 4—Djchlorobenzene 0.00 Not Requestedn—Butylbenzene 0.00 Not Raquested1 ,2—Dichloroberizene 0.00 Not Requestedi,2—Qibromo—3—chloropropans 000 Not Requested1,2, 4—Trichiorobenzer’e 0.00 No 1: RequestedHexachiorobutadjene 0.00 Not RequestedNaphthalsrle 0.06 Not Requested1,2,3—TricH].orob€nzene 0.0 Not RequestedDichiorodi tluorometh.ine 0.00 Not: Requested

1-4.z 4,st

t

/0

o 0

Finn 5 Soil Import orklist: 777

FSimol1 printed: 7/ S199

Data Analyst: Jeff Rcberson Analyzed by: LJRWorklist created: 7/ 0/99 Analysis Date: 7/ 7/99Coirnients:

LEVEL(L=LOW. il—Mod. UJJacr): LRUN CODE (null): S Total Solids: 92.18

Analysis Data/Time: 7/ 7/99 20:40DL or t1vr L.Jt(L/qrn or M/rng): 1.99

Instrument: finns99$SSSi Zi I- Sample Amt: 1.83 gm—dry—ut

Purgrs Volt 5.0%

SURROGATE RECOVERIES Amount Found tRec

dl—1 2—D1chlorOathane 52.100 104.dO—Toluene 7.B80SrDmofluarobentene ‘7.l9% 94.4d4—1 • 2—OichlcrobenzeTie 60.460 11.

Compound DL. Rat., mt plaoJt(Q)

Chioromethane 0.D3 0.00Vinyl Chloride 0.0 0.00Bromomethane 3.00 0.00Chloroetharie 3.00Tric?-lorofluoromethane 0.00Acroleir, 0.00 0.001,1.2—Trichlorotrjfluoroethane 0.00 0.00Acetone 0.00l,1—Oichloroethen g.ooBroinoethane 0.00 0.430Methyl Iodide 0.00Methylene Chloride 3.47 9.40 0Carbon Disulfide o,00Aerylonitrile 0.40 00trans—1,2—OicrloroeChene 0 .aoVinyl Acetate cc.oe1,1—Qichloroethan 0.00 0.002—Butanons t.00 0.002.2—Dichloroprcpane e.egcis—l .2—Dichioroetheris 0.00 0.00Chloroform 0.00S rochjorocpethane 0.00 0.001,i,1—Trichloroethane 0.00 0.00:.1—Dichloropropene 3.00 0.00 .. -<Carbon Tetraehlorjde 0.00 0.30 —

l,2—Dic1-,loroethane . -—

—6enzane 0.00 0ecIrichioroethene 0.00 D Cl.2—Oichioropropane a.ooSromodichjoroeiethane 43.00 a.og LiiOibromomnethane 0.00 0.00 rt2—Chloroethylvinylether 0.0% 0.004—Methyl—2—Pentanone (MIBK) 0.00 0.Oo .1cis—l,3—Oichlor’oprop.ne

.—Toluene 0.00trans—i ,3—Dich1oropropne a. oo1 1 2-Trich.loroethane 0.00 0.09Eb1ene Qjbromide 0.00 0.002—Hexanon 0.00 0.091,3—Dichloropropane 0.00 0.00Tetrachioroetnene g.oe

“I

0 C)

Finn S Soil Lnport .Jork1ist: 777FSlinp.wlf printed: 7/ 8/99

Qata Analyst: 39ff Roberson Analyzed by: LiPork1ist creatu,d: 7/ Sf99 Analysis Date: 7/ 7/99Coanients:

Dibrornochmorornethano 0.00 0.00Chlorobenzene 0.c,0i.1.1,2—TetrachLoroethano 0.00

C’Ethylbenzene 0.00‘rn,p—Xylane 0.00 0.00

o—Xylsrie 0.S0 0Styrene o.oe 0. 0Brornofor-m i. e.ol,1.22—Tetrach1oroothan 1.85 4.51 V1,2,3—Trichloropropane 000trans—I 4—Dichloro—2—outerie 0 00 0.00n—Propylbenzene 0.00omobenzene 0.00 0.00Isopropyi.Denzene 0.00 0.00—Ch1orotoLLgne 0.00 0.004—Chjorotojuene 0.n 0.00tert—Sutylben-z&ne 0.00 0.001.3,S—Trinethylbenzene 0.00 0.00l.2.4—Trirnethylbenzene 000 0.00sec—Sutylbenzerie Ø.Ø 0.09—Isopropy1 toluene -

1,3—Dichlorobenzene 0.0O 0.001,4—Dichiorooen.zene 0.00 0.00r—8ut1bpn2erie 0-00 0.001 • 2—D).cilo robenxene 0.00 0 00l,2—Dibromo—3—chloropropane 0.00 0.00i,2,4—Trichlorobenzone 0.00 0.00Nexachiorobutadiprie 0.00 0.00Naphthalne 0.0011,3—Trich1oroberzene 000 -

Dichlorodi rlooromethane 0.00 Not RequsGtd

‘a

ziowcc0

I2

Finn S Soil ImportF5imp.lf printed: 7/ Sf99

C

Qata Analyst; Jeff RobersonJorkljst createth 7/ 8/99Comments:

Chioromethanevsnyl ChlorideSromornethaneC hi or o € than eTrichiorofiuoromethanc’Acroje.jni,l,2—TricblorotrifljoroetrianeAcetone1 .1—DIchioroetheneU romoc thaneMethyl IodideMethylene ChlorideCarbon Disulfideckcrylonitr.Lletrans—I, 2—Ojol-iloroetherisVinyl Acetate1. 1—DichloroethaneZ—8uta,,one2. 2—Dichloropropanecls—l • 2—DichioroettieneChloroformBr ono chIc r ometh an e1,1, 1—Trichioroethane1, 1—Dichlo ropropeneCarbon TetrachlorjdeI .2—Qichioroethane

‘.—_— UenzeneYrjchjcroetheno

2—DichlcrcprcpaneBrocnodIchl oronethaneDibronomethane2—Chi o roethy I vi nyle the ra—Merhyl—2---Pentanoné (MISK)cis—l 3—Cichioropropene

—To1uenetrans—i .3—Dichioropropene1, 1,2—TnichloroetharieEthylene Dibrornide2—He,<anone1 .3—DichioropropaneTetrachloroetriene

Workiist: 777

naiyzed by: LJRAnalysis Date:

fTjme: 7/ 7/99 2i:esL/gm or M/mg); 0.710

InstrLArnent: finnsSample Ant: 0.662

Purge Vol: 5-0

i03.99.997.81 00.

C

7/ 7/99

Ramt mpJAmou(Q)

0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requostec0.00 Not Requested0.00 Not Requested0.00 Not RequSStcd0.00 Not Requested0.00 Not Requested0.00 NOt Requesteda47 Not Requested0.00 Not. Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested

Not Requested0.00 Not Requested0.00 NOt Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested4.47 t Rquastc.d0-00 0.000.08 o equested0.08 Not Requestec0.0€ Not Requested0.00 Not Requested0.00 Not Requested0.00 Not Requested0.00 quested

0.08 No equasted0.00 Not Requested0.00 Not Requested0.00 Not Requested

Not Requested0.00 Not Requested

LEVEL(LnLot.i, WtWater): LTotal Solids: 93.26

naiysis DateDL or .iet 1.Jt(

RUN CODE (null): S

7. AM31 H99—9859 WSY—C282


d—1 , Z—Oichi oroethaned8—IolueneBromofltjorobenzened4—l, 2—Oichlorobenzene

Compound

Amount Found tRec

gm—d ‘y—-t

51. 63049. 95048 - 910so.

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/3

Finn s soil ImportE5imp.wll printed: 7/ 8/99

C)

Data Analyst: .J€lf RobersonWorkljst created: 7/ 8/99Corwnents:

L4orklist: 777

Analyzed by: LJRAnalysis Date:

C

7/ 7/99

Dibromcchloriie thaneC blo robe rz erg1,1 • 1. 2—TetrachloroirtMare

‘“ Ethylbenzene,—rrt, p—Xylene— o—Xylene

Sty r e neS r omo to nfl

1 • 1,2. 2—Tetrachloroc thano1 .2,3—TrlchloropropanetranG—! • 4—(jjchloro—2—bjjtenen—PropylbenzeneOrocnobenzerieIsopropylbenzene2—Chlo rotoiupn’2—Chlo rotoluene1:ert—SutylLienzene1 • 3 .S—Trimethylbenzene1 ,2,4—Trimethylbenzenesec—Sutylbenzenel—Isop ropyl toiuer’e1,3—Ojchlorohenzene1 • 4—Dichlorobenzenen—Sutylbenzene3. • 2—Dichloroberizene1, 2—Dibromo—3—chloropropane1,2, 4—TrichiorobenzeneHex ach ‘a rob u tad i ene

N aph th a len c1,2, 3—Trichlor-obenzeneDichlorodj fluoromethane

e.Z .00

- 000 . 000.00

01.0 0.00

0.000 - 00

00

0 - 000 . 00

o . oe00.000,000.000 . 000 - 00O - 000-001 . 700.000.00o . oe0 - 00

Not RequestedNot Requested

,rt%?euested

Not RequestedNot RequestedNot RequestedNot RequestedNot RequestedN01 equested

Not; ReouesteNot equesteNot RequestedNot RequestedNot RequestedNot; RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNot RequestedNat Requested

>-cc

-Jowcca-

/1/

C

Fjnn s soil rethod Blank Jork1ist: 773PSimpb.lf printed: 7) 8/99

Data Analyst: Jeff Roberson Analyzed by: LJRorklist created: 7/ 8/99 Analysis Date: 7/ 7/99Cotwr€nts:

LEYEL(L’cLo, M=Med, W=.Jater): L

Analycis Date/Time: 7/ 7/99 i7:41. AM31 DI. or et Wt(L/gm or M/rriq): 5.00

99953 Method Blank Instrument: tinn5Soi1 Sample Amt; 5.00 gnm—dry--wt

Purge VoL 5.00

SURRDGATE RECOVERIES gmount Found tRec

d4—1 • 2—Dichi Droethno 49. 500 99.d8—Toluene ‘18.68% 97.GBromofluorobenzene 49.450 98.9tN—I • 2—Dichlorobenzene 48. ‘20 96.8

Compound DL Rn Amt Cmple Amount (Q)

Chioromethane 2.0 0.Ø 0.00Vinyl Chloride 2.0 0.00 0.00Bromomethiane 2.0 0.00 0.00Chloroetha,e 2.0 0.00 0.00Trichiorofluorornethanc 2.% 0.00 0.00rcroleii S 0.00 0.01,1,2—Trichlcrotritluoroethane 2.0 0.30 0.00Acetone 5.0 0.00 0.01,1—Dichloroethene 1.0 0.00 0.00Brornoethanc.? 2.0 0.00 0.00Methyl Iodide 1.0 3.00 0.00Metylene CHoride 2.0 2.86 2.8 3Carbon Disitioe 1.0 0.00 0.00Acrylonitrile 5.0 0.00 0.0trans—1,2—Cichloroethene 1.0 0.00 0.00Vinyl acetate 5.0 0.00 0.00l,1—Dichlcroethane 1.0 0.00 0.00—Sutanone 6.0 0.00 0.0

2,2—Dichloropropare 1.0 0.00 0.00cit—1,2—Cichloroethere 1.0 0.00 0.00Chloroform 1.0 e.oo 00oBromoctij.ortjrnethane 1.0 0.00 0.001.1,1—Trichioroethane 1,0 0.00 0.001.1—Dichioropropene i.0 0.00 0.0Carbon 1etrachlnide 1.0 0.00 o.oct1.2—Djchloroethane 1.0 0.00 0.00Benzene 1.0 0.00 0.00Tnichioroetherie 1.0 0.00 0.00 >1

1.2—Dichloropropane 1.0 0.00 0.00Bronodjchloroniethane 1.0 0.00 0.00Djbromomethane 1.0 000 3.09)2—Chloroet}iyl.viriyiether 5.0 0.00 0.04—Methyl—2—Pentanone (MISK) 5.0 0.00 0.0cis—l,3—Dicthloropropene 1.0 0.00 0.00 I-”—Toluene 1.0 0.00 o.ectrans—1.3-.Dichloropropene 1.0 0.00 0.00l,1,2—Trichloroethane 1.0 0.00 0.30Ethylene Dibrornide 1.0 0.00 0.00 [JJ2—kexanone 5.0 0.00 0.01,3—Dichioropropane 5.0 @.00 0.00Tetrachioroethene :1.0 0,00 0.00

1L9

/94 Ac

C

Fj 5 Soil ‘etnod Blank Uorklist: 773I’Simpb.1f printed; 7/ 8/99

Data Analyst: Jeff Roberson nalyzed by: LJRWorkllst created: 7/ 8/99 Analysis Date: 7/ 7/9SConrnents:

Oibrornochlorornethane LO 0.00 0.00Chioroberzene iS 0.00 0.001,1,i,2—TetracbiLoro,thns 1.0 000 0.0%Ethylbenzene 10 0.00 0.00in,p—Xylene 1.0 0.00 000D—Xylane 1.0 0.00 16.003tyrene 1.0 0.09 0.00Sromoforrn i.e e,oe1,1,2,2—Tetrachioroethane 1.0 0.00 0.1691.2,3-Jrichioropropane 1.0 0.00 0.00trans—i 4—Dlch1oro---2-bijtene 5.0 0.00 0-00n—Propylberizene 1.0 0.00 0.00f3romobenzerie 1.0 0.00 0.00Iscpropylbenzene 1.0 0.00 0.00.—Ch1oroto1uene 1.0 0.00 0.004—Chiorotoluene 1.0 0.00 0.00tert—SutylbenzerIe 1.0 0.00 0.0161 .3.5—Trimethy1benznc 1.0 0.’0 0.001.2.4—Trirn*thy1henz9ne 1.0 0.00 0.00sec—Butylbenzere 1.0 o.oo4—!sopropyttoluer 1.0 0.00 0.001.3—DjchjorQbenzene 1.0 0.;)0 0.001 ,4—Dichlorcber,zene LO 050 0.00n—6utylbcnzene 1.0 0.00 0.001,2—Dichioroberizene 2.0 0.00 0.001.2—Dibromo—3—chloropropane 5.0 0.00 0.01,2, l_Trichlorohenzc,ne 5.0 0-00 0.00HeyachicrobLtadiene 5.0 0.00 050Naphtha1sn 5.0 0-00 0.001,2.3—Tricblorobenzgne 5.0 0.00flichlorodifluoromethane 3. 0.00 0.00

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“liL4QLG2g3L44.3%j5421 - Alaska DEC...Whitestone Logging Project: Sortyard cleanup CLUe Sample...

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