ANALYTICAL REPORT...Location : COOK LOT Client Sample ID : COOK-COMP1-081315 Laboratory Sample ID :...
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Transcript of ANALYTICAL REPORT...Location : COOK LOT Client Sample ID : COOK-COMP1-081315 Laboratory Sample ID :...
Laboratory Job Number 269097ANALYTICAL REPORT
Robin Spencer Project : STANDARD 6 Via San Inigo Location : COOK LOT Orinda, CA 94563 Level : II
Sample ID Lab IDCOOK-COMP1-081315 269097-001COOK-COMP2-081715 269097-002COOK-COMP3-081715 269097-003COOK-COMP4-081715 269097-004COOK-COMP5-081715 269097-005
This data package has been reviewed for technical correctness and completeness.Release of this data has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature. The resultscontained in this report meet all requirements of NELAC and pertain only tothose samples which were submitted for analysis. This report may be reproducedonly in its entirety.
Signature: Date: 08/25/2015 Tracy BabjarProject Manager
[email protected](510) 204-2226
CA ELAP# 2896, NELAP# 4044-001
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CASE NARRATIVE
Laboratory number: 269097Client: Robin SpencerLocation: COOK LOTRequest Date: 08/17/15Samples Received: 08/17/15
This data package contains sample and QC results for five soil samples,requested for the above referenced project on 08/17/15. The samples werereceived cold and intact.
TPH-Extractables by GC (EPA 8015B):A number of samples were diluted due to the dark and viscous nature of thesample extracts. No other analytical problems were encountered.
Volatile Organics by GC/MS (EPA 8260B):No analytical problems were encountered.
Metals (EPA 6010B and EPA 7471A):No analytical problems were encountered.
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Detections Summary for 269097
Results for any subcontracted analyses are not included in this summary.
Client : Robin Spencer Project : STANDARD Location : COOK LOT
Client Sample ID : COOK-COMP1-081315 Laboratory Sample ID : 269097-001
Analyte Result Flags RL Units Basis IDF Method Prep Method Diesel C10-C24 44 Y 10 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Motor Oil C24-C36 470 50 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Antimony 1.3 0.53 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Arsenic 5.7 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Barium 190 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Beryllium 0.59 0.11 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cadmium 0.61 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Chromium 16 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cobalt 11 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Copper 22 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Lead 10 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Mercury 0.23 0.017 mg/Kg As Recd 1.000 EPA 7471A METHOD Molybdenum 0.30 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Nickel 23 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Vanadium 38 0.26 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Zinc 55 1.1 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B
Client Sample ID : COOK-COMP2-081715 Laboratory Sample ID : 269097-002
Analyte Result Flags RL Units Basis IDF Method Prep Method Diesel C10-C24 67 Y 10 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Motor Oil C24-C36 530 50 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Antimony 2.2 0.49 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Arsenic 5.2 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Barium 86 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Beryllium 0.46 0.097 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cadmium 0.75 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Chromium 22 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cobalt 13 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Copper 23 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Lead 10 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Mercury 0.14 0.017 mg/Kg As Recd 1.000 EPA 7471A METHOD Molybdenum 0.41 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Nickel 32 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Vanadium 60 0.24 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Zinc 53 0.97 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B
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Client Sample ID : COOK-COMP3-081715 Laboratory Sample ID : 269097-003
Analyte Result Flags RL Units Basis IDF Method Prep Method Diesel C10-C24 220 Y 10 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Motor Oil C24-C36 1,000 50 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Antimony 1.6 0.54 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Arsenic 8.1 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Barium 120 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Beryllium 0.53 0.11 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cadmium 0.74 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Chromium 53 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cobalt 14 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Copper 20 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Lead 15 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Mercury 0.12 0.018 mg/Kg As Recd 1.000 EPA 7471A METHOD Molybdenum 0.47 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Nickel 100 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Vanadium 46 0.27 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Zinc 60 1.1 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B
Client Sample ID : COOK-COMP4-081715 Laboratory Sample ID : 269097-004
Analyte Result Flags RL Units Basis IDF Method Prep Method Diesel C10-C24 87 Y 10 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Motor Oil C24-C36 780 50 mg/Kg As Recd 10.00 EPA 8015B EPA 3550B Antimony 1.4 0.46 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Arsenic 6.5 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Barium 170 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Beryllium 0.66 0.093 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cadmium 0.67 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Chromium 27 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cobalt 14 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Copper 22 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Lead 35 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Mercury 0.18 0.016 mg/Kg As Recd 1.000 EPA 7471A METHOD Molybdenum 0.62 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Nickel 36 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Vanadium 35 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Zinc 83 0.93 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B
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Client Sample ID : COOK-COMP5-081715 Laboratory Sample ID : 269097-005
Analyte Result Flags RL Units Basis IDF Method Prep Method Diesel C10-C24 88 Y 1.0 mg/Kg As Recd 1.000 EPA 8015B EPA 3550B Motor Oil C24-C36 440 5.0 mg/Kg As Recd 1.000 EPA 8015B EPA 3550B Antimony 1.4 0.46 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Arsenic 5.2 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Barium 150 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Beryllium 0.57 0.092 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cadmium 0.97 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Chromium 28 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Cobalt 12 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Copper 30 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Lead 39 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Mercury 0.18 0.016 mg/Kg As Recd 1.000 EPA 7471A METHOD Molybdenum 0.71 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Nickel 32 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Vanadium 32 0.23 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B Zinc 94 0.92 mg/Kg As Recd 1.000 EPA 6010B EPA 3050B
Y = Sample exhibits chromatographic pattern which does not resemble standardPage 3 of 3 29.0
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Total Extractable Hydrocarbons
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3550B Project#: STANDARD Analysis: EPA 8015B Matrix: Soil Received: 08/17/15 Units: mg/Kg Prepared: 08/19/15 Basis: as received Analyzed: 08/19/15 Batch#: 226277
Field ID: COOK-COMP1-081315 Diln Fac: 10.00 Type: SAMPLE Sampled: 08/13/15 Lab ID: 269097-001 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 44 Y 10 Motor Oil C24-C36 470 50
Surrogate %REC Limits o-Terphenyl DO 59-140
Field ID: COOK-COMP2-081715 Diln Fac: 10.00 Type: SAMPLE Sampled: 08/17/15 Lab ID: 269097-002 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 67 Y 10 Motor Oil C24-C36 530 50
Surrogate %REC Limits o-Terphenyl DO 59-140
Field ID: COOK-COMP3-081715 Diln Fac: 10.00 Type: SAMPLE Sampled: 08/17/15 Lab ID: 269097-003 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 220 Y 10 Motor Oil C24-C36 1,000 50
Surrogate %REC Limits o-Terphenyl DO 59-140
Field ID: COOK-COMP4-081715 Diln Fac: 10.00 Type: SAMPLE Sampled: 08/17/15 Lab ID: 269097-004 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 87 Y 10 Motor Oil C24-C36 780 50
Surrogate %REC Limits o-Terphenyl DO 59-140
Y= Sample exhibits chromatographic pattern which does not resemble standardDO= Diluted OutND= Not DetectedRL= Reporting LimitPage 1 of 2 11.0
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Total Extractable Hydrocarbons
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3550B Project#: STANDARD Analysis: EPA 8015B Matrix: Soil Received: 08/17/15 Units: mg/Kg Prepared: 08/19/15 Basis: as received Analyzed: 08/19/15 Batch#: 226277
Field ID: COOK-COMP5-081715 Diln Fac: 1.000 Type: SAMPLE Sampled: 08/17/15 Lab ID: 269097-005 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 88 Y 1.0 Motor Oil C24-C36 440 5.0
Surrogate %REC Limits o-Terphenyl 73 59-140
Type: BLANK Diln Fac: 1.000 Lab ID: QC800108 Cleanup Method: EPA 3630C
Analyte Result RL Diesel C10-C24 ND 1.0 Motor Oil C24-C36 ND 5.0
Surrogate %REC Limits o-Terphenyl 90 59-140
Y= Sample exhibits chromatographic pattern which does not resemble standardDO= Diluted OutND= Not DetectedRL= Reporting LimitPage 2 of 2 11.0
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Batch QC Report
Total Extractable Hydrocarbons
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3550B Project#: STANDARD Analysis: EPA 8015B Type: LCS Diln Fac: 1.000 Lab ID: QC800109 Batch#: 226277 Matrix: Soil Prepared: 08/19/15 Units: mg/Kg Analyzed: 08/20/15
Cleanup Method: EPA 3630C
Analyte Spiked Result %REC Limits Diesel C10-C24 49.94 38.71 78 58-137
Surrogate %REC Limits o-Terphenyl 80 59-140
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Batch QC Report
Total Extractable Hydrocarbons
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3550B Project#: STANDARD Analysis: EPA 8015B Field ID: ZZZZZZZZZZ Batch#: 226277 MSS Lab ID: 269090-001 Sampled: 08/12/15 Matrix: Soil Received: 08/18/15 Units: mg/Kg Prepared: 08/19/15 Basis: as received Analyzed: 08/20/15 Diln Fac: 1.000
Type: MS Lab ID: QC800110
Analyte MSS Result Spiked Result %REC Limits Diesel C10-C24 2.454 50.32 45.78 86 46-154
Surrogate %REC Limits o-Terphenyl 93 59-140
Type: MSD Lab ID: QC800111
Analyte Spiked Result %REC Limits RPD LimDiesel C10-C24 49.93 48.67 93 46-154 7 50
Surrogate %REC Limits o-Terphenyl 99 59-140
RPD= Relative Percent DifferencePage 1 of 1 13.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP1-081315 Diln Fac: 0.9785 Lab ID: 269097-001 Batch#: 226262 Matrix: Soil Sampled: 08/13/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Freon 12 ND 9.8 Chloromethane ND 9.8 Vinyl Chloride ND 9.8 Bromomethane ND 9.8 Chloroethane ND 9.8 Trichlorofluoromethane ND 4.9 Acetone ND 20 Freon 113 ND 4.9 1,1-Dichloroethene ND 4.9 Methylene Chloride ND 20 Carbon Disulfide ND 4.9 MTBE ND 4.9 trans-1,2-Dichloroethene ND 4.9 Vinyl Acetate ND 49 1,1-Dichloroethane ND 4.9 2-Butanone ND 9.8 cis-1,2-Dichloroethene ND 4.9 2,2-Dichloropropane ND 4.9 Chloroform ND 4.9 Bromochloromethane ND 4.9 1,1,1-Trichloroethane ND 4.9 1,1-Dichloropropene ND 4.9 Carbon Tetrachloride ND 4.9 1,2-Dichloroethane ND 4.9 Benzene ND 4.9 Trichloroethene ND 4.9 1,2-Dichloropropane ND 4.9 Bromodichloromethane ND 4.9 Dibromomethane ND 4.9 4-Methyl-2-Pentanone ND 9.8 cis-1,3-Dichloropropene ND 4.9 Toluene ND 4.9 trans-1,3-Dichloropropene ND 4.9 1,1,2-Trichloroethane ND 4.9 2-Hexanone ND 9.8 1,3-Dichloropropane ND 4.9 Tetrachloroethene ND 4.9
ND= Not DetectedRL= Reporting LimitPage 1 of 2 3.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP1-081315 Diln Fac: 0.9785 Lab ID: 269097-001 Batch#: 226262 Matrix: Soil Sampled: 08/13/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Dibromochloromethane ND 4.9 1,2-Dibromoethane ND 4.9 Chlorobenzene ND 4.9 1,1,1,2-Tetrachloroethane ND 4.9 Ethylbenzene ND 4.9 m,p-Xylenes ND 4.9 o-Xylene ND 4.9 Styrene ND 4.9 Bromoform ND 4.9 Isopropylbenzene ND 4.9 1,1,2,2-Tetrachloroethane ND 4.9 1,2,3-Trichloropropane ND 4.9 Propylbenzene ND 4.9 Bromobenzene ND 4.9 1,3,5-Trimethylbenzene ND 4.9 2-Chlorotoluene ND 4.9 4-Chlorotoluene ND 4.9 tert-Butylbenzene ND 4.9 1,2,4-Trimethylbenzene ND 4.9 sec-Butylbenzene ND 4.9 para-Isopropyl Toluene ND 4.9 1,3-Dichlorobenzene ND 4.9 1,4-Dichlorobenzene ND 4.9 n-Butylbenzene ND 4.9 1,2-Dichlorobenzene ND 4.9 1,2-Dibromo-3-Chloropropane ND 4.9 1,2,4-Trichlorobenzene ND 4.9 Hexachlorobutadiene ND 4.9 Naphthalene ND 4.9 1,2,3-Trichlorobenzene ND 4.9
Surrogate %REC Limits Dibromofluoromethane 106 78-134 1,2-Dichloroethane-d4 98 80-138 Toluene-d8 87 80-120 Bromofluorobenzene 91 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 3.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP2-081715 Diln Fac: 0.9980 Lab ID: 269097-002 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Freon 12 ND 10 Chloromethane ND 10 Vinyl Chloride ND 10 Bromomethane ND 10 Chloroethane ND 10 Trichlorofluoromethane ND 5.0 Acetone ND 20 Freon 113 ND 5.0 1,1-Dichloroethene ND 5.0 Methylene Chloride ND 20 Carbon Disulfide ND 5.0 MTBE ND 5.0 trans-1,2-Dichloroethene ND 5.0 Vinyl Acetate ND 50 1,1-Dichloroethane ND 5.0 2-Butanone ND 10 cis-1,2-Dichloroethene ND 5.0 2,2-Dichloropropane ND 5.0 Chloroform ND 5.0 Bromochloromethane ND 5.0 1,1,1-Trichloroethane ND 5.0 1,1-Dichloropropene ND 5.0 Carbon Tetrachloride ND 5.0 1,2-Dichloroethane ND 5.0 Benzene ND 5.0 Trichloroethene ND 5.0 1,2-Dichloropropane ND 5.0 Bromodichloromethane ND 5.0 Dibromomethane ND 5.0 4-Methyl-2-Pentanone ND 10 cis-1,3-Dichloropropene ND 5.0 Toluene ND 5.0 trans-1,3-Dichloropropene ND 5.0 1,1,2-Trichloroethane ND 5.0 2-Hexanone ND 10 1,3-Dichloropropane ND 5.0 Tetrachloroethene ND 5.0
ND= Not DetectedRL= Reporting LimitPage 1 of 2 4.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP2-081715 Diln Fac: 0.9980 Lab ID: 269097-002 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Dibromochloromethane ND 5.0 1,2-Dibromoethane ND 5.0 Chlorobenzene ND 5.0 1,1,1,2-Tetrachloroethane ND 5.0 Ethylbenzene ND 5.0 m,p-Xylenes ND 5.0 o-Xylene ND 5.0 Styrene ND 5.0 Bromoform ND 5.0 Isopropylbenzene ND 5.0 1,1,2,2-Tetrachloroethane ND 5.0 1,2,3-Trichloropropane ND 5.0 Propylbenzene ND 5.0 Bromobenzene ND 5.0 1,3,5-Trimethylbenzene ND 5.0 2-Chlorotoluene ND 5.0 4-Chlorotoluene ND 5.0 tert-Butylbenzene ND 5.0 1,2,4-Trimethylbenzene ND 5.0 sec-Butylbenzene ND 5.0 para-Isopropyl Toluene ND 5.0 1,3-Dichlorobenzene ND 5.0 1,4-Dichlorobenzene ND 5.0 n-Butylbenzene ND 5.0 1,2-Dichlorobenzene ND 5.0 1,2-Dibromo-3-Chloropropane ND 5.0 1,2,4-Trichlorobenzene ND 5.0 Hexachlorobutadiene ND 5.0 Naphthalene ND 5.0 1,2,3-Trichlorobenzene ND 5.0
Surrogate %REC Limits Dibromofluoromethane 106 78-134 1,2-Dichloroethane-d4 99 80-138 Toluene-d8 84 80-120 Bromofluorobenzene 91 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 4.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP3-081715 Diln Fac: 0.9960 Lab ID: 269097-003 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Freon 12 ND 10 Chloromethane ND 10 Vinyl Chloride ND 10 Bromomethane ND 10 Chloroethane ND 10 Trichlorofluoromethane ND 5.0 Acetone ND 20 Freon 113 ND 5.0 1,1-Dichloroethene ND 5.0 Methylene Chloride ND 20 Carbon Disulfide ND 5.0 MTBE ND 5.0 trans-1,2-Dichloroethene ND 5.0 Vinyl Acetate ND 50 1,1-Dichloroethane ND 5.0 2-Butanone ND 10 cis-1,2-Dichloroethene ND 5.0 2,2-Dichloropropane ND 5.0 Chloroform ND 5.0 Bromochloromethane ND 5.0 1,1,1-Trichloroethane ND 5.0 1,1-Dichloropropene ND 5.0 Carbon Tetrachloride ND 5.0 1,2-Dichloroethane ND 5.0 Benzene ND 5.0 Trichloroethene ND 5.0 1,2-Dichloropropane ND 5.0 Bromodichloromethane ND 5.0 Dibromomethane ND 5.0 4-Methyl-2-Pentanone ND 10 cis-1,3-Dichloropropene ND 5.0 Toluene ND 5.0 trans-1,3-Dichloropropene ND 5.0 1,1,2-Trichloroethane ND 5.0 2-Hexanone ND 10 1,3-Dichloropropane ND 5.0 Tetrachloroethene ND 5.0
ND= Not DetectedRL= Reporting LimitPage 1 of 2 5.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP3-081715 Diln Fac: 0.9960 Lab ID: 269097-003 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Dibromochloromethane ND 5.0 1,2-Dibromoethane ND 5.0 Chlorobenzene ND 5.0 1,1,1,2-Tetrachloroethane ND 5.0 Ethylbenzene ND 5.0 m,p-Xylenes ND 5.0 o-Xylene ND 5.0 Styrene ND 5.0 Bromoform ND 5.0 Isopropylbenzene ND 5.0 1,1,2,2-Tetrachloroethane ND 5.0 1,2,3-Trichloropropane ND 5.0 Propylbenzene ND 5.0 Bromobenzene ND 5.0 1,3,5-Trimethylbenzene ND 5.0 2-Chlorotoluene ND 5.0 4-Chlorotoluene ND 5.0 tert-Butylbenzene ND 5.0 1,2,4-Trimethylbenzene ND 5.0 sec-Butylbenzene ND 5.0 para-Isopropyl Toluene ND 5.0 1,3-Dichlorobenzene ND 5.0 1,4-Dichlorobenzene ND 5.0 n-Butylbenzene ND 5.0 1,2-Dichlorobenzene ND 5.0 1,2-Dibromo-3-Chloropropane ND 5.0 1,2,4-Trichlorobenzene ND 5.0 Hexachlorobutadiene ND 5.0 Naphthalene ND 5.0 1,2,3-Trichlorobenzene ND 5.0
Surrogate %REC Limits Dibromofluoromethane 106 78-134 1,2-Dichloroethane-d4 101 80-138 Toluene-d8 89 80-120 Bromofluorobenzene 91 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 5.0
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Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP4-081715 Diln Fac: 0.9452 Lab ID: 269097-004 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Freon 12 ND 9.5 Chloromethane ND 9.5 Vinyl Chloride ND 9.5 Bromomethane ND 9.5 Chloroethane ND 9.5 Trichlorofluoromethane ND 4.7 Acetone ND 19 Freon 113 ND 4.7 1,1-Dichloroethene ND 4.7 Methylene Chloride ND 19 Carbon Disulfide ND 4.7 MTBE ND 4.7 trans-1,2-Dichloroethene ND 4.7 Vinyl Acetate ND 47 1,1-Dichloroethane ND 4.7 2-Butanone ND 9.5 cis-1,2-Dichloroethene ND 4.7 2,2-Dichloropropane ND 4.7 Chloroform ND 4.7 Bromochloromethane ND 4.7 1,1,1-Trichloroethane ND 4.7 1,1-Dichloropropene ND 4.7 Carbon Tetrachloride ND 4.7 1,2-Dichloroethane ND 4.7 Benzene ND 4.7 Trichloroethene ND 4.7 1,2-Dichloropropane ND 4.7 Bromodichloromethane ND 4.7 Dibromomethane ND 4.7 4-Methyl-2-Pentanone ND 9.5 cis-1,3-Dichloropropene ND 4.7 Toluene ND 4.7 trans-1,3-Dichloropropene ND 4.7 1,1,2-Trichloroethane ND 4.7 2-Hexanone ND 9.5 1,3-Dichloropropane ND 4.7 Tetrachloroethene ND 4.7
ND= Not DetectedRL= Reporting LimitPage 1 of 2 6.0
25 of 43
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP4-081715 Diln Fac: 0.9452 Lab ID: 269097-004 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Dibromochloromethane ND 4.7 1,2-Dibromoethane ND 4.7 Chlorobenzene ND 4.7 1,1,1,2-Tetrachloroethane ND 4.7 Ethylbenzene ND 4.7 m,p-Xylenes ND 4.7 o-Xylene ND 4.7 Styrene ND 4.7 Bromoform ND 4.7 Isopropylbenzene ND 4.7 1,1,2,2-Tetrachloroethane ND 4.7 1,2,3-Trichloropropane ND 4.7 Propylbenzene ND 4.7 Bromobenzene ND 4.7 1,3,5-Trimethylbenzene ND 4.7 2-Chlorotoluene ND 4.7 4-Chlorotoluene ND 4.7 tert-Butylbenzene ND 4.7 1,2,4-Trimethylbenzene ND 4.7 sec-Butylbenzene ND 4.7 para-Isopropyl Toluene ND 4.7 1,3-Dichlorobenzene ND 4.7 1,4-Dichlorobenzene ND 4.7 n-Butylbenzene ND 4.7 1,2-Dichlorobenzene ND 4.7 1,2-Dibromo-3-Chloropropane ND 4.7 1,2,4-Trichlorobenzene ND 4.7 Hexachlorobutadiene ND 4.7 Naphthalene ND 4.7 1,2,3-Trichlorobenzene ND 4.7
Surrogate %REC Limits Dibromofluoromethane 105 78-134 1,2-Dichloroethane-d4 104 80-138 Toluene-d8 87 80-120 Bromofluorobenzene 88 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 6.0
26 of 43
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP5-081715 Diln Fac: 0.9940 Lab ID: 269097-005 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Freon 12 ND 9.9 Chloromethane ND 9.9 Vinyl Chloride ND 9.9 Bromomethane ND 9.9 Chloroethane ND 9.9 Trichlorofluoromethane ND 5.0 Acetone ND 20 Freon 113 ND 5.0 1,1-Dichloroethene ND 5.0 Methylene Chloride ND 20 Carbon Disulfide ND 5.0 MTBE ND 5.0 trans-1,2-Dichloroethene ND 5.0 Vinyl Acetate ND 50 1,1-Dichloroethane ND 5.0 2-Butanone ND 9.9 cis-1,2-Dichloroethene ND 5.0 2,2-Dichloropropane ND 5.0 Chloroform ND 5.0 Bromochloromethane ND 5.0 1,1,1-Trichloroethane ND 5.0 1,1-Dichloropropene ND 5.0 Carbon Tetrachloride ND 5.0 1,2-Dichloroethane ND 5.0 Benzene ND 5.0 Trichloroethene ND 5.0 1,2-Dichloropropane ND 5.0 Bromodichloromethane ND 5.0 Dibromomethane ND 5.0 4-Methyl-2-Pentanone ND 9.9 cis-1,3-Dichloropropene ND 5.0 Toluene ND 5.0 trans-1,3-Dichloropropene ND 5.0 1,1,2-Trichloroethane ND 5.0 2-Hexanone ND 9.9 1,3-Dichloropropane ND 5.0 Tetrachloroethene ND 5.0
ND= Not DetectedRL= Reporting LimitPage 1 of 2 7.0
27 of 43
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP5-081715 Diln Fac: 0.9940 Lab ID: 269097-005 Batch#: 226262 Matrix: Soil Sampled: 08/17/15 Units: ug/Kg Received: 08/17/15 Basis: as received Analyzed: 08/19/15
Analyte Result RL Dibromochloromethane ND 5.0 1,2-Dibromoethane ND 5.0 Chlorobenzene ND 5.0 1,1,1,2-Tetrachloroethane ND 5.0 Ethylbenzene ND 5.0 m,p-Xylenes ND 5.0 o-Xylene ND 5.0 Styrene ND 5.0 Bromoform ND 5.0 Isopropylbenzene ND 5.0 1,1,2,2-Tetrachloroethane ND 5.0 1,2,3-Trichloropropane ND 5.0 Propylbenzene ND 5.0 Bromobenzene ND 5.0 1,3,5-Trimethylbenzene ND 5.0 2-Chlorotoluene ND 5.0 4-Chlorotoluene ND 5.0 tert-Butylbenzene ND 5.0 1,2,4-Trimethylbenzene ND 5.0 sec-Butylbenzene ND 5.0 para-Isopropyl Toluene ND 5.0 1,3-Dichlorobenzene ND 5.0 1,4-Dichlorobenzene ND 5.0 n-Butylbenzene ND 5.0 1,2-Dichlorobenzene ND 5.0 1,2-Dibromo-3-Chloropropane ND 5.0 1,2,4-Trichlorobenzene ND 5.0 Hexachlorobutadiene ND 5.0 Naphthalene ND 5.0 1,2,3-Trichlorobenzene ND 5.0
Surrogate %REC Limits Dibromofluoromethane 104 78-134 1,2-Dichloroethane-d4 102 80-138 Toluene-d8 82 80-120 Bromofluorobenzene 90 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 7.0
28 of 43
Batch QC Report
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Matrix: Soil Batch#: 226262 Units: ug/Kg Analyzed: 08/19/15 Diln Fac: 1.000
Type: BS Lab ID: QC800058
Analyte Spiked Result %REC Limits 1,1-Dichloroethene 25.00 22.81 91 70-134 Benzene 25.00 24.26 97 80-123 Trichloroethene 25.00 23.77 95 80-128 Toluene 25.00 23.01 92 80-120 Chlorobenzene 25.00 26.03 104 80-123
Surrogate %REC Limits Dibromofluoromethane 100 78-134 1,2-Dichloroethane-d4 92 80-138 Toluene-d8 86 80-120 Bromofluorobenzene 87 78-123
Type: BSD Lab ID: QC800059
Analyte Spiked Result %REC Limits RPD Lim1,1-Dichloroethene 25.00 22.89 92 70-134 0 22 Benzene 25.00 23.32 93 80-123 4 21 Trichloroethene 25.00 22.94 92 80-128 4 23 Toluene 25.00 21.54 86 80-120 7 20 Chlorobenzene 25.00 24.92 100 80-123 4 20
Surrogate %REC Limits Dibromofluoromethane 100 78-134 1,2-Dichloroethane-d4 91 80-138 Toluene-d8 86 80-120 Bromofluorobenzene 87 78-123
RPD= Relative Percent DifferencePage 1 of 1 8.0
29 of 43
Batch QC Report
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Type: BLANK Diln Fac: 1.000 Lab ID: QC800060 Batch#: 226262 Matrix: Soil Analyzed: 08/19/15 Units: ug/Kg
Analyte Result RL Freon 12 ND 10 Chloromethane ND 10 Vinyl Chloride ND 10 Bromomethane ND 10 Chloroethane ND 10 Trichlorofluoromethane ND 5.0 Acetone ND 20 Freon 113 ND 5.0 1,1-Dichloroethene ND 5.0 Methylene Chloride ND 20 Carbon Disulfide ND 5.0 MTBE ND 5.0 trans-1,2-Dichloroethene ND 5.0 Vinyl Acetate ND 50 1,1-Dichloroethane ND 5.0 2-Butanone ND 10 cis-1,2-Dichloroethene ND 5.0 2,2-Dichloropropane ND 5.0 Chloroform ND 5.0 Bromochloromethane ND 5.0 1,1,1-Trichloroethane ND 5.0 1,1-Dichloropropene ND 5.0 Carbon Tetrachloride ND 5.0 1,2-Dichloroethane ND 5.0 Benzene ND 5.0 Trichloroethene ND 5.0 1,2-Dichloropropane ND 5.0 Bromodichloromethane ND 5.0 Dibromomethane ND 5.0 4-Methyl-2-Pentanone ND 10 cis-1,3-Dichloropropene ND 5.0 Toluene ND 5.0 trans-1,3-Dichloropropene ND 5.0 1,1,2-Trichloroethane ND 5.0 2-Hexanone ND 10 1,3-Dichloropropane ND 5.0 Tetrachloroethene ND 5.0
ND= Not DetectedRL= Reporting LimitPage 1 of 2 9.0
30 of 43
Batch QC Report
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Type: BLANK Diln Fac: 1.000 Lab ID: QC800060 Batch#: 226262 Matrix: Soil Analyzed: 08/19/15 Units: ug/Kg
Analyte Result RL Dibromochloromethane ND 5.0 1,2-Dibromoethane ND 5.0 Chlorobenzene ND 5.0 1,1,1,2-Tetrachloroethane ND 5.0 Ethylbenzene ND 5.0 m,p-Xylenes ND 5.0 o-Xylene ND 5.0 Styrene ND 5.0 Bromoform ND 5.0 Isopropylbenzene ND 5.0 1,1,2,2-Tetrachloroethane ND 5.0 1,2,3-Trichloropropane ND 5.0 Propylbenzene ND 5.0 Bromobenzene ND 5.0 1,3,5-Trimethylbenzene ND 5.0 2-Chlorotoluene ND 5.0 4-Chlorotoluene ND 5.0 tert-Butylbenzene ND 5.0 1,2,4-Trimethylbenzene ND 5.0 sec-Butylbenzene ND 5.0 para-Isopropyl Toluene ND 5.0 1,3-Dichlorobenzene ND 5.0 1,4-Dichlorobenzene ND 5.0 n-Butylbenzene ND 5.0 1,2-Dichlorobenzene ND 5.0 1,2-Dibromo-3-Chloropropane ND 5.0 1,2,4-Trichlorobenzene ND 5.0 Hexachlorobutadiene ND 5.0 Naphthalene ND 5.0 1,2,3-Trichlorobenzene ND 5.0
Surrogate %REC Limits Dibromofluoromethane 104 78-134 1,2-Dichloroethane-d4 99 80-138 Toluene-d8 84 80-120 Bromofluorobenzene 92 78-123
ND= Not DetectedRL= Reporting LimitPage 2 of 2 9.0
31 of 43
Batch QC Report
Purgeable Organics by GC/MS
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 5030B Project#: STANDARD Analysis: EPA 8260B Field ID: COOK-COMP3-081715 Batch#: 226262 MSS Lab ID: 269097-003 Sampled: 08/17/15 Matrix: Soil Received: 08/17/15 Units: ug/Kg Analyzed: 08/19/15 Basis: as received
Type: MS Diln Fac: 0.9823 Lab ID: QC800118
Analyte MSS Result Spiked Result %REC Limits 1,1-Dichloroethene <0.4755 49.12 40.45 82 56-133 Benzene <0.4094 49.12 39.09 80 57-120 Trichloroethene <0.3392 49.12 38.28 78 49-145 Toluene <0.4716 49.12 34.37 70 51-120 Chlorobenzene <0.5020 49.12 36.11 74 47-120
Surrogate %REC Limits Dibromofluoromethane 102 78-134 1,2-Dichloroethane-d4 100 80-138 Toluene-d8 90 80-120 Bromofluorobenzene 90 78-123
Type: MSD Diln Fac: 0.9862 Lab ID: QC800119
Analyte Spiked Result %REC Limits RPD Lim1,1-Dichloroethene 49.31 39.14 79 56-133 4 46 Benzene 49.31 39.36 80 57-120 0 44 Trichloroethene 49.31 37.23 75 49-145 3 46 Toluene 49.31 32.85 67 51-120 5 47 Chlorobenzene 49.31 32.88 67 47-120 10 50
Surrogate %REC Limits Dibromofluoromethane 101 78-134 1,2-Dichloroethane-d4 101 80-138 Toluene-d8 85 80-120 Bromofluorobenzene 91 78-123
RPD= Relative Percent DifferencePage 1 of 1 10.0
32 of 43
California Title 22 Metals
Lab #: 269097 Project#: STANDARD Client: Robin Spencer Location: COOK LOT Field ID: COOK-COMP1-081315 Basis: as received Lab ID: 269097-001 Diln Fac: 1.000 Matrix: Soil Sampled: 08/13/15 Units: mg/Kg Received: 08/17/15
Analyte Result RL Batch# Prepared Analyzed Prep Analysis Antimony 1.3 0.53 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Arsenic 5.7 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Barium 190 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Beryllium 0.59 0.11 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cadmium 0.61 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Chromium 16 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cobalt 11 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Copper 22 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Lead 10 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Mercury 0.23 0.017 226311 08/21/15 08/21/15 METHOD EPA 7471A Molybdenum 0.30 0.26 226301 08/19/15 08/21/15 EPA 3050B EPA 6010B Nickel 23 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Selenium ND 0.53 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Silver ND 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Thallium ND 0.53 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Vanadium 38 0.26 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Zinc 55 1.1 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B
ND= Not DetectedRL= Reporting LimitPage 1 of 1 14.1
33 of 43
California Title 22 Metals
Lab #: 269097 Project#: STANDARD Client: Robin Spencer Location: COOK LOT Field ID: COOK-COMP2-081715 Basis: as received Lab ID: 269097-002 Diln Fac: 1.000 Matrix: Soil Sampled: 08/17/15 Units: mg/Kg Received: 08/17/15
Analyte Result RL Batch# Prepared Analyzed Prep Analysis Antimony 2.2 0.49 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Arsenic 5.2 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Barium 86 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Beryllium 0.46 0.097 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cadmium 0.75 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Chromium 22 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cobalt 13 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Copper 23 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Lead 10 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Mercury 0.14 0.017 226311 08/21/15 08/21/15 METHOD EPA 7471A Molybdenum 0.41 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Nickel 32 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Selenium ND 0.49 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Silver ND 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Thallium ND 0.49 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Vanadium 60 0.24 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Zinc 53 0.97 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B
ND= Not DetectedRL= Reporting LimitPage 1 of 1 15.1
34 of 43
California Title 22 Metals
Lab #: 269097 Project#: STANDARD Client: Robin Spencer Location: COOK LOT Field ID: COOK-COMP3-081715 Basis: as received Lab ID: 269097-003 Diln Fac: 1.000 Matrix: Soil Sampled: 08/17/15 Units: mg/Kg Received: 08/17/15
Analyte Result RL Batch# Prepared Analyzed Prep Analysis Antimony 1.6 0.54 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Arsenic 8.1 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Barium 120 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Beryllium 0.53 0.11 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cadmium 0.74 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Chromium 53 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cobalt 14 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Copper 20 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Lead 15 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Mercury 0.12 0.018 226311 08/21/15 08/21/15 METHOD EPA 7471A Molybdenum 0.47 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Nickel 100 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Selenium ND 0.54 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Silver ND 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Thallium ND 0.54 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Vanadium 46 0.27 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Zinc 60 1.1 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B
ND= Not DetectedRL= Reporting LimitPage 1 of 1 16.1
35 of 43
California Title 22 Metals
Lab #: 269097 Project#: STANDARD Client: Robin Spencer Location: COOK LOT Field ID: COOK-COMP4-081715 Basis: as received Lab ID: 269097-004 Diln Fac: 1.000 Matrix: Soil Sampled: 08/17/15 Units: mg/Kg Received: 08/17/15
Analyte Result RL Batch# Prepared Analyzed Prep Analysis Antimony 1.4 0.46 226301 08/19/15 08/21/15 EPA 3050B EPA 6010B Arsenic 6.5 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Barium 170 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Beryllium 0.66 0.093 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cadmium 0.67 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Chromium 27 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cobalt 14 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Copper 22 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Lead 35 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Mercury 0.18 0.016 226311 08/21/15 08/21/15 METHOD EPA 7471A Molybdenum 0.62 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Nickel 36 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Selenium ND 0.46 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Silver ND 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Thallium ND 0.46 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Vanadium 35 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Zinc 83 0.93 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B
ND= Not DetectedRL= Reporting LimitPage 1 of 1 17.1
36 of 43
California Title 22 Metals
Lab #: 269097 Project#: STANDARD Client: Robin Spencer Location: COOK LOT Field ID: COOK-COMP5-081715 Basis: as received Lab ID: 269097-005 Diln Fac: 1.000 Matrix: Soil Sampled: 08/17/15 Units: mg/Kg Received: 08/17/15
Analyte Result RL Batch# Prepared Analyzed Prep Analysis Antimony 1.4 0.46 226301 08/19/15 08/21/15 EPA 3050B EPA 6010B Arsenic 5.2 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Barium 150 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Beryllium 0.57 0.092 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cadmium 0.97 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Chromium 28 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Cobalt 12 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Copper 30 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Lead 39 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Mercury 0.18 0.016 226311 08/21/15 08/21/15 METHOD EPA 7471A Molybdenum 0.71 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Nickel 32 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Selenium ND 0.46 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Silver ND 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Thallium ND 0.46 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Vanadium 32 0.23 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B Zinc 94 0.92 226301 08/19/15 08/20/15 EPA 3050B EPA 6010B
ND= Not DetectedRL= Reporting LimitPage 1 of 1 18.1
37 of 43
Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3050B Project#: STANDARD Analysis: EPA 6010B Type: BLANK Diln Fac: 1.000 Lab ID: QC800202 Batch#: 226301 Matrix: Soil Prepared: 08/19/15 Units: mg/Kg Analyzed: 08/20/15
Analyte Result RL Antimony ND 0.50 Arsenic ND 0.25 Barium ND 0.25 Beryllium ND 0.10 Cadmium ND 0.25 Chromium ND 0.25 Cobalt ND 0.25 Copper ND 0.25 Lead ND 0.25 Molybdenum ND 0.25 Nickel ND 0.25 Selenium ND 0.50 Silver ND 0.25 Thallium ND 0.50 Vanadium ND 0.25 Zinc ND 1.0
ND= Not DetectedRL= Reporting LimitPage 1 of 1 19.0
38 of 43
Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3050B Project#: STANDARD Analysis: EPA 6010B Matrix: Soil Prepared: 08/19/15 Units: mg/Kg Analyzed: 08/20/15 Batch#: 226301
Type: BS Lab ID: QC800203
Analyte Spiked Result %REC Limits Diln Fac Antimony 50.00 49.57 99 80-120 1.000 Arsenic 50.00 51.28 103 80-120 1.000 Barium 50.00 48.32 97 80-120 1.000 Beryllium 50.00 59.82 120 80-120 5.000 Cadmium 50.00 49.53 99 80-120 1.000 Chromium 50.00 49.48 99 80-120 1.000 Cobalt 50.00 45.88 92 80-120 1.000 Copper 50.00 50.32 101 80-120 1.000 Lead 50.00 45.88 92 80-120 1.000 Molybdenum 50.00 49.57 99 80-120 1.000 Nickel 50.00 46.22 92 80-120 1.000 Selenium 50.00 48.53 97 80-120 1.000 Silver 50.00 48.74 97 80-120 1.000 Thallium 50.00 46.07 92 80-120 1.000 Vanadium 50.00 52.36 105 80-120 1.000 Zinc 50.00 49.22 98 80-120 1.000
Type: BSD Lab ID: QC800204
Analyte Spiked Result %REC Limits RPD Lim Diln Fac Antimony 50.00 51.12 102 80-120 3 20 1.000 Arsenic 50.00 52.64 105 80-120 3 20 1.000 Barium 50.00 49.89 100 80-120 3 20 1.000 Beryllium 50.00 55.18 110 80-120 8 20 5.000 Cadmium 50.00 51.14 102 80-120 3 20 1.000 Chromium 50.00 51.06 102 80-120 3 20 1.000 Cobalt 50.00 47.39 95 80-120 3 20 1.000 Copper 50.00 52.18 104 80-120 4 20 1.000 Lead 50.00 47.18 94 80-120 3 20 1.000 Molybdenum 50.00 51.28 103 80-120 3 20 1.000 Nickel 50.00 47.66 95 80-120 3 20 1.000 Selenium 50.00 50.09 100 80-120 3 20 1.000 Silver 50.00 50.33 101 80-120 3 20 1.000 Thallium 50.00 47.32 95 80-120 3 20 1.000 Vanadium 50.00 54.03 108 80-120 3 20 1.000 Zinc 50.00 50.20 100 80-120 2 20 1.000
RPD= Relative Percent DifferencePage 1 of 1 20.0
39 of 43
Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: EPA 3050B Project#: STANDARD Analysis: EPA 6010B Field ID: ZZZZZZZZZZ Batch#: 226301 MSS Lab ID: 269137-001 Sampled: 08/19/15 Matrix: Soil Received: 08/19/15 Units: mg/Kg Prepared: 08/19/15 Basis: as received Analyzed: 08/20/15
Type: MS Lab ID: QC800205
Analyte MSS Result Spiked Result %REC Limits Diln Fac Antimony 1.916 47.17 24.67 48 15-120 5.000 Arsenic 5.876 47.17 53.53 101 69-120 1.000 Barium 113.5 47.17 137.7 51 35-154 1.000 Beryllium 0.4043 47.17 56.56 119 75-120 5.000 Cadmium 0.9240 47.17 44.46 92 71-120 1.000 Chromium 36.62 47.17 78.71 89 57-133 1.000 Cobalt 9.785 47.17 50.31 86 56-125 1.000 Copper 36.35 47.17 96.54 128 54-144 1.000 Lead 62.31 47.17 95.73 71 53-125 1.000 Molybdenum 0.7387 47.17 43.15 90 66-120 1.000 Nickel 41.79 47.17 78.47 78 44-141 1.000 Selenium <0.1597 47.17 45.01 95 61-120 1.000 Silver 0.06281 47.17 47.09 100 69-120 1.000 Thallium <0.1404 47.17 39.96 85 59-120 1.000 Vanadium 38.18 47.17 90.33 111 52-144 1.000 Zinc 192.6 47.17 218.6 55 NM 45-145 1.000
Type: MSD Lab ID: QC800206
Analyte Spiked Result %REC Limits RPD Lim Diln Fac Antimony 52.08 25.85 46 15-120 5 41 5.000 Arsenic 52.08 56.18 97 69-120 4 35 1.000 Barium 52.08 161.4 92 35-154 13 36 1.000 Beryllium 52.08 58.48 112 75-120 6 20 5.000 Cadmium 52.08 48.35 91 71-120 1 25 1.000 Chromium 52.08 88.17 99 57-133 6 33 1.000 Cobalt 52.08 54.44 86 56-125 0 36 1.000 Copper 52.08 93.57 110 54-144 9 38 1.000 Lead 52.08 111.4 94 53-125 11 42 1.000 Molybdenum 52.08 46.66 88 66-120 2 20 1.000 Nickel 52.08 88.84 90 44-141 7 39 1.000 Selenium 52.08 46.47 89 61-120 7 33 1.000 Silver 52.08 50.68 97 69-120 3 22 1.000 Thallium 52.08 41.17 79 59-120 7 27 1.000 Vanadium 52.08 91.36 102 52-144 4 29 1.000 Zinc 52.08 256.2 122 45-145 14 39 1.000
NM= Not Meaningful: Sample concentration > 4X spike concentrationRPD= Relative Percent DifferencePage 1 of 1 21.0
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Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: METHOD Project#: STANDARD Analysis: EPA 7471A Analyte: Mercury Diln Fac: 1.000 Type: BLANK Batch#: 226311 Lab ID: QC800228 Prepared: 08/20/15 Matrix: Soil Analyzed: 08/20/15 Units: mg/Kg
Result RL ND 0.017
ND= Not DetectedRL= Reporting LimitPage 1 of 1 22.0
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Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: METHOD Project#: STANDARD Analysis: EPA 7471A Analyte: Mercury Batch#: 226311 Matrix: Soil Prepared: 08/20/15 Units: mg/Kg Analyzed: 08/20/15 Diln Fac: 1.000
Type Lab ID Spiked Result %REC Limits RPD LimBS QC800229 0.2083 0.2031 98 80-120 BSD QC800230 0.2083 0.2099 101 80-120 3 20
RPD= Relative Percent DifferencePage 1 of 1 23.0
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Batch QC Report
California Title 22 Metals
Lab #: 269097 Location: COOK LOT Client: Robin Spencer Prep: METHOD Project#: STANDARD Analysis: EPA 7471A Analyte: Mercury Diln Fac: 1.000 Field ID: ZZZZZZZZZZ Batch#: 226311 MSS Lab ID: 269086-001 Sampled: 08/17/15 Matrix: Soil Received: 08/18/15 Units: mg/Kg Prepared: 08/20/15 Basis: as received Analyzed: 08/20/15
Type Lab ID MSS Result Spiked Result %REC Limits RPD LimMS QC800231 0.009440 0.2232 0.2322 100 69-142 MSD QC800232 0.2232 0.2310 99 69-142 1 36
RPD= Relative Percent DifferencePage 1 of 1 24.0
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