ANALYTICAL REPORT 6 - Energy.gov · 2016-09-26 · ANALYTICAL REPORT TestAmerica Laboratories, Inc....
Transcript of ANALYTICAL REPORT 6 - Energy.gov · 2016-09-26 · ANALYTICAL REPORT TestAmerica Laboratories, Inc....
ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica St. Louis13715 Rider Trail NorthEarth City, MO 63045Tel: (314)298-8566
TestAmerica Job ID: 160-18570-2Client Project/Site: ORNL Y-12 Outfall 200 Characterization
For:Alliant Corporation320 N Cedar Bluff RoadSuite 200Knoxville, Tennessee 37923
Attn: Doug Milloway
Authorized for release by:9/26/2016 3:18:59 PM
Erika Gish, Project Manager II(314)[email protected]
This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Alliant CorporationProject/Site: ORNL Y-12 Outfall 200 Characterization
TestAmerica Job ID: 160-18570-2
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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
Tracer Carrier Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Subcontract Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
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Case NarrativeClient: Alliant Corporation TestAmerica Job ID: 160-18570-2Project/Site: ORNL Y-12 Outfall 200 Characterization
Job ID: 160-18570-2
Laboratory: TestAmerica St. Louis
Narrative
CASE NARRATIVE
Client: Alliant Corporation
Project: ORNL Y-12 Outfall 200 Characterization
Report Number: 160-18570-2
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses
performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the application methods. TestAmerica’s operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any exceptions
to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a % solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and
disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the client.”
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPTThe samples were received on 8/10/2016 9:20 AM; the samples arrived in good condition, properly preserved. The temperature of the
cooler at receipt was 0.7º C.
Receipt Exceptions
The container label for the following sample did not match the information listed on the Chain-of-Custody (COC): YMTFA 32 SO 002 (160-18570-8). The container labels lists YMTFA 32 SO 010, while the COC lists YMTFA 32 SO 002. Sample was logged per CoC.
CommentsPlease see attached subcontract report for analyses performed at TestAmerica Richland.
RADIUM-226 BY ALPHA SPECTROMETRYSamples YMTFA 42 SO 030 (160-18570-1), YMTFA 42 SO 030D (160-18570-2), YMTFA 43 SO 030 (160-18570-3), YMTFA 43 SO 030D
(160-18570-4), YMTFA 49 SO 005 (160-18570-5), YMTFA 36 SO 002 (160-18570-6), YMTFA 35 SO 002 (160-18570-7), YMTFA 32 SO 002 (160-18570-8) and YMTFA 34 SO 002 (160-18570-9) were analyzed for Radium-226 by Alpha Spectrometry in accordance with
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Case NarrativeClient: Alliant Corporation TestAmerica Job ID: 160-18570-2Project/Site: ORNL Y-12 Outfall 200 Characterization
Job ID: 160-18570-2 (Continued)
Laboratory: TestAmerica St. Louis (Continued)
ST-RC-0301. The samples were dried on 08/10/2016, prepared on 08/22/2016 and analyzed on 09/15/2016 and 09/16/2016.
The At-217 tracer recovery for the following samples was low outside the QC limits of 30%: LCS 160-266021/2-A: 28.2%. The DOE/DOD
Quality Systems Manual for Environmental Laboratories (QSM Rev. 5.0) allows for reporting results as quantitative when tracer recoveries
are below 30% if a) the relative uncertainty associated with the tracer recovery is less than 10% (2 sigma), b) spectral resolution requirements are met and there are no indications of spectral interferences, and c) detection limit requirements are met. All three of these
criteria are met for these samples: a) a minimum of 400 counts (which leads to 10% count uncertainty at 2 sigma) in the tracer peak, b) resolution of < 100 keV is met for all peaks, and c) the activity in the sample is well above the MDC. The data have been qualified and
reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Page 5 of 52 9/26/2016
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Login Sample Receipt Checklist
Client: Alliant Corporation Job Number: 160-18570-2
Login Number: 18570
Question Answer Comment
Creator: Clarke, Jill C
List Source: TestAmerica St. Louis
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
FalseThere are no discrepancies between the containers received and the COC. Sample #8 COC and container do not match. Logged per container.
TrueSamples are received within Holding Time (excluding tests with immediate HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
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Definitions/GlossaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Qualifiers
Rad
Qualifier Description
S Tracer is outside acceptance limits.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Method SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Method Method Description LaboratoryProtocol
TAL-STLST-RC-0301 Radium-226 (Alpha Spectrometry) TAL SL
NONEAm-241 General Sub Contract Method TAL RCH
NONEC-14 General Sub Contract Method TAL RCH
NONENp-237 General Sub Contract Method TAL RCH
NONEPu-238,
Pu-239/240
General Sub Contract Method TAL RCH
NONETh-228, Th-230,
Th-232
General Sub Contract Method TAL RCH
NONEU-233/234,
U-235/236, U-238
General Sub Contract Method TAL RCH
Protocol References:
NONE = NONE
TAL-STL = TestAmerica Laboratories, St. Louis, Facility Standard Operating Procedure.
Laboratory References:
TAL RCH = TestAmerica Richland, 2800 George Washington Way, Richland, WA 99352, TEL (509)375-3131
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566
TestAmerica St. Louis
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Sample SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
160-18570-1 YMTFA 42 SO 030 Solid 08/09/16 09:20 08/10/16 09:20
160-18570-2 YMTFA 42 SO 030D Solid 08/09/16 09:20 08/10/16 09:20
160-18570-3 YMTFA 43 SO 030 Solid 08/09/16 10:50 08/10/16 09:20
160-18570-4 YMTFA 43 SO 030D Solid 08/09/16 10:50 08/10/16 09:20
160-18570-5 YMTFA 49 SO 005 Solid 08/09/16 13:00 08/10/16 09:20
160-18570-6 YMTFA 36 SO 002 Solid 08/09/16 13:05 08/10/16 09:20
160-18570-7 YMTFA 35 SO 002 Solid 08/09/16 14:01 08/10/16 09:20
160-18570-8 YMTFA 32 SO 002 Solid 08/09/16 14:48 08/10/16 09:20
160-18570-9 YMTFA 34 SO 002 Solid 08/09/16 15:10 08/10/16 09:20
TestAmerica St. Louis
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Client Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Lab Sample ID: 160-18570-1Client Sample ID: YMTFA 42 SO 030Matrix: SolidDate Collected: 08/09/16 09:20
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.66
(2σ+/-)
0.291
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.1391.00
RL MDC
0.255
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
43.2
Lab Sample ID: 160-18570-2Client Sample ID: YMTFA 42 SO 030DMatrix: SolidDate Collected: 08/09/16 09:20
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.53
(2σ+/-)
0.246
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.09251.00
RL MDC
0.210
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
55.1
Lab Sample ID: 160-18570-3Client Sample ID: YMTFA 43 SO 030Matrix: SolidDate Collected: 08/09/16 10:50
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.57
(2σ+/-)
0.253
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.07041.00
RL MDC
0.216
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
49.1
Lab Sample ID: 160-18570-4Client Sample ID: YMTFA 43 SO 030DMatrix: SolidDate Collected: 08/09/16 10:50
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.62
(2σ+/-)
0.260
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.07151.00
RL MDC
0.222
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
50.5
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Client Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Lab Sample ID: 160-18570-5Client Sample ID: YMTFA 49 SO 005Matrix: SolidDate Collected: 08/09/16 13:00
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.48
(2σ+/-)
0.241
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.02151.00
RL MDC
0.206
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
49.2
Lab Sample ID: 160-18570-6Client Sample ID: YMTFA 36 SO 002Matrix: SolidDate Collected: 08/09/16 13:05
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 0.537
(2σ+/-)
0.158
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.1161.00
RL MDC
0.152
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
40.3
Lab Sample ID: 160-18570-7Client Sample ID: YMTFA 35 SO 002Matrix: SolidDate Collected: 08/09/16 14:01
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.83
(2σ+/-)
0.278
(2σ+/-)
109/16/16 10:1708/22/16 18:53pCi/g0.05601.00
RL MDC
0.232
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/16/16 10:17 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
50.2
Lab Sample ID: 160-18570-8Client Sample ID: YMTFA 32 SO 002Matrix: SolidDate Collected: 08/09/16 14:48
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.72
(2σ+/-)
0.278
(2σ+/-)
109/16/16 10:1708/22/16 18:53pCi/g0.07731.00
RL MDC
0.238
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/16/16 10:17 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
46.2
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Client Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Lab Sample ID: 160-18570-9Client Sample ID: YMTFA 34 SO 002Matrix: SolidDate Collected: 08/09/16 15:10
Date Received: 08/10/16 09:20
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Analyte
Radium-226 1.25
(2σ+/-)
0.244
(2σ+/-)
109/15/16 10:1908/22/16 18:53pCi/g0.1211.00
RL MDC
0.220
Dil FacAnalyzedPreparedUnitResult Qualifier
Count Total
Uncert. Uncert.
At-217 30 - 110
Tracer
08/22/16 18:53 09/15/16 10:19 1
Dil FacAnalyzedPreparedQualifier Limits%Yield
39.4
TestAmerica St. Louis
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QC Sample ResultsTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)
Client Sample ID: Method BlankLab Sample ID: MB 160-266021/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270177 Prep Batch: 266021
Radium-226
Analyte
109/15/16 10:2008/22/16 18:53pCi/g0.0787
MDC
1.00
RL
0.09560.0942
(2σ+/-) (2σ+/-)
MB
0.1953
MB
Dil FacPrepared AnalyzedUnitResult Qualifier
Uncert.
Count
Uncert.
Total
Tracer
At-217 30 - 110 08/22/16 18:53 09/15/16 10:20 1
Dil FacPrepared AnalyzedQualifier Limits%Yield
36.5
MB MB
Client Sample ID: Lab Control SampleLab Sample ID: LCS 160-266021/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270178 Prep Batch: 266021
Radium-226
Analyte
130-7011714.0712.1 1.47 1.00 0.103
RL MDC(2σ+/-)
LCS LCS
pCi/g
UnitResult Qual %RecAdded
Spike
Limits
%Rec.Uncert.
Total
At-217
Tracer
S 30 - 110
LCS
Qualifier Limits%Yield
28.2
LCS
Client Sample ID: DuplicateLab Sample ID: 160-18504-F-1-Q DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 270180 Prep Batch: 266021
Radium-226
Analyte
10.310.65920.772 0.171 1.00 0.152
RL MDC(2σ+/-)
DU DU
pCi/g
UnitResult Qual LimitResult
Sample Sample
Qual
Uncert.
Total
RER
RER
At-217
Tracer
30 - 110
DU
Qualifier Limits%Yield
50.0
DU
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QC Association SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Rad
Leach Batch: 263919
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Dry and Grind160-18504-F-1-Q DU Duplicate Total/NA
Leach Batch: 264331
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Dry and Grind160-18570-1 YMTFA 42 SO 030 Total/NA
Solid Dry and Grind160-18570-2 YMTFA 42 SO 030D Total/NA
Solid Dry and Grind160-18570-3 YMTFA 43 SO 030 Total/NA
Solid Dry and Grind160-18570-4 YMTFA 43 SO 030D Total/NA
Solid Dry and Grind160-18570-5 YMTFA 49 SO 005 Total/NA
Solid Dry and Grind160-18570-6 YMTFA 36 SO 002 Total/NA
Solid Dry and Grind160-18570-7 YMTFA 35 SO 002 Total/NA
Solid Dry and Grind160-18570-8 YMTFA 32 SO 002 Total/NA
Solid Dry and Grind160-18570-9 YMTFA 34 SO 002 Total/NA
Prep Batch: 266021
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid DPS-0 264331160-18570-1 YMTFA 42 SO 030 Total/NA
Solid DPS-0 264331160-18570-2 YMTFA 42 SO 030D Total/NA
Solid DPS-0 264331160-18570-3 YMTFA 43 SO 030 Total/NA
Solid DPS-0 264331160-18570-4 YMTFA 43 SO 030D Total/NA
Solid DPS-0 264331160-18570-5 YMTFA 49 SO 005 Total/NA
Solid DPS-0 264331160-18570-6 YMTFA 36 SO 002 Total/NA
Solid DPS-0 264331160-18570-7 YMTFA 35 SO 002 Total/NA
Solid DPS-0 264331160-18570-8 YMTFA 32 SO 002 Total/NA
Solid DPS-0 264331160-18570-9 YMTFA 34 SO 002 Total/NA
Solid DPS-0MB 160-266021/1-A Method Blank Total/NA
Solid DPS-0LCS 160-266021/2-A Lab Control Sample Total/NA
Solid DPS-0 263919160-18504-F-1-Q DU Duplicate Total/NA
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Tracer/Carrier SummaryTestAmerica Job ID: 160-18570-2Client: Alliant Corporation
Project/Site: ORNL Y-12 Outfall 200 Characterization
Method: ST-RC-0301 - Radium-226 (Alpha Spectrometry)Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (30-110)
At-217
50.0160-18504-F-1-Q DU
Percent Yield (Acceptance Limits)
Duplicate
43.2160-18570-1 YMTFA 42 SO 030
55.1160-18570-2 YMTFA 42 SO 030D
49.1160-18570-3 YMTFA 43 SO 030
50.5160-18570-4 YMTFA 43 SO 030D
49.2160-18570-5 YMTFA 49 SO 005
40.3160-18570-6 YMTFA 36 SO 002
50.2160-18570-7 YMTFA 35 SO 002
46.2160-18570-8 YMTFA 32 SO 002
39.4160-18570-9 YMTFA 34 SO 002
28.2 SLCS 160-266021/2-A Lab Control Sample
36.5MB 160-266021/1-A Method Blank
Tracer/Carrier Legend
At-217 = At-217
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Analytical Data Package Prepared For
Radiochemical Analysis By
TESTAMERICA ST. LOUIS
TestAmerica Inc
2800 G.W. Way, Richland Wa, 99354, (509)-375-3131.
Data Package Contains ______ Pages
Assigned Laboratory Code: TA-RL
Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.
Report No.: 69364
Order No. Report DB ID Batch No.
Results in this report relate only to the sample(s) analyzed.
YMTFA 32 SO 002(160-
18570-8)
9M84VV1051961 J6H180408-8 M84VV1AE 6231057
YMTFA 32 SO 002(160-
18570-8)
9M84VV10J6H180408-8 M84VV1AG 6231058
YMTFA 32 SO 002(160-
18570-8)
9M84VV10J6H180408-8 M84VV1AC 6231059
YMTFA 32 SO 002(160-
18570-8)
9M84VV10J6H180408-8 M84VV1AF 6231060
YMTFA 32 SO 002(160-
18570-8)
9M84VV10J6H180408-8 M84VV1AA 6231061
YMTFA 32 SO 002(160-
18570-8)
9M84VV10J6H180408-8 M84VV1AD 6231062
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AE 6231057
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AG 6231058
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AC 6231059
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AF 6231060
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AA 6231061
YMTFA 34 SO 002(160-
18570-9)
9M84VW10J6H180408-9 M84VW1AD 6231062
YMTFA 35 SO 002(160-
18570-7)
9M84VR10J6H180408-7 M84VR1AE 6231057
YMTFA 35 SO 002(160-
18570-7)
9M84VR10J6H180408-7 M84VR1AG 6231058
YMTFA 35 SO 002(160-
18570-7)
9M84VR10J6H180408-7 M84VR1AC 6231059
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Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.
Report No.: 69364
Order No. Report DB ID Batch No.
Results in this report relate only to the sample(s) analyzed.
YMTFA 35 SO 002(160-
18570-7)
9M84VR1051961 J6H180408-7 M84VR1AF 6231060
YMTFA 35 SO 002(160-
18570-7)
9M84VR10J6H180408-7 M84VR1AA 6231061
YMTFA 35 SO 002(160-
18570-7)
9M84VR10J6H180408-7 M84VR1AD 6231062
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AE 6231057
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AG 6231058
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AC 6231059
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AF 6231060
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AA 6231061
YMTFA 36 SO 002(160-
18570-6)
9M84VQ10J6H180408-6 M84VQ1AD 6231062
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AE 6231057
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AG 6231058
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AC 6231059
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AF 6231060
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AA 6231061
YMTFA 42 SO 030(160-
18570-1)
9M84VK10J6H180408-1 M84VK1AD 6231062
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AE 6231057
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AG 6231058
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AC 6231059
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AF 6231060
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AA 6231061
YMTFA 42 SO 030D(160-
18570-2)
9M84VL10J6H180408-2 M84VL1AD 6231062
YMTFA 43 SO 030(160-
18570-3)
9M84VM10J6H180408-3 M84VM1AE 6231057
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Client Sample ID (List Order) Lot-Sa No. Work OrderSDG No.
Report No.: 69364
Order No. Report DB ID Batch No.
Results in this report relate only to the sample(s) analyzed.
YMTFA 43 SO 030(160-
18570-3)
9M84VM1051961 J6H180408-3 M84VM1AG 6231058
YMTFA 43 SO 030(160-
18570-3)
9M84VM10J6H180408-3 M84VM1AC 6231059
YMTFA 43 SO 030(160-
18570-3)
9M84VM10J6H180408-3 M84VM1AF 6231060
YMTFA 43 SO 030(160-
18570-3)
9M84VM10J6H180408-3 M84VM1AA 6231061
YMTFA 43 SO 030(160-
18570-3)
9M84VM10J6H180408-3 M84VM1AD 6231062
YMTFA 43 SO 030D(160-
18570-4)
9M84VN10J6H180408-4 M84VN1AE 6231057
YMTFA 43 SO 030D(160-
18570-4)
9M84VN20J6H180408-4 M84VN2AG 6231058
YMTFA 43 SO 030D(160-
18570-4)
9M84VN10J6H180408-4 M84VN1AC 6231059
YMTFA 43 SO 030D(160-
18570-4)
9M84VN10J6H180408-4 M84VN1AF 6231060
YMTFA 43 SO 030D(160-
18570-4)
9M84VN10J6H180408-4 M84VN1AA 6231061
YMTFA 43 SO 030D(160-
18570-4)
9M84VN10J6H180408-4 M84VN1AD 6231062
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AE 6231057
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AG 6231058
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AC 6231059
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AF 6231060
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AA 6231061
YMTFA 49 SO 005(160-
18570-5)
9M84VP10J6H180408-5 M84VP1AD 6231062
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Certificate of Analysis
September 23, 2016
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Attention: Erika Gish
Date Received in Lab : August 18, 2016
Sample Type : Nine (9) Solid
SDG Number : 51961
Job Number : 160-18570-1
Project Number/Name : 16005502/ORNL Y-12 Outfall 200 Characterization
CASE NARRATIVE
I. Introduction
On August 18, 2016, nine solid samples were received at the TestAmerica Richland laboratory for
radiochemical analysis. Upon receipt the samples were assigned to Lot Number J6H180408 with the
laboratory ID number corresponding to the client ID as shown on the cover page.
II. Sample Receipt
The samples were received in good condition; no anomalies were noted upon check-in.
III. Analytical Results/Methodology
The analytical results for this report are presented by laboratory sample ID. Each set of data includes
sample identification information; analytical results and the appropriate associated statistical
uncertainties.
The analyses requested were:
Alpha Spectroscopy
Americium 241 by method RL-ALP-003
Neptunium-237 by method RL-ALP-013
Plutonium-238, -239/240 by method RL-ALP-002
Thorium-228,230,232 by method RL-ALP-001
Uranium 234, 235 and 238 by method RL-ALP-004
Liquid Scintillation Counting
Carbon-14 by method RL-LSC-008
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TestAmerica St. Louis
September 23, 2016
IV. Quality Control
The analytical result for each analysis performed includes a minimum of one laboratory control sample
(LCS), and one reagent blank sample analysis. Any exceptions have been noted in the “Comments”
section.
V. Comments
Alpha Spectroscopy
Americium 241 by method RL-ALP-003:
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
Neptunium-237 by method RL-ALP-013:
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
Plutonium-238, -239/240 by method RL-ALP-002:
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
Thorium-228,230,232 by method RL-ALP-001
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
Uranium 234, 235 and 238 by method RL-ALP-004
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
Liquid Scintillation Counting
Carbon-14 by method RL-LSC-008:
The LCS, batch blank, sample duplicate and sample results are within acceptance limits.
I certify that this Certificate of Analysis is in compliance with the SOW and/or NELAC, both technically
and for completeness, for other than the conditions detailed above. The Laboratory Manager or a
designee, as verified by the following signature has authorized release of the data contained in this hard
copy data package.
Reviewed and approved:
____________________________
Roger A. Stringer
Project Manager I
TestAmerica Laboratories, Inc. 5
Roger A. StringerDigitally signed by Roger A. Stringer
DN: cn=Roger A. Stringer, o, ou,
[email protected], c=US
Date: 2016.09.23 11:40:33 -07'00'
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DRINKING WATER ASTM METHOD CROSS REFERENCES
Referenced Method Isotope(s) TestAmerica Richland's SOP No.
EPA 901.1 Cs-134, I-131 RL-GAM-001
EPA 900.0 Alpha & Beta RL-GPC-001
EPA 00-02 Gross Alpha (Coprecipitation) RL-GPC-002
EPA 903.0 Total Alpha Radium (Ra-226) RL-RA-002
EPA 903.1 Ra-226 RL-RA-001
EPA 904.0 Ra-228 RL-RA-001
EPA 905.0 Sr-89/90 RL-GPC-003
ASTM D5174 Uranium RL-KPA-003
EPA 906.0 Tritium RL-LSC-005
TestAmerica Richland has adopted the internationally accepted approach to estimating
uncertainties described in “NIST Technical Note 1297, 1994 Edition”. The approach, "Law of Propagation
of Errors", involves the identification of all variables in an analytical method which are used to derive a
result. These variables are related to the analytical result (R) by some functional relationship, R = constants
* f(x,y,z,...). The components (x,y,z) are evaluated to determine their contribution to the overall method
uncertainty. The individual component uncertainties (ui) are then combined using a statistical model that
provides the most probable overall uncertainty value. All component uncertainties are categorized as type
A, evaluated by statistical methods, or type B, evaluated by other means. Uncertainties not included in the
components, such as sample homogeneity, are combined with the component uncertainty as the square root
of the sum-of-the-squares of the individual uncertainties. The uncertainty associated with the derived result
is the combined uncertainty (uc) multiplied by the coverage factor (1,2, or 3).
When three or more sample replicates are used to derive the analytical result, the type A
uncertainty is the standard deviation of the mean value (S/?n), where S is the standard deviation of the
derived results. The type B uncertainties are all other random or non-random components that are not
included in the standard deviation.
The derivation of the general "Law of Propagation of Errors" equations and specific example are
available on request.
Uncertainty Estimation
Drinking Water Method Cross References
Results in this report relate only to the sample(s) analyzed.
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Action Lev An agreed upon activity level used to trigger some action when the final result is greater than or equal to the Action
Level. Often the Action Level is related to the Decision Limit.
Batch The QC preparation batch number that relates laboratory samples to QC samples that were prepared and analyzed
together.
Bias Defined by the equation (Result/Expected)-1 as defined by ANSI N13.30.
COC No Chain of Custody Number assigned by the Client or TestAmerica.
Count Error (#s) Poisson counting statistics of the gross sample count and background. The uncertainty is absolute and in the same
units as the result. For Liquid Scintillation Counting (LSC) the batch blank count is the background.
CSU (#s)
uc Combined
Standard Uncert.
All known uncertainties associated with the preparation and analysis of the sample are propagated to give a measure
of the uncertainty associated with the result, uc the combined standard uncertainty. The uncertainty is absolute and
in the same units as the result.
(#s), Coverage
Factor
The coverage factor defines the width of the confidence interval, 1, 2 or 3 standard deviations.
CRDL (RL) Contractual Required Detection Limit as defined in the Client’s Statement Of Work or TestAmerica “default”
nominal detection limit. Often referred to the reporting level (RL)
Lc Decision Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
associated with the sample. The Type I error probability is approximately 5%. Lc=(1.645 *
Sqrt(2*(BkgrndCnt/BkgrndCntMin)/SCntMin)) * (ConvFct/(Eff*Yld*Abn*Vol) * IngrFct). For LSC methods the
batch blank is used as a measure of the background variability. Lc cannot be calculated when the background count
is zero.
Lot-Sample No The number assigned by the LIMS software to track samples received on the same day for a given client. The
sample number is a sequential number assigned to each sample in the Lot.
MDC|MDA|MDL Detection Level based on instrument background or blank, adjusted by the Efficiency, Chemical Yield, and Volume
with a Type I and II error probability of approximately 5%. MDC = (4.65 *
Sqrt((BkgrndCnt/BkgrndCntMin)/SCntMin) + 2.71/SCntMin) * (ConvFct/(Eff * Yld * Abn * Vol) * IngrFct). For
LSC methods the batch blank is used as a measure of the background variability.
Primary Detector The instrument identifier associated with the analysis of the sample aliquot.
Ratio U-234/U-238 The U-234 result divided by the U-238 result. The U-234/U-238 ratio for natural uranium in NIST SRM 4321C is
1.038.
Rst/MDC Ratio of the Result to the MDC. A value greater than 1 may indicate activity above background at a high level of
confidence. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Rst/TotUcert Ratio of the Result to the Total Uncertainty. If the uncertainty has a coverage factor of 2 a value greater than 1 may
indicate activity above background at approximately the 95% level of confidence assuming a two-sided confidence
interval. Caution should be used when applying this factor and it should be used in concert with the qualifiers
associated with the result.
Report DB No Sample Identifier used by the report system. The number is based upon the first five digits of the Work Order
Number.
RER The equation Replicate Error Ratio = (S-D)/[sqrt(TPUs2 + TPUd2)] as defined by ICPT BOA where S is the original
sample result, D is the result of the duplicate, TPUs is the total uncertainty of the original sample and TPUd is the
total uncertainty of the duplicate sample.
SDG Sample Delivery Group Number assigned by the Client or assigned by TestAmerica upon sample receipt.
Sum Rpt Alpha
Spec Rst(s)
The sum of the reported alpha spec results for tests derived from the same sample excluding duplicate result where
the results are in the same units.
Work Order The LIMS software assign test specific identifier.
Yield The recovery of the tracer added to the sample such as Pu-242 used to trace a Pu-239/40 method.
Report Definitions
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22-Sep-16Date:
Parameter MDLUnits
Client Id
Work Order
Report No. : 69359
Result +- CSU ( s) Tracer
Yield
51966SDG No:
TestAmerica Inc TA-RL
Qual
Sample Results Summary
Ordered by Method, Batch No., Client Sample ID.
2 RER2CRDLBatch
6231051 L4SO
YMTFA60 SO 010(160-18615-6)
5.88E-02PLUTONIUM-238 PCI_GM840L1AE -3.04E-03 96% +- 2.5E-02 1.00E+00U
5.49E-02PLUTONIUM-239/240 PCI_G1.06E-02 96% +- 2.5E-02 1.00E+00U
YMTFA61 SO 010(160-18615-5)
8.02E-02PLUTONIUM-238 PCI_GM840K1AE 7.83E-03 93% +- 3.0E-02 1.00E+00U
5.53E-02PLUTONIUM-239/240 PCI_G1.44E-02 93% +- 3.0E-02 1.00E+00U
YMTFA62 SO 010(160-18615-4)
7.30E-02PLUTONIUM-238 PCI_GM840J1AE 9.32E-03 94% +- 2.9E-02 1.00E+00U
5.74E-02PLUTONIUM-239/240 PCI_G-1.16E-03 94% +- 2.9E-02 1.00E+00U
YMTFA67 SO 010(160-18615-3)
9.70E-02PLUTONIUM-238 PCI_GM840G1AE -8.75E-03 67% +- 3.7E-02 1.00E+00U
7.90E-02PLUTONIUM-239/240 PCI_G-2.91E-03 67% +- 3.7E-02 1.00E+00U
YMTFA69 SO 010(160-18615-2)
6.65E-02PLUTONIUM-238 PCI_GM840E1AE 1.09E-02 87% +- 2.9E-02 1.00E+00U
6.44E-02PLUTONIUM-239/240 PCI_G-2.86E-03 87% +- 2.9E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1)
8.11E-02PLUTONIUM-238 PCI_GM84X91AE 7.92E-03 95% +- 3.1E-02 1.00E+00U
5.59E-02PLUTONIUM-239/240 PCI_G0.00E+00 95% +- 3.0E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1) DU
5.47E-02PLUTONIUM-238 PCI_GM84X91AH 1.63E-02 104% 0.4 +- 3.0E-02 1.00E+00U
4.36E-02PLUTONIUM-239/240 PCI_G-1.26E-03 104% 0.1 +- 2.1E-02 1.00E+00U
6231052 C0SR
YMTFA60 SO 010(160-18615-6)
9.64E-02URANIUM-233/234 PCI_GM840L1AG 2.19E-01 56% +- 1.5E-01 1.00E+00
8.15E-02URANIUM-235/236 PCI_G4.35E-02 56% +- 6.3E-02 1.00E+00U
8.15E-02URANIUM-238 PCI_G1.55E-01 56% +- 1.2E-01 1.00E+00
YMTFA61 SO 010(160-18615-5)
5.98E-02URANIUM-233/234 PCI_GM840K1AG 2.42E-01 89% +- 1.3E-01 1.00E+00
5.27E-02URANIUM-235/236 PCI_G-5.74E-04 89% +- 2.9E-02 1.00E+00U
6.46E-02URANIUM-238 PCI_G2.56E-01 89% +- 1.3E-01 1.00E+00
YMTFA67 SO 010(160-18615-3)
6.19E-02URANIUM-233/234 PCI_GM840G1AG 2.53E-01 75% +- 1.4E-01 1.00E+00
6.19E-02URANIUM-235/236 PCI_G0.00E+00 75% +- 3.4E-02 1.00E+00U
7.02E-02URANIUM-238 PCI_G2.34E-01 75% +- 1.3E-01 1.00E+00
YMTFA69 SO 010(160-18615-2)
6.13E-02URANIUM-233/234 PCI_GM840E1AG 3.71E-01 84% +- 1.7E-01 1.00E+00
5.70E-02URANIUM-235/236 PCI_G1.55E-02 84% +- 3.1E-02 1.00E+00U
6.13E-02URANIUM-238 PCI_G1.85E-01 84% +- 1.1E-01 1.00E+00
TestAmerica Inc
U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan
software.
RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum
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22-Sep-16Date:
Parameter MDLUnits
Client Id
Work Order
Report No. : 69359
Result +- CSU ( s) Tracer
Yield
51966SDG No:
TestAmerica Inc TA-RL
Qual
Sample Results Summary
Ordered by Method, Batch No., Client Sample ID.
2 RER2CRDLBatch
6231052 C0SR
YMTFA70 SO 010(160-18615-1)
7.07E-02URANIUM-233/234 PCI_GM84X91AG 3.81E-01 85% +- 1.7E-01 1.00E+00
5.44E-02URANIUM-235/236 PCI_G-5.93E-04 85% +- 3.0E-02 1.00E+00U
5.85E-02URANIUM-238 PCI_G3.40E-01 85% +- 1.5E-01 1.00E+00
YMTFA70 SO 010(160-18615-1) DU
5.43E-02URANIUM-233/234 PCI_GM84X91AJ 3.84E-01 70% 0.0 +- 1.6E-01 1.00E+00
5.05E-02URANIUM-235/236 PCI_G-5.50E-04 70% 0.0 +- 2.8E-02 1.00E+00U
5.43E-02URANIUM-238 PCI_G2.74E-01 70% 0.6 +- 1.3E-01 1.00E+00
6231053 L4SX
YMTFA60 SO 010(160-18615-6)
7.24E-02AMERICIUM-241 PCI_GM840L1AC 1.98E-02 101% +- 3.8E-02 1.00E+00U
YMTFA61 SO 010(160-18615-5)
6.77E-02AMERICIUM-241 PCI_GM840K1AC 1.11E-02 94% +- 2.9E-02 1.00E+00U
YMTFA62 SO 010(160-18615-4)
7.29E-02AMERICIUM-241 PCI_GM840J1AC -6.14E-03 101% +- 2.8E-02 1.00E+00U
YMTFA67 SO 010(160-18615-3)
6.63E-02AMERICIUM-241 PCI_GM840G1AC -1.91E-03 77% +- 3.2E-02 1.00E+00U
YMTFA69 SO 010(160-18615-2)
7.54E-02AMERICIUM-241 PCI_GM840E1AC 4.58E-02 95% +- 5.5E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1)
8.49E-02AMERICIUM-241 PCI_GM84X91AC -8.15E-03 93% +- 3.2E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1) DU
5.95E-02AMERICIUM-241 PCI_GM84X91AK 1.70E-02 92% 1.1 +- 3.2E-02 1.00E+00U
6231054 L4S1
YMTFA60 SO 010(160-18615-6)
5.22E-02THORIUM-228 PCI_GM840L1AF 4.84E-01 94% +- 1.9E-01 1.00E+00
5.02E-02THORIUM-230 PCI_G2.46E-01 94% +- 1.2E-01 1.00E+00
5.02E-02THORIUM-232 PCI_G6.56E-01 94% +- 2.2E-01 1.00E+00
YMTFA61 SO 010(160-18615-5)
7.14E-02THORIUM-228 PCI_GM840K1AF 7.19E-01 94% +- 2.5E-01 1.00E+00
5.84E-02THORIUM-230 PCI_G8.75E-02 94% +- 7.4E-02 1.00E+00
5.43E-02THORIUM-232 PCI_G4.43E-01 94% +- 1.8E-01 1.00E+00
YMTFA62 SO 010(160-18615-4)
5.99E-02THORIUM-228 PCI_GM840J1AF 6.93E-01 93% +- 2.3E-01 1.00E+00
4.55E-02THORIUM-230 PCI_G1.61E-01 93% +- 9.4E-02 1.00E+00
4.55E-02THORIUM-232 PCI_G3.34E-01 93% +- 1.4E-01 1.00E+00
YMTFA67 SO 010(160-18615-3)
7.57E-02THORIUM-228 PCI_GM840G1AF 4.74E-01 64% +- 2.2E-01 1.00E+00
TestAmerica Inc
U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan
software.
RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum
mary2 V5.6 A2002
TestAmerica Laboratories, Inc. 9Page 24 of 52 9/26/2016
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2
3
4
5
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7
8
9
10
11
12
13
22-Sep-16Date:
Parameter MDLUnits
Client Id
Work Order
Report No. : 69359
Result +- CSU ( s) Tracer
Yield
51966SDG No:
TestAmerica Inc TA-RL
Qual
Sample Results Summary
Ordered by Method, Batch No., Client Sample ID.
2 RER2CRDLBatch
6231054 L4S1
YMTFA67 SO 010(160-18615-3)
7.83E-02THORIUM-230 PCI_GM840G1AF 3.55E-01 64% +- 1.9E-01 1.00E+00
7.28E-02THORIUM-232 PCI_G3.56E-01 64% +- 1.9E-01 1.00E+00
YMTFA69 SO 010(160-18615-2)
4.88E-02THORIUM-228 PCI_GM840E1AF 2.58E-01 92% +- 1.2E-01 1.00E+00
4.35E-02THORIUM-230 PCI_G2.49E-01 92% +- 1.2E-01 1.00E+00
4.35E-02THORIUM-232 PCI_G3.68E-01 92% +- 1.5E-01 1.00E+00
YMTFA70 SO 010(160-18615-1)
8.19E-02THORIUM-228 PCI_GM84X91AF 5.42E-01 91% +- 2.2E-01 1.00E+00
9.31E-02THORIUM-230 PCI_G2.71E-01 91% +- 1.5E-01 1.00E+00
6.42E-02THORIUM-232 PCI_G3.66E-01 91% +- 1.7E-01 1.00E+00
YMTFA70 SO 010(160-18615-1) DU
5.85E-02THORIUM-228 PCI_GM84X91AL 5.60E-01 91% 0.1 +- 2.0E-01 1.00E+00
5.33E-02THORIUM-230 PCI_G2.69E-01 91% 0.0 +- 1.3E-01 1.00E+00
4.95E-02THORIUM-232 PCI_G3.64E-01 91% 0.0 +- 1.5E-01 1.00E+00
6231056 E7XW
YMTFA60 SO 010(160-18615-6)
3.35E-02NEPTUNIUM-237 PCI_GM840L1AD -6.77E-04 91% +- 1.7E-02 1.00E+00U
YMTFA61 SO 010(160-18615-5)
1.85E-02NEPTUNIUM-237 PCI_GM840K1AD 4.67E-03 92% +- 9.5E-03 1.00E+00U
YMTFA62 SO 010(160-18615-4)
2.86E-02NEPTUNIUM-237 PCI_GM840J1AD 5.49E-03 92% +- 1.3E-02 1.00E+00U
YMTFA67 SO 010(160-18615-3)
3.11E-02NEPTUNIUM-237 PCI_GM840G1AD 3.61E-03 89% +- 1.2E-02 1.00E+00U
YMTFA69 SO 010(160-18615-2)
3.05E-02NEPTUNIUM-237 PCI_GM840E1AD -1.57E-03 94% +- 1.3E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1)
2.71E-02NEPTUNIUM-237 PCI_GM84X91AD -9.93E-04 88% +- 1.2E-02 1.00E+00U
YMTFA70 SO 010(160-18615-1) DU
3.94E-02NEPTUNIUM-237 PCI_GM84X91AN -1.45E-03 87% 0.0 +- 1.8E-02 1.00E+00U
6231049 RL-LSC-008
YMTFA60 C(160-18613-1) DUP
1.88E-01CARBON-14 PCI_GM84XV1AM 3.99E-02 100% 0.1 +- 9.7E-02 1.00E+01U
YMTFA60 SO 010(160-18615-6)
1.93E-01CARBON-14 PCI_GM840L1AA -5.27E-02 100% +- 9.6E-02 1.00E+01U
YMTFA61 SO 010(160-18615-5)
1.89E-01CARBON-14 PCI_GM840K1AA -8.97E-02 100% +- 9.3E-02 1.00E+01U
YMTFA62 SO 010(160-18615-4)
TestAmerica Inc
U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan
software.
RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum
mary2 V5.6 A2002
TestAmerica Laboratories, Inc. 10Page 25 of 52 9/26/2016
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2
3
4
5
6
7
8
9
10
11
12
13
22-Sep-16Date:
Parameter MDLUnits
Client Id
Work Order
Report No. : 69359
Result +- CSU ( s) Tracer
Yield
51966SDG No:
TestAmerica Inc TA-RL
Qual
Sample Results Summary
Ordered by Method, Batch No., Client Sample ID.
2 RER2CRDLBatch
6231049 RL-LSC-008
YMTFA62 SO 010(160-18615-4)
1.85E-01CARBON-14 PCI_GM840J1AA -7.21E-02 100% +- 9.2E-02 1.00E+01U
YMTFA67 SO 010(160-18615-3)
1.88E-01CARBON-14 PCI_GM840G1AA -5.48E-02 100% +- 9.4E-02 1.00E+01U
YMTFA69 SO 010(160-18615-2)
1.88E-01CARBON-14 PCI_GM840E1AA -3.31E-02 100% +- 9.4E-02 1.00E+01U
YMTFA70 SO 010(160-18615-1)
1.92E-01CARBON-14 PCI_GM84X91AA -7.75E-02 100% +- 9.5E-02 1.00E+01U
74No. of Results:
TestAmerica Inc
U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan
software.
RER2 - Replicate Error Ratio = (S-D)/[sqrt(sq(TPUs)+sq(TPUd))] as defined by ICPT BOA.
rptTALRchSaSum
mary2 V5.6 A2002
TestAmerica Laboratories, Inc. 11Page 26 of 52 9/26/2016
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2
3
4
5
6
7
8
9
10
11
12
13
23-Sep-16Date:
Parameter MDLUnits
Batch
Work Order
Report No. : 69364
Result +- CSU ( s) Tracer
Yield
51961SDG No.:
TestAmerica Inc TA-RL
Qual
QC Results Summary
LCS
Recovery Bias
Ordered by Method, Batch No, QC Type,.
2
L4SO
6231057 BLANK QC,
6.46E-02PLUTONIUM-238 PCI_GM842A1AA 93% 1.62E-02 +- 3.3E-02 U
4.56E-02PLUTONIUM-239/240 PCI_G 93% 1.06E-02 +- 2.3E-02 U
6231057 LCS,
5.08E-02PLUTONIUM-239/240 PCI_GM842A1AC 90% 97% 0.03.26E+00 +- 7.0E-01
C0SR
6231058 BLANK QC,
4.79E-02URANIUM-233/234 PCI_GM842C1AA 95% 5.14E-03 +- 1.9E-02 U
3.82E-02URANIUM-235/236 PCI_G 95% -1.10E-03 +- 1.8E-02 U
4.13E-02URANIUM-238 PCI_G 95% -1.83E-03 +- 1.8E-02 U
6231058 LCS,
4.13E-02URANIUM-233/234 PCI_GM842C1AC 105% 88% -0.11.89E+00 +- 4.1E-01
3.52E-02URANIUM-238 PCI_G 105% 86% -0.11.93E+00 +- 4.2E-01
L4SX
6231059 BLANK QC,
9.56E-02AMERICIUM-241 PCI_GM842D1AA 62% 2.61E-02 +- 5.0E-02 U
6231059 LCS,
1.50E-01AMERICIUM-241 PCI_GM842D1AC 35% 104% 0.03.44E+00 +- 1.0E+00
L4S1
6231060 BLANK QC,
5.53E-02THORIUM-228 PCI_GM842E1AA 97% 9.82E-03 +- 2.5E-02 U
4.32E-02THORIUM-230 PCI_G 97% 1.18E-02 +- 2.4E-02 U
4.32E-02THORIUM-232 PCI_G 97% -4.71E-04 +- 2.4E-02 U
6231060 LCS,
6.29E-02THORIUM-230 PCI_GM842E1AC 71% 78% -0.21.30E+00 +- 3.7E-01
E7XW
6231062 BLANK QC,
4.95E-02NEPTUNIUM-237 PCI_GM842G1AA 78% -1.43E-03 +- 2.4E-02 U
6231062 LCS,
5.60E-02NEPTUNIUM-237 PCI_GM842G1AC 73% 99% 0.01.25E+00 +- 4.4E-01
RL-LSC-008
6231061 BLANK QC,
1.91E-01CARBON-14 PCI_GM842F1AA 100% -3.38E-02 +- 9.5E-02 U
6231061 LCS,
1.92E-01CARBON-14 PCI_GM842F1AC 100% 99% 0.07.24E+00 +- 5.1E-01
18No. of Results:
TestAmerica Inc
U Qual - Analyzed for but not detected above limiting criteria, Mdc/Mda/Mdl, Total Uncert, RDL or not identified by gamma scan software.
Bias - (Result/Expected)-1 as defined by ANSI N13.30.
rptSTLRchQcSum
mary V5.6 A2002
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2
3
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7
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9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
2 S
O 0
02(1
60-1
8570-8
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
2:4
8:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-8
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
V1A
EW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:L4S
O
1.3
5E
-02
3.8
E-0
28
.99
E-0
27
1%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
7 p
1.0
5A
LP
424
g
0.1
5
0.7
1
U
1.0
0E
+0
02
.32
E-0
2
- 7.5
2E
-04
3.8
E-0
26
.91
E-0
27
1%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
7 p
1.0
5A
LP
424
g
-0.0
1
-0.0
4
U
1.0
0E
+0
01
.35
E-0
2
6231058
Batc
h:
M84V
V1A
GW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:C
0S
R
5.2
8E
-01
2.0
E-0
17
.60
E-0
28
6%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.0
4A
LP
217
g
(6.9
)
(5.2
)1
.00
E+
00
2.0
8E
-02
0.0
0E
+0
03
.0E
-02
5.4
4E
-02
86
%U
RA
NIU
M-2
35/2
36
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.0
4A
LP
217
g
0.
0.
U
1.0
0E
+0
01
.06
E-0
2
2.7
9E
-01
1.4
E-0
16
.44
E-0
28
6%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.0
4A
LP
217
g
(4.3
)
(4.)
1.0
0E
+0
01
.52
E-0
2
Rati
o U
-234/2
38
= 1
.9
6231059
Batc
h:
M84V
V1A
CW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:L4S
X
-1.3
9E
-02
4.7
E-0
21
.30
E-0
16
0%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:33
p1.0
5A
LP
419
g
-0.1
1
-0.5
9
U
1.0
0E
+0
03
.80
E-0
2
6231060
Batc
h:
M84V
V1A
FW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:L4S
1
4.4
0E
-01
1.9
E-0
16
.87
E-0
29
3%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
5A
LP
404
g
(6.4
)
(4.8
)1
.00
E+
00
1.6
2E
-02
5.4
6E
-01
2.1
E-0
15
.57
E-0
29
3%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
5A
LP
404
g
(9.8
)
(5.3
)1
.00
E+
00
1.0
9E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
13
Page 28 of 52 9/26/2016
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2
3
4
5
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7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
2 S
O 0
02(1
60-1
8570-8
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
2:4
8:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-8
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
4.0
9E
-01
1.7
E-0
15
.57
E-0
29
3%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
5A
LP
404
g
(7.4
)
(4.7
)1
.00
E+
00
1.0
9E
-02
6231061
Batc
h:
M84V
V1A
AW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.7
7E
-01
9.1
E-0
21
.92
E-0
11
00
%7
.7E
-02
CA
RB
ON
-14
PC
I_G
9/3
/16
12
:21
a5.0
LS
C4
g
-0.9
2
-(3
.9)
U
1.0
0E
+0
19
.32
E-0
2
6231062
Batc
h:
M84V
V1A
DW
ork
Ord
er:
9M
84V
V10
Rep
ort
DB
ID
:E
7X
W
-1.0
9E
-03
2.7
E-0
25
.36
E-0
29
1%
2.7
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
3 p
1.1
6A
LP
128
g
-0.0
2
-0.0
8
U
1.0
0E
+0
01
.14
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
14
Page 29 of 52 9/26/2016
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2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
4 S
O 0
02(1
60-1
8570-9
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
3:1
0:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-9
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
W1A
EW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:L4S
O
9.1
0E
-03
3.5
E-0
29
.32
E-0
28
0%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
8 p
1.0
7A
LP
426
g
0.1
0.5
1
U
1.0
0E
+0
02
.63
E-0
2
- 1.4
0E
-03
3.5
E-0
26
.91
E-0
28
0%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
8 p
1.0
7A
LP
426
g
-0.0
2
-0.0
8
U
1.0
0E
+0
01
.47
E-0
2
6231058
Batc
h:
M84V
W1A
GW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:C
0S
R
2.7
3E
-01
1.4
E-0
16
.36
E-0
27
8%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
9 p
1.0
1A
LP
218
g
(4.3
)
(3.8
)1
.00
E+
00
1.3
5E
-02
1.4
8E
-02
3.2
E-0
26
.36
E-0
27
8%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
9 p
1.0
1A
LP
218
g
0.2
3
0.9
2
U
1.0
0E
+0
01
.35
E-0
2
2.4
0E
-01
1.3
E-0
16
.36
E-0
27
8%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
9 p
1.0
1A
LP
218
g
(3.8
)
(3.6
)1
.00
E+
00
1.3
5E
-02
Rati
o U
-234/2
38
= 1
.1
6231059
Batc
h:
M84V
W1A
CW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:L4S
X
1.7
4E
-02
3.8
E-0
27
.49
E-0
27
1%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:34
p1.0
7A
LP
420
g
0.2
3
0.9
1
U
1.0
0E
+0
01
.59
E-0
2
6231060
Batc
h:
M84V
W1A
FW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:L4S
1
4.0
2E
-01
1.7
E-0
16
.23
E-0
29
8%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
7A
LP
405
g
(6.5
)
(4.7
)1
.00
E+
00
1.4
0E
-02
2.1
5E
-01
1.2
E-0
15
.27
E-0
29
8%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
7A
LP
405
g
(4.1
)
(3.6
)1
.00
E+
00
1.0
3E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
15
Page 30 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
4 S
O 0
02(1
60-1
8570-9
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
3:1
0:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-9
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
3.0
1E
-01
1.4
E-0
15
.27
E-0
29
8%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
7 a
1.0
7A
LP
405
g
(5.7
)
(4.2
)1
.00
E+
00
1.0
3E
-02
6231061
Batc
h:
M84V
W1A
AW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.0
4E
-01
8.9
E-0
21
.83
E-0
11
00
%7
.5E
-02
CA
RB
ON
-14
PC
I_G
9/3
/16
02
:25
a5.2
LS
C4
g
-0.5
7
-(2
.3)
U
1.0
0E
+0
18
.89
E-0
2
6231062
Batc
h:
M84V
W1A
DW
ork
Ord
er:
9M
84V
W10
Rep
ort
DB
ID
:E
7X
W
-3.4
5E
-03
2.5
E-0
25
.89
E-0
28
4%
2.5
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
5 p
1.2
2A
LP
129
g
-0.0
6
-0.2
8
U
1.0
0E
+0
01
.52
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
16
Page 31 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
5 S
O 0
02(1
60-1
8570-7
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
2:0
1:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-7
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
R1A
EW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:L4S
O
8.3
1E
-03
3.5
E-0
29
.39
E-0
28
5%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
6 p
1.0
AL
P4
23
g
0.0
9
0.4
7
U
1.0
0E
+0
02
.68
E-0
2
1.7
3E
-02
3.5
E-0
26
.36
E-0
28
5%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
6 p
1.0
AL
P4
23
g
0.2
7
1.
U
1.0
0E
+0
01
.24
E-0
2
6231058
Batc
h:
M84V
R1A
GW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:C
0S
R
6.5
2E
-01
2.1
E-0
16
.90
E-0
28
7%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.2
6A
LP
215
g
(9.5
)
(6.2
)1
.00
E+
00
2.0
8E
-02
1.9
8E
-02
3.4
E-0
25
.78
E-0
28
7%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.2
6A
LP
215
g
0.3
4
(1.2
)
U
1.0
0E
+0
01
.52
E-0
2
2.3
0E
-01
1.1
E-0
16
.40
E-0
28
7%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
8 p
1.2
6A
LP
215
g
(3.6
)
(4.1
)1
.00
E+
00
1.8
3E
-02
Rati
o U
-234/2
38
= 2
.8
6231059
Batc
h:
M84V
R1A
CW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:L4S
X
5.2
3E
-02
7.5
E-0
21
.18
E-0
16
9%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:32
p1.0
AL
P4
14
g
0.4
4
(1.4
)
U
1.0
0E
+0
03
.41
E-0
2
6231060
Batc
h:
M84V
R1A
FW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:L4S
1
6.4
1E
-01
2.3
E-0
16
.52
E-0
21
07
%T
HO
RIU
M-2
28
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.0
AL
P4
03
g
(9.8
)
(5.5
)1
.00
E+
00
1.4
7E
-02
3.7
6E
-01
1.6
E-0
15
.51
E-0
21
07
%T
HO
RIU
M-2
30
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.0
AL
P4
03
g
(6.8
)
(4.6
)1
.00
E+
00
1.0
8E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
17
Page 32 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
5 S
O 0
02(1
60-1
8570-7
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
2:0
1:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-7
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
3.7
5E
-01
1.6
E-0
15
.51
E-0
21
07
%T
HO
RIU
M-2
32
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.0
AL
P4
03
g
(6.8
)
(4.6
)1
.00
E+
00
1.0
8E
-02
6231061
Batc
h:
M84V
R1A
AW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.4
0E
-01
8.8
E-0
21
.80
E-0
11
00
%7
.4E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
10
:18
p5.2
LS
C4
g
-0.7
8
-(3
.2)
U
1.0
0E
+0
18
.74
E-0
2
6231062
Batc
h:
M84V
R1A
DW
ork
Ord
er:
9M
84V
R10
Rep
ort
DB
ID
:E
7X
W
-2.3
9E
-03
3.0
E-0
26
.48
E-0
29
1%
3.0
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
3 p
1.0
6A
LP
127
g
-0.0
4
-0.1
6
U
1.0
0E
+0
01
.53
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
18
Page 33 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
6 S
O 0
02(1
60-1
8570-6
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
1:0
5:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-6
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
Q1A
EW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:L4S
O
1.8
0E
-02
5.3
E-0
21
.30
E-0
14
5%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
5 p
1.1
7A
LP
421
g
0.1
4
0.6
7
U
1.0
0E
+0
03
.42
E-0
2
2.4
4E
-02
5.3
E-0
21
.05
E-0
14
5%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
5 p
1.1
7A
LP
421
g
0.2
3
0.9
1
U
1.0
0E
+0
02
.22
E-0
2
6231058
Batc
h:
M84V
Q1A
GW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:C
0S
R
1.1
2E
-01
6.8
E-0
23
.94
E-0
29
3%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
7 p
1.5
AL
P2
12
g
(2.9
)
(3.3
)1
.00
E+
00
8.8
8E
-03
1.8
9E
-02
2.7
E-0
23
.47
E-0
29
3%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
7 p
1.5
AL
P2
12
g
0.5
4
(1.4
)
U
1.0
0E
+0
06
.78
E-0
3
1.2
3E
-01
7.1
E-0
23
.47
E-0
29
3%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
7 p
1.5
AL
P2
12
g
(3.5
)
(3.4
)1
.00
E+
00
6.7
8E
-03
Rati
o U
-234/2
38
= 0
.9
6231059
Batc
h:
M84V
Q1A
CW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:L4S
X
-6.6
1E
-03
3.0
E-0
27
.85
E-0
28
7%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:32
p1.1
7A
LP
413
g
-0.0
8
-0.4
4
U
1.0
0E
+0
02
.18
E-0
2
6231060
Batc
h:
M84V
Q1A
FW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:L4S
1
5.2
8E
-02
6.1
E-0
27
.98
E-0
29
6%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.1
7A
LP
401
g
0.6
6
(1.7
)
U
1.0
0E
+0
02
.25
E-0
2
2.3
0E
-01
1.2
E-0
15
.27
E-0
29
6%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.1
7A
LP
401
g
(4.4
)
(3.7
)1
.00
E+
00
1.0
3E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
19
Page 34 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 3
6 S
O 0
02(1
60-1
8570-6
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
1:0
5:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-6
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
2.8
7E
-02
4.1
E-0
25
.27
E-0
29
6%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
6 a
1.1
7A
LP
401
g
0.5
4
(1.4
)
U
1.0
0E
+0
01
.03
E-0
2
6231061
Batc
h:
M84V
Q1A
AW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.5
8E
-01
8.9
E-0
21
.81
E-0
11
00
%7
.4E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
08
:14
p5.1
LS
C4
g
-0.8
7
-(3
.6)
U
1.0
0E
+0
18
.81
E-0
2
6231062
Batc
h:
M84V
Q1A
DW
ork
Ord
er:
9M
84V
Q10
Rep
ort
DB
ID
:E
7X
W
-4.9
9E
-04
2.5
E-0
24
.58
E-0
28
7%
2.5
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
2 p
1.4
5A
LP
119
g
-0.0
1
-0.0
4
U
1.0
0E
+0
08
.94
E-0
3
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
20
Page 35 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30(1
60-1
8570-1
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
9:2
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-1
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
K1A
EW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:L4S
O
4.5
9E
-02
5.7
E-0
27
.37
E-0
28
8%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
4:5
9 p
1.0
1A
LP
409
g
0.6
2
(1.6
)
U
1.0
0E
+0
01
.80
E-0
2
1.4
4E
-02
3.3
E-0
26
.81
E-0
28
8%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
4:5
9 p
1.0
1A
LP
409
g
0.2
1
0.8
8
U
1.0
0E
+0
01
.54
E-0
2
6231058
Batc
h:
M84V
K1A
GW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:C
0S
R
4.6
7E
-01
1.9
E-0
19
.00
E-0
27
8%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
4 p
1.0
7A
LP
3
g
(5.2
)
(5.)
1.0
0E
+0
02
.85
E-0
2
9.0
6E
-03
2.9
E-0
27
.10
E-0
27
8%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
4 p
1.0
7A
LP
3
g
0.1
3
0.6
3
U
1.0
0E
+0
01
.91
E-0
2
2.6
3E
-01
1.4
E-0
19
.95
E-0
27
8%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
4 p
1.0
7A
LP
3
g
(2.6
)
(3.9
)1
.00
E+
00
3.3
2E
-02
Rati
o U
-234/2
38
= 1
.8
6231059
Batc
h:
M84V
K1A
CW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:L4S
X
0.0
0E
+0
05
.2E
-02
9.5
7E
-02
56
%A
ME
RIC
IUM
-241
PC
I_G
9/1
/16
02
:24
p1.0
1A
LP
439
g
0.
0.
U
1.0
0E
+0
01
.87
E-0
2
6231060
Batc
h:
M84V
K1A
FW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:L4S
1
7.7
1E
-01
2.6
E-0
15
.98
E-0
29
8%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
127
g
(12
.9)
(6.)
1.0
0E
+0
01
.27
E-0
2
5.3
5E
-01
2.0
E-0
16
.04
E-0
29
8%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
127
g
(8.9
)
(5.3
)1
.00
E+
00
1.3
6E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
21
Page 36 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30(1
60-1
8570-1
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
9:2
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-1
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
5.0
8E
-01
1.9
E-0
15
.33
E-0
29
8%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
127
g
(9.5
)
(5.2
)1
.00
E+
00
1.0
4E
-02
6231061
Batc
h:
M84V
K1A
AW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:R
L-L
SC
-008
-7.1
7E
-02
9.3
E-0
21
.91
E-0
11
00
%7
.9E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
07
:52
a5.0
LS
C4
g
-0.3
8
-(1
.5)
U
1.0
0E
+0
19
.26
E-0
2
6231062
Batc
h:
M84V
K1A
DW
ork
Ord
er:
9M
84V
K10
Rep
ort
DB
ID
:E
7X
W
-1.7
8E
-03
3.0
E-0
26
.19
E-0
28
1%
3.0
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 1
2:5
8 p
1.0
4A
LP
111
g
-0.0
3
-0.1
2
U
1.0
0E
+0
01
.39
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
22
Page 37 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30D
(160-1
8570-2
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
9:2
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-2
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
L1A
EW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:L4S
O
2.3
4E
-02
5.1
E-0
21
.02
E-0
17
9%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
2 p
1.0
1A
LP
411
g
0.2
3
0.9
2
U
1.0
0E
+0
03
.05
E-0
2
- 2.8
4E
-03
3.6
E-0
27
.71
E-0
27
9%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
2 p
1.0
1A
LP
411
g
-0.0
4
-0.1
6
U
1.0
0E
+0
01
.82
E-0
2
6231058
Batc
h:
M84V
L1A
GW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:C
0S
R
5.2
8E
-01
1.8
E-0
16
.40
E-0
29
2%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
1A
LP
6
g
(8.2
)
(5.8
)1
.00
E+
00
1.8
5E
-02
3.3
9E
-02
4.1
E-0
24
.59
E-0
29
2%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
1A
LP
6
g
0.7
4
(1.7
)
U
1.0
0E
+0
09
.76
E-0
3
3.0
3E
-01
1.3
E-0
17
.23
E-0
29
2%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
1A
LP
6
g
(4.2
)
(4.6
)1
.00
E+
00
2.2
6E
-02
Rati
o U
-234/2
38
= 1
.7
6231059
Batc
h:
M84V
L1A
CW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:L4S
X
1.5
8E
-02
3.3
E-0
26
.04
E-0
28
3%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:27
p1.0
1A
LP
444
g
0.2
6
0.9
6
U
1.0
0E
+0
01
.18
E-0
2
6231060
Batc
h:
M84V
L1A
FW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:L4S
1
5.8
9E
-01
2.1
E-0
16
.05
E-0
29
7%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
129
g
(9.7
)
(5.6
)1
.00
E+
00
1.4
8E
-02
5.2
6E
-01
1.9
E-0
15
.80
E-0
29
7%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
129
g
(9.1
)
(5.4
)1
.00
E+
00
1.4
2E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
23
Page 38 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30D
(160-1
8570-2
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
9:2
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-2
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
4.3
7E
-01
1.7
E-0
15
.09
E-0
29
7%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
1A
LP
129
g
(8.6
)
(5.1
)1
.00
E+
00
1.0
8E
-02
6231061
Batc
h:
M84V
L1A
AW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:R
L-L
SC
-008
-9.9
9E
-03
9.5
E-0
21
.91
E-0
11
00
%8
.0E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
11
:59
a5.0
LS
C4
g
-0.0
5
-0.2
1
U
1.0
0E
+0
19
.28
E-0
2
6231062
Batc
h:
M84V
L1A
DW
ork
Ord
er:
9M
84V
L10
Rep
ort
DB
ID
:E
7X
W
-1.1
8E
-03
3.0
E-0
25
.84
E-0
28
5%
3.0
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
1 p
0.9
8A
LP
114
g
-0.0
2
-0.0
8
U
1.0
0E
+0
01
.24
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
24
Page 39 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
3 S
O 0
30(1
60-1
8570-3
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
10:5
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-3
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
M1A
EW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:L4S
O
9.8
2E
-03
3.5
E-0
29
.16
E-0
27
6%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
3 p
1.0
8A
LP
412
g
0.1
1
0.5
5
U
1.0
0E
+0
02
.55
E-0
2
5.1
2E
-02
6.2
E-0
26
.92
E-0
27
6%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
3 p
1.0
8A
LP
412
g
0.7
4
(1.7
)
U
1.0
0E
+0
01
.47
E-0
2
6231058
Batc
h:
M84V
M1A
GW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:C
0S
R
6.5
1E
-01
2.1
E-0
19
.20
E-0
21
00
%U
RA
NIU
M-2
33/2
34
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
3A
LP
11
g
(7.1
)
(6.3
)1
.00
E+
00
3.2
6E
-02
7.7
9E
-03
2.3
E-0
25
.62
E-0
21
00
%U
RA
NIU
M-2
35/2
36
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
3A
LP
11
g
0.1
4
0.6
7
U
1.0
0E
+0
01
.48
E-0
2
3.1
1E
-01
1.3
E-0
18
.72
E-0
21
00
%U
RA
NIU
M-2
38
PC
I_G
9/1
9/1
6 0
6:1
5 p
1.0
3A
LP
11
g
(3.6
)
(4.6
)1
.00
E+
00
3.0
2E
-02
Rati
o U
-234/2
38
= 2
.1
6231059
Batc
h:
M84V
M1A
CW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:L4S
X
1.6
9E
-02
3.5
E-0
26
.45
E-0
27
4%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:28
p1.0
8A
LP
445
g
0.2
6
0.9
6
U
1.0
0E
+0
01
.26
E-0
2
6231060
Batc
h:
M84V
M1A
FW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:L4S
1
5.0
3E
-01
2.1
E-0
16
.37
E-0
21
02
%T
HO
RIU
M-2
28
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
8A
LP
130
g
(7.9
)
(4.9
)1
.00
E+
00
1.2
4E
-02
3.6
6E
-01
1.7
E-0
16
.10
E-0
21
02
%T
HO
RIU
M-2
30
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
8A
LP
130
g
(6.)
(4.4
)1
.00
E+
00
1.1
9E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
25
Page 40 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
3 S
O 0
30(1
60-1
8570-3
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
10:5
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-3
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6.8
1E
-01
2.4
E-0
16
.10
E-0
21
02
%T
HO
RIU
M-2
32
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
8A
LP
130
g
(11
.2)
(5.6
)1
.00
E+
00
1.1
9E
-02
6231061
Batc
h:
M84V
M1A
AW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.9
0E
-02
9.5
E-0
21
.91
E-0
11
00
%8
.0E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
02
:03
p5.0
LS
C4
g
-0.1
-0.4
U
1.0
0E
+0
19
.27
E-0
2
6231062
Batc
h:
M84V
M1A
DW
ork
Ord
er:
9M
84V
M10
Rep
ort
DB
ID
:E
7X
W
-2.5
9E
-03
2.6
E-0
25
.82
E-0
28
9%
2.6
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
1 p
1.0
7A
LP
115
g
-0.0
4
-0.2
U
1.0
0E
+0
01
.42
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
26
Page 41 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
3 S
O 0
30D
(160-1
8570-4
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
10:5
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-4
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
N1A
EW
ork
Ord
er:
9M
84V
N10
Rep
ort
DB
ID
:L4S
O
-1.4
4E
-02
5.2
E-0
21
.42
E-0
14
2%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
4 p
1.3
7A
LP
419
g
-0.1
-0.5
5
U
1.0
0E
+0
04
.10
E-0
2
2.3
7E
-02
5.2
E-0
21
.02
E-0
14
2%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
4 p
1.3
7A
LP
419
g
0.2
3
0.9
1
U
1.0
0E
+0
02
.16
E-0
2
6231058
Batc
h:
M84V
N2A
GW
ork
Ord
er:
9M
84V
N20
Rep
ort
DB
ID
:C
0S
R
6.7
9E
-01
2.2
E-0
15
.58
E-0
28
6%
UR
AN
IUM
-233/2
34
PC
I_G
9/2
1/1
6 1
0:4
5 a
1.1
7A
LP
211
g
(12
.2)
(6.1
)1
.00
E+
00
1.3
2E
-02
3.6
5E
-02
4.5
E-0
25
.58
E-0
28
6%
UR
AN
IUM
-235/2
36
PC
I_G
9/2
1/1
6 1
0:4
5 a
1.1
7A
LP
211
g
0.6
5
(1.6
)
U
1.0
0E
+0
01
.32
E-0
2
5.4
8E
-01
1.9
E-0
16
.44
E-0
28
6%
UR
AN
IUM
-238
PC
I_G
9/2
1/1
6 1
0:4
5 a
1.1
7A
LP
211
g
(8.5
)
(5.6
)1
.00
E+
00
1.7
3E
-02
Rati
o U
-234/2
38
= 1
.2
6231059
Batc
h:
M84V
N1A
CW
ork
Ord
er:
9M
84V
N10
Rep
ort
DB
ID
:L4S
X
5.8
2E
-02
6.0
E-0
25
.40
E-0
27
0%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:30
p1.3
7A
LP
446
g
(1.1
)
(1.9
)1
.00
E+
00
1.0
5E
-02
6231060
Batc
h:
M84V
N1A
FW
ork
Ord
er:
9M
84V
N10
Rep
ort
DB
ID
:L4S
1
5.3
1E
-01
2.0
E-0
15
.42
E-0
27
2%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.3
7A
LP
131
g
(9.8
)
(5.3
)1
.00
E+
00
1.0
6E
-02
5.2
3E
-01
2.0
E-0
15
.19
E-0
27
2%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.3
7A
LP
131
g
(10
.1)
(5.3
)1
.00
E+
00
1.0
1E
-02
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
27
Page 42 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
3 S
O 0
30D
(160-1
8570-4
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
10:5
0:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-4
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
5.0
9E
-01
1.9
E-0
15
.19
E-0
27
2%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.3
7A
LP
131
g
(9.8
)
(5.3
)1
.00
E+
00
1.0
1E
-02
6231061
Batc
h:
M84V
N1A
AW
ork
Ord
er:
9M
84V
N10
Rep
ort
DB
ID
:R
L-L
SC
-008
-8.9
5E
-02
9.3
E-0
21
.91
E-0
11
00
%7
.9E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
04
:06
p5.0
LS
C4
g
-0.4
7
-(1
.9)
U
1.0
0E
+0
19
.29
E-0
2
6231062
Batc
h:
M84V
N1A
DW
ork
Ord
er:
9M
84V
N10
Rep
ort
DB
ID
:E
7X
W
-2.0
0E
-03
2.5
E-0
25
.43
E-0
28
6%
2.5
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
1 p
1.1
3A
LP
116
g
-0.0
4
-0.1
6
U
1.0
0E
+0
01
.28
E-0
2
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
28
Page 43 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
9 S
O 0
05(1
60-1
8570-5
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
1:0
0:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-5
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
6231057
Batc
h:
M84V
P1A
EW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:L4S
O
1.4
2E
-02
3.1
E-0
26
.08
E-0
28
9%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
5 p
1.0
5A
LP
420
g
0.2
3
0.9
2
U
1.0
0E
+0
01
.29
E-0
2
- 1.2
3E
-03
3.1
E-0
26
.08
E-0
28
9%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
5 p
1.0
5A
LP
420
g
-0.0
2
-0.0
8
U
1.0
0E
+0
01
.29
E-0
2
6231058
Batc
h:
M84V
P1A
GW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:C
0S
R
3.9
9E
-01
1.6
E-0
15
.27
E-0
29
6%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
6 p
1.1
1A
LP
211
g
(7.6
)
(5.1
)1
.00
E+
00
1.2
4E
-02
1.1
2E
-02
2.4
E-0
24
.79
E-0
29
6%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
6 p
1.1
1A
LP
211
g
0.2
3
0.9
2
U
1.0
0E
+0
01
.02
E-0
2
3.4
8E
-01
1.4
E-0
15
.95
E-0
29
6%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
6 p
1.1
1A
LP
211
g
(5.9
)
(4.8
)1
.00
E+
00
1.5
7E
-02
Rati
o U
-234/2
38
= 1
.1
6231059
Batc
h:
M84V
P1A
CW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:L4S
X
1.7
5E
-02
4.0
E-0
28
.26
E-0
27
0%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:31
p1.0
5A
LP
447
g
0.2
1
0.8
7
U
1.0
0E
+0
01
.86
E-0
2
6231060
Batc
h:
M84V
P1A
FW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:L4S
1
3.8
7E
-01
1.6
E-0
15
.26
E-0
29
5%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.0
5A
LP
132
g
(7.4
)
(4.7
)1
.00
E+
00
1.0
3E
-02
3.3
0E
-01
1.5
E-0
15
.04
E-0
29
5%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.0
5A
LP
132
g
(6.5
)
(4.5
)1
.00
E+
00
9.8
5E
-03
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
29
Page 44 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
9 S
O 0
05(1
60-1
8570-5
)
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
01
6 1
0:0
0:0
0 A
M
Lab
Nam
e:
Clien
t S
am
ple
ID
:
Para
mete
rR
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
CR
DL
(RL
)
MD
L,
Acti
on
Lev
Rp
t U
nit
,
Lc
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Aliq
uo
t
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016
1:0
0:0
0 P
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
Tes
tAm
eri
ca In
c
J6H
180408-5
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
Ord
ere
d b
y C
lien
t S
am
ple
ID
, B
atc
h N
o.
SA
MP
LE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
SO
3.3
0E
-01
1.5
E-0
15
.04
E-0
29
5%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
5 a
1.0
5A
LP
132
g
(6.5
)
(4.5
)1
.00
E+
00
9.8
5E
-03
6231061
Batc
h:
M84V
P1A
AW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:R
L-L
SC
-008
-1.2
3E
-01
8.8
E-0
21
.81
E-0
11
00
%7
.4E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
06
:10
p5.2
LS
C4
g
-0.6
8
-(2
.8)
U
1.0
0E
+0
18
.78
E-0
2
6231062
Batc
h:
M84V
P1A
DW
ork
Ord
er:
9M
84V
P10
Rep
ort
DB
ID
:E
7X
W
0.0
0E
+0
02
.6E
-02
4.7
3E
-02
85
%0
.0E
+00
NE
PT
UN
IUM
-237
PC
I_G
9/1
5/1
6 0
1:0
2 p
1.1
2A
LP
117
g
0.
0.
U
1.0
0E
+0
09
.23
E-0
3
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ual
- A
naly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
cri
teri
a,
Md
c/M
da/M
dl,
To
tal
Un
cert
, R
DL
or
no
t id
en
tifi
ed
by g
am
ma s
can
so
ftw
are
.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Level
based
on
in
str
um
en
t b
ackg
rou
nd
or
bla
nk,
ad
juste
d b
y t
he s
am
ple
Eff
icie
ncy, Y
ield
, an
d V
olu
me.
rptS
TL
Rch
Sam
ple
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
30
Page 45 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
DU
PL
ICA
TE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
I
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30(1
60-1
8570-1
) D
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
016 1
0:0
0:0
0 A
M
Lab
Na
me:
Clien
t S
am
ple
ID
:
Para
me
ter
Res
ult
,
Ori
g R
st
Co
un
t
Err
or
( s
)
CS
U
(
s)
Yie
ld
MD
L,
Acti
on
Lev
Rp
t U
nit
,
CR
DL
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Ali
qu
ot
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016 9
:20:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
TestA
me
rica In
c
J6
H180408-1
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
SO
6231057
Batc
h:
M84V
K1A
HW
ork
Ord
er:
M84V
K1H
RR
ep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:L4S
O
-1.8
9E
-03
3.2
E-0
26
.57
E-0
28
9%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
1 p
1.0
5A
LP
41
0
g
-0.0
3
-0.1
2
U
1.0
0E
+0
04
.59
E-0
21
.5R
ER
2U
-1.2
6E
-03
3.2
E-0
26
.23
E-0
28
9%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
1 p
1.0
5A
LP
41
0
g
-0.0
2
-0.0
8
U
1.0
0E
+0
01
.44
E-0
20
.7R
ER
2U
6231058
Batc
h:
M84V
K1A
JW
ork
Ord
er:
M84V
K1JR
Rep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:C
0S
R
5.8
2E
-01
2.0
E-0
18
.23
E-0
29
8%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 0
6:1
4 p
0.9
7A
LP
4
g
(7.1
)
(5.8
)1
.00
E+
00
4.6
7E
-01
0.8
RE
R2
9.8
3E
-03
2.6
E-0
26
.01
E-0
29
8%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 0
6:1
4 p
0.9
7A
LP
4
g
0.1
6
0.7
5
U
1.0
0E
+0
09
.06
E-0
30
.0R
ER
2U
1.8
7E
-01
1.1
E-0
19
.24
E-0
29
8%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 0
6:1
4 p
0.9
7A
LP
4
g
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)1
.00
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00
2.6
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0.9
RE
R2
Rati
o U
-234/2
38 =
3.1
Alp
ha
Sp
ec R
esu
lt S
um
= 7
.8E
-01
6231059
Batc
h:
M84V
K1A
KW
ork
Ord
er:
M84V
K1K
RR
ep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:L4S
X
-1.1
4E
-03
5.7
E-0
21
.04
E-0
14
9%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:25
p1
.05
AL
P4
43
g
-0.0
1
-0.0
4
U
1.0
0E
+0
00
.00
E+
00
0.0
RE
R2
U
Alp
ha
Sp
ec R
esu
lt S
um
= 7
.8E
-01
6231060
Batc
h:
M84V
K1A
LW
ork
Ord
er:
M84V
K1LR
Rep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:L4S
1
6.4
2E
-01
2.2
E-0
15
.24
E-0
21
01
%T
HO
RIU
M-2
28
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
5A
LP
12
8
g
(12
.3)
(5.8
)1
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00
7.7
1E
-01
0.8
RE
R2
TestA
meri
ca I
nc
U Q
ua
l -
An
aly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
crit
eria
, M
dc/
Md
a/M
dl,
To
tal
Un
cert,
RD
L o
r n
ot
iden
tifi
ed
by
ga
mm
a s
ca
n s
oft
wa
re.
RE
R2
-
Rep
licate
Erro
r R
ati
o =
(S
-D)/
[sq
rt(
sq(T
PU
s)+
sq(T
PU
d))
] a
s d
efi
ned
by
IC
PT
BO
A.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Lev
el
ba
sed
on
in
stru
men
t b
ack
gro
un
d o
r b
lan
k,
ad
just
ed
by
th
e s
am
ple
Eff
icie
ncy
, Y
ield
, a
nd
Vo
lum
e.
rptS
TL
Rch
Du
pV
5.
6 A
2002
TestA
merica L
abora
tories,
Inc.
31
Page 46 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
DU
PL
ICA
TE
RE
SU
LT
S
23
-Sep-1
6D
ate
:F
OR
M I
I
Lo
t-S
am
ple
No
.:
SD
G:
YM
TF
A 4
2 S
O 0
30(1
60-1
8570-1
) D
51961
Matr
ix:
SO
LID
Receiv
ed
Date
:8/1
8/2
016 1
0:0
0:0
0 A
M
Lab
Na
me:
Clien
t S
am
ple
ID
:
Para
me
ter
Res
ult
,
Ori
g R
st
Co
un
t
Err
or
( s
)
CS
U
(
s)
Yie
ld
MD
L,
Acti
on
Lev
Rp
t U
nit
,
CR
DL
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Ali
qu
ot
Siz
e
Pri
mary
Dete
cto
r
Co
llecti
on
Date
:8/9
/2016 9
:20:0
0 A
M
69364
Rst/
MD
L,
Rst/
To
tUcert
22
TestA
me
rica In
c
J6
H180408-1
To
tal
Sa
Siz
eQ
ua
l
CO
C N
o. :
SO
4.1
0E
-01
1.7
E-0
15
.02
E-0
21
01
%T
HO
RIU
M-2
30
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
5A
LP
12
8
g
(8.2
)
(5.)
1.0
0E
+0
05
.35
E-0
11
.0R
ER
2
5.2
0E
-01
1.9
E-0
15
.02
E-0
21
01
%T
HO
RIU
M-2
32
PC
I_G
9/2
1/1
6 1
1:0
4 a
1.0
5A
LP
12
8
g
(10
.3)
(5.5
)1
.00
E+
00
5.0
8E
-01
0.1
RE
R2
Alp
ha
Sp
ec R
esu
lt S
um
= 9
.3E
-01
6231061
Batc
h:
M84V
K1A
MW
ork
Ord
er:
M84V
K1M
RR
ep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:R
L-L
SC
-008
-3.8
7E
-02
9.2
E-0
21
.85
E-0
11
00
%7
.8E
-02
CA
RB
ON
-14
PC
I_G
9/2
/16
09
:55
a5.1
LS
C4
g
-0.2
1
-0.8
4
U
1.0
0E
+0
1-7
.17
E-0
20
.5R
ER
2U
Alp
ha
Sp
ec R
esu
lt S
um
= 9
.3E
-01
6231062
Batc
h:
M84V
K1A
NW
ork
Ord
er:
M84V
K1N
RR
ep
ort
DB
ID
:9M
84V
K10
Ori
g S
a D
B ID
:E
7X
W
1.6
3E
-02
3.3
E-0
25
.98
E-0
28
4%
3.3
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
1:0
0 p
1.1
6A
LP
11
2
g
0.2
7
0.9
9
U
1.0
0E
+0
0-1
.78
E-0
30
.8R
ER
2U
Alp
ha
Sp
ec R
esu
lt S
um
= 9
.5E
-01
11
No
. o
f R
esu
lts:
Co
mm
en
ts:
TestA
meri
ca I
nc
U Q
ua
l -
An
aly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
crit
eria
, M
dc/
Md
a/M
dl,
To
tal
Un
cert,
RD
L o
r n
ot
iden
tifi
ed
by
ga
mm
a s
ca
n s
oft
wa
re.
RE
R2
-
Rep
licate
Erro
r R
ati
o =
(S
-D)/
[sq
rt(
sq(T
PU
s)+
sq(T
PU
d))
] a
s d
efi
ned
by
IC
PT
BO
A.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ecis
ion
Lev
el
ba
sed
on
in
stru
men
t b
ack
gro
un
d o
r b
lan
k,
ad
just
ed
by
th
e s
am
ple
Eff
icie
ncy
, Y
ield
, a
nd
Vo
lum
e.
rptS
TL
Rch
Du
pV
5.
6 A
2002
TestA
merica L
abora
tories,
Inc.
32
Page 47 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
BL
AN
K R
ES
UL
TS
23
-Sep-1
6D
ate
:F
OR
M I
I
SD
G:
51961
Matr
ix:
SO
LID
La
b N
am
e:
Para
mete
r R
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
MD
L,
Lc
Rp
t U
nit
,
CR
DL
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Ali
qu
ot
Siz
e
Pri
mary
Dete
cto
r
69364
Rst/
MD
L,
Rst/
To
tUcert
22
TestA
meri
ca In
c
To
tal
Sa
Siz
eQ
ua
l
62
31
06
1B
atc
h:
M842F
1A
AW
ork
Ord
er:
M842F
1A
BR
ep
ort
DB
ID
:R
L-L
SC
-008
-3.3
8E
-02
9.5
E-0
21
.91
E-0
11
00%
8.0
E-0
2C
AR
BO
N-1
4P
CI_
G9
/3/1
6 0
4:2
9 a
5.0
LS
C4
g
-0.1
8
-0.7
2
U
9.2
9E
-02
1.0
0E
+0
1
62
31
05
8B
atc
h:
M842C
1A
AW
ork
Ord
er:
M842C
1A
BR
ep
ort
DB
ID
:C
0S
R
5.1
4E
-03
1.9
E-0
24
.79
E-0
29
5%
UR
AN
IUM
-233/2
34
PC
I_G
9/1
9/1
6 1
0:1
7 p
1.5
8A
LP
42
5
g
0.1
1
0.5
5
U
1.3
3E
-02
1.0
0E
+0
0
-1.1
0E
-03
1.8
E-0
23
.82
E-0
29
5%
UR
AN
IUM
-235/2
36
PC
I_G
9/1
9/1
6 1
0:1
7 p
1.5
8A
LP
42
5
g
-0.0
3
-0.1
2
U
8.6
0E
-03
1.0
0E
+0
0
-1.8
3E
-03
1.8
E-0
24
.13
E-0
29
5%
UR
AN
IUM
-238
PC
I_G
9/1
9/1
6 1
0:1
7 p
1.5
8A
LP
42
5
g
-0.0
4
-0.2
U
1.0
1E
-02
1.0
0E
+0
0
Ra
tio
U-2
34
/23
8 =
-2
.8
62
31
06
2B
atc
h:
M842G
1A
AW
ork
Ord
er:
M842G
1A
BR
ep
ort
DB
ID
:E
7X
W
-1.4
3E
-03
2.4
E-0
24
.95
E-0
27
8%
2.4
E-0
2N
EP
TU
NIU
M-2
37
PC
I_G
9/1
5/1
6 0
3:1
0 p
1.3
4A
LP
11
1
g
-0.0
3
-0.1
2
U
1.1
2E
-02
1.0
0E
+0
0
62
31
06
0B
atc
h:
M842E
1A
AW
ork
Ord
er:
M842E
1A
BR
ep
ort
DB
ID
:L4S
1
9.8
2E
-03
2.5
E-0
25
.53
E-0
29
7%
TH
OR
IUM
-228
PC
I_G
9/2
1/1
6 1
1:0
8 a
1.3
4A
LP
40
6
g
0.1
8
0.7
9
U
1.3
5E
-02
1.0
0E
+0
0
1.1
8E
-02
2.4
E-0
24
.32
E-0
29
7%
TH
OR
IUM
-230
PC
I_G
9/2
1/1
6 1
1:0
8 a
1.3
4A
LP
40
6
g
0.2
7
0.9
9
U
8.4
3E
-03
1.0
0E
+0
0
-4.7
1E
-04
2.4
E-0
24
.32
E-0
29
7%
TH
OR
IUM
-232
PC
I_G
9/2
1/1
6 1
1:0
8 a
1.3
4A
LP
40
6
g
-0.0
1
-0.0
4
U
8.4
3E
-03
1.0
0E
+0
0
62
31
05
7B
atc
h:
M842A
1A
AW
ork
Ord
er:
M842A
1A
BR
ep
ort
DB
ID
:L4S
O
TestA
meri
ca I
nc
U Q
ua
l -
An
aly
zed
fo
r b
ut
no
t d
ete
cte
d a
bo
ve l
imit
ing
crit
eria
, M
dc/
Md
a/M
dl,
To
tal
Un
cert,
RD
L o
r n
ot
iden
tifi
ed
by
ga
mm
a s
ca
n s
oft
wa
re.
MD
C|M
DA
,Lc -
Dete
cti
on
, D
ec
isio
n L
ev
el
ba
se
d o
n i
nstr
um
en
t b
ac
kg
rou
nd
or
bla
nk
, a
dju
ste
d b
y t
he
sam
ple
Eff
icie
nc
y,
Yie
ld,
an
d V
olu
me.
rptS
TL
Rch
Bla
nk
V5.6
A2002
TestA
merica L
abora
tories,
Inc.
33
Page 48 of 52 9/26/2016
1
2
3
4
5
6
7
8
9
10
11
12
13
BL
AN
K R
ES
UL
TS
23
-Sep-1
6D
ate
:F
OR
M I
I
SD
G:
51961
Matr
ix:
SO
LID
La
b N
am
e:
Para
mete
r R
esu
lt
Co
un
t
Err
or
(
s)
CS
U
(
s)
Yie
ld
MD
L,
Lc
Rp
t U
nit
,
CR
DL
Rep
ort
No
. :
An
aly
sis
,
Pre
p D
ate
Ali
qu
ot
Siz
e
Pri
mary
Dete
cto
r
69364
Rst/
MD
L,
Rst/
To
tUcert
22
TestA
meri
ca In
c
To
tal
Sa
Siz
eQ
ua
l
1.6
2E
-02
3.3
E-0
26
.46
E-0
29
3%
PLU
TO
NIU
M-2
38
PC
I_G
8/3
0/1
6 0
5:0
9 p
1.3
4A
LP
42
9
g
0.2
5
0.9
8
U
1.8
9E
-02
1.0
0E
+0
0
1.0
6E
-02
2.3
E-0
24
.56
E-0
29
3%
PLU
TO
NIU
M-2
39/2
40
PC
I_G
8/3
0/1
6 0
5:0
9 p
1.3
4A
LP
42
9
g
0.2
3
0.9
2
U
9.6
8E
-03
1.0
0E
+0
0
62
31
05
9B
atc
h:
M842D
1A
AW
ork
Ord
er:
M842D
1A
BR
ep
ort
DB
ID
:L4S
X
2.6
1E
-02
5.0
E-0
29
.56
E-0
26
2%
AM
ER
ICIU
M-2
41
PC
I_G
9/1
/16
02
:35
p1.3
4A
LP
42
3
g
0.2
7
(1.)
U
2.7
3E
-02
1.0
0E
+0
0
11
No
. o
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34
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Rec L
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AN
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34
PC
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9/1
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Rec L
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TestA
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Inc.
35
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TestAmerica Laboratories, Inc. 36Page 51 of 52 9/26/2016
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TestAmerica Laboratories, Inc. 37Page 52 of 52 9/26/2016
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