Analysis of Mir Archival Water Samples - NASA · DISCUSSION Status of Data Analysis Chemical...
Transcript of Analysis of Mir Archival Water Samples - NASA · DISCUSSION Status of Data Analysis Chemical...
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Analysis of Mir Archival Water SamplesU.S. Principal Investigator: RICHARD L. SAUER, P.E., NASA/Johnson Space Center
Russian Principal Investigator: YURI SINYAK, M.D., Institute of Biomedical Problems
Co-Investigator: John Schultz, Ph.D.
Co-Author: Lizanna M. Pierre
(NASA 7 Final Research Report)
INTRODUCTION
A portion of the potable water supplied to the Russiancosmonauts, American astronauts, and other occupants ofthe Russian Mir Space Station is produced by the directrecycle of water from humidity condensate. Additionalsupplies come from ground supplied (stored) potable waterthat is delivered on a Progress resupply spacecraft, orprocessed fuel cell water transferred from the Shuttle. Thisproject was conducted to determine the potability of thewater supplied on Mir, to assess the reliability of thewater reclamation and distribution systems and to aid indeveloping water quality monitoring procedures andstandards for International Space Station.
Hypothesis
Detailed analysis of recycled and other Mir suppliedpotable waters will confirm that the design of the Mirpurification and distribution systems are adequate tomaintain water of potable quality.
Objectives
1. Characterize the chemical composition of Mirrecycled water to evaluate the efficiency of on-board waterprocessors and to aid in the development of ISS watersampling and monitoring technology.
2. Characterize the chemical composition of Mirhumidity condensate to support development and testingof the water recycling and monitoring systems for theInternational Space Station (ISS).
3. Characterize the chemical composition of the ground-resupply water prior to launch and on orbit.
4. Determine the chemical composition of Mir andShuttle humidity condensate.
5. Provide inflight testing of water collection hardwarebeing developed to collect water samples on ISS.
Background/History
Historically, water provided for crew consumption duringU.S. space missions has either been launched from the
ground or produced as a byproduct of fuel cell operation.Reclamation and purification of spacecraft wastewaters, aspracticed on the Russian Space Station Mir, will berequired for supplying crewmembers of the InternationalSpace Station with potable and hygiene water.
This experiment has flown under the Human Life SciencesDiscipline during the Mir 18/NASA 1, Mir 19, Mir20/STS-74, Mir 21/NASA 2/STS-79, and Mir 22/NASA3/STS-81 missions. In addition, this activity wasperformed under the Space Medicine Program during theMir 23/NASA 4/STS-84, Mir 24/NASA 5/STS-86, Mir25/NASA 6/STS-89, and Mir 25/NASA 7/STS-91missions.
METHODS/RESEARCH OPERATIONS
Method/Protocol
During Mir 18, Mir 19, and Mir 20 samples werecollected using a water sampling kit. This kit containedpotable water samplers (adapters), disinfectant wipes,waste bags, and sample bags needed for sample collection.During an inflight water sampling session, the kit wasunstowed from its storage location. A prepackageddisinfectant wipe containing benzalkonium chloride wasretrieved from the kit and used to disinfect the Mir galley-hot, galley-cold, and SVO-ZV water ports. Afterdisinfection, a potable water sampler was connected to theport. A waste bag was then connected to the potable watersampler. Using the waste bag, 200 ml of water wascollected and discarded. The chemical sample bag was thenattached and 1000 ml of water were collected. The samplebag was placed in a self sealing storage bag and stowed atambient temperature for return on the Shuttle or Soyuz.These procedures, as outlined in Figure 1, were used tocollect galley-hot, galley-cold, and SVO-ZV (stored) waterfor postflight chemical analysis. Figure 1 outlines thesample collection procedures for Mir 18 to Mir 21. Inaddition, humidity condensate samples were also collected.
For Mir 21 and subsequent missions, a water experimentkit was used for sample collection. Along with existinghardware, this kit contained new waste and sample bagsthat were developed to resolve problems with and to reducesample volumes from 1000 ml to 700 ml and waste
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volumes from 200 ml to 50 ml. These new sample bagswere commercially available Teflon bags that weremodified for microgravity. Figure 2 shows the hardwareused for Mir 21 through Mir 25.
Postflight chemical analysis of samples occurred atJohnson Space Center (JSC), the Institute for BiomedicalProblems (IBMP) and Research and Design Institute ofChemical Engineering (NIICHIMMASH). Followingrecovery of the samples on the ground, the samples wereallocated for distribution to the water analysis laboratoriesat JSC, NIICHIMMASH, and IBMP. Parameters tested atJSC included total carbon (total inorganic carbon,purgeable organic carbon, nonpurgeable organic carbonand total organic carbon), specific organics (alcohols,organic acids, semivolatiles, volatiles, nonvolatiles,formaldehyde), and silver. Parameters tested by IBMPincluded conductivity, pH, color, chemical oxygendemand, calcium, magnesium, total hardness, and silver.The NIICHIMMASH laboratory performed total carbon,alcohol and organic acids analyses.
Functional Objectives
FO1. Preflight collection of ground-supplied water atRSC Energia, Korolev, Russia.
FO2. Water Sampling Hardware Setup.
FO3. Inflight collection of hot, cold, and SVO-ZV(stored) water.
FO4. Inflight collection of humidity condensate.
FO5. Postflight analysis of samples.
Hardware Items
Major hardware items used in flight for this experiment:
HW1. Atmospheric Condensate Sampler - RSAprovided
HW2. Water Sampling Kit - NASA provided
HW3. Water Experiment Kit – NASA provided
Both kits contained the following items:
HW4. Disinfectant/Antiseptic Wipes - NASA provided
HW5. Potable Water Samplers (with Mir port adapterinterfaces) - NASA provided
HW6. Waste bags and Chemical Sample, PostflightAnalysis Bags - NASA provided
HW7. Self Sealing Storage Bags - NASA provided
Major hardware items used postflight for this experiment:
HW8. HP 5890 Gas Chromatograph (GC) withHP5971A Mass Spectrometer (MS)- NASA provided
HW9. Waters Quanta 4000 Capillary ElectrophoresisSystem - NASA provided
HW10. OI 700 Carbon Analyzer - NASA provided
HW11. Sievers Model 800 Total Organic CarbonAnalyzer - NASA and RSA provided
HW12. HP 7694 Headspace sampler with a HP 5890 GCand 5972 Mass Selective Detector - NASA provided
HW13. HP 5989 Mass Spectrometer (MS) with a 1090Liquid Chromatograph with Particle beam & Thermosprayinterfaces - NASA provided
HW14. pH meter - RSA and NASA provided
HW15. Conductivity meter - RSA provided
HW16. Inductively Coupled Plasma/Mass Spectrometer– NASA provided
RESULTS
List of Pre-, In-, Postflight Anomalies
Preflight Anomalies
Not applicable to this experiment
Inflight Anomalies
Throughout the Phase One Program (Mir 18 to Mir 25),samples were planned to be collected at the beginning andthe middle of each Mir mission, as well as during eachShuttle docking period. Because of problems withschedule changes due to crew time constraints andCondensate Recovery System (CRS) activities, thissample collection schedule could not always be followed.However, key samples were collected following a fire onboard Mir, during crew changeover periods of up to sixcrewmembers, before and after water system maintenanceactivities, and during periods when crewmembers detected“aftertastes” in the water.
Postflight Anomalies
None
Completeness/Quality of Data
A total of 65 samples were collected throughout the PhaseOne Program. Of these, 29 were recycled water samplescollected from the condensate recovery system (CRS), 8were stored water samples taken from the SVO-ZVsystem, and 28 were humidity condensate samplescollected at the inlet of the CRS. Six additional samples
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of ground supplied stored water were also collected inKorolev, Russia before shipment to Baykonur for launchon a Progress resupply vehicle.
DISCUSSION
Status of Data Analysis
Chemical analyses of the water samples have beencompleted.
Final Research Findings
Regenerated Water
Twenty-nine recycled water samples were collected fromthe condensate recovery system (CRS). A summary of theanalytical results for these samples is reported in Table 3.
Physical Parameters - Turbidity levels in the samplescollected often exceeded the U.S. limit of 1 NTU (range:0.3 – 7.3 NTU; mean: 2.9 NTU). All other physicalparameters measured, including pH, color, odor, and totalhardness, were within acceptable limits. Conductivitylevels in the recycled water samples ranged from 14.3 –1130 µS/cm (mean, 151.2 µS/cm).
Inorganic Parameters - Ionic compounds identified in therecycled water samples include chloride sulfate, calcium,magnesium, potassium, fluoride, ammonium, nitrate, andsodium. Metallic species detected in the samples includesilver, aluminum, barium, chromium, copper, iron,manganese, molybdenum, nickel, lead, and zinc. Thedetection of calcium, magnesium, and silver was expectedas these compounds are added by the CRS [1]. Of theionic compounds found in the recycled water samples,fluoride, barium, silver, nickel, and manganese, onoccasion, exceeded the NASA/Russian Space Agency(RSA) maximum contaminant levels as outlined in Table2. In addition, increasing levels of iron and nickel weredetected as shown in Figures 4 and 5.
Organic Parameters - Nearly 250 organic compounds weretested for in the samples. These compounds were classifiedas volatile organic compounds, semivolatile organiccompounds, carboxylates, alcohols, aldehydes, and urea.Total organic carbon (TOC) analyses were also performed.
Volatile organic compounds detected in the Mir 18-25samples at a mean concentration of 1 µg/L or higherincluded acetaldehyde, acetone, bromodichloromethane,carbon tetrachloride, chloroform, dibromo-chloromethane,methylene chloride, and toluene. A sample collected on3/28/95 had a methylene chloride level of 92.8 µg/Lwhich is believed to be due to laboratory contamination.In the case of chloroform, there were only one or twooccasions where detected levels exceeded U.S.
Environmental Protection Agency (EPA) maximumcontaminant level (MCL) or health advisory. (NoNASA/RSA specification exists for this compound.) Withthe replacement of purification columns in the CRS,chloroform levels were reduced. A sample collected on12/14/96 contained 20.6 µg/L of chloroform compared toa sample collected ten days earlier before changeout of thepurification columns which contained 177.2 µg/L ofchloroform.
Approximately 20 semivolatile organic compounds weredetected at a mean concentration at or above 1 µg/L. Ofthese, di-n-butyl phthalate and benzothiazole were themost prevalent. Other organic compounds detected insignificant concentrations in the recycled water wereformate, ethylene glycol, ethanol, acetate, and methanol.Ethylene glycol was detected at 45 mg/L in one of the 29samples analyzed, six times the U.S. EPA HealthAdvisory level of 7 mg/L. The presence of this compoundwas due to ethylene glycol coolant leaks on board Mir.Recycled water was not consumed until additional waterprocessing hardware, a catalytic reactor unit, was installedto the CRS in December, 1996 to ensure the removal ofthis compound. Ethylene glycol levels are shown inFigure 6.
The mean concentration of total organic carbon (TOC) inthe Mir samples was 5.4 mg/L which exceeded the NASAmaximum contaminant level of 0.5 mg/L. Figure 7shows the TOC values observed in the Mir samples.Accountability of organic carbon was calculated bysumming the concentration of organic carbon for eachorganic compound analyzed and comparing this result tothe total organic carbon value. This comparison gives anindication of the theoretical yield of all organiccompounds in the sample and is referred to as the organiccarbon recovery. With regard to recovery of organiccarbon, an average of 14% of the organic content wasidentified using present analytical techniques.
Stored Water
Stored water provided to Mir crewmembers originated aseither Korolev, Russia tapwater processed and treated forspace flight and launched on a Progress resupply vehicleor U.S.-supplied fuel-cell water processed for potable useand delivered during Shuttle-Mir docking activities [17].The Russian-supplied water was transferred to Mir viaRodnik tanks or EDVs, while the U.S. water wasdelivered via Contingency Water Containers (CWCs).These water sources were then connected to the SVO-ZVsystem, a system for pressurizing and dispensing water forcrew use, or the SRV-K which recycles humiditycondensate into recycled water.
To assess continuing potability, six samples of Korolevwater were collected during preflight processing of thewater. Samples of U.S. supplied water were also collected
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before transfer to the Mir; results of these samples arereported elsewhere [17]. Eight samples of water at thepoint of use, i.e. SVO-ZV system, were collected inflight. SVO-ZV water could consist of either the Russiansupplied water, the U.S. supplied water, or a mixture ofboth. A summary of the inflight stored water results arereported in Table 4. In addition, a comparison of preflightand inflight stored water results for selected parameters isreported in Table 5.
Physical Parameters - Turbidity levels in the preflightstored water samples ranged from 0.43 to 11.14 NTU(average: 6.66 NTU), while samples collected in flightranged from 1.7 to 8.3 NTU (average: 5.7 NTU). pHlevels in both water types were neutral, with averagelevels of 7.3 and 7.8 respectively. Chemical OxygenDemand (COD) levels were not measured in the preflightsamples, although levels detected in the inflight samplesaveraged 43.8 mg/L (range: 10.5 – 105 mg/L). Only oneof the eight inflight samples exceeded the 100 mg/L RSAspecification for COD. This sample has 105 mg/L ofCOD and is believed to be U.S. Shuttle water since levelsof ethanol and formate were also high in this sample.Ethanol is used in preflight servicing of the Shuttle watersystem, while formate is used as a counterion during thepreparation of solutions used to add calcium andmagnesium to the Shuttle water transferred to Mir.Conductivity in the preflight stored water samplesaveraged 272 µS/cm. The conductivity averaged 238µS/cm for the inflight samples.
Inorganic Parameters - Inorganic compounds detectedabove 1 µg/L (mean concentration) in the preflight storedwater samples include silver, iron, aluminum, zinc,nickel, calcium, barium, manganese, cadmium, sulfate,magnesium, chloride, copper, sodium, and potassium.Silver is added to stored water supplies for microbialcontrol, and calcium and magnesium are added to meetRussian requirements. In general, none of the inorganiccompounds measured exceeded the U.S./Russian waterspecifications for stored water.
Organic Parameters - Ethanol, acetaldehyde, 2-propanol,caprolactam, and chloroform were the organic compoundsdetected in the highest concentrations in the stored watersamples. These compounds were found both in thepreflight and the inflight samples collected. Ethanol levelsin the stored water can be attributed to the U.S. Shuttlesupplied water, where ethanol is used to service theShuttle water system before launch [17]. Chloroformlevels were found in both the preflight and inflightsamples, indicating that this compound was initially acomponent of the Russian-supplied water. Additionalprocessing (activated carbon filtration) of the ground-supplied water was performed to reduce chloroform levels.Samples from later servicing show that the chloroformwas subsequently not found in the stored water supply.
Humidity Condensate Results
Twenty-eight humidity condensate samples were collectedat the inlet of the Condensate Recovery System (CRS).The CRS or SRV-K, located in the Mir core module, isused to recycle atmospheric moisture into potable water asshown in Figure 8. It may also be used to processtechnical CWCs into potable water and as a dispensingmechanism for CWC potable water.
To generate recycled water, humidity condensate iscollected from the Mir and Soyuz thermal controlsystems. Next, the condensate is filtered and processed bya catalytic reactor subsystem and then a gas separator thatremoves any residual air from the water. Following this,the water is processed by purification columns thatremove organic and inorganic contaminants from thewater. The water is then treated with silver and mineralsby a conditioning bed, pasteurized using a regenerativeheat exchanger, and stored for crew use. Crewmembersmay select either hot or ambient water for consumption[1,4,5]. A summary of results for the humidity condensatesamples is listed in Table 6.
Physical Parameters - The physical parameters measuredin the humidity condensate samples were pH,conductivity, and turbidity. The respective average valuesfor these parameters were 7.0 pH units, 244 µS/cm, and12 NTU.
Inorganic Parameters - Inorganic compounds detected inthe highest concentrations were ammonium (as N),sodium, sulfate, potassium, chloride, nickel, and zinc.These results were similar to results previously reportedby Samsonov et al [16].
Organic Parameters - Approximately 160 organiccompounds were detected in the humidity condensatesamples. Of these, ethylene glycol, ethanol, caprolactam,acetate, N,N-dimethylformamide, methylene chloride, and1-methoxy-2-propanol were the most prevalent. Ethyleneglycol levels were due to several coolant leaks previouslydiscussed. Figure 9 depicts the ethylene glycol levels inthe condensate. Ethanol levels detected may have originsas a crew metabolic product or as a component of crewhygiene items and disinfectant products. Table 7 lists theorganic compounds detected in the humidity condensate ator above 10 µg/L (mean concentration).
The average TOC level in the humidity condensatesamples was 118.9 mg/L. Of the 28 samples analyzed, theminimum TOC level seen was 17.6 mg/L and themaximum value detected was 411 mg/L. Figure 10 showsthe TOC levels in the condensate samples. Chemicaloxygen demand averaged 400 mg/L.
An analysis of condensate collected before and after a fireon board Mir did not reveal any significant differences inthe organic composition of the condensate. Accountability
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of organic matter in the condensate was much higher ascompared to the recycled water, because of the increasedconcentrations and quantities of chemical constituentsdetected in the samples. The organic carbon recovery inthe condensate average 48% (range: 3.8 – 92.5%).
Conclusions
During the Phase One Program, samples of humiditycondensate, recycled potable water, and stored water weresuccessfully collected on board the Mir Space Station andanalyzed on the ground by the Institute for BiomedicalProblems, the NASA-Johnson Space Center Water andFood Analytical Laboratory and NIICHIMASH. Theanalysis of these samples has provided important data forassessing the potability of the recycled water, especiallyduring the off-nominal conditions experienced with theMir thermal cooling system. Findings from the analysisof the regenerated and stored water sample show that thewater generally met Joint U.S./Russian specifications forthe Mir Space Station. It is noted, however, that the morestringent U.S. Segment NASA requirements for TOC andturbidity were exceeded in many of the samples.
Investigation Results
Based on this investigation and results from Mir 18 toMir 25, the following lessons were learned:
1. The results indicate that the Mir water supply met theU.S. and Russian water quality standards with thefollowing exceptions:
• Turbidity levels in the recycled water often exceededthe U.S. specification of 1 NTU. Because ofdifferences in analytical methodology between theU.S. and Russia, U.S. turbidity values could not bedirectly compared to the Russian specification
• TOC levels in the recycled water usually did not meetthe NASA U.S. Segment specification of 0.5 mg/L,although it did meet the Russian standard of no morethan 25 mg/L.
2. Collection and subsequent ground analysis ofcondensate and recycled water during repeated episodes ofethylene glycol coolant leaks and after the Mir fire werecritical in making operational decisions.
• Because an inflight capability did not exist to assessthe impact of the ethylene glycol spills on the qualityof the recycled water, consumption of the recycledwater was curtailed for extended periods.
3. Except for ethylene glycol and chloroform, fewcompounds have been detected at toxicologicallysignificant levels in the recycled water samples. Acatalytic reactor unit, installed in the CRS in 1996, wasfound to be effective at oxidizing ethylene glycols (andother glycols) and eliminating the threat to the potable
water supply. Additional ground-based processing of storedwater was successfully incorporated to reduce the level ofchloroform detected in the preflight stored water samplesfrom Korolev, Russia.
4. Over 210 organic and inorganic components weredetected in the condensate samples. Comparing the sum oforganic carbon contributed by each detected organiccompound to the total organic carbon measurementshowed that only about 48% of the carbon in the humiditycondensate samples was accounted and about 14% of thecarbon in the recycled water samples was accountedc.
5. Traces of various metals were detected in thecondensate and recycled water samples. Iron and nickellevels in the recycled water in particular tended to beincreasing over time.
Investigation Applications
This research will provide benefits on Earth through:
• Improvements in methods development for theanalysis of drinking water, and in particular, recycledpotable water.
• Better insight and understanding of water recyclinghardware operation and reliability.
• Increased knowledge of recycled potable watercontaminants.
• Practical support to the eventual recycle of water onthe Earth.
REFERENCES
1. Samsonov, N.M, Bobe, L.S., Novikov, V.M,Farafonov, N.S., Pinsky, B.Ja., Abromov, G. et al.,Systems for Water Reclamation from HumidityCondensate and Urine for Space Station, SAETechnical Paper Series no. #941536, 24thInternational Conference on Environmental Systemsand 5th European Symposium on SpaceEnvironmental Control Systems, Friedrichshafen,Germany, June 1994.
2. Pierre, L.M., Schultz, J.R., Johnson, S.M., Sauer,R.L., Sinyak, Y.E., Skuratov, V.M., and Protasov,N.N., Collection and Chemical Analysis ofReclaimed Water and Condensate from the Mir SpaceStation, SAE #961569, 26th International Conferenceon Environmental Systems, Monterey, CaliforniaJuly 1996.
3. Pierre, L.M., Schultz, J.R., Sauer, R.L. Sinyak,Y.E., Skuratov, V.M., and Protasov, N.N., ChemicalAnalysis of Potable Water and Humidity CondensateCollected During the Mir 21 Mission, SAE #972462,27th International Conference on EnvironmentalSystems, Lake Tahoe, Nevada July 1997
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4. Mitchell, K., Technical Assessment of Mir-1 LifeSupport Hardware for the International Space Station,Life Support Systems Branch/ED62, Marshall SpaceFlight Center, AL, 1993.
5. Samsonov, N.M, Bobe, L.S., Novikov, V.M,Farafonov, N.S., Abromov, G. Kh., Pinsky, B.Ja.,Grigorov, E.I., Zaitsev, E.N., Protasov, N.N.,Komolov, V.V., Grigoriev A.I., and Sinyak, Y.E.,Water Supply Based on Water Reclamation fromHumidity Condensate and Urine on a Space Station,SAE Technical Paper Series no. #961408, 26thInternational Conference on Environmental Systems,Monterey, California, July 1996.
6. United States Environmental Protection Agency,Office of Water, Drinking Water Regulations andHealth Advisories, EPA 822-B-95-002, October1996.
7. Standard Methods for the Examination of Water and Wastewater , 18th edition, American Public HealthAssociation, Washington, D.C. 1992
8. EPA Methods and Guidance for Analysis of Water onCD-ROM, United States Environmental ProtectionAgency, Office of Water, Washington D.C., April1997.
9. USSR State S tandards for Drinking Water , PublicHealth Ministry, Russia
10. Test Methods for Evaluating Solid WastePhysical/Chemical Methods (SW-846) on CD-ROM,Version 2, United States Environmental ProtectionAgency, Washington, D.C., December 1997.
11. American Society for Testing and Materials, StandardTest Method for Total Carbon, Inorganic Carbon, andOrganic Carbon in Water by Ultraviolet, PersulfateOxidation, and Membrane conductivity Detection,1996
12. Jandik, Peter and Gunther Bonn, Capillary Electrophoresis of Small Molecules and Ions , VCHPublishers, Inc. 1993
13. Standard Methods for the Examination of Water and Wastewater , 19th edition, American Public HealthAssociation, Washington, D.C. 1995
14. Samsonov, N.M, Bobe, L.S., Novikov, V.M,Farafonov, N.S., Amiragov, M.S., Gurovskaya,R.A., Protasov, N.N., Komolov, V.V., Sinyak,Y.E., and Skuratov, V.M., Testing and Operation ofthe Purification Unit of the System for WaterRecovery from Humidity Condensate (WRS-C) witha Higher Content of Organic Contaminants, SAETechnical Paper Series no. #981715, 28thInternational Conference on Environmental Systems,Danvers, MA, July 1998.
15. Samsonov, N.M, Bobe, L.S., Novikov, V.M,Farafonov, N.S., Pinsky, B.Ja., Abromov, G. Kh.,Berezkin, S.V., Grigorov, E.I., Zaitsev, E.N.,Protasov, N.N., Komolov, V.V., Grigoriev, A. I.,Sinyak, Y.E., Rakov, V.V., and Rifert, V.G.,Updated Systems for Water Recovery from HumidityCondensate and Urine for the International SpaceStation, SAE Technical Paper Series no. #972559,27th International Conference on EnvironmentalSystems, Lake Tahoe, NV, July 1997.
16. Samsonov, N.M, Farafonov, N.S., Novikov, V.M.,Bobe, L.I., Gavrilov, L.H.., Abramov, A. Y.Podrugin, Y.E. Sinyak, E.I. Grigorov, and E. N.Zaitsev. A Physical/Chemical System for Water andAtmosphere Recovery Aboard a Space Station, SAETechnical Paper Series no. #932077, 23rdInternational Conference on Environmental Systems,Colorado Springs, CO, July 1993.
17. Mudgett, P.D., Schultz, J.R., Packham, N.J.,Veselka, D.J., Brasseaux, Jr., H.J., Rotter, H.A., andSauer, R.L. Potable Water Treatment and Transferfrom Shuttle to Mir, SAE Technical Paper Series no.#972461, 27th International Conference onEnvironmental Systems, Lake Tahoe, NV, July1997.
18. Table 6.4-6 NASA Space Shuttle Specification,“Fluid Procurement and Use Control,” SE-S-0073,Rev F, Change 61, June 1996.
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Session Scheduled Actual Samples/Name FO# HW# Day Day Parameters
Mir 18preflight ground supplied 1 NA NA L-54 1000 ml of waterwater collection at RSC-Energia, 19 Jan 95 Split: 1000 ml US,Kalingrad, Russia 0 ml RSAgalley-hot water collection 2,3 2-7 MD13 MD 13 965 ml of water
28 Mar 95 Split: 630 ml US,335 ml RSA
humidity condensate collection 4 1 MD57 MD57 sample not received11 May 96 (sample could not be
found for return to Earth)galley-hot water collection 2,3 2-7 MD 97 MD 97 193 ml of water
20 Jun 95 Split: 145 ml US,48 ml RSA
galley-hot water collection 2,3 2-7 FD7 MD110 583 ml of water3 Jul 95 Split: 395 ml US,
188 ml RSAstored water collection 2,3 2-7 FD7 MD110 291 ml of water
3 Jul 95 Split: 145 ml US,146 ml RSA
Mir 19preflight ground supplied 1 NA NA L-113 1000 ml of waterwater collection at RSC-Energia, 6 Mar 95 Split: 1000 ml US,Kalingrad, Russia 0 ml RSAgalley-hot water collection 2,3 2-7 MD8 MD23 821.5 ml of water
27 Jul 95 Split: 537.5 ml US,284 ml RSA
galley-hot water collection 2,3 2-7 MD32 MD42 1003 ml of water15 Aug 95 Split: 582.5 ml US,
448 ml RSAgalley-hot water collection 2,3 2-7 MD55 MD55 1024 ml of water
28 Aug 95 Split: 582.5 ml US,442 ml RSA
humidity condensate collection 4 1 unknown MD62-MD65 ?? ml of condensate4-7 Sept 1995 Split: 21 ml US,
?? ml RSAMir 20humidity condensate collection 4 1 unknown MD43 78.5 ml of condensate
30 Oct 95 Split: 73 ml US,5.5 ml RSA
humidity condensate collection 4 2-7 MD60 MD60 848 ml of condensatefrom EDV #1 16 Nov 95 Split: 537.5 ml US,
310.5 ml RSAhumidity condensate collection 4 2-7 MD60 MD60 910 ml of condensatefrom EDV #2 16 Nov 95 Split: 537.5 ml US,
372.5 ml RSAhumidity condensate collection 4 2-7 MD60 MD60 976.5 ml of condensatefrom EDV #3 16 Nov 95 Split: 582.5 ml US,
400 ml RSASVO-ZV (stored) water collection 2,3 2-7 MD60 MD61 914 ml of water
17 Nov 95 Split: 537.5 ml US,376 ml RSA
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Session Scheduled Actual Samples/Name FO# HW# Day Day Parameters
Mir 21ground supplied water collection 1 NA NA L-120 1000 ml of waterat RSC-Energia, Korolev, Russia 2 Nov 95 Split: 1000 US,
0 ml RSAgalley-hot water collection 2,3 2-7 MD10 MD10 860 ml of water
1 Mar 96 Split: 517.5 ml US,342.5 ml RSA
humidity condensate collection 4 1 MD10-13 MD10-13 25 ml of condensate1-4-Mar-96 Split: 21 ml US,
4 ml RSAgalley-hot water collection 2,3 2-7 MD28 MD28 770 ml of water
19 Mar 96 Split: 517.5 ml US,252.5 ml RSA
galley-cold water collection 2,3 2-7 MD28 MD28 855 ml of water19 Mar 96 Split: 517.5 ml US,
337.5 ml RSAhumidity condensate collection 4 1 MD28-31 MD28-31 89 ml of condensate
19-22- Mar-96 Split: 58.5 ml US,30.5 ml RSA
galley-hot water collection 2,3 2-7 MD35 MD36 747.9 ml of water27 Mar 96 Split: 487.5 ml US,
260.4 ml RSAgalley-cold water collection 2,3 2-7 MD35 MD36 309.5 ml of water
27 Mar 96 Split: 196.5 ml US,113 ml RSA
SVO-ZV (ground supplied) 2,3 2-7 MD35 MD36 24 ml of waterwater collection 27 Mar 96 Split: 22 ml US,
2 ml RSAhumidity condensate collection 4 1 unknown MD 120-124 80 ml of condensate
18-22 -June-96 Split: 55 ml US,25 ml RSA
galley-hot water collection 2,3 2-7 MD146 MD146 748 ml of water15 Jul 96 Split: 520 ml US,
228ml RSAhumidity condensate collection 4 1 unknown MD154-157 73 ml of condensate
23-26-Jul-96 Split: 50 ml US,23 ml RSA
galley-hot water collection 2,3 2-7 MD177 MD177 768.5 ml of water15 Aug 96 Split: 520 ml US,
248.5ml RSAMir 22ground supplied water collection 1,5 7-14 NA L-74 1000 ml of waterat RSC-Energia, Korolev, Russia 3 Jun 96 Split: 1000 US,
0 ml RSAgalley-hot water collection 2,3 2-7 MD19 MD19 250 ml of water
5 Sep 96 Split: 186 ml US,64 ml RSA
galley-cold water collection 2,3 2-7 MD19 MD19 309.5 ml of water5 Sep 96 Split: 196.5 ml US,
113 ml RSA
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4-49
TTTTAAAABBBBLLLLEEEE 1111.... DDDDAAAATTTTAAAA CCCCOOOOLLLLLLLLEEEECCCCTTTTIIIIOOOONNNNSSSS SSSSEEEESSSSSSSSIIIIOOOONNNNSSSS////FFFFUUUUNNNNCCCCTTTTIIIIOOOONNNNAAAALLLL OOOOBBBBJJJJEEEECCCCTTTTIIIIVVVVEEEESSSS
Session Scheduled Actual Samples/Name FO# HW# Day Day Parameters
Mir 22 contd.SVO-ZV (stored) water collection 2,3 2-7 MD19 MD19 862 ml of water
5 Sep 96 Split: 520 ml US,342 ml RSA
humidity condensate collection 4 1 unknown MD24-26 214 ml of condensate10-12-Sep-96 Split: 131 ml US,
83 ml RSAhumidity condensate collection 4 1 unknown MD30-32 347 ml of condensate
16-18-Sep-96 Split: 211 ml US,136 ml RSA
galley-cold water collection 2,3 2-7 MD35 MD38 789 ml of water23 Sep 96 Split: 520 ml US,
269 ml RSAhumidity condensate collection 4 1 MD 53-60 MD 53-60 72 ml of condensate
8-15- Oct-96 Split: 50 ml US,22 ml RSA
galley-hot water collection 2,3 2-7 MD82 MD82 695 ml of water6 Nov 96 Split: 495 ml US,
200 ml RSAgalley-cold water collection 2,3 2-7 not MD82 769 ml of water
scheduled 6 Nov 96 Split: 569 ml US,200 ml RSA
SVO-ZV (stored) water collection 2,3 2-7 not MD82 908 ml of waterscheduled 6 Nov 96 Split: 658 ml US,
250 ml RSAhumidity condensate collection 4 1 MD 107-110 MD 107-110 88 ml of condensate
1-4-Dec-96 Split: 60 ml US,28 ml RSA
humidity condensate collection 4 1 not MD110 788 ml of condensatescheduled 4 Dec 96 Split: 559 ml US,
229 ml RSAgalley-hot water collection 2,3 2-7 MD110 MD110 754 ml of water
4 Dec 96 Split: 559 ml US,195 ml RSA
galley-hot water collection 2,3 2-7 MD120 MD120 748 ml of water14 Dec 96 Split: 546 ml US,
202 ml RSAgalley-cold water collection 2,3 2-7 MD120 MD120 778 ml of water
14 Dec 96 Split: 559 ml US,219 ml RSA
galley-hot water collection 2,3 2-7 MD154 MD155 607 ml of water18 Jan 97 Split: 415 ml US,
192 ml RSASVO-ZV (ground supplied) 2,3 2-7 MD154 MD155 509 ml of waterwater collection 18 Jan 97 Split: 365 ml US,
144 ml RSAMir 22/ Mir 23humidity condensate collection 4 2-7 not MD 195-197 551ml of condensate
scheduled MD 17-19 Split: 401 ml US,2/26-3/1/97 150 ml RSA
SAUER POSTFLIGHT SCI ENCE REPORT
4-50
TTTTAAAABBBBLLLLEEEE 1111.... DDDDAAAATTTTAAAA CCCCOOOOLLLLLLLLEEEECCCCTTTTIIIIOOOONNNNSSSS SSSSEEEESSSSSSSSIIIIOOOONNNNSSSS////FFFFUUUUNNNNCCCCTTTTIIIIOOOONNNNAAAALLLL OOOOBBBBJJJJEEEECCCCTTTTIIIIVVVVEEEESSSS
Session Scheduled Actual Samples/Name FO# HW# Day Day Parameters
Mir 22/ Mir 23 contd.4 2-7 not MD 197 787 ml of condensate
scheduled MD 19 Split: 537 ml US,1 Mar 97 250 ml RSA
Mir 23galley-hot water collection 2,3 2-7 MD 88 MD88 719 ml of water
8 May 97 Split: 519 ml US,200 ml RSA
galley-hot water collection 2,3 2-7 not MD 99 755 ml of waterscheduled 19 May 97 Split: 522 ml US,
233 ml RSA
galley-cold water collection 2,3 2-7 MD 99 MD 99 741 ml of water19 May 97 Split: 522 ml US,
219 ml RSASVO-ZV (ground supplied) 2,3 2-7 MD 99 MD 99 750 ml of waterwater collection 19 May 97 Split: 522 ml US,
228 ml RSAhumidity condensate collection 4 1 MD93-96 MD93-96 58 ml of condensate
13-16-May-97 Split: 46 ml US,12 ml RSA
humidity condensate collection 4 1 MD96-99 MD96-99 81 ml of condensate16-19-May-97 Split: 62 ml US,
19 ml RSAsurface condensate 4 2-7 not MD101 683 ml of condensate
scheduled 21 May 97 Split: 483 ml US,200 ml RSA
surface condensate 4 2-7 not MD 101 694 ml of condensatescheduled 21 May 97 Split: 494 ml US,
200 ml RSAgalley-hot water collection 2,3 2-7 MD185 did not occur
galley-hot water collection 2,3 2-7 MD195 did not occur
galley-cold water collection 2,3 2-7 MD195 did not occur
Mir 24humidity condensate collection 4 1 MD26 MD28 sample not received
2 Sep 97
galley-cold water collection 2,3 2-7 MD57 MD57 752 ml of water1 Oct 97 Split: 526 ml US,
226 ml RSASVO-ZV (ground supplied) 2,3 2-7 MD57 cancelledwater collection
humidity condensate collection 4 1 MD29 did not occur
POSTFLIGHT SCIENCE REPORT SAUER
4-51
TTTTAAAABBBBLLLLEEEE 1111.... DDDDAAAATTTTAAAA CCCCOOOOLLLLLLLLEEEECCCCTTTTIIIIOOOONNNNSSSS SSSSEEEESSSSSSSSIIIIOOOONNNNSSSS////FFFFUUUUNNNNCCCCTTTTIIIIOOOONNNNAAAALLLL OOOOBBBBJJJJEEEECCCCTTTTIIIIVVVVEEEESSSS
Session Scheduled Actual Samples/Name FO# HW# Day Day Parameters
Mir 24 contd.galley-hot water collection 2,3 2-7 MD104 MD104 209 ml of water
17 Nov 97 Split: 139 ml US,70 ml RSA
humidity condensate collection 4 1 MD104 MD104 67 ml of water17 Nov 97 Split: 48 ml US,
19 ml RSAgalley-hot water collection 2,3 2-7 MD114 MD114 835 ml of water
27 Nov 97 Split: 585 ml US,250 ml RSA
SVO-ZV (ground supplied) water 2,3 2-7 MD114 MD114 767 ml of watercollection 27 Nov 97 Split: 537 US,
230 ml RSAhumidity condensate collection 4 2-7 MD114 MD115 702 ml of water
29 Nov 97 Split: 502 ml US,200 ml RSA
galley-hot water collection 2,3 2-7 MD162 MD167 108 ml of water19 Jan 98 Split: 79 ml US,
29 ml RSAhumidity condensate collection 4 1 MD162 MD167 71 ml of water
19 Jan 98 Split: 49 ml US,22 ml RSA
Mir 25galley-hot water collection 2,3 2-7 MD115 MD77 741 ml of water
9 Apr 98 Split: 474 ml US,267 ml RSA
galley-hot water collection 2,3 2-7 MD50 MD85 703 ml of water23 Apr 98 Split: 472 ml US,
231 ml RSAhumidity condensate collection 4 1 MD93 MD90 139 ml of water
28 Apr 98 Split: 96 ml US,43 ml RSA
humidity condensate collection 4 1 MD122 MD103 137 ml of water11 May 98 Split: 99 ml US,
38 ml RSAgalley-hot water collection 2,3 2-7 MD60 MD91 353 ml of water
21 May 98 Split: 243 ml US,110 ml RSA
galley-hot water collection 2,3 2-7 MD130 MD130 385 ml of water7 Jun 98 Split: 261 ml US,
124 ml RSASVO-ZV (ground supplied) water 2,3 2-7 MD130 MD130 381 ml of watercollection 7 Jun 98 Split: 261 US,
120 ml RSAhumidity condensate collection 4 1 MD130 MD130 165 ml of water
7 Jun 98 Split: 114 ml US,51 ml RSA
humidity condensate collection 4 1 MD199 MD199 ? ml of water(returned on Soyuz) 15 Aug 98 Split: 64 ml US,
? ml RSA
SAUER POSTFLIGHT SCI ENCE REPORT
4-52
TTTTAAAABBBBLLLLEEEE 2222.... JJJJOOOOIIIINNNNTTTT UUUU....SSSS....////RRRRUUUUSSSSSSSSIIIIAAAANNNN PPPPOOOOTTTTAAAABBBBLLLLEEEE WWWWAAAATTTTEEEERRRRSSSSPPPPEEEECCCCIIIIFFFFIIIICCCCAAAATTTTIIIIOOOONNNNSSSS FFFFOOOORRRR TTTTHHHHEEEE MMMMIIIIRRRR SSSSPPPPAAAACCCCEEEE SSSSTTTTAAAATTTTIIIIOOOONNNN
U.S. Maximum Russian MaximumWater Parameter Contaminant Level (MCL) Contaminant Level (MCL)
pH1 5.5-9.0 pH units 5.5-9.0 pH unitsColor2 15 Pt-Co units 20 degreesTaste2 3 TTN 2 pointsOdor2 3 TON 2 pointsTotal Dissolved Solids3 100-1,000 mg/L 100-1,000 mg/LTurbidity2 1 NTU 1.5 mg/LTotal Gas 5% volume @1 ATM, 20oC 5% volume @1 ATM, 20oCAmmonia (NH3
-N) 2 mg/L 2 mg/LArsenic 0.01 mg/L 0.01 mg/LBarium 1 mg/L 1 mg/LCadium 0.005 mg/L 0.005 mg/LCalcium 100 mg/L 100 mg/LChlorine-total (includes Cl-) 250 mg/L 250 mg/LChromium 0.1 mg/L 0.1 mg/LCopper 1 mg/L 1 mg/LFluorine 1.5 mg/L 1.5 mg/LIodine-total (includes I-) 15 mg/L 15 mg/LIodine-residual4 1.0-4.0 mg/L 1.0-4.0 mg/LIron 0.3 mg/L 0.3 mg/LLead 0.05 mg/L 0.05 mg/LMagnesium 50 mg/L 50 mg/LManganese 0.05 mg/L 0.05 mg/LMercury 0.002 mg/L 0.002 mg/LNickel 0.1 mg/L 0.1 mg/LNitrate (NO3
-N) 10 mg/L 10 mg/LSelenium 0.01 mg/L 0.01 mg/LSilver 0.5 mg/L 0.5 mg/LSulfate 250 mg/L 250 mg/LZinc 5 mg/L 5 mg/LTotal Hardness (Ca & Mg) 7 meq/L 7 meq/LTotal Bacteria2 100 CFU/100 ml 10,000 CFU/100 mlColiform Bacteria <1 CFU/100 ml <1 CFU/100 mlVirus <1 PFU/100 ml <1 PFU/100 mlCyanide 200 µg/L 200 µg/LTotal Phenols 1 µg/L 1 µg/LTotal Organic Carbon (TOC) 500 µg/L 25,000 µg/LUncharacterized TOC 100 µg/L no limitOxygen Consumption-COD no limit 100 mg/L
1pH range applies only before iodination2Parameters have different values for U.S. and Russian supplied waterbecause of different analytical methods used
3The 100 mg/L limit applies to the water before mineralization.After mineralization, this parameter will not exceed 1,000 mg/L
4Range of required level if iodine is used as a biocide
POSTFLIGHT SCIENCE REPORT SAUER
4-53
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Cond
uctiv
ityµ
S/cm
U.S
.29
151.
214
.311
30.0
Cond
uctiv
ityµ
S/cm
Russ
ia16
99.1
15.0
224.
0pH
pH u
nits
U.S
.5.
5-9.
0N
ASA/
RSA
287.
02.
610
.0pH
pH u
nits
Russ
ia5.
5-9.
0N
ASA/
RSA
227.
36.
18.
0Tu
rbid
ityN
TUU
.S.
1N
ASA/
RSA
232.
90.
37.
3Tu
rbid
itym
g/L
Russ
ia1.
5N
ASA/
RSA
70.
20.
01.
5Co
lor T
rue
degr
ees
Russ
ia15
Pt-C
oN
ASA/
RSA
1610
.310
.015
.0un
its/2
0O
dor a
t 20o C
grad
eRu
ssia
3 TO
N/2
NAS
A/RS
A18
0.3
02
Tast
e at
20o C
grad
eRu
ssia
3 TT
N/2
NAS
A/RS
A3
00
0To
tal S
olid
sm
g/L
Russ
ia1.
5N
ASA/
RSA
30
00
Tota
l Har
dnes
sm
eq/L
Russ
ia7
NAS
A/RS
A17
0.9
0.1
2.4
Chem
ical
Oxy
gen
Dem
and
mg O
2/L
Russ
iano
limit/
100
NAS
A/RS
A25
18.8
3.0
85.0
Anio
ns (C
E/IC
)Br
omid
em
g/L
U.S
.23
ND
ND
<0.
50Ch
lorid
em
g/L
U.S
.20
0N
ASA/
RSA
233.
6N
D13
.0Fl
uorid
em
g/L
U.S
.1.
5N
ASA/
RSA
230.
2N
D3.
7N
itrat
e as N
itrog
en (N
O3-
N)
mg/
LU
.S.
10N
ASA/
RSA
230.
1N
D0.
7N
itrite
as N
itrog
en (N
O2-
N)
mg/
LU
.S.
23N
DN
D<
0.0
8Ph
osph
ate a
s P (P
O4-
P)m
g/L
U.S
.23
0.0
ND
1.0
Sulfa
tem
g/L
U.S
.25
0N
ASA/
RSA
233.
7N
D27
.6Ca
tions
(CE/
IC)
Amm
onia
as N
itrog
en (N
H3-
N)
mg/
LU
.S.
2N
ASA/
RSA
250.
0N
D0.
4Ca
lcium
mg/
LU
.S.
100
NAS
A/RS
A25
13.7
2.4
38.9
Lith
ium
mg/
LU
.S.
250.
0N
D0.
4M
agne
sium
mg/
LU
.S.
50N
ASA/
RSA
252.
2N
D9.
4Po
tass
ium
mg/
LU
.S.
250.
6N
D2.
8So
dium
mg/
LU
.S.
251.
6N
D6.
0M
iner
als
Amm
oniu
m (N
H4)
mg/
LRu
ssia
2N
ASA/
RSA
160.
1N
D0.
8Ca
lcium
mg/
LRu
ssia
100
NAS
A/RS
A9
14.8
2.0
28.8
Mag
nesiu
mm
g/L
Russ
ia50
NAS
A/RS
A9
3.3
0.9
8.5
SAUER POSTFLIGHT SCI ENCE REPORT
4-54
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Met
als
Calci
umµ
g/L
U.S
.10
0000
NAS
A/RS
A0
NA
NA
NA
Mag
nesiu
mµ
g/L
U.S
.50
000
NAS
A/RS
A0
NA
NA
NA
Sodi
umµ
g/L
U.S
.0
NA
NA
NA
Pota
ssiu
mµ
g/L
U.S
.0
NA
NA
NA
Silv
erµ
g/L
U.S
.50
0N
ASA/
RSA
2811
3.6
8.4
674.
0Si
lver
ion
µg/
LRu
ssia
1534
.0N
D20
0.0
Alum
inum
µg/
LU
.S.
NAS
A16
44.5
<10
577.
0Ar
seni
cµ
g/L
U.S
.10
NAS
A22
ND
ND
<5
Bariu
mµ
g/L
U.S
.10
00N
ASA
2218
9.7
ND
2440
.0Ca
dmiu
mµ
g/L
U.S
.5
NAS
A22
0.0
ND
0.9
Chro
miu
mµ
g/L
U.S
.10
0N
ASA
220.
1N
D0.
6Co
balt
µg/
LU
.S.
NAS
A22
ND
ND
<5
Copp
erµ
g/L
U.S
.10
00N
ASA
2214
.95.
330
.3Iro
nµ
g/L
U.S
.30
0N
ASA
2264
.49.
326
5.0
Mer
cury
µg/
LU
.S.
2N
ASA
180.
0N
D0.
8M
anga
nese
µg/
LU
.S.
50N
ASA
229.
2N
D51
.7M
olyb
denu
mµ
g/L
U.S
.N
ASA
100.
2N
D1.
5N
ickel
µg/
LU
.S.
100
NAS
A22
31.3
5.6
157.
0Le
adµ
g/L
U.S
.50
NAS
A22
2.0
ND
5.5
Sele
nium
µg/
LU
.S.
10N
ASA
220.
4N
D9.
2Zi
ncµ
g/L
U.S
.50
00N
ASA
2269
.510
.447
5.0
Palla
dium
µg/
LU
.S.
NAS
A0
NA
NA
NA
Silic
onµ
g/L
U.S
.N
ASA
0N
AN
AN
ATu
ngst
enµ
g/L
U.S
.0
NA
NA
NA
Tota
l Org
anic
Car
bon
TIC
(OI 1
010)
mg/
LU
.S.
127.
60.
331
.5PO
C (O
I 101
0)m
g/L
U.S
.3
0.1
0.1
0.1
NPO
C (O
I 101
0)m
g/L
U.S
.12
6.7
1.0
23.7
TOC
(OI 1
010)
mg/
LU
.S.
0.5/
25N
ASA/
RSA
34.
71.
36.
7TI
C (S
ieve
rs 8
00)
mg/
LU
.S.
2010
.01.
828
.3TO
C (S
ieve
rs 8
00)
mg/
LU
.S.
0.5/
25N
ASA/
RSA
225.
40.
325
.1TO
C (S
ieve
rs 8
00)
mg/
LRu
ssia
0.5/
25N
ASA/
RSA
910
.70.
523
.2
POSTFLIGHT SCIENCE REPORT SAUER
4-55
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Vola
tile
Org
anic
sAc
etal
dehy
deµ
g/L
U.S
.23
2.2
ND
50.9
Acet
one
µg/
LU
.S.
2622
.5N
D13
1.7
Acry
loni
ltrile
µg/
LU
.S.
26N
DN
DN
DAl
lyl c
hlor
ide
ND
U.S
.26
ND
ND
ND
Benz
ene
µg/
LU
.S.
5.0
EPA
26N
DN
DN
DBr
omob
enze
neµ
g/L
U.S
.26
ND
ND
ND
Brom
ochl
orom
etha
neµ
g/L
U.S
.50
.0EP
A D
WEL
26N
DN
DN
DBr
omod
ichlo
rom
etha
neµ
g/L
U.S
.10
0EP
A26
0.4
ND
5.8
Brom
ofor
mµ
g/L
U.S
.10
0EP
A26
ND
ND
ND
Brom
omet
hane
µg/
LU
.S.
10EP
A H
A26
ND
ND
ND
2-Bu
tano
neµ
g/L
U.S
.26
ND
ND
ND
n-Bu
tylb
enze
neµ
g/L
U.S
.26
ND
ND
ND
s-Bu
tylb
enze
neµ
g/L
U.S
.26
ND
ND
ND
t-But
ylbe
nzen
eµ
g/L
U.S
.26
ND
ND
ND
Carb
on di
sulfi
deµ
g/L
U.S
.26
1.6
ND
<20
.0Ca
rbon
tetra
chlo
ride
µg/
LU
.S.
5EP
A26
1.3
ND
32.8
Chlo
roac
eton
itrile
µg/
LU
.S.
26N
DN
DN
DCh
loro
benz
ene
µg/
LU
.S.
100
EPA
26N
DN
DN
D1-
Chlo
robu
tane
µg/
LU
.S.
26N
DN
DN
DCh
loro
etha
neµ
g/L
U.S
.26
ND
ND
ND
Chlo
rofo
rmµ
g/L
U.S
.10
0EP
A26
17.6
ND
177.
2Ch
loro
met
hane
µg/
LU
.S.
3EP
A H
A26
ND
ND
ND
2-Ch
loro
tolu
ene
µg/
LU
.S.
100
EPA
HA
26N
DN
DN
D4-
Chlo
roto
luen
eµ
g/L
U.S
.10
0EP
A H
A26
ND
ND
ND
Dib
rom
ochl
orom
etha
neµ
g/L
U.S
.10
0EP
A26
0.2
ND
4.7
1,2-
Dib
rom
o-3-
chlo
ropr
opan
eµ
g/L
U.S
.0.
2EP
A26
ND
ND
ND
1,2-
Dib
rom
oeth
ane
µg/
LU
.S.
0.05
EPA
26N
DN
DN
DD
ibro
mom
etha
neµ
g/L
U.S
.26
ND
ND
ND
1,2-
Dich
loro
benz
ene
µg/
LU
.S.
600
EPA
26N
DN
DN
D1,
3-D
ichlo
robe
nzen
eµ
g/L
U.S
.60
0EP
A26
ND
ND
ND
1,4-
Dich
loro
benz
ene
µg/
LU
.S.
75EP
A26
0.0
ND
0.5
trans
-1,4
-dich
loro
-2-b
uten
eµ
g/L
U.S
.26
ND
ND
ND
SAUER POSTFLIGHT SCI ENCE REPORT
4-56
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Vola
tile
Org
anic
s con
td.
Dich
loro
diflu
orom
etha
neµ
g/L
U.S
.10
00EP
A H
A26
0.0
ND
0.9
1,1-
Dich
loro
etha
neµ
g/L
U.S
.26
ND
ND
ND
1,2-
Dich
loro
etha
neµ
g/L
U.S
.5
EPA
26N
DN
DN
D1,
1-D
ichlo
roet
hene
µg/
LU
.S.
7EP
A26
0.2
ND
5.1
cis1,
2-di
chlo
roet
hene
µg/
LU
.S.
70EP
A26
0.2
ND
4.4
trans
-1,2
-dich
loro
ethe
neµ
g/L
U.S
.10
0EP
A26
0.2
ND
5.7
1,2-
Dich
loro
prop
ane
µg/
LU
.S.
5EP
A26
ND
ND
ND
1,3-
Dich
loro
prop
ane
µg/
LU
.S.
26N
DN
DN
D2,
2-D
ichlo
ropr
opan
eµ
g/L
U.S
.26
ND
ND
ND
1,2-
Dich
loro
prop
ene
µg/
LU
.S.
26N
DN
DN
Dcis
-1,3
-Dich
loro
prop
ene
µg/
LU
.S.
26N
DN
DN
Dtra
ns-1
,3-D
ichlo
ropr
open
eµ
g/L
U.S
.26
ND
ND
ND
Die
thyl
ethe
rµ
g/L
U.S
.26
ND
ND
ND
Ethy
lben
zene
µg/
LU
.S.
26N
DN
DN
DEt
hyl m
etha
cyla
teµ
g/L
U.S
.26
ND
ND
ND
Hex
achl
orob
utad
iene
µg/
LU
.S.
26N
DN
DN
DH
exac
hlor
oeth
ane
µg/
LU
.S.
1EP
A H
A26
ND
ND
ND
2-H
exan
one
µg/
LU
.S.
26N
DN
DN
DIo
dom
etha
neµ
g/L
U.S
.26
ND
ND
ND
Isopr
opyl
benz
ene
µg/
LU
.S.
26N
DN
DN
D4-
Isopr
opyl
tolu
ene
µg/
LU
.S.
26N
DN
DN
DLi
nolo
olµ
g/L
U.S
.26
ND
ND
ND
Met
hacr
ylon
itrile
µg/
LU
.S.
26N
DN
DN
DM
ethy
lacr
ylat
eµ
g/L
U.S
.26
ND
ND
ND
Met
hyl-t
-but
ylet
her
µg/
LU
.S.
20EP
A H
A26
ND
ND
ND
Met
hyle
ne ch
lorid
eµ
g/L
U.S
.5
EPA
264.
3N
D92
.9M
ethy
lmet
hacr
ylat
eµ
g/L
U.S
.26
ND
ND
ND
4-M
ethy
l-2-p
enta
none
µg/
LU
.S.
26N
DN
DN
Dal
pha-
Met
hyl s
tyre
neµ
g/L
U.S
.26
ND
ND
ND
Pent
achl
oroe
than
eµ
g/L
U.S
.26
ND
ND
ND
Perfl
uoro
-1,3
-dim
ethy
lcyclo
hexa
neµ
g/L
U.S
.26
ND
ND
ND
Tetra
hydr
ofur
anµ
g/L
U.S
.26
ND
ND
ND
POSTFLIGHT SCIENCE REPORT SAUER
4-57
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Vola
tile
Org
anic
s con
td.
Tolu
ene
µg/
LU
.S.
260.
1N
D2.
7Tr
ichlo
roet
hene
µg/
LU
.S.
5EP
A26
ND
ND
ND
m&p
-Xyl
ene
µg/
LU
.S.
Tota
l Xyl
enes
EPA
260.
0N
D0.
510
000
o-Xy
lene
µg/
LU
.S.
Tota
l Xyl
enes
EPA
26N
DN
DN
D10
000
Extr
acta
ble
Org
anic
sAc
etop
heno
neµ
g/L
U.S
.27
2.5
ND
41.0
2-Am
inon
apht
hale
neµ
g/L
U.S
.27
0.0
ND
0.5
Anili
neµ
g/L
U.S
.27
0.1
ND
0.9
Azob
enze
neµ
g/L
U.S
.27
ND
ND
ND
2,2'
-Azo
bis-
isobu
tyro
nitri
leµ
g/L
U.S
.27
ND
ND
ND
Benz
alde
hyde
µg/
LU
.S.
270.
3N
D2.
8Be
nzoi
c acid
µg/
LU
.S.
270.
2N
D4.
6Be
nzot
hiaz
ole
µg/
LU
.S.
2710
.1N
D11
0.7
Benz
yl al
coho
lµ
g/L
U.S
.27
1.3
ND
8.2
Benz
yl bu
tyl p
hthl
ate
µg/
LU
.S.
7000
EPA
DW
EL27
0.3
ND
3.8
2-Bu
toxy
etha
nol
µg/
LU
.S.
27N
DN
DN
D2-
(2-B
utox
yeth
oxy)
etha
nol
µg/
LU
.S.
270.
0N
D0.
52-
(2-B
utox
yeth
oxy)
ethy
l ace
tate
µg/
LU
.S.
27N
DN
DN
Dn-
Buty
lpal
mita
teµ
g/L
U.S
.27
ND
ND
ND
Buty
late
d hyd
roxy
aniso
le (B
HA)
µg/
LU
.S.
270.
1N
D3.
5N
-But
ylbe
nzen
esul
fona
mid
eµ
g/L
U.S
.27
0.3
ND
2.7
3-te
rt-Bu
tylp
heno
lµ
g/L
U.S
.27
4.2
ND
113.
4Ca
ffein
eµ
g/L
U.S
.27
ND
ND
ND
Capr
olac
tam
µg/
LU
.S.
271.
1N
D27
.4tri
s-2-
Chlo
roet
hyl p
hosp
hate
µg/
LU
.S.
270.
3N
D5.
8o-
Cres
ol (2
-Met
hylp
heno
l)µ
g/L
U.S
.27
ND
ND
ND
Cyclo
dode
cane
µg/
LU
.S.
275.
4N
D14
6.4
Cyclo
hexa
none
µg/
LU
.S.
270.
0N
D0.
4D
ecam
ethy
lcyclo
pent
asilo
xane
µg/
LU
.S.
270.
4N
D5.
61,
4 D
iace
tylb
enze
neµ
g/L
U.S
.27
0.2
ND
5.6
SAUER POSTFLIGHT SCI ENCE REPORT
4-58
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Extr
acta
ble
Org
anic
s con
td.
1,3-
Dich
loro
benz
ene
µg/
LU
.S.
600
EPA
270.
1N
D1.
41,
4-D
ichlo
robe
nzen
eµ
g/L
U.S
.75
EPA
270.
0N
D0.
9D
i-n-b
utyl
amin
eµ
g/L
U.S
.27
ND
ND
ND
Dia
llyl P
htha
late
µg/
LU
.S.
27N
DN
DN
DD
i-n-b
utyl
phth
alat
eµ
g/L
U.S
.40
00EP
A D
WEL
2714
.4N
D29
6.7
N,N
-Dib
utyl
form
amid
eµ
g/L
U.S
.27
0.3
ND
8.8
2,6-
Di-t
-but
yl-1
,4-b
enzo
quin
one
µg/
LU
.S.
270.
2N
D3.
73,
5-D
i-t-b
utyl
-4-h
ydro
xybe
nzal
dehy
deµ
g/L
U.S
.27
0.0
ND
0.1
2,6-
Di-t
-but
yl-4
-met
hylp
heno
lµ
g/L
U.S
.27
0.6
ND
15.8
2,4-
Di-t
-but
ylph
enol
µg/
LU
.S.
270.
1N
D1.
3D
icyclo
hexy
lµ
g/L
U.S
.27
ND
ND
ND
N,N
-Die
thyl
form
amid
eµ
g/L
U.S
.27
1.1
ND
30.9
N,N
-Die
thyl
-m-to
luam
ide
µg/
LU
.S.
270.
0N
D0.
5D
ieth
ylen
e gly
col d
i-n-b
utyl
ethe
rµ
g/L
U.S
.27
ND
ND
ND
Die
thyl
ene g
lyco
l mon
oeth
yl et
her
µg/
LU
.S.
270.
9N
D25
.0D
ieth
yl ph
thal
ate
µg/
LU
.S.
5000
EPA
HA
270.
3N
D3.
4D
iisop
ropy
l Adi
pate
µg/
LU
.S.
270.
1N
D0.
9N
,N-D
imet
hyla
ceta
mid
eµ
g/L
U.S
.27
1.6
ND
43.9
N,N
-Dim
ethy
lben
zyla
min
eµ
g/L
U.S
.27
0.1
ND
2.1
Dim
ethy
lcarb
amyl
chlo
ride
µg/
LU
.S.
270.
3N
D3.
2N
,N-D
imet
hylfo
rmam
ide
µg/
LU
.S.
27N
DN
DN
DD
imet
hyl p
htha
late
µg/
LU
.S.
27N
DN
DN
DD
imet
hylth
ioca
rbam
oyl c
hlor
ide
µg/
LU
.S.
27N
DN
DN
DD
ipro
pyle
ne gl
ycol
met
hyl e
ther
µg/
LU
.S.
27N
DN
DN
DD
odec
amet
hylcy
clohe
xasil
oxan
eµ
g/L
U.S
.27
0.1
ND
1.4
Dod
ecan
oic a
cidµ
g/L
U.S
.27
ND
ND
ND
Eico
sane
µg/
LU
.S.
270.
1N
D2.
02-
Etho
xyet
hano
lµ
g/L
U.S
.27
0.3
ND
7.7
2-Et
hylh
exan
oic a
cidµ
g/L
U.S
.27
0.1
ND
3.9
2-Et
hyl-1
-hex
anol
µg/
LU
.S.
270.
8N
D12
.8bi
s-2-
Ethy
lhex
yl ad
ipat
eµ
g/L
U.S
.40
0EP
A27
0.0
ND
0.5
bis-
2-Et
hylh
exyl
phth
alat
e (D
ioct
yl ph
thla
te)
µg/
LU
.S.
6EP
A H
A27
2.0
ND
27.9
POSTFLIGHT SCIENCE REPORT SAUER
4-59
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Extr
acta
ble
Org
anic
s con
td.
4-Et
hylm
orph
olin
eµ
g/L
U.S
.27
1.2
ND
31.8
4-Et
hylp
heno
lµ
g/L
U.S
.27
ND
ND
ND
1-Fo
rmyl
pipe
ridin
eµ
g/L
U.S
.27
ND
ND
ND
Hen
eico
sane
µg/
LU
.S.
270.
2N
D5.
42-
Hep
tano
neµ
g/L
U.S
.27
0.0
ND
0.4
Hex
anoi
c acid
µg/
LU
.S.
27N
DN
DN
D2-
Hex
anol
µg/
LU
.S.
27N
DN
DN
DH
exan
amid
eµ
g/L
U.S
.27
ND
ND
ND
Hyd
rocin
nam
ic ac
idµ
g/L
U.S
.27
ND
ND
ND
2-H
ydro
xybe
nzot
hiaz
ole
µg/
LU
.S.
271.
2N
D6.
8In
dole
µg/
LU
.S.
270.
0N
D0.
3Iso
phor
one
µg/
LU
.S.
27N
DN
DN
DLi
mon
ene
µg/
LU
.S.
270.
0N
D0.
8p-
Men
th-1
-en-
8-ol
(alp
ha-T
erpi
neol
)µ
g/L
U.S
.27
0.9
ND
24.5
Men
thol
µg/
LU
.S.
27N
DN
DN
DM
enth
one
µg/
LU
.S.
27N
DN
DN
D2-
Mer
capt
oben
zoth
iazo
leµ
g/L
U.S
.27
4.2
ND
41.8
2,2'
-Met
hyle
nebi
s(6-
t-but
yl-4
-eth
ylph
enol
)µ
g/L
U.S
.27
ND
ND
ND
3-M
ethy
l-2-c
yclo
hexe
n-1-
one
µg/
LU
.S.
270.
2N
D6.
1M
ethy
l-4-h
ydro
xybe
nzoa
teµ
g/L
U.S
.27
0.2
ND
5.1
3-M
ethy
lindo
leµ
g/L
U.S
.27
ND
ND
ND
2-M
ethy
l-2,4
-pen
tane
diol
µg/
LU
.S.
27N
DN
DN
D4-
Met
hylp
heno
lµ
g/L
U.S
.27
0.0
ND
0.1
2-M
ethy
lpyr
azin
eµ
g/L
U.S
.27
0.2
ND
6.1
1-M
ethy
l-2-p
yrro
lidin
one
µg/
LU
.S.
270.
5N
D11
.4M
ethy
l sul
fone
µg/
LU
.S.
270.
0N
D0.
62-
Met
hylth
iobe
nzot
hiaz
ole
µg/
LU
.S.
274.
9N
D48
.5M
onom
ethy
l pht
hala
teµ
g/L
U.S
.27
0.2
ND
5.0
Neo
men
thol
µg/
LU
.S.
27N
DN
DN
DN
icotin
eµ
g/L
U.S
.27
ND
ND
ND
Non
adec
ane
µg/
LU
.S.
27N
DN
DN
DO
ctad
ecan
olµ
g/L
U.S
.27
0.4
ND
8.8
SAUER POSTFLIGHT SCI ENCE REPORT
4-60
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Extr
acta
ble
Org
anic
s con
td.
Oct
amet
hylcy
clote
trasil
oxan
eµ
g/L
U.S
.27
0.1
ND
1.0
Oct
anoi
c Acid
µg/
LU
.S.
270.
1N
D2.
64-
t-Oct
ylph
enol
µg/
LU
.S.
27N
DN
DN
DO
xindo
leµ
g/L
U.S
.27
ND
ND
ND
Pent
acos
ane
µg/
LU
.S.
270.
2N
D3.
7s-
Phen
ethy
l alco
hol
µg/
LU
.S.
270.
3N
D8.
4Ph
enol
µg/
LU
.S.
1/40
00N
ASA/
EPA
HA
270.
9N
D6.
0bi
s-Ph
enol
Aµ
g/L
U.S
.27
ND
ND
ND
Phen
oxya
cetic
acid
µg/
LU
.S.
27N
DN
DN
D2-
Phen
oxye
than
olµ
g/L
U.S
.27
ND
ND
ND
N-P
heny
l-2-n
apht
hyla
min
eµ
g/L
U.S
.27
1.6
ND
13.1
2-Ph
enyl
acet
ic Ac
idµ
g/L
U.S
.27
0.3
ND
7.6
Phen
ylet
hyl a
lcoho
lµ
g/L
U.S
.27
ND
ND
ND
2-Ph
enyl
phen
olµ
g/L
U.S
.27
0.1
ND
3.2
2-Ph
enyl
-2-p
ropa
nol
µg/
LU
.S.
271.
1N
D30
.6Ph
enyl
sulfo
neµ
g/L
U.S
.27
2.8
ND
75.1
Phth
alid
eµ
g/L
U.S
.27
0.1
ND
2.8
Salic
yclic
Acid
µg/
LU
.S.
27N
DN
DN
DSq
uale
neµ
g/L
U.S
.27
0.0
ND
1.2
1-Te
trade
cano
lµ
g/L
U.S
.27
0.6
ND
6.2
Tetra
met
hylsu
ccin
onitr
ileµ
g/L
U.S
.27
1.2
ND
31.7
Tetra
met
hylth
iour
eaµ
g/L
U.S
.27
1.3
ND
24.6
Tetra
met
hylu
rea
µg/
LU
.S.
270.
2N
D6.
0Th
ymol
µg/
LU
.S.
230.
0N
D0.
1o-
Tolu
ic ac
idµ
g/L
U.S
.27
ND
ND
ND
1,3,
5-Tr
ially
l-1,3
,5-tr
iazin
e-µ
g/L
U.S
.27
ND
ND
ND
2,4
,6(1
H,3
H,5
H)-t
rione
Trico
sane
µg/
LU
.S.
270.
0N
D0.
5Tr
ibut
yl Ph
osph
ate
µg/
LU
.S.
27N
DN
DN
DTr
ieth
yl Ph
osph
ate
µg/
LU
.S.
270.
2N
D4.
6Tr
ieth
ylam
ine
µg/
LU
.S.
270.
4N
D11
.8
POSTFLIGHT SCIENCE REPORT SAUER
4-61
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Extr
acta
ble
Org
anic
s con
td.
2,2,
4-Tr
imet
hyl-
µg/
LU
.S.
270.
0N
D0.
1 1
,3-p
enta
nedi
ol di
isobu
tyra
teU
ndec
anoi
c Acid
µg/
LU
.S.
270.
2N
D5.
82-
Und
ecan
one
µg/
LU
.S.
27N
DN
DN
DU
reth
ane
µg/
LU
.S.
270.
6N
D2.
8Va
nilli
nµ
g/L
U.S
.27
0.1
ND
2.3
Alco
hols
(DAI
/GC/
MS)
1-Bu
tano
lµ
g/L
U.S
.29
ND
ND
ND
Etha
nol
µg/
LU
.S.
2912
8.83
ND
2447
.0M
etha
nol
µg/
LU
.S.
2916
.86
ND
489.
01-
Met
hoxy
-2-p
ropa
nol
µg/
LU
.S.
29N
DN
DN
D2-
Met
hyl-2
-but
anol
µg/
LU
.S.
29N
DN
DN
D2-
Met
hyl-2
-pro
pano
lµ
g/L
U.S
.29
ND
ND
ND
1-Pr
opan
olµ
g/L
U.S
.29
ND
ND
ND
2-Pr
opan
olµ
g/L
U.S
.29
ND
ND
ND
Alco
hols
/Ace
tone
Acet
one
µg/
LRu
ssia
1138
0.0
ND
3500
.0Bu
tano
lµ
g/L
Russ
ia5
ND
ND
ND
Etha
nol
µg/
LRu
ssia
1122
.7N
D25
0.0
Isoam
yl al
coho
lµ
g/L
Russ
ia11
ND
ND
ND
Met
hano
lµ
g/L
Russ
ia5
ND
ND
ND
Prop
anol
µg/
LRu
ssia
1181
.8N
D90
0.0
Gly
cols
(DAI
/GC/
MS)
1,2-
Etha
nedi
olµ
g/L
U.S
.70
00EP
A H
A25
1821
.2N
D45
530.
01,
2-Pr
opan
edio
lµ
g/L
U.S
.25
ND
ND
ND
1,2-
Etha
nedi
olµ
g/L
Russ
ia70
00EP
A H
A11
ND
ND
ND
1,2-
Prop
aned
iol
µg/
LRu
ssia
812
37.5
ND
3700
.0O
rgan
ic A
cids
(SPE
/GC/
MS)
Acet
ic ac
idµ
g/L
U.S
.7
ND
ND
ND
Acet
ic ac
idµ
g/L
Russ
ia11
381.
8N
D22
00.0
Lact
ic ac
idµ
g/L
U.S
.7
ND
ND
ND
Prop
ioni
c acid
µg/
LU
.S.
7N
DN
DN
D
SAUER POSTFLIGHT SCI ENCE REPORT
4-62
TABL
E 3
. SU
MM
AR
Y O
F R
EGEN
ERA
TED
WA
TER
RES
ULT
SM
issi
onM
ir 1
8-25
Mir
18-
25M
ir 1
8-25
Mir
18-
25Sa
mpl
e Lo
catio
nM
axim
umM
axim
umN
umbe
rM
ean
Min
imum
Max
imum
Sam
ple
Des
crip
tion
Test
Cont
amin
ant
Cont
amin
ant
of Sa
mpl
es(X
)Sa
mpl
e D
ate
Cond
ucte
dLe
vel
Leve
lAn
alyz
edAn
alys
is/S
ampl
e ID
Uni
tsby
(MCL
)So
urce
(n)
Alde
hyde
sAc
etal
dehy
deµ
g/L
U.S
.1
ND
ND
ND
Form
alde
hyde
µg/
LU
.S.
1000
EPA
HA
277.
5N
D63
.4Ca
rbox
ylat
es (C
E)Ac
etat
em
g/L
U.S
.29
0.1
ND
1.5
Buty
rate
mg/
LU
.S.
0N
AN
AN
AFo
rmat
em
g/L
U.S
.29
2.5
ND
29.1
Gly
cola
tem
g/L
U.S
.29
ND
ND
<0.
25G
lyox
ylat
em
g/L
U.S
.29
ND
ND
<0.
25La
ctat
em
g/L
U.S
.29
ND
ND
<0.
25Pr
opio
nate
mg/
LU
.S.
29N
DN
D<
0.25
Oxa
late
mg/
LU
.S.
29N
DN
D<
0.25
Amin
es (C
E)Et
hyla
min
em
g/L
U.S
.29
ND
ND
<0.
25M
ethy
lam
ine
mg/
LU
.S.
29N
DN
D<
0.63
Prop
ylam
ine
mg/
LU
.S.
290.
0N
D0.
3Tr
imet
hyla
min
em
g/L
U.S
.29
ND
ND
< 0
.25
Ure
am
g/L
U.S
.27
0.0
ND
1.1
Org
anic
Car
bon
Reco
very
perc
ent
U.S
.27
14.2
0.1
76.3
NA
= n
ot an
alyz
edN
D =
not
dete
cted
DW
EL =
drin
king
wat
er eq
uiva
lent
leve
lH
A =
hea
lth ad
viso
ry
POSTFLIGHT SCIENCE REPORT SAUER
4-63
TTTTAAAABBBBLLLLEEEE 4444.... SSSSUUUUMMMMMMMMAAAARRRRYYYY OOOOFFFF SSSSTTTTOOOORRRREEEEDDDD WWWWAAAATTTTEEEERRRR RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Conductivity µS/cm U.S. 7 238.1 177.0 322.0Conductivity µS/cm Russia 6 202.0 171.0 280.0pH pH units U.S. 7 7.3 7.0 7.7pH pH units Russia 6 7.4 7.0 8.2Turbidity NTU U.S. 6 5.7 1.7 8.3Turbidity mg/L Russia 2 0.0 0.0 0.0Color True degrees Russia 3 10.0 10.0 10.0Odor at 20oC grade Russia 4 0.3 0.0 1.0Taste at 20oC grade Russia 0 NA NA NATotal Solids mg/L Russia 0 NA NA NATotal Hardness meq/L Russia 6 2.0 1.4 2.3Chemical Oxygen Demand mg O2/L Russia 6 43.8 10.5 105.0Anions (CE/IC)Bromide mg/L U.S. 7 ND ND <0.50Chloride mg/L U.S. 8 6.4 ND 13.3Fluoride mg/L U.S. 8 0.4 ND 2.1Nitrate as Nitrogen (NO3-N) mg/L U.S. 8 1.0 ND 6.5Nitrite as Nitrogen (NO2-N) mg/L U.S. 8 ND ND <0.08Phosphate as P (PO4-P) mg/L U.S. 8 0.0 ND 0.1Sulfate mg/L U.S. 8 10.6 ND 29.9Cations (CE/IC)Ammonia as Nitrogen (NH3-N) mg/L U.S. 8 0.0 ND 0.0Calcium mg/L U.S. 8 33.4 23.3 41.7Lithium mg/L U.S. 8 0.0 ND 0.0Magnesium mg/L U.S. 8 7.9 4.2 11.9Potassium mg/L U.S. 8 1.3 ND 2.5Sodium mg/L U.S. 8 4.2 0.5 7.5MineralsAmmonium (NH4) mg/L Russia 5 0.1 <0.001 0.3Calcium mg/L Russia 3 16.9 <0.001 30.0Magnesium mg/L Russia 3 3.2 <0.001 4.8MetalsCalcium µg/L U.S. 0 NA NA NAMagnesium µg/L U.S. 0 NA NA NASodium µg/L U.S. 0 NA NA NAPotassium µg/L U.S. 0 NA NA NASilver µg/L U.S. 8 388.3 77.0 889.0Silver ion µg/L Russia 4 107.8 1.0 180.0Aluminum µg/L U.S. 5 137.0 1.5 620.0Arsenic µg/L U.S. 7 0.3 ND 1.1Barium µg/L U.S. 7 24.4 2.2 44.1Cadmium µg/L U.S. 7 14.3 <1 43.6Chromium µg/L U.S. 7 0.1 ND 0.4Cobalt µg/L U.S. 5 ND ND NDCopper µg/L U.S. 7 4.9 ND 21.0Iron µg/L U.S. 7 156.7 4.2 290.0Mercury µg/L U.S. 5 ND ND <0.5Manganese µg/L U.S. 7 15.6 ND 62.7
SAUER POSTFLIGHT SCI ENCE REPORT
4-64
TTTTAAAABBBBLLLLEEEE 4444.... SSSSUUUUMMMMMMMMAAAARRRRYYYY OOOOFFFF SSSSTTTTOOOORRRREEEEDDDD WWWWAAAATTTTEEEERRRR RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Metals contd.Molybdenum µg/L U.S. 3 ND ND NDNickel µg/L U.S. 7 37.9 1.2 79.3Lead µg/L U.S. 7 0.2 ND 1.1Selenium µg/L U.S. 7 ND ND NDZinc µg/L U.S. 7 119.4 29.4 549.0Palladium µg/L U.S. 0 NA NA NASilicon µg/L U.S. 0 NA NA NATungsten µg/L U.S. 0 NA NA NATotal Organic CarbonTIC (OI 1010) mg/L U.S. 4 17.9 3.6 30.0POC (OI 1010) mg/L U.S. 0 NA NA NANPOC (OI 1010) mg/L U.S. 4 14.3 8.4 30.5TOC (OI 1010) mg/L U.S. 0 NA NA NATIC (Sievers 800) mg/L U.S. 7 18.6 6.9 31.8TOC (Sievers 800) mg/L U.S. 7 19.0 7.0 54.8TOC (Sievers 800) mg/L Russia 3 19.2 7.5 30.2Volatile Organics Acetaldehyde µg/L U.S. 7 433.4 ND 3034.0Acetone µg/L U.S. 8 71.4 ND 230.2Acryloniltrile µg/L U.S. 8 ND ND NDAllyl chloride ND U.S. 8 ND ND NDBenzene µg/L U.S. 8 ND ND NDBromobenzene µg/L U.S. 8 ND ND NDBromochloromethane µg/L U.S. 8 ND ND NDBromodichloromethane µg/L U.S. 8 2.6 ND 9.0Bromoform µg/L U.S. 8 ND ND NDBromomethane µg/L U.S. 8 ND ND ND2-Butanone µg/L U.S. 8 4.4 ND 35.4n-Butylbenzene µg/L U.S. 8 ND ND NDs-Butylbenzene µg/L U.S. 8 ND ND NDt-Butylbenzene µg/L U.S. 8 ND ND NDCarbon disulfide µg/L U.S. 8 0.2 ND 1.4Carbon tetrachloride µg/L U.S. 8 ND ND NDChloroacetonitrile µg/L U.S. 8 ND ND NDChlorobenzene µg/L U.S. 8 ND ND ND1-Chlorobutane µg/L U.S. 8 ND ND NDChloroethane µg/L U.S. 8 ND ND NDChloroform µg/L U.S. 8 81.2 ND 243.6Chloromethane µg/L U.S. 8 ND ND ND2-Chlorotoluene µg/L U.S. 8 ND ND ND4-Chlorotoluene µg/L U.S. 8 ND ND NDDibromochloromethane µg/L U.S. 8 ND ND ND1,2-Dibromo-3-chloropropane µg/L U.S. 8 ND ND ND1,2-Dibromoethane µg/L U.S. 8 ND ND NDDibromomethane µg/L U.S. 8 ND ND ND1,2-Dichlorobenzene µg/L U.S. 8 ND ND ND1,3-Dichlorobenzene µg/L U.S. 8 ND ND ND
POSTFLIGHT SCIENCE REPORT SAUER
4-65
TTTTAAAABBBBLLLLEEEE 4444.... SSSSUUUUMMMMMMMMAAAARRRRYYYY OOOOFFFF SSSSTTTTOOOORRRREEEEDDDD WWWWAAAATTTTEEEERRRR RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Volatile Organics contd.1,4-Dichlorobenzene µg/L U.S. 8 ND ND NDtrans-1,4-dichloro-2-butene µg/L U.S. 8 ND ND NDDichlorodifluoromethane µg/L U.S. 8 ND ND ND1,1-Dichloroethane µg/L U.S. 8 ND ND ND1,2-Dichloroethane µg/L U.S. 8 ND ND ND1,1-Dichloroethene µg/L U.S. 8 ND ND NDcis1,2-dichloroethene µg/L U.S. 8 ND ND NDtrans-1,2-dichloroethene µg/L U.S. 8 ND ND ND1,2-Dichloropropane µg/L U.S. 8 ND ND ND1,3-Dichloropropane µg/L U.S. 8 ND ND ND2,2-Dichloropropane µg/L U.S. 8 ND ND ND1,2-Dichloropropene µg/L U.S. 8 ND ND NDcis-1,3-Dichloropropene µg/L U.S. 8 ND ND NDtrans-1,3-Dichloropropene µg/L U.S. 8 ND ND NDDiethyl ether µg/L U.S. 8 ND ND NDEthylbenzene µg/L U.S. 8 ND ND NDEthyl methacylate µg/L U.S. 8 ND ND NDHexachlorobutadiene µg/L U.S. 8 ND ND NDHexachloroethane µg/L U.S. 8 ND ND ND2-Hexanone µg/L U.S. 8 ND ND NDIodomethane µg/L U.S. 8 ND ND NDIsopropylbenzene µg/L U.S. 8 ND ND ND4-Isopropyltoluene µg/L U.S. 8 ND ND NDLinolool µg/L U.S. 8 ND ND NDMethacrylonitrile µg/L U.S. 8 ND ND NDMethylacrylate µg/L U.S. 8 ND ND NDMethyl-t-butylether µg/L U.S. 8 ND ND NDMethylene chloride µg/L U.S. 8 0.7 ND 3.8Methylmethacrylate µg/L U.S. 8 ND ND ND4-Methyl-2-pentanone µg/L U.S. 8 ND ND NDalpha-Methyl styrene µg/L U.S. 8 ND ND NDPentachloroethane µg/L U.S. 8 ND ND NDPerfluoro-1,3- µg/L U.S. 8 ND ND ND dimethylcyclohexaneTetrahydrofuran µg/L U.S. 8 1.9 ND 14.8Toluene µg/L U.S. 8 1.5 ND 11.9Trichloroethene µg/L U.S. 8 ND ND NDm&p-Xylene µg/L U.S. 8 ND ND NDo-Xylene µg/L U.S. 8 ND ND NDExtractable Organics Acetophenone µg/L U.S. 8 0.2 ND 1.62-Aminonaphthalene µg/L U.S. 8 ND ND NDAniline µg/L U.S. 8 ND ND NDAzobenzene µg/L U.S. 8 ND ND ND2,2'-Azobis-isobutyronitrile µg/L U.S. 8 ND ND NDBenzaldehyde µg/L U.S. 8 0.6 ND 4.9Benzoic acid µg/L U.S. 8 ND ND ND
SAUER POSTFLIGHT SCI ENCE REPORT
4-66
TTTTAAAABBBBLLLLEEEE 4444.... SSSSUUUUMMMMMMMMAAAARRRRYYYY OOOOFFFF SSSSTTTTOOOORRRREEEEDDDD WWWWAAAATTTTEEEERRRR RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.Benzothiazole µg/L U.S. 8 1.4 ND 6.9Benzyl alcohol µg/L U.S. 8 13.2 ND 62.4Benzyl butyl phthlate µg/L U.S. 8 0.9 ND 4.72-Butoxyethanol µg/L U.S. 8 ND ND ND2-(2-Butoxyethoxy)ethanol µg/L U.S. 8 0.2 ND 1.92-(2-Butoxyethoxy)ethyl acetate µg/L U.S. 8 ND ND NDn-Butylpalmitate µg/L U.S. 8 ND ND NDButylated hydroxyanisole (BHA) µg/L U.S. 8 ND ND NDN-Butylbenzenesulfonamide µg/L U.S. 8 0.5 ND 2.23-tert-Butylphenol µg/L U.S. 8 0.1 ND 0.8Caffeine µg/L U.S. 8 ND ND NDCaprolactam µg/L U.S. 8 107.4 ND 576.7tris-2-Chloroethyl phosphate µg/L U.S. 8 ND ND NDo-Cresol (2-Methylphenol) µg/L U.S. 8 ND ND NDCyclododecane µg/L U.S. 8 ND ND NDCyclohexanone µg/L U.S. 8 ND ND NDDecamethylcyclopentasiloxane µg/L U.S. 8 0.8 ND 3.21,4 Diacetylbenzene µg/L U.S. 8 ND ND ND1,3- Dichlorobenzene µg/L U.S. 8 ND ND ND1,4-Dichlorobenzene µg/L U.S. 8 ND ND NDDi-n-butylamine µg/L U.S. 8 ND ND NDDiallyl Phthalate µg/L U.S. 8 ND ND NDDi-n-butyl phthalate µg/L U.S. 8 0.4 ND 1.8N,N-Dibutylformamide µg/L U.S. 8 0.2 ND 1.62,6-Di-t-butyl-1,4-benzoquinone µg/L U.S. 8 ND ND ND3,5-Di-t-butyl- µg/L U.S. 8 ND ND ND 4-hydroxybenzaldehyde2,6-Di-t-butyl-4-methylphenol µg/L U.S. 8 ND ND ND2,4-Di-t-butylphenol µg/L U.S. 8 0.1 ND 0.8Dicyclohexyl µg/L U.S. 8 ND ND NDN,N-Diethylformamide µg/L U.S. 8 ND ND NDN,N-Diethyl-m-toluamide µg/L U.S. 8 ND ND NDDiethylene glycol di-n-butyl ether µg/L U.S. 8 ND ND NDDiethylene glycol monoethyl ether µg/L U.S. 8 0.4 ND 3.2Diethyl phthalate µg/L U.S. 8 1.8 ND 6.6Diisopropyl Adipate µg/L U.S. 8 ND ND NDN,N-Dimethylacetamide µg/L U.S. 8 0.7 ND 5.9N,N-Dimethylbenzylamine µg/L U.S. 8 ND ND NDDimethylcarbamyl chloride µg/L U.S. 8 0.2 ND 1.6N,N-Dimethylformamide µg/L U.S. 8 ND ND NDDimethyl phthalate µg/L U.S. 8 0.2 ND 0.8Dimethylthiocarbamoyl chloride µg/L U.S. 8 ND ND NDDipropylene glycol methyl ether µg/L U.S. 8 ND ND NDDodecamethylcyclohexasiloxane µg/L U.S. 8 0.0 ND 0.2Dodecanoic acid µg/L U.S. 8 ND ND NDEicosane µg/L U.S. 8 ND ND ND2-Ethoxyethanol µg/L U.S. 8 ND ND ND
POSTFLIGHT SCIENCE REPORT SAUER
4-67
TTTTAAAABBBBLLLLEEEE 4444.... SSSSUUUUMMMMMMMMAAAARRRRYYYY OOOOFFFF SSSSTTTTOOOORRRREEEEDDDD WWWWAAAATTTTEEEERRRR RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.2-Ethylhexanoic acid µg/L U.S. 8 2.1 ND 16.62-Ethyl-1-hexanol µg/L U.S. 8 3.1 ND 20.2bis-2-Ethylhexyl adipate µg/L U.S. 8 0.1 ND 0.7bis-2-Ethylhexyl phthalate µg/L U.S. 8 0.3 ND 2.0 (Dioctyl phthlate)4-Ethylmorpholine µg/L U.S. 8 ND ND ND4-Ethylphenol µg/L U.S. 8 ND ND ND1-Formylpiperidine µg/L U.S. 8 ND ND NDHeneicosane µg/L U.S. 8 ND ND ND2-Heptanone µg/L U.S. 8 ND ND NDHexanoic acid µg/L U.S. 8 ND ND ND2-Hexanol µg/L U.S. 8 ND ND NDHexanamide µg/L U.S. 8 ND ND NDHydrocinnamic acid µg/L U.S. 8 ND ND ND4-Hydroxy-4-methyl-2-pentanone µg/L U.S. 8 ND ND ND2-Hydroxybenzothiazole µg/L U.S. 8 0.4 ND 2.9Indole µg/L U.S. 8 ND ND NDIsophorone µg/L U.S. 8 ND ND NDIsophorone µg/L U.S. 8 ND ND NDLimonene µg/L U.S. 8 ND ND NDp-Menth-1-en-8-ol µg/L U.S. 8 ND ND ND (alpha-Terpineol)Menthol µg/L U.S. 8 ND ND NDMenthone µg/L U.S. 8 ND ND ND2-Mercaptobenzothiazole µg/L U.S. 8 ND ND ND2,2'-Methylenebis µg/L U.S. 8 ND ND ND (6-t-butyl-4-ethylphenol) 3-Methyl-2-cyclohexen-1-one µg/L U.S. 8 ND ND NDMethyl-4-hydroxybenzoate µg/L U.S. 8 ND ND ND3-Methylindole µg/L U.S. 8 ND ND ND2-Methyl-2,4-pentanediol µg/L U.S. 8 ND ND ND4-Methylphenol µg/L U.S. 8 ND ND ND2-Methylpyrazine µg/L U.S. 8 ND ND ND1-Methyl-2-pyrrolidinone µg/L U.S. 8 0.4 ND 3.0Methyl sulfone µg/L U.S. 8 ND ND ND2-Methylthiobenzothiazole µg/L U.S. 8 0.4 ND 1.3Monomethyl phthalate µg/L U.S. 8 0.7 ND 5.7Neomenthol µg/L U.S. 8 ND ND NDNicotine µg/L U.S. 8 ND ND NDNonadecane µg/L U.S. 8 ND ND NDOctadecanol µg/L U.S. 8 ND ND NDOctamethylcyclotetrasiloxane µg/L U.S. 8 ND ND NDOctanoic Acid µg/L U.S. 8 ND ND ND4-t-Octylphenol µg/L U.S. 8 0.0 ND 0.1Oxindole µg/L U.S. 8 ND ND NDPentacosane µg/L U.S. 8 3.4 ND 26.7s-Phenethyl alcohol µg/L U.S. 8 ND ND ND
SAUER POSTFLIGHT SCI ENCE REPORT
4-68
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.Phenol µg/L U.S. 8 5.4 ND 24.8bis-Phenol A µg/L U.S. 8 ND ND NDPhenoxyacetic acid µg/L U.S. 8 ND ND ND2-Phenoxyethanol µg/L U.S. 8 ND ND NDN-Phenyl-2-naphthylamine µg/L U.S. 8 0.3 ND 2.52-Phenylacetic Acid µg/L U.S. 8 ND ND NDPhenylethyl alcohol µg/L U.S. 8 ND ND ND2-Phenylphenol µg/L U.S. 8 ND ND ND2-Phenyl-2-propanol µg/L U.S. 8 0.3 ND 1.2Phenyl sulfone µg/L U.S. 8 ND ND NDPhthalide µg/L U.S. 8 ND ND NDSalicyclic Acid µg/L U.S. 8 ND ND NDSqualene µg/L U.S. 8 ND ND ND1-Tetradecanol µg/L U.S. 8 ND ND NDTetramethylsuccinonitrile µg/L U.S. 8 ND ND NDTetramethylthiourea µg/L U.S. 8 ND ND NDTetramethylurea µg/L U.S. 8 ND ND NDThymol µg/L U.S. 8 ND ND NDo-Toluic acid µg/L U.S. 8 ND ND ND1,3,5-Triallyl-1,3,5-triazine- µg/L U.S. 8 ND ND ND 2,4,6(1H,3H,5H)-trioneTricosane µg/L U.S. 8 3.0 ND 23.6Tributyl Phosphate µg/L U.S. 8 0.1 ND 1.1Triethyl Phosphate µg/L U.S. 8 ND ND NDTriethylamine µg/L U.S. 8 ND ND ND2,2,4-Trimethyl- µg/L U.S. 8 0.3 ND 2.3 1,3-pentanediol diisobutyrateUndecanoic Acid µg/L U.S. 8 ND ND ND2-Undecanone µg/L U.S. 8 ND ND NDUrethane µg/L U.S. 8 ND ND NDVanillin µg/L U.S. 8 ND ND NDAlcohols (DAI/GC/MS)1-Butanol µg/L U.S. 8 ND ND NDEthanol µg/L U.S. 8 14457.1 ND 86642.0Methanol µg/L U.S. 8 ND ND ND1-Methoxy-2-propanol µg/L U.S. 8 ND ND ND2-Methyl-2-butanol µg/L U.S. 8 ND ND ND2-Methyl-2-propanol µg/L U.S. 8 ND ND ND1-Propanol µg/L U.S. 8 ND ND ND2-Propanol µg/L U.S. 8 53.8 ND 430.0Alcohols/AcetoneAcetone µg/L Russia 3 733.3 ND 2200.0Butanol µg/L Russia 0 NA NA NAEthanol µg/L Russia 3 ND ND NDIsoamyl alcohol µg/L Russia 3 666.7 ND 2000.0Methanol µg/L Russia 1 ND ND NDPropanol µg/L Russia 3 300.0 ND 900.0
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Glycols (DAI/GC/MS)1,2-Ethanediol µg/L U.S. 8 ND ND ND1,2-Propanediol µg/L U.S. 8 ND ND ND1,2-Ethanediol µg/L Russia 3 500.0 ND 1500.01,2-Propanediol µg/L Russia 2 4500.0 ND 9000.0Organic Acids (SPE/GC/MS) Acetic acid µg/L U.S. 1 ND ND NDAcetic acid µg/L Russia 3 5400.0 ND 15400.0Lactic acid µg/L U.S. 1 ND ND NDPropionic acid µg/L U.S. 1 ND ND NDAldehydesAcetaldehyde µg/L U.S. 1 71.6 71.6 71.6Formaldehyde µg/L U.S. 8 2.8 ND 12.6Carboxylates (CE)Acetate mg/L U.S. 8 0.0 ND 0.2Butyrate mg/L U.S. 0 NA NA NAFormate mg/L U.S. 8 21.9 ND 73.0Glycolate mg/L U.S. 8 ND ND <0.25Glyoxylate mg/L U.S. 8 ND ND <0.25Lactate mg/L U.S. 8 ND ND <0.25Propionate mg/L U.S. 8 ND ND <0.25Oxalate mg/L U.S. 8 ND ND <0.25Amines (CE)Ethylamine mg/L U.S. 8 ND ND <1.25Methylamine mg/L U.S. 8 ND ND <1.25Propylamine mg/L U.S. 8 ND ND <1.25Trimethylamine mg/L U.S. 8 ND ND <2.5Urea mg/L U.S. 8 ND ND <1.0Organic Carbon Recovery percent U.S. 8 41.9 0.1 102.4NA = not analyzedND = not detectedDWEL = drinking water equivalent levelHA = health advisory
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Preflight Stored Water In-flight Stored WaterParameter Units (Mean Concentration) (Mean Concentration)
Conductivity mS/cm 272.3 238.1pH pH units 7.56 7.3Turbidity NTU 6.66 5.7Chloride mg/L 11.9 6.4Sulfate mg/L 12.4 10.6Calcium mg/L 29.95 33.4Magnesium mg/L 8.78 7.9Potassium mg/L 2 1.3Sodium mg/L 6.14 4.2Aluminum µg/L 22.2 137Barium µg/L 36.2 24.4Silver µg/L 445.8 388.3Iron µg/L 81.82 156.7Manganese µg/L 17.8 15.6Zinc mg/L 6.6 119.4TOC mg/L 7.12 18.6Acetaldehyde mg/L ND 433.4Acetone mg/L 13.3 71.4Chloroform µg/L 113.87 81.2Caprolactam µg/L ND 107.4Formate mg/L ND 21.92-Propanol µg/L ND 53.8Ethanol µg/L 300 14457Organic Carbon Recovery percent 0.27 41.9ND= not detected
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Conductivity µS/cm U.S. 27 244.1 118.0 506.0Conductivity µS/cm Russia 16 258.9 165.0 497.0pH pH units U.S. 27 7.0 6.2 7.7pH pH units Russia 19 7.3 6.3 7.9Turbidity NTU U.S. 22 11.7 4.0 39.5Turbidity mg/L Russia 7 0.8 0.1 2.0Color True degrees Russia 10 12.5 10.0 15.0Odor at 20oC grade Russia 15 2.3 1 3Taste at 20oC grade Russia 0 NA NA NATotal Solids mg/L Russia 0 NA NA NATotal Hardness meq/L Russia 2 1.1 0.3 2.0Chemical Oxygen Demand mg O2/L Russia 20 400.1 90.0 1520.0Anions (CE/IC)Bromide mg/L U.S. 26 ND ND <5.0Chloride mg/L U.S. 28 1.7 ND 16.8Fluoride mg/L U.S. 28 0.1 ND 0.7Nitrate as Nitrogen (NO3-N) mg/L U.S. 28 0.5 ND 8.2Nitrite as Nitrogen (NO2-N) mg/L U.S. 28 0.0 ND 0.3Phosphate as P (PO4-P) mg/L U.S. 28 0.4 ND 9.5Sulfate mg/L U.S. 28 6.3 ND 114.0Cations (CE/IC)Ammonia as Nitrogen (NH3-N) mg/L U.S. 28 25.0 <0.002 48.0Calcium mg/L U.S. 28 1.0 ND 6.1Lithium mg/L U.S. 28 0.3 ND 4.7Magnesium mg/L U.S. 28 0.6 ND 6.6Potassium mg/L U.S. 28 1.8 ND 20.4Sodium mg/L U.S. 28 8.3 ND 123.4MineralsAmmonium (NH4) mg/L Russia 12 43.8 15.7 135.0Calcium mg/L Russia 0 NA NA NAMagnesium mg/L Russia 0 NA NA NAMetalsCalcium µg/L U.S. 0 NA NA NAMagnesium µg/L U.S. 0 NA NA NASodium µg/L U.S. 0 NA NA NAPotassium µg/L U.S. 0 NA NA NASilver µg/L U.S. 26 82.8 ND 982.0Silver ion µg/L Russia 2 0.0 0.0 0.0Aluminum µg/L U.S. 18 47.9 <20 166.0Arsenic µg/L U.S. 23 ND ND <2Barium µg/L U.S. 23 635.7 ND 13920.0Cadmium µg/L U.S. 23 27.4 ND 240.0Chromium µg/L U.S. 23 12.4 ND 161.0Cobalt µg/L U.S. 23 ND ND NDCopper µg/L U.S. 23 16.4 ND 102.0Iron µg/L U.S. 23 107.9 ND 618.0Mercury µg/L U.S. 19 4.9 ND 83.7Manganese µg/L U.S. 23 63.7 ND 336.0
SAUER POSTFLIGHT SCI ENCE REPORT
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Metals contd.Molybdenum µg/L U.S. 16 75.9 ND 618.0Nickel µg/L U.S. 23 1399.9 10.2 14700.0Lead µg/L U.S. 23 40.9 ND 311.0Selenium µg/L U.S. 23 0.5 ND 8.2Zinc µg/L U.S. 23 1260.2 3.5 5334.0Palladium µg/L U.S. 2 12.1 11.5 12.6Silicon µg/L U.S. 0 NA NA NATungsten µg/L U.S. 1 1290.0 1290.0 1290.0Total Organic CarbonTIC (OI 1010) mg/L U.S. 13 21.5 6.3 35.1POC (OI 1010) mg/L U.S. 1 3.9 3.9 3.9NPOC (OI 1010) mg/L U.S. 13 47.7 14.5 97.0TOC (OI 1010) mg/L U.S. 1 18.5 18.5 18.5TIC (Sievers 800) mg/L U.S. 23 28.1 4.9 44.4TOC (Sievers 800) mg/L U.S. 24 118.9 17.6 411.0TOC (Sievers 800) mg/L Russia 11 176.5 49.0 447.0Volatile Organics Acetaldehyde µg/L U.S. 22 353.6 ND 2563.2Acetone µg/L U.S. 28 743.4 ND 10145.0Acryloniltrile µg/L U.S. 28 0.8 ND 22.0Allyl chloride ND U.S. 28 ND ND NDBenzene µg/L U.S. 28 0.2 ND 5.4Bromobenzene µg/L U.S. 28 ND ND NDBromochloromethane µg/L U.S. 28 ND ND NDBromodichloromethane µg/L U.S. 28 ND ND NDBromoform µg/L U.S. 28 ND ND NDBromomethane µg/L U.S. 28 ND ND ND2-Butanone µg/L U.S. 28 4.3 ND 35.2n-Butylbenzene µg/L U.S. 28 ND ND NDs-Butylbenzene µg/L U.S. 28 ND ND NDt-Butylbenzene µg/L U.S. 28 ND ND NDCarbon disulfide µg/L U.S. 28 403.5 ND 2750.9Carbon tetrachloride µg/L U.S. 28 5.4 ND 150.5Chloroacetonitrile µg/L U.S. 28 ND ND NDChlorobenzene µg/L U.S. 28 ND ND ND1-Chlorobutane µg/L U.S. 28 1.6 ND 44.5Chloroethane µg/L U.S. 28 ND ND 0.0Chloroform µg/L U.S. 28 0.4 ND 5.8Chloromethane µg/L U.S. 28 ND ND ND2-Chlorotoluene µg/L U.S. 28 ND ND ND4-Chlorotoluene µg/L U.S. 28 ND ND NDDibromochloromethane µg/L U.S. 28 ND ND ND1,2-Dibromo-3-chloropropane µg/L U.S. 28 ND ND ND1,2-Dibromoethane µg/L U.S. 28 ND ND NDDibromomethane µg/L U.S. 28 ND ND ND1,2-Dichlorobenzene µg/L U.S. 28 ND ND ND1,3-Dichlorobenzene µg/L U.S. 28 ND ND ND
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Volatile Organics contd.1,4-Dichlorobenzene µg/L U.S. 28 ND ND NDtrans-1,4-dichloro-2-butene µg/L U.S. 28 ND ND NDDichlorodifluoromethane µg/L U.S. 28 ND ND ND1,1-Dichloroethane µg/L U.S. 28 ND ND ND1,2-Dichloroethane µg/L U.S. 28 ND ND ND1,1-Dichloroethene µg/L U.S. 28 ND ND NDcis1,2-dichloroethene µg/L U.S. 28 ND ND NDtrans-1,2-dichloroethene µg/L U.S. 28 ND ND ND1,2-Dichloropropane µg/L U.S. 28 ND ND ND1,3-Dichloropropane µg/L U.S. 28 ND ND ND2,2-Dichloropropane µg/L U.S. 28 ND ND ND1,2-Dichloropropene µg/L U.S. 28 ND ND NDcis-1,3-Dichloropropene µg/L U.S. 28 ND ND NDtrans-1,3-Dichloropropene µg/L U.S. 28 ND ND NDDiethyl ether µg/L U.S. 28 0.1 ND 2.1Ethylbenzene µg/L U.S. 28 ND ND NDEthyl methacylate µg/L U.S. 28 ND ND NDHexachlorobutadiene µg/L U.S. 28 ND ND NDHexachloroethane µg/L U.S. 28 ND ND ND2-Hexanone µg/L U.S. 28 ND ND NDIodomethane µg/L U.S. 28 0.0 ND 1.3Isopropylbenzene µg/L U.S. 28 ND ND ND4-Isopropyltoluene µg/L U.S. 28 ND ND NDLinolool µg/L U.S. 28 0.0 ND 1.2Methacrylonitrile µg/L U.S. 28 ND ND NDMethylacrylate µg/L U.S. 28 ND ND NDMethyl-t-butylether µg/L U.S. 28 ND ND NDMethylene chloride µg/L U.S. 28 1011.8 ND 28296.0Methylmethacrylate µg/L U.S. 28 ND ND ND4-Methyl-2-pentanone µg/L U.S. 28 0.1 ND 2.2alpha-Methyl styrene µg/L U.S. 28 0.0 ND 1.0Pentachloroethane µg/L U.S. 28 0.2 ND 6.9Perfluoro-1,3- µg/L U.S. 28 0.5 ND 13.0 dimethylcyclohexaneTetrahydrofuran µg/L U.S. 28 17.5 ND 212.7Toluene µg/L U.S. 28 ND ND NDTrichloroethene µg/L U.S. 28 ND ND NDm&p-Xylene µg/L U.S. 28 ND ND NDo-Xylene µg/L U.S. 28 0.2 ND 3.8Extractable Organics Acetophenone µg/L U.S. 28 24.8 ND 76.42-Aminonaphthalene µg/L U.S. 28 ND ND NDAniline µg/L U.S. 28 ND ND NDAzobenzene µg/L U.S. 28 ND ND ND2,2'-Azobis-isobutyronitrile µg/L U.S. 28 7.4 ND 61.7Benzaldehyde µg/L U.S. 28 26.3 ND 212.4Benzoic acid µg/L U.S. 28 5.7 ND 108.6
SAUER POSTFLIGHT SCI ENCE REPORT
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.Benzothiazole µg/L U.S. 28 81.7 5.1 184.5Benzyl alcohol µg/L U.S. 28 827.9 ND 9633.6Benzyl butyl phthlate µg/L U.S. 28 ND ND ND2-Butoxyethanol µg/L U.S. 28 13.2 ND 111.12-(2-Butoxyethoxy)ethanol µg/L U.S. 28 6.5 ND 76.82-(2-Butoxyethoxy)ethyl acetate µg/L U.S. 28 0.7 ND 20.0n-Butylpalmitate µg/L U.S. 28 ND ND NDButylated hydroxyanisole (BHA) µg/L U.S. 28 4.1 ND 13.5N-Butylbenzenesulfonamide µg/L U.S. 28 0.3 ND 3.23-tert-Butylphenol µg/L U.S. 28 301.9 70.6 867.6Caffeine µg/L U.S. 28 0.1 ND 2.7Caprolactam µg/L U.S. 28 1348.4 ND 17996.7tris-2-Chloroethyl phosphate µg/L U.S. 28 0.2 ND 5.8o-Cresol (2-Methylphenol) µg/L U.S. 28 481.2 ND 7936.7Cyclododecane µg/L U.S. 28 0.3 ND 7.5Cyclohexanone µg/L U.S. 28 0.5 ND 3.8Decamethylcyclopentasiloxane µg/L U.S. 28 0.4 ND 5.61,4 Diacetylbenzene µg/L U.S. 28 6.5 ND 21.91,3- Dichlorobenzene µg/L U.S. 28 ND ND ND1,4-Dichlorobenzene µg/L U.S. 28 ND ND NDDi-n-butylamine µg/L U.S. 28 2.8 ND 28.0Diallyl Phthalate µg/L U.S. 28 ND ND NDDi-n-butyl phthalate µg/L U.S. 28 21.9 ND 355.5N,N-Dibutylformamide µg/L U.S. 28 1.1 ND 6.52,6-Di-t-butyl-1,4-benzoquinone µg/L U.S. 28 4.9 ND 31.23,5-Di-t-butyl- µg/L U.S. 28 1.6 ND 20.3 4-hydroxybenzaldehyde2,6-Di-t-butyl-4-methylphenol µg/L U.S. 28 0.7 ND 16.02,4-Di-t-butylphenol µg/L U.S. 28 0.2 ND 1.8Dicyclohexyl µg/L U.S. 28 0.5 ND 8.8N,N-Diethylformamide µg/L U.S. 28 83.9 ND 219.6N,N-Diethyl-m-toluamide µg/L U.S. 28 0.0 ND 1.0Diethylene glycol di-n-butyl ether µg/L U.S. 28 0.3 ND 7.9Diethylene glycol monoethyl ether µg/L U.S. 28 114.9 ND 763.8Diethyl phthalate µg/L U.S. 28 0.6 ND 5.1Diisopropyl Adipate µg/L U.S. 28 ND ND NDN,N-Dimethylacetamide µg/L U.S. 28 599.1 ND 4203.1N,N-Dimethylbenzylamine µg/L U.S. 28 2.1 ND 11.7Dimethylcarbamyl chloride µg/L U.S. 28 34.8 ND 355.8N,N-Dimethylformamide µg/L U.S. 28 1099.2 ND 4222.5Dimethyl phthalate µg/L U.S. 28 0.7 ND 8.2Dimethylthiocarbamoyl chloride µg/L U.S. 28 2.0 ND 56.1Dipropylene glycol methyl ether µg/L U.S. 28 64.2 ND 303.2Dodecamethylcyclohexasiloxane µg/L U.S. 28 3.3 ND 23.8Dodecanoic acid µg/L U.S. 28 ND ND NDEicosane µg/L U.S. 28 ND ND ND2-Ethoxyethanol µg/L U.S. 28 603.2 ND 2428.4
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.2-Ethylhexanoic acid µg/L U.S. 28 15.3 ND 142.92-Ethyl-1-hexanol µg/L U.S. 28 82.6 ND 768.2bis-2-Ethylhexyl adipate µg/L U.S. 28 666.9 ND 18674.0bis-2-Ethylhexyl phthalate µg/L U.S. 28 71.4 ND 928.0 (Dioctyl phthlate)4-Ethylmorpholine µg/L U.S. 28 149.5 ND 546.34-Ethylphenol µg/L U.S. 28 1.5 ND 13.61-Formylpiperidine µg/L U.S. 28 0.0 ND 0.4Heneicosane µg/L U.S. 28 ND ND ND2-Heptanone µg/L U.S. 28 4.2 ND 117.3Hexanoic acid µg/L U.S. 28 0.7 ND 19.72-Hexanol µg/L U.S. 28 ND ND NDHexanamide µg/L U.S. 28 6.6 ND 105.0Hydrocinnamic acid µg/L U.S. 28 1.9 ND 53.62-Hydroxybenzothiazole µg/L U.S. 28 64.2 ND 359.7Indole µg/L U.S. 28 ND ND NDIsophorone µg/L U.S. 28 ND ND NDLimonene µg/L U.S. 28 ND ND NDp-Menth-1-en-8-ol µg/L U.S. 28 13.9 ND 50.3 (alpha-Terpineol)Menthol µg/L U.S. 28 0.5 ND 5.4Menthone µg/L U.S. 28 ND ND ND2-Mercaptobenzothiazole µg/L U.S. 28 10.2 ND 155.72,2'-Methylenebis µg/L U.S. 28 ND ND ND (6-t-butyl-4-ethylphenol) 3-Methyl-2-cyclohexen-1-one µg/L U.S. 28 0.6 ND 9.8Methyl-4-hydroxybenzoate µg/L U.S. 28 0.2 ND 28.53-Methylindole µg/L U.S. 28 ND ND ND2-Methyl-2,4-pentanediol µg/L U.S. 28 5.5 ND 114.84-Methylphenol µg/L U.S. 28 24.2 ND 523.12-Methylpyrazine µg/L U.S. 28 0.2 ND 17.11-Methyl-2-pyrrolidinone µg/L U.S. 28 131.4 ND 675.7Methyl sulfone µg/L U.S. 28 0.0 ND 195.12-Methylthiobenzothiazole µg/L U.S. 28 38.2 3.9 146.4Monomethyl phthalate µg/L U.S. 28 1.6 ND 35.1Neomenthol µg/L U.S. 28 8.4 ND 74.6Nicotine µg/L U.S. 28 0.1 ND 2.0Nonadecane µg/L U.S. 28 ND ND NDOctadecanol µg/L U.S. 28 ND ND NDOctamethylcyclotetrasiloxane µg/L U.S. 28 0.1 ND 2.9Octanoic Acid µg/L U.S. 28 ND ND ND4-t-Octylphenol µg/L U.S. 28 ND ND NDOxindole µg/L U.S. 28 0.2 ND 5.2Pentacosane µg/L U.S. 28 0.8 ND 15.0s-Phenethyl alcohol µg/L U.S. 28 16.8 ND 154.3Phenol µg/L U.S. 28 46.4 ND 1197.6bis-Phenol A µg/L U.S. 28 ND ND ND
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Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Extractable Organics contd.Phenoxyacetic acid µg/L U.S. 28 10.7 ND 122.72-Phenoxyethanol µg/L U.S. 28 7.6 ND 58.1N-Phenyl-2-naphthylamine µg/L U.S. 28 14.8 ND 75.32-Phenylacetic Acid µg/L U.S. 28 ND ND NDPhenylethyl alcohol µg/L U.S. 28 2.2 ND 39.72-Phenylphenol µg/L U.S. 28 1.4 ND 9.92-Phenyl-2-propanol µg/L U.S. 28 87.8 ND 201.1Phenyl sulfone µg/L U.S. 28 23.8 ND 93.3Phthalide µg/L U.S. 28 0.5 ND 7.3Salicyclic Acid µg/L U.S. 28 ND ND NDSqualene µg/L U.S. 28 ND ND ND1-Tetradecanol µg/L U.S. 28 0.3 ND 7.3Tetramethylsuccinonitrile µg/L U.S. 28 48.1 ND 146.4Tetramethylthiourea µg/L U.S. 28 219.6 ND 1291.4Tetramethylurea µg/L U.S. 28 90.3 ND 388.5Thymol µg/L U.S. 28 59.3 ND 333.9o-Toluic acid µg/L U.S. 28 2.9 ND 80.51,3,5-Triallyl-1,3,5-triazine- µg/L U.S. 28 2.7 ND 13.4 2,4,6(1H,3H,5H)-trioneTricosane µg/L U.S. 28 0.3 ND 8.1Tributyl Phosphate µg/L U.S. 28 ND ND NDTriethyl Phosphate µg/L U.S. 28 0.1 ND 1.3Triethylamine µg/L U.S. 28 1.6 ND 16.22,2,4-Trimethyl- µg/L U.S. 28 0.3 ND 8.6 1,3-pentanediol diisobutyrateUndecanoic Acid µg/L U.S. 28 0.8 ND 22.92-Undecanone µg/L U.S. 28 0.4 ND 7.1Urethane µg/L U.S. 28 1.6 ND 17.2Vanillin µg/L U.S. 28 ND ND NDAlcohols (DAI/GC/MS)1-Butanol µg/L U.S. 28 399.5 ND 5471.0Ethanol µg/L U.S. 28 26382.2 ND 333518.0Methanol µg/L U.S. 28 788.5 ND 13939.01-Methoxy-2-propanol µg/L U.S. 18 1010.1 ND 3964.02-Methyl-2-butanol µg/L U.S. 27 8.6 ND 240.02-Methyl-2-propanol µg/L U.S. 28 44.75 ND 224.01-Propanol µg/L U.S. 28 15.7 ND 439.02-Propanol µg/L U.S. 27 689.4 ND 11816.0Alcohols/AcetoneAcetone µg/L Russia 12 2275.8 ND 13800.0Butanol µg/L Russia 5 5640.0 ND 16700.0Ethanol µg/L Russia 12 70973.3 ND 405800.0Isoamyl alcohol µg/L Russia 8 3875.0 ND 30100.0Methanol µg/L Russia 7 6900.0 ND 16100.0Propanol µg/L Russia 8 275.0 ND 600.0
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TTTTAAAABBBBLLLLEEEE 6666.... HHHHUUUUMMMMIIIIDDDDIIIITTTTYYYY AAAANNNNDDDD SSSSUUUURRRRFFFFAAAACCCCEEEE CCCCOOOONNNNDDDDEEEENNNNSSSSAAAATTTTEEEE RRRREEEESSSSUUUULLLLTTTTSSSS
Mission Mir 18-25 Mir 18-25 Mir 18-25 Mir 18-25Sample Location Number Mean Minimum MaximumSample Description Test of Samples (X)Sample Date Conducted AnalyzedAnalysis/Sample ID Units by (n)Glycols (DAI/GC/MS)1,2-Ethanediol µg/L U.S. 28 135051.5 ND 474000.01,2-Propanediol µg/L U.S. 28 4592.8 ND 21100.01,2-Ethanediol µg/L Russia 14 139157.1 ND 463100.01,2-Propanediol µg/L Russia 6 1716.7 ND 10000.0Organic Acids (SPE/GC/MS) Acetic acid µg/L U.S. 5 ND ND NDAcetic acid µg/L Russia 7 18528.6 ND 37500.0Lactic acid µg/L U.S. 5 28.0 ND 140.0Propionic acid µg/L U.S. 5 ND ND NDAldehydesAcetaldehyde µg/L U.S. 4 688.3 ND >1840Formaldehyde µg/L U.S. 28 25.5 5.8 60.4Carboxylates (CE)Acetate mg/L U.S. 28 1.3 ND 34.8Butyrate mg/L U.S. 17 ND ND <1.25Formate mg/L U.S. 28 0.0 ND 0.5Glycolate mg/L U.S. 28 0.8 ND 5.9Glyoxylate mg/L U.S. 27 ND ND <6.25Lactate mg/L U.S. 28 0.1 ND 3.1Propionate mg/L U.S. 28 0.4 ND 4.7Oxalate mg/L U.S. 28 0.1 ND 3.0Amines (CE)Ethylamine mg/L U.S. 28 ND ND <6.25Methylamine mg/L U.S. 28 0.9 ND <6.25Propylamine mg/L U.S. 28 ND ND <6.25Trimethylamine mg/L U.S. 28 0.0 ND <6.25Urea mg/L U.S. 28 0.8 ND 6.8Organic Carbon Recovery percent U.S. 27 48.4 3.8 92.5NA = not analyzedND = not detected
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TTTTAAAABBBBLLLLEEEE 7777.... OOOORRRRGGGGAAAANNNNIIIICCCC CCCCOOOOMMMMPPPPOOOOUUUUNNNNDDDDSSSS DDDDEEEETTTTEEEECCCCTTTTEEEEDDDD IIIINNNN TTTTHHHHEEEE HHHHUUUUMMMMIIIIDDDDIIIITTTTYYYYCCCCOOOONNNNDDDDEEEENNNNSSSSAAAATTTTEEEE LLLLEEEEVVVVEEEELLLLSSSS AAAATTTT OOOORRRR AAAABBBBOOOOVVVVEEEE 11110000 µGGGG////LLLL
Compound Units Mean Min MaxEthylene glycol µg/L 135051.5 ND 474000Ethanol µg/L 26382.2 ND 333518Caprolactam µg/L 1348.4 ND 17996.7Acetate µg/L 1296.6 ND 34800N,N-Dimethylformamide µg/L 1099.2 ND 4222.5Methylene chloride µg/L 1011.8 ND 282961-Methoxy-2-propanol µg/L 1010.1 ND 3964Benzyl alcohol µg/L 827.9 ND 9633.6Glycolate µg/L 803.9 ND 5880Methanol µg/L 788.5 ND 13939Urea µg/L 752.5 ND 6780Acetone µg/L 743.4 ND 101452-Propanol µg/L 689.4 ND 11816bis-2-Ethylhexyl adipate µg/L 666.9 ND 186742-Ethoxyethanol µg/L 603.2 ND 2428.4N,N-Dimethylacetamide µg/L 599.1 ND 4203.1o-Cresol µg/L 481.2 ND 7936.7Propionate µg/L 427.5 ND 4710Carbon disulfide µg/L 403.5 ND 2750.91-Butanol µg/L 399.5 ND 5471Acetaldehyde µg/L 353.6 ND 2563.23-t-Butylphenol µg/L 301.9 70.6 867.6Tetramethylthiourea µg/L 219.6 ND 1291.44-Ethylmorpholine µg/L 149.5 ND 546.3Lactate µg/L 141.4 ND 31101-Methyl-2-pyrrolidinone µg/L 131.4 ND 675.7Diethylene glycol monoethyl ether µg/L 114.9 ND 763.8Oxalate µg/L 105.7 ND 2960Methylamine µg/L 92.4 ND 530Tetramethylurea µg/L 90.3 ND 388.52-Phenyl-2-propanol µg/L 87.8 ND 201.1N,N-Diethylformamide µg/L 83.9 ND 219.62-Ethyl-1-hexanol µg/L 82.6 ND 768.2Benzothiazole µg/L 81.7 5.1 184.5Dioctyl phthalate µg/L 71.4 ND 9282-Hydroxybenzothiazole µg/L 64.2 ND 359.7Dipropylene glycol methyl ether µg/L 64.2 ND 303.2Thymol µg/L 59.3 ND 333.9Tetramethysuccinonitrile µg/L 48.1 ND 146.4Phenol µg/L 46.4 ND 1197.62-Methyl-2-propanol µg/L 44.8 ND 2242-Methylthiobenzothiazole µg/L 38.2 3.9 146.4Dimethylcarbamyl chloride µg/L 34.8 ND 355.8Formate µg/L 31.8 ND 500Lactic acid µg/L 28 ND 140Benzaldehyde µg/L 26.3 ND 212.4Formaldehyde µg/L 25.5 5.8 60.4Acetophenone µg/L 24.8 ND 76.4
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TTTTAAAABBBBLLLLEEEE 7777.... OOOORRRRGGGGAAAANNNNIIIICCCC CCCCOOOOMMMMPPPPOOOOUUUUNNNNDDDDSSSS DDDDEEEETTTTEEEECCCCTTTTEEEEDDDD IIIINNNN TTTTHHHHEEEE HHHHUUUUMMMMIIIIDDDDIIIITTTTYYYYCCCCOOOONNNNDDDDEEEENNNNSSSSAAAATTTTEEEE LLLLEEEEVVVVEEEELLLLSSSS AAAATTTT OOOORRRR AAAABBBBOOOOVVVVEEEE 11110000 µGGGG////LLLL
Compound Units Mean Min Max4-Methylphenol µg/L 24.2 ND 523.1Phenyl sulfone µg/L 23.8 ND 93.3Di-n-butylphthalate µg/L 21.9 ND 355.5Tetrahydrofuran µg/L 17.5 ND 212.7s-Phenethyl alcohol µg/L 16.8 ND 154.31-Propanol µg/L 15.7 ND 4392-Ethylhexanoic acid µg/L 15.3 ND 142.9N-Phenyl-2-napthylamine µg/L 14.8 ND 75.3alpha Terpineol µg/L 13.9 ND 50.32-Butoxyethanol µg/L 13.2 ND 111.1Phenoxyacetic acid µg/L 10.7 ND 122.72-Mercaptobenzothiazole µg/L 10.2 ND 155.7
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Figure 1. Mir 18 to Mir 21 Sample Collection Methodology.
Figure 2. Mir 21 to Mir 25 Sample Collection Methodology .
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Figure 4. Iron Levels in the Recycled Water Samples Collected from Mir 18 to Mir 25.
Figure 5. Nickel Levels in the Recycled Water Samples Collected from Mir 18 to Mir 25.
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Figure 6. Ethylene Glycol Levels in the Recycled Water Samples Collected from Mir 18 to Mir 25.
Figure 7. TOC in Recycled Water Samples Collected from Mir 18 to Mir 25.
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Figure 9. Ethylene Glycol Levels in the Humidity Condensate Samples Collected from Mir 18 to Mir 25.
Figure 10. TOC Levels in the Humidity Condensate Samples Collected from Mir 18 to Mir 25.