AN ENVIRONMENTAL ANALYTICAL LABORATORY€¦ · the Project Manager: Brandon Dunmore at 916-985-1000...
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Transcript of AN ENVIRONMENTAL ANALYTICAL LABORATORY€¦ · the Project Manager: Brandon Dunmore at 916-985-1000...
AN ENVIRONMENTAL ANALYTICAL LABORATORY
3/23/2009
Mr. Doug LamTrihydro Corporation5000 State Route 128
Cleves OH 45002
Project Name: Hooven VI 2008-2009Project #: 500-016-012
Dear Mr. Doug Lam
The following report includes the data for the above referenced project for sample(s) received on 3/10/2009 at Air Toxics Ltd.
The data and associated QC analyzed by Modified TO-15 (5&20 ppbv) are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative.
Thank you for choosing Air Toxics Ltd. for you air analysis needs. Air Toxics Ltd. is committed to providing accurate data of the highest quality. Please feel free to contactthe Project Manager: Brandon Dunmore at 916-985-1000 if you have any questions regarding the data in this report.
Regards,
Brandon DunmoreProject Manager
Workorder #: 0903253A
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 .FAX (916) 985-1020
Hours 8:00 A.M to 6:00 P.M. PacificPage 1 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Mr. Doug LamTrihydro Corporation5000 State Route 128Cleves, OH 45002
WORK ORDER #: 0903253A
CLIENT: BILL TO:
PHONE:
Mr. Tim GunnTrihydro Corporation5000 State Route 128Cleves, OH 45002
03/10/2009DATE COMPLETED: 03/23/2009
P.O. # 08-050WO-L
PROJECT # 500-016-012 Hooven VI 2008-2009
Work Order Summary
FAX:
DATE RECEIVED: CONTACT: Brandon Dunmore
NAMEFRACTION # TEST VAC./PRES.RECEIPT
PRESSUREFINAL
01A VW-96(55),030409 Modified TO-15 (5&20 ppbv) 8.0 "Hg 15 psi02A VW-96(50),030409 Modified TO-15 (5&20 ppbv) 4.0 "Hg 15 psi02AA VW-96(50),030409 Lab Duplicate Modified TO-15 (5&20 ppbv) 4.0 "Hg 15 psi03A VW-96(45),030409 Modified TO-15 (5&20 ppbv) 3.0 "Hg 15 psi04A VW-96(40)030409 Modified TO-15 (5&20 ppbv) 2.5 "Hg 15 psi05A VW-96(35)030409 Modified TO-15 (5&20 ppbv) 3.0 "Hg 15 psi06A VW-96(30)030409 Modified TO-15 (5&20 ppbv) 5.0 "Hg 15 psi07A VW-96(25)030409 Modified TO-15 (5&20 ppbv) 5.0 "Hg 15 psi08A VW-96(20)030509 Modified TO-15 (5&20 ppbv) 7.0 "Hg 15 psi09A VW-96(15)030509 Modified TO-15 (5&20 ppbv) 3.5 "Hg 15 psi10A VW-96(10)030509 Modified TO-15 (5&20 ppbv) 6.0 "Hg 15 psi11A VW-96(5)030509 Modified TO-15 (5&20 ppbv) 5.0 "Hg 15 psi12A BD-1,030509 Modified TO-15 (5&20 ppbv) 6.0 "Hg 15 psi13A Lab Blank Modified TO-15 (5&20 ppbv) NA NA13B Lab Blank Modified TO-15 (5&20 ppbv) NA NA14A CCV Modified TO-15 (5&20 ppbv) NA NA14B CCV Modified TO-15 (5&20 ppbv) NA NA
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020
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Continued on next page
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Mr. Doug LamTrihydro Corporation5000 State Route 128Cleves, OH 45002
WORK ORDER #: 0903253A
CLIENT: BILL TO:
PHONE:
Mr. Tim GunnTrihydro Corporation5000 State Route 128Cleves, OH 45002
03/10/2009
DATE COMPLETED: 03/23/2009
P.O. # 08-050WO-L
PROJECT # 500-016-012 Hooven VI 2008-2009
Work Order Summary
FAX:
DATE RECEIVED:CONTACT: Brandon Dunmore
NAMEFRACTION # TEST VAC./PRES.RECEIPT
PRESSUREFINAL
15A LCS Modified TO-15 (5&20 ppbv) NA NA15B LCS Modified TO-15 (5&20 ppbv) NA NA
CERTIFIED BY:
Laboratory Director
DATE:
Name of Accrediting Agency: NELAP/Florida Department of Health, Scope of Application: Clean Air Act, Accreditation number: E87680, Effective date: 07/01/08, Expiration date: 06/30/09
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020
03/23/09
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This report shall not be reproduced, except in full, without the written approval of Air Toxics Ltd.
Air Toxics Ltd. certifies that the test results contained in this report meet all requirements of the NELAC standards
Certfication numbers: CA NELAP - 02110CA, LA NELAP/LELAP- AI 30763, NJ NELAP - CA004NY NELAP - 11291, UT NELAP - 9166389892, AZ Licensure AZ0719
LABORATORY NARRATIVEModified TO-15
Trihydro CorporationWorkorder# 0903253A
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Twelve 1 Liter Summa Canister (100% Certified) samples were received on March 10, 2009. Thelaboratory performed analysis via modified EPA Method TO-15 using GC/MS in the full scan mode. Themethod involves concentrating up to 0.2 liters of air. The concentrated aliquot is then flash vaporized andswept through a water management system to remove water vapor. Following dehumidification, the samplepasses directly into the GC/MS for analysis.
This workorder was independently validated prior to submittal using 'USEPA National Functional Guidelines' as generally applied to the analysis of volatile organic compounds in air. A rules-based, logic driven,independent validation engine was employed to assess completeness, evaluate pass/fail of relevant project quality control requirements and verification of all quantified amounts.
Method modifications taken to run these samples are summarized in the table below. Specific projectrequirements may over-ride the ATL modifications.
Requirement ATL ModificationsTO-15Daily CCV </= 30% Difference </= 30% Difference; Compounds exceeding this criterion
and associated data are flagged and narrated.
Sample collection media Summa canister ATL recommends use of summa canisters to insure data defensibility, but will report results from Tedlar bags at client request
Method Detection Limit Follow 40CFR Pt.136 App. B
The MDL met all relevant requirements in Method TO-15 (statistical MDL less than the LOQ). The concentration of the spiked replicate may have exceeded 10X the calculated MDL in some cases
Receiving Notes
There were no receiving discrepancies.
All Quality Control Limit failures and affected sample results are noted by flags. Each flag is defined at thebottom of this Case Narrative and on each Sample Result Summary page.
The reported CCV for each daily batch may be derived from more than one analytical file due to the client's request for non-standard compounds.
Non-standard compounds may have different acceptance criteria than the standard TO-14A/TO-15compound list as per contract or verbal agreement.
The reported LCS for each daily batch has been derived from more than one analytical file.
Analytical Notes
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Eight qualifiers may have been used on the data analysis sheets and indicates as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction notperformed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.
File extensions may have been used on the data analysis sheets and indicates as follows: a-File was requantified b-File was quantified by a second column and detector r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
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MODIFIED EPA METHOD TO-15 GC/MSSummary of Detected Compounds
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(55),030409
Lab ID#: 0903253A-01A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
460 14000 1600 51000Hexane460 50000 1600 170000Cyclohexane460 250000 2100 12000002,2,4-Trimethylpentane460 480 1500 1500Benzene460 3800 1900 15000Heptane
1800 320000 5400 940000Isopentane1800 28000 4400 67000Butane1800 86000 7400 340000Methylcyclohexane
Client Sample ID: VW-96(50),030409
Lab ID#: 0903253A-02A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 8400 1400 30000Hexane390 39000 1300 130000Cyclohexane390 280000 1800 13000002,2,4-Trimethylpentane390 570 1200 1800Benzene390 940 1600 3800Heptane
1600 310000 4600 920000Isopentane1600 27000 3700 64000Butane1600 69000 6200 280000Methylcyclohexane
Client Sample ID: VW-96(50),030409 Lab Duplicate
Lab ID#: 0903253A-02AA
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 8200 1400 29000Hexane390 38000 1300 130000Cyclohexane390 270000 1800 13000002,2,4-Trimethylpentane390 550 1200 1800Benzene390 990 1600 4100Heptane
1600 310000 4600 910000Isopentane1600 27000 3700 64000Butane1600 68000 6200 270000Methylcyclohexane
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MODIFIED EPA METHOD TO-15 GC/MSSummary of Detected Compounds
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(45),030409
Lab ID#: 0903253A-03A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
370 1300 1300 4600Hexane370 8000 1300 28000Cyclohexane370 230000 1700 11000002,2,4-Trimethylpentane
1500 120000 4400 350000Isopentane1500 12000 3600 29000Butane1500 12000 6000 49000Methylcyclohexane
Client Sample ID: VW-96(40)030409
Lab ID#: 0903253A-04A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
220 240 1100 1200Chloroform220 970 M 760 3400 MCyclohexane220 200000 1000 9400002,2,4-Trimethylpentane880 68000 2600 200000Isopentane880 8000 2100 19000Butane
Client Sample ID: VW-96(35)030409
Lab ID#: 0903253A-05A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
430 190000 2000 9000002,2,4-Trimethylpentane1700 20000 5100 60000Isopentane1700 4000 4100 9400Butane
Client Sample ID: VW-96(30)030409
Lab ID#: 0903253A-06A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
240 140000 1100 6600002,2,4-Trimethylpentane970 5300 2800 16000Isopentane970 2100 2300 5000Butane
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MODIFIED EPA METHOD TO-15 GC/MSSummary of Detected Compounds
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(25)030409
Lab ID#: 0903253A-07A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
120 110000 560 5200002,2,4-Trimethylpentane
Client Sample ID: VW-96(20)030509
Lab ID#: 0903253A-08A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
13 5600 62 260002,2,4-Trimethylpentane
Client Sample ID: VW-96(15)030509
Lab ID#: 0903253A-09A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
38 23000 180 1100002,2,4-Trimethylpentane150 430 450 1300Isopentane
Client Sample ID: VW-96(10)030509
Lab ID#: 0903253A-10A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
130 59000 590 2800002,2,4-Trimethylpentane500 2700 1500 7900Isopentane
Client Sample ID: VW-96(5)030509
Lab ID#: 0903253A-11A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
1.2 14 5.6 672,2,4-Trimethylpentane4.8 20 14 58Isopentane
Client Sample ID: BD-1,030509
Lab ID#: 0903253A-12A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
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MODIFIED EPA METHOD TO-15 GC/MSSummary of Detected Compounds
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: BD-1,030509
Lab ID#: 0903253A-12A
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
100 61000 490 2800002,2,4-Trimethylpentane420 2700 1200 8100Isopentane420 450 1000 1100Butane
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(55),030409
Lab ID#: 0903253A-01A
MODIFIED EPA METHOD TO-15 GC/MS
b031317File Name:Dil. Factor: 92.0
Date of Collection: 3/4/09 11:35:00 AMDate of Analysis: 3/13/09 04:14 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
460 Not Detected 2300 Not DetectedFreon 12460 Not Detected 3200 Not DetectedFreon 114
1800 Not Detected 3800 Not DetectedChloromethane460 Not Detected 1200 Not DetectedVinyl Chloride460 Not Detected 1000 Not Detected1,3-Butadiene460 Not Detected 1800 Not DetectedBromomethane460 Not Detected 1200 Not DetectedChloroethane460 Not Detected 2600 Not DetectedFreon 11
1800 Not Detected 3500 Not DetectedEthanol460 Not Detected 3500 Not DetectedFreon 113460 Not Detected 1800 Not Detected1,1-Dichloroethene
1800 Not Detected 4400 Not DetectedAcetone1800 Not Detected 4500 Not Detected2-Propanol460 Not Detected 1400 Not DetectedCarbon Disulfide
1800 Not Detected 5800 Not Detected3-Chloropropene460 Not Detected 1600 Not DetectedMethylene Chloride460 Not Detected 1600 Not DetectedMethyl tert-butyl ether460 Not Detected 1800 Not Detectedtrans-1,2-Dichloroethene460 14000 1600 51000Hexane460 Not Detected 1900 Not Detected1,1-Dichloroethane460 Not Detected 1400 Not Detected2-Butanone (Methyl Ethyl Ketone)460 Not Detected 1800 Not Detectedcis-1,2-Dichloroethene460 Not Detected 1400 Not DetectedTetrahydrofuran460 Not Detected 2200 Not DetectedChloroform460 Not Detected 2500 Not Detected1,1,1-Trichloroethane460 50000 1600 170000Cyclohexane460 Not Detected 2900 Not DetectedCarbon Tetrachloride460 250000 2100 12000002,2,4-Trimethylpentane460 480 1500 1500Benzene460 Not Detected 1900 Not Detected1,2-Dichloroethane460 3800 1900 15000Heptane460 Not Detected 2500 Not DetectedTrichloroethene460 Not Detected 2100 Not Detected1,2-Dichloropropane
1800 Not Detected 6600 Not Detected1,4-Dioxane460 Not Detected 3100 Not DetectedBromodichloromethane460 Not Detected 2100 Not Detectedcis-1,3-Dichloropropene460 Not Detected 1900 Not Detected4-Methyl-2-pentanone460 Not Detected 1700 Not DetectedToluene460 Not Detected 2100 Not Detectedtrans-1,3-Dichloropropene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(55),030409
Lab ID#: 0903253A-01A
MODIFIED EPA METHOD TO-15 GC/MS
b031317File Name:Dil. Factor: 92.0
Date of Collection: 3/4/09 11:35:00 AMDate of Analysis: 3/13/09 04:14 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
460 Not Detected 2500 Not Detected1,1,2-Trichloroethane460 Not Detected 3100 Not DetectedTetrachloroethene
1800 Not Detected 7500 Not Detected2-Hexanone460 Not Detected 3900 Not DetectedDibromochloromethane460 Not Detected 3500 Not Detected1,2-Dibromoethane (EDB)460 Not Detected 2100 Not DetectedChlorobenzene460 Not Detected 2000 Not DetectedEthyl Benzene460 Not Detected 2000 Not Detectedm,p-Xylene460 Not Detected 2000 Not Detectedo-Xylene460 Not Detected 2000 Not DetectedStyrene460 Not Detected 4800 Not DetectedBromoform460 Not Detected 2300 Not DetectedCumene460 Not Detected 3200 Not Detected1,1,2,2-Tetrachloroethane460 Not Detected 2300 Not DetectedPropylbenzene460 Not Detected 2300 Not Detected4-Ethyltoluene460 Not Detected 2300 Not Detected1,3,5-Trimethylbenzene460 Not Detected 2300 Not Detected1,2,4-Trimethylbenzene460 Not Detected 2800 Not Detected1,3-Dichlorobenzene460 Not Detected 2800 Not Detected1,4-Dichlorobenzene460 Not Detected 2400 Not Detectedalpha-Chlorotoluene460 Not Detected 2800 Not Detected1,2-Dichlorobenzene
1800 Not Detected 14000 Not Detected1,2,4-Trichlorobenzene1800 Not Detected 20000 Not DetectedHexachlorobutadiene1800 Not Detected 9600 Not DetectedNaphthalene1800 Not Detected 10000 Not DetectedButylbenzene1800 Not Detected 10000 Not Detectedsec-Butylbenzene1800 320000 5400 940000Isopentane1800 28000 4400 67000Butane1800 86000 7400 340000Methylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
120 70-1301,2-Dichloroethane-d4104 70-130Toluene-d896 70-1304-Bromofluorobenzene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(50),030409
Lab ID#: 0903253A-02A
MODIFIED EPA METHOD TO-15 GC/MS
b031318File Name:Dil. Factor: 77.7
Date of Collection: 3/4/09 2:38:00 PMDate of Analysis: 3/13/09 04:40 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 Not Detected 1900 Not DetectedFreon 12390 Not Detected 2700 Not DetectedFreon 114
1600 Not Detected 3200 Not DetectedChloromethane390 Not Detected 990 Not DetectedVinyl Chloride390 Not Detected 860 Not Detected1,3-Butadiene390 Not Detected 1500 Not DetectedBromomethane390 Not Detected 1000 Not DetectedChloroethane390 Not Detected 2200 Not DetectedFreon 11
1600 Not Detected 2900 Not DetectedEthanol390 Not Detected 3000 Not DetectedFreon 113390 Not Detected 1500 Not Detected1,1-Dichloroethene
1600 Not Detected 3700 Not DetectedAcetone1600 Not Detected 3800 Not Detected2-Propanol390 Not Detected 1200 Not DetectedCarbon Disulfide
1600 Not Detected 4900 Not Detected3-Chloropropene390 Not Detected 1300 Not DetectedMethylene Chloride390 Not Detected 1400 Not DetectedMethyl tert-butyl ether390 Not Detected 1500 Not Detectedtrans-1,2-Dichloroethene390 8400 1400 30000Hexane390 Not Detected 1600 Not Detected1,1-Dichloroethane390 Not Detected 1100 Not Detected2-Butanone (Methyl Ethyl Ketone)390 Not Detected 1500 Not Detectedcis-1,2-Dichloroethene390 Not Detected 1100 Not DetectedTetrahydrofuran390 Not Detected 1900 Not DetectedChloroform390 Not Detected 2100 Not Detected1,1,1-Trichloroethane390 39000 1300 130000Cyclohexane390 Not Detected 2400 Not DetectedCarbon Tetrachloride390 280000 1800 13000002,2,4-Trimethylpentane390 570 1200 1800Benzene390 Not Detected 1600 Not Detected1,2-Dichloroethane390 940 1600 3800Heptane390 Not Detected 2100 Not DetectedTrichloroethene390 Not Detected 1800 Not Detected1,2-Dichloropropane
1600 Not Detected 5600 Not Detected1,4-Dioxane390 Not Detected 2600 Not DetectedBromodichloromethane390 Not Detected 1800 Not Detectedcis-1,3-Dichloropropene390 Not Detected 1600 Not Detected4-Methyl-2-pentanone390 Not Detected 1500 Not DetectedToluene390 Not Detected 1800 Not Detectedtrans-1,3-Dichloropropene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(50),030409
Lab ID#: 0903253A-02A
MODIFIED EPA METHOD TO-15 GC/MS
b031318File Name:Dil. Factor: 77.7
Date of Collection: 3/4/09 2:38:00 PMDate of Analysis: 3/13/09 04:40 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 Not Detected 2100 Not Detected1,1,2-Trichloroethane390 Not Detected 2600 Not DetectedTetrachloroethene
1600 Not Detected 6400 Not Detected2-Hexanone390 Not Detected 3300 Not DetectedDibromochloromethane390 Not Detected 3000 Not Detected1,2-Dibromoethane (EDB)390 Not Detected 1800 Not DetectedChlorobenzene390 Not Detected 1700 Not DetectedEthyl Benzene390 Not Detected 1700 Not Detectedm,p-Xylene390 Not Detected 1700 Not Detectedo-Xylene390 Not Detected 1600 Not DetectedStyrene390 Not Detected 4000 Not DetectedBromoform390 Not Detected 1900 Not DetectedCumene390 Not Detected 2700 Not Detected1,1,2,2-Tetrachloroethane390 Not Detected 1900 Not DetectedPropylbenzene390 Not Detected 1900 Not Detected4-Ethyltoluene390 Not Detected 1900 Not Detected1,3,5-Trimethylbenzene390 Not Detected 1900 Not Detected1,2,4-Trimethylbenzene390 Not Detected 2300 Not Detected1,3-Dichlorobenzene390 Not Detected 2300 Not Detected1,4-Dichlorobenzene390 Not Detected 2000 Not Detectedalpha-Chlorotoluene390 Not Detected 2300 Not Detected1,2-Dichlorobenzene
1600 Not Detected 12000 Not Detected1,2,4-Trichlorobenzene1600 Not Detected 16000 Not DetectedHexachlorobutadiene1600 Not Detected 8100 Not DetectedNaphthalene1600 Not Detected 8500 Not DetectedButylbenzene1600 Not Detected 8500 Not Detectedsec-Butylbenzene1600 310000 4600 920000Isopentane1600 27000 3700 64000Butane1600 69000 6200 280000Methylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
127 70-1301,2-Dichloroethane-d4104 70-130Toluene-d895 70-1304-Bromofluorobenzene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(50),030409 Lab Duplicate
Lab ID#: 0903253A-02AA
MODIFIED EPA METHOD TO-15 GC/MS
b031319File Name:Dil. Factor: 77.7
Date of Collection: 3/4/09 2:38:00 PMDate of Analysis: 3/13/09 05:02 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 Not Detected 1900 Not DetectedFreon 12390 Not Detected 2700 Not DetectedFreon 114
1600 Not Detected 3200 Not DetectedChloromethane390 Not Detected 990 Not DetectedVinyl Chloride390 Not Detected 860 Not Detected1,3-Butadiene390 Not Detected 1500 Not DetectedBromomethane390 Not Detected 1000 Not DetectedChloroethane390 Not Detected 2200 Not DetectedFreon 11
1600 Not Detected 2900 Not DetectedEthanol390 Not Detected 3000 Not DetectedFreon 113390 Not Detected 1500 Not Detected1,1-Dichloroethene
1600 Not Detected 3700 Not DetectedAcetone1600 Not Detected 3800 Not Detected2-Propanol390 Not Detected 1200 Not DetectedCarbon Disulfide
1600 Not Detected 4900 Not Detected3-Chloropropene390 Not Detected 1300 Not DetectedMethylene Chloride390 Not Detected 1400 Not DetectedMethyl tert-butyl ether390 Not Detected 1500 Not Detectedtrans-1,2-Dichloroethene390 8200 1400 29000Hexane390 Not Detected 1600 Not Detected1,1-Dichloroethane390 Not Detected 1100 Not Detected2-Butanone (Methyl Ethyl Ketone)390 Not Detected 1500 Not Detectedcis-1,2-Dichloroethene390 Not Detected 1100 Not DetectedTetrahydrofuran390 Not Detected 1900 Not DetectedChloroform390 Not Detected 2100 Not Detected1,1,1-Trichloroethane390 38000 1300 130000Cyclohexane390 Not Detected 2400 Not DetectedCarbon Tetrachloride390 270000 1800 13000002,2,4-Trimethylpentane390 550 1200 1800Benzene390 Not Detected 1600 Not Detected1,2-Dichloroethane390 990 1600 4100Heptane390 Not Detected 2100 Not DetectedTrichloroethene390 Not Detected 1800 Not Detected1,2-Dichloropropane
1600 Not Detected 5600 Not Detected1,4-Dioxane390 Not Detected 2600 Not DetectedBromodichloromethane390 Not Detected 1800 Not Detectedcis-1,3-Dichloropropene390 Not Detected 1600 Not Detected4-Methyl-2-pentanone390 Not Detected 1500 Not DetectedToluene390 Not Detected 1800 Not Detectedtrans-1,3-Dichloropropene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(50),030409 Lab Duplicate
Lab ID#: 0903253A-02AA
MODIFIED EPA METHOD TO-15 GC/MS
b031319File Name:Dil. Factor: 77.7
Date of Collection: 3/4/09 2:38:00 PMDate of Analysis: 3/13/09 05:02 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
390 Not Detected 2100 Not Detected1,1,2-Trichloroethane390 Not Detected 2600 Not DetectedTetrachloroethene
1600 Not Detected 6400 Not Detected2-Hexanone390 Not Detected 3300 Not DetectedDibromochloromethane390 Not Detected 3000 Not Detected1,2-Dibromoethane (EDB)390 Not Detected 1800 Not DetectedChlorobenzene390 Not Detected 1700 Not DetectedEthyl Benzene390 Not Detected 1700 Not Detectedm,p-Xylene390 Not Detected 1700 Not Detectedo-Xylene390 Not Detected 1600 Not DetectedStyrene390 Not Detected 4000 Not DetectedBromoform390 Not Detected 1900 Not DetectedCumene390 Not Detected 2700 Not Detected1,1,2,2-Tetrachloroethane390 Not Detected 1900 Not DetectedPropylbenzene390 Not Detected 1900 Not Detected4-Ethyltoluene390 Not Detected 1900 Not Detected1,3,5-Trimethylbenzene390 Not Detected 1900 Not Detected1,2,4-Trimethylbenzene390 Not Detected 2300 Not Detected1,3-Dichlorobenzene390 Not Detected 2300 Not Detected1,4-Dichlorobenzene390 Not Detected 2000 Not Detectedalpha-Chlorotoluene390 Not Detected 2300 Not Detected1,2-Dichlorobenzene
1600 Not Detected 12000 Not Detected1,2,4-Trichlorobenzene1600 Not Detected 16000 Not DetectedHexachlorobutadiene1600 Not Detected 8100 Not DetectedNaphthalene1600 Not Detected 8500 Not DetectedButylbenzene1600 Not Detected 8500 Not Detectedsec-Butylbenzene1600 310000 4600 910000Isopentane1600 27000 3700 64000Butane1600 68000 6200 270000Methylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
126 70-1301,2-Dichloroethane-d4104 70-130Toluene-d896 70-1304-Bromofluorobenzene
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AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(45),030409
Lab ID#: 0903253A-03A
MODIFIED EPA METHOD TO-15 GC/MS
b031320File Name:Dil. Factor: 74.7
Date of Collection: 3/4/09 3:25:00 PMDate of Analysis: 3/13/09 05:34 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
370 Not Detected 1800 Not DetectedFreon 12370 Not Detected 2600 Not DetectedFreon 114
1500 Not Detected 3100 Not DetectedChloromethane370 Not Detected 950 Not DetectedVinyl Chloride370 Not Detected 830 Not Detected1,3-Butadiene370 Not Detected 1400 Not DetectedBromomethane370 Not Detected 980 Not DetectedChloroethane370 Not Detected 2100 Not DetectedFreon 11
1500 Not Detected 2800 Not DetectedEthanol370 Not Detected 2900 Not DetectedFreon 113370 Not Detected 1500 Not Detected1,1-Dichloroethene
1500 Not Detected 3500 Not DetectedAcetone1500 Not Detected 3700 Not Detected2-Propanol370 Not Detected 1200 Not DetectedCarbon Disulfide
1500 Not Detected 4700 Not Detected3-Chloropropene370 Not Detected 1300 Not DetectedMethylene Chloride370 Not Detected 1300 Not DetectedMethyl tert-butyl ether370 Not Detected 1500 Not Detectedtrans-1,2-Dichloroethene370 1300 1300 4600Hexane370 Not Detected 1500 Not Detected1,1-Dichloroethane370 Not Detected 1100 Not Detected2-Butanone (Methyl Ethyl Ketone)370 Not Detected 1500 Not Detectedcis-1,2-Dichloroethene370 Not Detected 1100 Not DetectedTetrahydrofuran370 Not Detected 1800 Not DetectedChloroform370 Not Detected 2000 Not Detected1,1,1-Trichloroethane370 8000 1300 28000Cyclohexane370 Not Detected 2400 Not DetectedCarbon Tetrachloride370 230000 1700 11000002,2,4-Trimethylpentane370 Not Detected 1200 Not DetectedBenzene370 Not Detected 1500 Not Detected1,2-Dichloroethane370 Not Detected 1500 Not DetectedHeptane370 Not Detected 2000 Not DetectedTrichloroethene370 Not Detected 1700 Not Detected1,2-Dichloropropane
1500 Not Detected 5400 Not Detected1,4-Dioxane370 Not Detected 2500 Not DetectedBromodichloromethane370 Not Detected 1700 Not Detectedcis-1,3-Dichloropropene370 Not Detected 1500 Not Detected4-Methyl-2-pentanone370 Not Detected 1400 Not DetectedToluene370 Not Detected 1700 Not Detectedtrans-1,3-Dichloropropene
Page 16 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(45),030409
Lab ID#: 0903253A-03A
MODIFIED EPA METHOD TO-15 GC/MS
b031320File Name:Dil. Factor: 74.7
Date of Collection: 3/4/09 3:25:00 PMDate of Analysis: 3/13/09 05:34 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
370 Not Detected 2000 Not Detected1,1,2-Trichloroethane370 Not Detected 2500 Not DetectedTetrachloroethene
1500 Not Detected 6100 Not Detected2-Hexanone370 Not Detected 3200 Not DetectedDibromochloromethane370 Not Detected 2900 Not Detected1,2-Dibromoethane (EDB)370 Not Detected 1700 Not DetectedChlorobenzene370 Not Detected 1600 Not DetectedEthyl Benzene370 Not Detected 1600 Not Detectedm,p-Xylene370 Not Detected 1600 Not Detectedo-Xylene370 Not Detected 1600 Not DetectedStyrene370 Not Detected 3900 Not DetectedBromoform370 Not Detected 1800 Not DetectedCumene370 Not Detected 2600 Not Detected1,1,2,2-Tetrachloroethane370 Not Detected 1800 Not DetectedPropylbenzene370 Not Detected 1800 Not Detected4-Ethyltoluene370 Not Detected 1800 Not Detected1,3,5-Trimethylbenzene370 Not Detected 1800 Not Detected1,2,4-Trimethylbenzene370 Not Detected 2200 Not Detected1,3-Dichlorobenzene370 Not Detected 2200 Not Detected1,4-Dichlorobenzene370 Not Detected 1900 Not Detectedalpha-Chlorotoluene370 Not Detected 2200 Not Detected1,2-Dichlorobenzene
1500 Not Detected 11000 Not Detected1,2,4-Trichlorobenzene1500 Not Detected 16000 Not DetectedHexachlorobutadiene1500 Not Detected 7800 Not DetectedNaphthalene1500 Not Detected 8200 Not DetectedButylbenzene1500 Not Detected 8200 Not Detectedsec-Butylbenzene1500 120000 4400 350000Isopentane1500 12000 3600 29000Butane1500 12000 6000 49000Methylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
117 70-1301,2-Dichloroethane-d4103 70-130Toluene-d896 70-1304-Bromofluorobenzene
Page 17 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(40)030409
Lab ID#: 0903253A-04A
MODIFIED EPA METHOD TO-15 GC/MS
b031321File Name:Dil. Factor: 44.0
Date of Collection: 3/4/09 3:55:00 PMDate of Analysis: 3/13/09 06:03 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
220 Not Detected 1100 Not DetectedFreon 12220 Not Detected 1500 Not DetectedFreon 114880 Not Detected 1800 Not DetectedChloromethane220 Not Detected 560 Not DetectedVinyl Chloride220 Not Detected 490 Not Detected1,3-Butadiene220 Not Detected 850 Not DetectedBromomethane220 Not Detected 580 Not DetectedChloroethane220 Not Detected 1200 Not DetectedFreon 11880 Not Detected 1600 Not DetectedEthanol220 Not Detected 1700 Not DetectedFreon 113220 Not Detected 870 Not Detected1,1-Dichloroethene880 Not Detected 2100 Not DetectedAcetone880 Not Detected 2200 Not Detected2-Propanol220 Not Detected 680 Not DetectedCarbon Disulfide880 Not Detected 2800 Not Detected3-Chloropropene220 Not Detected 760 Not DetectedMethylene Chloride220 Not Detected 790 Not DetectedMethyl tert-butyl ether220 Not Detected 870 Not Detectedtrans-1,2-Dichloroethene220 Not Detected 780 Not DetectedHexane220 Not Detected 890 Not Detected1,1-Dichloroethane220 Not Detected 650 Not Detected2-Butanone (Methyl Ethyl Ketone)220 Not Detected 870 Not Detectedcis-1,2-Dichloroethene220 Not Detected 650 Not DetectedTetrahydrofuran220 240 1100 1200Chloroform220 Not Detected 1200 Not Detected1,1,1-Trichloroethane220 970 M 760 3400 MCyclohexane220 Not Detected 1400 Not DetectedCarbon Tetrachloride220 200000 1000 9400002,2,4-Trimethylpentane220 Not Detected 700 Not DetectedBenzene220 Not Detected 890 Not Detected1,2-Dichloroethane220 Not Detected 900 Not DetectedHeptane220 Not Detected 1200 Not DetectedTrichloroethene220 Not Detected 1000 Not Detected1,2-Dichloropropane880 Not Detected 3200 Not Detected1,4-Dioxane220 Not Detected 1500 Not DetectedBromodichloromethane220 Not Detected 1000 Not Detectedcis-1,3-Dichloropropene220 Not Detected 900 Not Detected4-Methyl-2-pentanone220 Not Detected 830 Not DetectedToluene220 Not Detected 1000 Not Detectedtrans-1,3-Dichloropropene
Page 18 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(40)030409
Lab ID#: 0903253A-04A
MODIFIED EPA METHOD TO-15 GC/MS
b031321File Name:Dil. Factor: 44.0
Date of Collection: 3/4/09 3:55:00 PMDate of Analysis: 3/13/09 06:03 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
220 Not Detected 1200 Not Detected1,1,2-Trichloroethane220 Not Detected 1500 Not DetectedTetrachloroethene880 Not Detected 3600 Not Detected2-Hexanone220 Not Detected 1900 Not DetectedDibromochloromethane220 Not Detected 1700 Not Detected1,2-Dibromoethane (EDB)220 Not Detected 1000 Not DetectedChlorobenzene220 Not Detected 960 Not DetectedEthyl Benzene220 Not Detected 960 Not Detectedm,p-Xylene220 Not Detected 960 Not Detectedo-Xylene220 Not Detected 940 Not DetectedStyrene220 Not Detected 2300 Not DetectedBromoform220 Not Detected 1100 Not DetectedCumene220 Not Detected 1500 Not Detected1,1,2,2-Tetrachloroethane220 Not Detected 1100 Not DetectedPropylbenzene220 Not Detected 1100 Not Detected4-Ethyltoluene220 Not Detected 1100 Not Detected1,3,5-Trimethylbenzene220 Not Detected 1100 Not Detected1,2,4-Trimethylbenzene220 Not Detected 1300 Not Detected1,3-Dichlorobenzene220 Not Detected 1300 Not Detected1,4-Dichlorobenzene220 Not Detected 1100 Not Detectedalpha-Chlorotoluene220 Not Detected 1300 Not Detected1,2-Dichlorobenzene880 Not Detected 6500 Not Detected1,2,4-Trichlorobenzene880 Not Detected 9400 Not DetectedHexachlorobutadiene880 Not Detected 4600 Not DetectedNaphthalene880 Not Detected 4800 Not DetectedButylbenzene880 Not Detected 4800 Not Detectedsec-Butylbenzene880 68000 2600 200000Isopentane880 8000 2100 19000Butane880 Not Detected 3500 Not DetectedMethylcyclohexane
M = Reported value may be biased due to apparent matrix interferences.Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
117 70-1301,2-Dichloroethane-d4103 70-130Toluene-d896 70-1304-Bromofluorobenzene
Page 19 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(35)030409
Lab ID#: 0903253A-05A
MODIFIED EPA METHOD TO-15 GC/MS
b031322File Name:Dil. Factor: 86.2
Date of Collection: 3/4/09 4:25:00 PMDate of Analysis: 3/13/09 06:25 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
430 Not Detected 2100 Not DetectedFreon 12430 Not Detected 3000 Not DetectedFreon 114
1700 Not Detected 3600 Not DetectedChloromethane430 Not Detected 1100 Not DetectedVinyl Chloride430 Not Detected 950 Not Detected1,3-Butadiene430 Not Detected 1700 Not DetectedBromomethane430 Not Detected 1100 Not DetectedChloroethane430 Not Detected 2400 Not DetectedFreon 11
1700 Not Detected 3200 Not DetectedEthanol430 Not Detected 3300 Not DetectedFreon 113430 Not Detected 1700 Not Detected1,1-Dichloroethene
1700 Not Detected 4100 Not DetectedAcetone1700 Not Detected 4200 Not Detected2-Propanol430 Not Detected 1300 Not DetectedCarbon Disulfide
1700 Not Detected 5400 Not Detected3-Chloropropene430 Not Detected 1500 Not DetectedMethylene Chloride430 Not Detected 1600 Not DetectedMethyl tert-butyl ether430 Not Detected 1700 Not Detectedtrans-1,2-Dichloroethene430 Not Detected 1500 Not DetectedHexane430 Not Detected 1700 Not Detected1,1-Dichloroethane430 Not Detected 1300 Not Detected2-Butanone (Methyl Ethyl Ketone)430 Not Detected 1700 Not Detectedcis-1,2-Dichloroethene430 Not Detected 1300 Not DetectedTetrahydrofuran430 Not Detected 2100 Not DetectedChloroform430 Not Detected 2400 Not Detected1,1,1-Trichloroethane430 Not Detected 1500 Not DetectedCyclohexane430 Not Detected 2700 Not DetectedCarbon Tetrachloride430 190000 2000 9000002,2,4-Trimethylpentane430 Not Detected 1400 Not DetectedBenzene430 Not Detected 1700 Not Detected1,2-Dichloroethane430 Not Detected 1800 Not DetectedHeptane430 Not Detected 2300 Not DetectedTrichloroethene430 Not Detected 2000 Not Detected1,2-Dichloropropane
1700 Not Detected 6200 Not Detected1,4-Dioxane430 Not Detected 2900 Not DetectedBromodichloromethane430 Not Detected 2000 Not Detectedcis-1,3-Dichloropropene430 Not Detected 1800 Not Detected4-Methyl-2-pentanone430 Not Detected 1600 Not DetectedToluene430 Not Detected 2000 Not Detectedtrans-1,3-Dichloropropene
Page 20 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(35)030409
Lab ID#: 0903253A-05A
MODIFIED EPA METHOD TO-15 GC/MS
b031322File Name:Dil. Factor: 86.2
Date of Collection: 3/4/09 4:25:00 PMDate of Analysis: 3/13/09 06:25 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
430 Not Detected 2400 Not Detected1,1,2-Trichloroethane430 Not Detected 2900 Not DetectedTetrachloroethene
1700 Not Detected 7100 Not Detected2-Hexanone430 Not Detected 3700 Not DetectedDibromochloromethane430 Not Detected 3300 Not Detected1,2-Dibromoethane (EDB)430 Not Detected 2000 Not DetectedChlorobenzene430 Not Detected 1900 Not DetectedEthyl Benzene430 Not Detected 1900 Not Detectedm,p-Xylene430 Not Detected 1900 Not Detectedo-Xylene430 Not Detected 1800 Not DetectedStyrene430 Not Detected 4400 Not DetectedBromoform430 Not Detected 2100 Not DetectedCumene430 Not Detected 3000 Not Detected1,1,2,2-Tetrachloroethane430 Not Detected 2100 Not DetectedPropylbenzene430 Not Detected 2100 Not Detected4-Ethyltoluene430 Not Detected 2100 Not Detected1,3,5-Trimethylbenzene430 Not Detected 2100 Not Detected1,2,4-Trimethylbenzene430 Not Detected 2600 Not Detected1,3-Dichlorobenzene430 Not Detected 2600 Not Detected1,4-Dichlorobenzene430 Not Detected 2200 Not Detectedalpha-Chlorotoluene430 Not Detected 2600 Not Detected1,2-Dichlorobenzene
1700 Not Detected 13000 Not Detected1,2,4-Trichlorobenzene1700 Not Detected 18000 Not DetectedHexachlorobutadiene1700 Not Detected 9000 Not DetectedNaphthalene1700 Not Detected 9500 Not DetectedButylbenzene1700 Not Detected 9500 Not Detectedsec-Butylbenzene1700 20000 5100 60000Isopentane1700 4000 4100 9400Butane1700 Not Detected 6900 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
112 70-1301,2-Dichloroethane-d4101 70-130Toluene-d897 70-1304-Bromofluorobenzene
Page 21 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(30)030409
Lab ID#: 0903253A-06A
MODIFIED EPA METHOD TO-15 GC/MS
b031325File Name:Dil. Factor: 48.4
Date of Collection: 3/4/09 5:05:00 PMDate of Analysis: 3/13/09 07:38 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
240 Not Detected 1200 Not DetectedFreon 12240 Not Detected 1700 Not DetectedFreon 114970 Not Detected 2000 Not DetectedChloromethane240 Not Detected 620 Not DetectedVinyl Chloride240 Not Detected 540 Not Detected1,3-Butadiene240 Not Detected 940 Not DetectedBromomethane240 Not Detected 640 Not DetectedChloroethane240 Not Detected 1400 Not DetectedFreon 11970 Not Detected 1800 Not DetectedEthanol240 Not Detected 1800 Not DetectedFreon 113240 Not Detected 960 Not Detected1,1-Dichloroethene970 Not Detected 2300 Not DetectedAcetone970 Not Detected 2400 Not Detected2-Propanol240 Not Detected 750 Not DetectedCarbon Disulfide970 Not Detected 3000 Not Detected3-Chloropropene240 Not Detected 840 Not DetectedMethylene Chloride240 Not Detected 870 Not DetectedMethyl tert-butyl ether240 Not Detected 960 Not Detectedtrans-1,2-Dichloroethene240 Not Detected 850 Not DetectedHexane240 Not Detected 980 Not Detected1,1-Dichloroethane240 Not Detected 710 Not Detected2-Butanone (Methyl Ethyl Ketone)240 Not Detected 960 Not Detectedcis-1,2-Dichloroethene240 Not Detected 710 Not DetectedTetrahydrofuran240 Not Detected 1200 Not DetectedChloroform240 Not Detected 1300 Not Detected1,1,1-Trichloroethane240 Not Detected 830 Not DetectedCyclohexane240 Not Detected 1500 Not DetectedCarbon Tetrachloride240 140000 1100 6600002,2,4-Trimethylpentane240 Not Detected 770 Not DetectedBenzene240 Not Detected 980 Not Detected1,2-Dichloroethane240 Not Detected 990 Not DetectedHeptane240 Not Detected 1300 Not DetectedTrichloroethene240 Not Detected 1100 Not Detected1,2-Dichloropropane970 Not Detected 3500 Not Detected1,4-Dioxane240 Not Detected 1600 Not DetectedBromodichloromethane240 Not Detected 1100 Not Detectedcis-1,3-Dichloropropene240 Not Detected 990 Not Detected4-Methyl-2-pentanone240 Not Detected 910 Not DetectedToluene240 Not Detected 1100 Not Detectedtrans-1,3-Dichloropropene
Page 22 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(30)030409
Lab ID#: 0903253A-06A
MODIFIED EPA METHOD TO-15 GC/MS
b031325File Name:Dil. Factor: 48.4
Date of Collection: 3/4/09 5:05:00 PMDate of Analysis: 3/13/09 07:38 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
240 Not Detected 1300 Not Detected1,1,2-Trichloroethane240 Not Detected 1600 Not DetectedTetrachloroethene970 Not Detected 4000 Not Detected2-Hexanone240 Not Detected 2100 Not DetectedDibromochloromethane240 Not Detected 1800 Not Detected1,2-Dibromoethane (EDB)240 Not Detected 1100 Not DetectedChlorobenzene240 Not Detected 1000 Not DetectedEthyl Benzene240 Not Detected 1000 Not Detectedm,p-Xylene240 Not Detected 1000 Not Detectedo-Xylene240 Not Detected 1000 Not DetectedStyrene240 Not Detected 2500 Not DetectedBromoform240 Not Detected 1200 Not DetectedCumene240 Not Detected 1700 Not Detected1,1,2,2-Tetrachloroethane240 Not Detected 1200 Not DetectedPropylbenzene240 Not Detected 1200 Not Detected4-Ethyltoluene240 Not Detected 1200 Not Detected1,3,5-Trimethylbenzene240 Not Detected 1200 Not Detected1,2,4-Trimethylbenzene240 Not Detected 1400 Not Detected1,3-Dichlorobenzene240 Not Detected 1400 Not Detected1,4-Dichlorobenzene240 Not Detected 1200 Not Detectedalpha-Chlorotoluene240 Not Detected 1400 Not Detected1,2-Dichlorobenzene970 Not Detected 7200 Not Detected1,2,4-Trichlorobenzene970 Not Detected 10000 Not DetectedHexachlorobutadiene970 Not Detected 5100 Not DetectedNaphthalene970 Not Detected 5300 Not DetectedButylbenzene970 Not Detected 5300 Not Detectedsec-Butylbenzene970 5300 2800 16000Isopentane970 2100 2300 5000Butane970 Not Detected 3900 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
116 70-1301,2-Dichloroethane-d4102 70-130Toluene-d895 70-1304-Bromofluorobenzene
Page 23 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(25)030409
Lab ID#: 0903253A-07A
MODIFIED EPA METHOD TO-15 GC/MS
b031330File Name:Dil. Factor: 24.2
Date of Collection: 3/4/09 3:40:00 PMDate of Analysis: 3/13/09 10:03 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
120 Not Detected 600 Not DetectedFreon 12120 Not Detected 840 Not DetectedFreon 114480 Not Detected 1000 Not DetectedChloromethane120 Not Detected 310 Not DetectedVinyl Chloride120 Not Detected 270 Not Detected1,3-Butadiene120 Not Detected 470 Not DetectedBromomethane120 Not Detected 320 Not DetectedChloroethane120 Not Detected 680 Not DetectedFreon 11480 Not Detected 910 Not DetectedEthanol120 Not Detected 930 Not DetectedFreon 113120 Not Detected 480 Not Detected1,1-Dichloroethene480 Not Detected 1100 Not DetectedAcetone480 Not Detected 1200 Not Detected2-Propanol120 Not Detected 380 Not DetectedCarbon Disulfide480 Not Detected 1500 Not Detected3-Chloropropene120 Not Detected 420 Not DetectedMethylene Chloride120 Not Detected 440 Not DetectedMethyl tert-butyl ether120 Not Detected 480 Not Detectedtrans-1,2-Dichloroethene120 Not Detected 430 Not DetectedHexane120 Not Detected 490 Not Detected1,1-Dichloroethane120 Not Detected 360 Not Detected2-Butanone (Methyl Ethyl Ketone)120 Not Detected 480 Not Detectedcis-1,2-Dichloroethene120 Not Detected 360 Not DetectedTetrahydrofuran120 Not Detected 590 Not DetectedChloroform120 Not Detected 660 Not Detected1,1,1-Trichloroethane120 Not Detected 420 Not DetectedCyclohexane120 Not Detected 760 Not DetectedCarbon Tetrachloride120 110000 560 5200002,2,4-Trimethylpentane120 Not Detected 390 Not DetectedBenzene120 Not Detected 490 Not Detected1,2-Dichloroethane120 Not Detected 500 Not DetectedHeptane120 Not Detected 650 Not DetectedTrichloroethene120 Not Detected 560 Not Detected1,2-Dichloropropane480 Not Detected 1700 Not Detected1,4-Dioxane120 Not Detected 810 Not DetectedBromodichloromethane120 Not Detected 550 Not Detectedcis-1,3-Dichloropropene120 Not Detected 500 Not Detected4-Methyl-2-pentanone120 Not Detected 460 Not DetectedToluene120 Not Detected 550 Not Detectedtrans-1,3-Dichloropropene
Page 24 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(25)030409
Lab ID#: 0903253A-07A
MODIFIED EPA METHOD TO-15 GC/MS
b031330File Name:Dil. Factor: 24.2
Date of Collection: 3/4/09 3:40:00 PMDate of Analysis: 3/13/09 10:03 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
120 Not Detected 660 Not Detected1,1,2-Trichloroethane120 Not Detected 820 Not DetectedTetrachloroethene480 Not Detected 2000 Not Detected2-Hexanone120 Not Detected 1000 Not DetectedDibromochloromethane120 Not Detected 930 Not Detected1,2-Dibromoethane (EDB)120 Not Detected 560 Not DetectedChlorobenzene120 Not Detected 520 Not DetectedEthyl Benzene120 Not Detected 520 Not Detectedm,p-Xylene120 Not Detected 520 Not Detectedo-Xylene120 Not Detected 520 Not DetectedStyrene120 Not Detected 1200 Not DetectedBromoform120 Not Detected 590 Not DetectedCumene120 Not Detected 830 Not Detected1,1,2,2-Tetrachloroethane120 Not Detected 590 Not DetectedPropylbenzene120 Not Detected 590 Not Detected4-Ethyltoluene120 Not Detected 590 Not Detected1,3,5-Trimethylbenzene120 Not Detected 590 Not Detected1,2,4-Trimethylbenzene120 Not Detected 730 Not Detected1,3-Dichlorobenzene120 Not Detected 730 Not Detected1,4-Dichlorobenzene120 Not Detected 630 Not Detectedalpha-Chlorotoluene120 Not Detected 730 Not Detected1,2-Dichlorobenzene480 Not Detected 3600 Not Detected1,2,4-Trichlorobenzene480 Not Detected 5200 Not DetectedHexachlorobutadiene480 Not Detected 2500 Not DetectedNaphthalene480 Not Detected 2600 Not DetectedButylbenzene480 Not Detected 2600 Not Detectedsec-Butylbenzene480 Not Detected 1400 Not DetectedIsopentane480 Not Detected 1200 Not DetectedButane480 Not Detected 1900 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
114 70-1301,2-Dichloroethane-d4102 70-130Toluene-d894 70-1304-Bromofluorobenzene
Page 25 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(20)030509
Lab ID#: 0903253A-08A
MODIFIED EPA METHOD TO-15 GC/MS
b031331File Name:Dil. Factor: 2.64
Date of Collection: 3/5/09 9:10:00 AMDate of Analysis: 3/13/09 10:20 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
13 Not Detected 65 Not DetectedFreon 1213 Not Detected 92 Not DetectedFreon 11453 Not Detected 110 Not DetectedChloromethane13 Not Detected 34 Not DetectedVinyl Chloride13 Not Detected 29 Not Detected1,3-Butadiene13 Not Detected 51 Not DetectedBromomethane13 Not Detected 35 Not DetectedChloroethane13 Not Detected 74 Not DetectedFreon 1153 Not Detected 99 Not DetectedEthanol13 Not Detected 100 Not DetectedFreon 11313 Not Detected 52 Not Detected1,1-Dichloroethene53 Not Detected 120 Not DetectedAcetone53 Not Detected 130 Not Detected2-Propanol13 Not Detected 41 Not DetectedCarbon Disulfide53 Not Detected 160 Not Detected3-Chloropropene13 Not Detected 46 Not DetectedMethylene Chloride13 Not Detected 48 Not DetectedMethyl tert-butyl ether13 Not Detected 52 Not Detectedtrans-1,2-Dichloroethene13 Not Detected 46 Not DetectedHexane13 Not Detected 53 Not Detected1,1-Dichloroethane13 Not Detected 39 Not Detected2-Butanone (Methyl Ethyl Ketone)13 Not Detected 52 Not Detectedcis-1,2-Dichloroethene13 Not Detected 39 Not DetectedTetrahydrofuran13 Not Detected 64 Not DetectedChloroform13 Not Detected 72 Not Detected1,1,1-Trichloroethane13 Not Detected 45 Not DetectedCyclohexane13 Not Detected 83 Not DetectedCarbon Tetrachloride13 5600 62 260002,2,4-Trimethylpentane13 Not Detected 42 Not DetectedBenzene13 Not Detected 53 Not Detected1,2-Dichloroethane13 Not Detected 54 Not DetectedHeptane13 Not Detected 71 Not DetectedTrichloroethene13 Not Detected 61 Not Detected1,2-Dichloropropane53 Not Detected 190 Not Detected1,4-Dioxane13 Not Detected 88 Not DetectedBromodichloromethane13 Not Detected 60 Not Detectedcis-1,3-Dichloropropene13 Not Detected 54 Not Detected4-Methyl-2-pentanone13 Not Detected 50 Not DetectedToluene13 Not Detected 60 Not Detectedtrans-1,3-Dichloropropene
Page 26 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(20)030509
Lab ID#: 0903253A-08A
MODIFIED EPA METHOD TO-15 GC/MS
b031331File Name:Dil. Factor: 2.64
Date of Collection: 3/5/09 9:10:00 AMDate of Analysis: 3/13/09 10:20 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
13 Not Detected 72 Not Detected1,1,2-Trichloroethane13 Not Detected 90 Not DetectedTetrachloroethene53 Not Detected 220 Not Detected2-Hexanone13 Not Detected 110 Not DetectedDibromochloromethane13 Not Detected 100 Not Detected1,2-Dibromoethane (EDB)13 Not Detected 61 Not DetectedChlorobenzene13 Not Detected 57 Not DetectedEthyl Benzene13 Not Detected 57 Not Detectedm,p-Xylene13 Not Detected 57 Not Detectedo-Xylene13 Not Detected 56 Not DetectedStyrene13 Not Detected 140 Not DetectedBromoform13 Not Detected 65 Not DetectedCumene13 Not Detected 91 Not Detected1,1,2,2-Tetrachloroethane13 Not Detected 65 Not DetectedPropylbenzene13 Not Detected 65 Not Detected4-Ethyltoluene13 Not Detected 65 Not Detected1,3,5-Trimethylbenzene13 Not Detected 65 Not Detected1,2,4-Trimethylbenzene13 Not Detected 79 Not Detected1,3-Dichlorobenzene13 Not Detected 79 Not Detected1,4-Dichlorobenzene13 Not Detected 68 Not Detectedalpha-Chlorotoluene13 Not Detected 79 Not Detected1,2-Dichlorobenzene53 Not Detected 390 Not Detected1,2,4-Trichlorobenzene53 Not Detected 560 Not DetectedHexachlorobutadiene53 Not Detected 280 Not DetectedNaphthalene53 Not Detected 290 Not DetectedButylbenzene53 Not Detected 290 Not Detectedsec-Butylbenzene53 Not Detected 160 Not DetectedIsopentane53 Not Detected 120 Not DetectedButane53 Not Detected 210 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
110 70-1301,2-Dichloroethane-d4100 70-130Toluene-d894 70-1304-Bromofluorobenzene
Page 27 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(15)030509
Lab ID#: 0903253A-09A
MODIFIED EPA METHOD TO-15 GC/MS
b031332File Name:Dil. Factor: 7.63
Date of Collection: 3/5/09 9:55:00 AMDate of Analysis: 3/13/09 10:38 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
38 Not Detected 190 Not DetectedFreon 1238 Not Detected 270 Not DetectedFreon 114150 Not Detected 320 Not DetectedChloromethane38 Not Detected 98 Not DetectedVinyl Chloride38 Not Detected 84 Not Detected1,3-Butadiene38 Not Detected 150 Not DetectedBromomethane38 Not Detected 100 Not DetectedChloroethane38 Not Detected 210 Not DetectedFreon 11150 Not Detected 290 Not DetectedEthanol38 Not Detected 290 Not DetectedFreon 11338 Not Detected 150 Not Detected1,1-Dichloroethene150 Not Detected 360 Not DetectedAcetone150 Not Detected 380 Not Detected2-Propanol38 Not Detected 120 Not DetectedCarbon Disulfide150 Not Detected 480 Not Detected3-Chloropropene38 Not Detected 130 Not DetectedMethylene Chloride38 Not Detected 140 Not DetectedMethyl tert-butyl ether38 Not Detected 150 Not Detectedtrans-1,2-Dichloroethene38 Not Detected 130 Not DetectedHexane38 Not Detected 150 Not Detected1,1-Dichloroethane38 Not Detected 110 Not Detected2-Butanone (Methyl Ethyl Ketone)38 Not Detected 150 Not Detectedcis-1,2-Dichloroethene38 Not Detected 110 Not DetectedTetrahydrofuran38 Not Detected 190 Not DetectedChloroform38 Not Detected 210 Not Detected1,1,1-Trichloroethane38 Not Detected 130 Not DetectedCyclohexane38 Not Detected 240 Not DetectedCarbon Tetrachloride38 23000 180 1100002,2,4-Trimethylpentane38 Not Detected 120 Not DetectedBenzene38 Not Detected 150 Not Detected1,2-Dichloroethane38 Not Detected 160 Not DetectedHeptane38 Not Detected 200 Not DetectedTrichloroethene38 Not Detected 180 Not Detected1,2-Dichloropropane150 Not Detected 550 Not Detected1,4-Dioxane38 Not Detected 260 Not DetectedBromodichloromethane38 Not Detected 170 Not Detectedcis-1,3-Dichloropropene38 Not Detected 160 Not Detected4-Methyl-2-pentanone38 Not Detected 140 Not DetectedToluene38 Not Detected 170 Not Detectedtrans-1,3-Dichloropropene
Page 28 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(15)030509
Lab ID#: 0903253A-09A
MODIFIED EPA METHOD TO-15 GC/MS
b031332File Name:Dil. Factor: 7.63
Date of Collection: 3/5/09 9:55:00 AMDate of Analysis: 3/13/09 10:38 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
38 Not Detected 210 Not Detected1,1,2-Trichloroethane38 Not Detected 260 Not DetectedTetrachloroethene150 Not Detected 620 Not Detected2-Hexanone38 Not Detected 320 Not DetectedDibromochloromethane38 Not Detected 290 Not Detected1,2-Dibromoethane (EDB)38 Not Detected 180 Not DetectedChlorobenzene38 Not Detected 160 Not DetectedEthyl Benzene38 Not Detected 160 Not Detectedm,p-Xylene38 Not Detected 160 Not Detectedo-Xylene38 Not Detected 160 Not DetectedStyrene38 Not Detected 390 Not DetectedBromoform38 Not Detected 190 Not DetectedCumene38 Not Detected 260 Not Detected1,1,2,2-Tetrachloroethane38 Not Detected 190 Not DetectedPropylbenzene38 Not Detected 190 Not Detected4-Ethyltoluene38 Not Detected 190 Not Detected1,3,5-Trimethylbenzene38 Not Detected 190 Not Detected1,2,4-Trimethylbenzene38 Not Detected 230 Not Detected1,3-Dichlorobenzene38 Not Detected 230 Not Detected1,4-Dichlorobenzene38 Not Detected 200 Not Detectedalpha-Chlorotoluene38 Not Detected 230 Not Detected1,2-Dichlorobenzene150 Not Detected 1100 Not Detected1,2,4-Trichlorobenzene150 Not Detected 1600 Not DetectedHexachlorobutadiene150 Not Detected 800 Not DetectedNaphthalene150 Not Detected 840 Not DetectedButylbenzene150 Not Detected 840 Not Detectedsec-Butylbenzene150 430 450 1300Isopentane150 Not Detected 360 Not DetectedButane150 Not Detected 610 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
116 70-1301,2-Dichloroethane-d4102 70-130Toluene-d894 70-1304-Bromofluorobenzene
Page 29 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(10)030509
Lab ID#: 0903253A-10A
MODIFIED EPA METHOD TO-15 GC/MS
b031333File Name:Dil. Factor: 25.2
Date of Collection: 3/5/09 11:35:00 AMDate of Analysis: 3/13/09 11:00 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
130 Not Detected 620 Not DetectedFreon 12130 Not Detected 880 Not DetectedFreon 114500 Not Detected 1000 Not DetectedChloromethane130 Not Detected 320 Not DetectedVinyl Chloride130 Not Detected 280 Not Detected1,3-Butadiene130 Not Detected 490 Not DetectedBromomethane130 Not Detected 330 Not DetectedChloroethane130 Not Detected 710 Not DetectedFreon 11500 Not Detected 950 Not DetectedEthanol130 Not Detected 960 Not DetectedFreon 113130 Not Detected 500 Not Detected1,1-Dichloroethene500 Not Detected 1200 Not DetectedAcetone500 Not Detected 1200 Not Detected2-Propanol130 Not Detected 390 Not DetectedCarbon Disulfide500 Not Detected 1600 Not Detected3-Chloropropene130 Not Detected 440 Not DetectedMethylene Chloride130 Not Detected 450 Not DetectedMethyl tert-butyl ether130 Not Detected 500 Not Detectedtrans-1,2-Dichloroethene130 Not Detected 440 Not DetectedHexane130 Not Detected 510 Not Detected1,1-Dichloroethane130 Not Detected 370 Not Detected2-Butanone (Methyl Ethyl Ketone)130 Not Detected 500 Not Detectedcis-1,2-Dichloroethene130 Not Detected 370 Not DetectedTetrahydrofuran130 Not Detected 620 Not DetectedChloroform130 Not Detected 690 Not Detected1,1,1-Trichloroethane130 Not Detected 430 Not DetectedCyclohexane130 Not Detected 790 Not DetectedCarbon Tetrachloride130 59000 590 2800002,2,4-Trimethylpentane130 Not Detected 400 Not DetectedBenzene130 Not Detected 510 Not Detected1,2-Dichloroethane130 Not Detected 520 Not DetectedHeptane130 Not Detected 680 Not DetectedTrichloroethene130 Not Detected 580 Not Detected1,2-Dichloropropane500 Not Detected 1800 Not Detected1,4-Dioxane130 Not Detected 840 Not DetectedBromodichloromethane130 Not Detected 570 Not Detectedcis-1,3-Dichloropropene130 Not Detected 520 Not Detected4-Methyl-2-pentanone130 Not Detected 470 Not DetectedToluene130 Not Detected 570 Not Detectedtrans-1,3-Dichloropropene
Page 30 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(10)030509
Lab ID#: 0903253A-10A
MODIFIED EPA METHOD TO-15 GC/MS
b031333File Name:Dil. Factor: 25.2
Date of Collection: 3/5/09 11:35:00 AMDate of Analysis: 3/13/09 11:00 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
130 Not Detected 690 Not Detected1,1,2-Trichloroethane130 Not Detected 850 Not DetectedTetrachloroethene500 Not Detected 2100 Not Detected2-Hexanone130 Not Detected 1100 Not DetectedDibromochloromethane130 Not Detected 970 Not Detected1,2-Dibromoethane (EDB)130 Not Detected 580 Not DetectedChlorobenzene130 Not Detected 550 Not DetectedEthyl Benzene130 Not Detected 550 Not Detectedm,p-Xylene130 Not Detected 550 Not Detectedo-Xylene130 Not Detected 540 Not DetectedStyrene130 Not Detected 1300 Not DetectedBromoform130 Not Detected 620 Not DetectedCumene130 Not Detected 860 Not Detected1,1,2,2-Tetrachloroethane130 Not Detected 620 Not DetectedPropylbenzene130 Not Detected 620 Not Detected4-Ethyltoluene130 Not Detected 620 Not Detected1,3,5-Trimethylbenzene130 Not Detected 620 Not Detected1,2,4-Trimethylbenzene130 Not Detected 760 Not Detected1,3-Dichlorobenzene130 Not Detected 760 Not Detected1,4-Dichlorobenzene130 Not Detected 650 Not Detectedalpha-Chlorotoluene130 Not Detected 760 Not Detected1,2-Dichlorobenzene500 Not Detected 3700 Not Detected1,2,4-Trichlorobenzene500 Not Detected 5400 Not DetectedHexachlorobutadiene500 Not Detected 2600 Not DetectedNaphthalene500 Not Detected 2800 Not DetectedButylbenzene500 Not Detected 2800 Not Detectedsec-Butylbenzene500 2700 1500 7900Isopentane500 Not Detected 1200 Not DetectedButane500 Not Detected 2000 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
112 70-1301,2-Dichloroethane-d4102 70-130Toluene-d895 70-1304-Bromofluorobenzene
Page 31 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(5)030509
Lab ID#: 0903253A-11A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031314File Name:Dil. Factor: 2.42
Date of Collection: 3/5/09 12:55:00 PMDate of Analysis: 3/13/09 07:44 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 6.0 Not DetectedFreon 121.2 Not Detected 8.4 Not DetectedFreon 1141.2 Not Detected 3.1 Not DetectedVinyl Chloride1.2 Not Detected 4.7 Not DetectedBromomethane1.2 Not Detected 3.2 Not DetectedChloroethane1.2 Not Detected 6.8 Not DetectedFreon 111.2 Not Detected 4.8 Not Detected1,1-Dichloroethene1.2 Not Detected 9.3 Not DetectedFreon 1131.2 Not Detected 4.2 Not DetectedMethylene Chloride1.2 Not Detected 4.9 Not Detected1,1-Dichloroethane1.2 Not Detected 4.8 Not Detectedcis-1,2-Dichloroethene1.2 Not Detected 5.9 Not DetectedChloroform1.2 Not Detected 6.6 Not Detected1,1,1-Trichloroethane1.2 Not Detected 7.6 Not DetectedCarbon Tetrachloride1.2 Not Detected 3.9 Not DetectedBenzene1.2 Not Detected 4.9 Not Detected1,2-Dichloroethane1.2 Not Detected 6.5 Not DetectedTrichloroethene1.2 Not Detected 5.6 Not Detected1,2-Dichloropropane1.2 Not Detected 5.5 Not Detectedcis-1,3-Dichloropropene1.2 Not Detected 4.6 Not DetectedToluene1.2 Not Detected 5.5 Not Detectedtrans-1,3-Dichloropropene1.2 Not Detected 6.6 Not Detected1,1,2-Trichloroethane1.2 Not Detected 8.2 Not DetectedTetrachloroethene1.2 Not Detected 9.3 Not Detected1,2-Dibromoethane (EDB)1.2 Not Detected 5.6 Not DetectedChlorobenzene1.2 Not Detected 5.2 Not DetectedEthyl Benzene1.2 Not Detected 5.2 Not Detectedm,p-Xylene1.2 Not Detected 5.2 Not Detectedo-Xylene1.2 Not Detected 5.2 Not DetectedStyrene1.2 Not Detected 8.3 Not Detected1,1,2,2-Tetrachloroethane1.2 Not Detected 5.9 Not Detected1,3,5-Trimethylbenzene1.2 Not Detected 5.9 Not Detected1,2,4-Trimethylbenzene1.2 Not Detected 7.3 Not Detected1,3-Dichlorobenzene1.2 Not Detected 7.3 Not Detected1,4-Dichlorobenzene1.2 Not Detected 6.3 Not Detectedalpha-Chlorotoluene1.2 Not Detected 7.3 Not Detected1,2-Dichlorobenzene1.2 Not Detected 2.7 Not Detected1,3-Butadiene1.2 Not Detected 4.3 Not DetectedHexane1.2 Not Detected 4.2 Not DetectedCyclohexane
Page 32 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: VW-96(5)030509
Lab ID#: 0903253A-11A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031314File Name:Dil. Factor: 2.42
Date of Collection: 3/5/09 12:55:00 PMDate of Analysis: 3/13/09 07:44 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
1.2 Not Detected 5.0 Not DetectedHeptane1.2 Not Detected 8.1 Not DetectedBromodichloromethane1.2 Not Detected 10 Not DetectedDibromochloromethane1.2 Not Detected 5.9 Not DetectedCumene1.2 Not Detected 5.9 Not DetectedPropylbenzene4.8 Not Detected 10 Not DetectedChloromethane4.8 Not Detected 36 Not Detected1,2,4-Trichlorobenzene4.8 Not Detected 52 Not DetectedHexachlorobutadiene4.8 Not Detected 11 Not DetectedAcetone1.2 Not Detected 3.8 Not DetectedCarbon Disulfide4.8 Not Detected 12 Not Detected2-Propanol1.2 Not Detected 4.8 Not Detectedtrans-1,2-Dichloroethene1.2 Not Detected 3.6 Not Detected2-Butanone (Methyl Ethyl Ketone)1.2 Not Detected 3.6 Not DetectedTetrahydrofuran4.8 Not Detected 17 Not Detected1,4-Dioxane1.2 Not Detected 5.0 Not Detected4-Methyl-2-pentanone4.8 Not Detected 20 Not Detected2-Hexanone1.2 Not Detected 12 Not DetectedBromoform1.2 Not Detected 5.9 Not Detected4-Ethyltoluene4.8 Not Detected 9.1 Not DetectedEthanol1.2 Not Detected 4.4 Not DetectedMethyl tert-butyl ether4.8 Not Detected 15 Not Detected3-Chloropropene1.2 14 5.6 672,2,4-Trimethylpentane4.8 Not Detected 25 Not DetectedNaphthalene4.8 Not Detected 26 Not DetectedButylbenzene4.8 Not Detected 26 Not Detectedsec-Butylbenzene4.8 20 14 58Isopentane4.8 Not Detected 12 Not DetectedButane4.8 Not Detected 19 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
99 70-130Toluene-d8105 70-1301,2-Dichloroethane-d493 70-1304-Bromofluorobenzene
Page 33 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: BD-1,030509
Lab ID#: 0903253A-12A
MODIFIED EPA METHOD TO-15 GC/MS
b031334File Name:Dil. Factor: 21.0
Date of Collection: 3/5/09 1/1/1990Date of Analysis: 3/13/09 11:31 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
100 Not Detected 520 Not DetectedFreon 12100 Not Detected 730 Not DetectedFreon 114420 Not Detected 870 Not DetectedChloromethane100 Not Detected 270 Not DetectedVinyl Chloride100 Not Detected 230 Not Detected1,3-Butadiene100 Not Detected 410 Not DetectedBromomethane100 Not Detected 280 Not DetectedChloroethane100 Not Detected 590 Not DetectedFreon 11420 Not Detected 790 Not DetectedEthanol100 Not Detected 800 Not DetectedFreon 113100 Not Detected 420 Not Detected1,1-Dichloroethene420 Not Detected 1000 Not DetectedAcetone420 Not Detected 1000 Not Detected2-Propanol100 Not Detected 330 Not DetectedCarbon Disulfide420 Not Detected 1300 Not Detected3-Chloropropene100 Not Detected 360 Not DetectedMethylene Chloride100 Not Detected 380 Not DetectedMethyl tert-butyl ether100 Not Detected 420 Not Detectedtrans-1,2-Dichloroethene100 Not Detected 370 Not DetectedHexane100 Not Detected 420 Not Detected1,1-Dichloroethane100 Not Detected 310 Not Detected2-Butanone (Methyl Ethyl Ketone)100 Not Detected 420 Not Detectedcis-1,2-Dichloroethene100 Not Detected 310 Not DetectedTetrahydrofuran100 Not Detected 510 Not DetectedChloroform100 Not Detected 570 Not Detected1,1,1-Trichloroethane100 Not Detected 360 Not DetectedCyclohexane100 Not Detected 660 Not DetectedCarbon Tetrachloride100 61000 490 2800002,2,4-Trimethylpentane100 Not Detected 340 Not DetectedBenzene100 Not Detected 420 Not Detected1,2-Dichloroethane100 Not Detected 430 Not DetectedHeptane100 Not Detected 560 Not DetectedTrichloroethene100 Not Detected 480 Not Detected1,2-Dichloropropane420 Not Detected 1500 Not Detected1,4-Dioxane100 Not Detected 700 Not DetectedBromodichloromethane100 Not Detected 480 Not Detectedcis-1,3-Dichloropropene100 Not Detected 430 Not Detected4-Methyl-2-pentanone100 Not Detected 400 Not DetectedToluene100 Not Detected 480 Not Detectedtrans-1,3-Dichloropropene
Page 34 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: BD-1,030509
Lab ID#: 0903253A-12A
MODIFIED EPA METHOD TO-15 GC/MS
b031334File Name:Dil. Factor: 21.0
Date of Collection: 3/5/09 1/1/1990Date of Analysis: 3/13/09 11:31 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
100 Not Detected 570 Not Detected1,1,2-Trichloroethane100 Not Detected 710 Not DetectedTetrachloroethene420 Not Detected 1700 Not Detected2-Hexanone100 Not Detected 890 Not DetectedDibromochloromethane100 Not Detected 810 Not Detected1,2-Dibromoethane (EDB)100 Not Detected 480 Not DetectedChlorobenzene100 Not Detected 460 Not DetectedEthyl Benzene100 Not Detected 460 Not Detectedm,p-Xylene100 Not Detected 460 Not Detectedo-Xylene100 Not Detected 450 Not DetectedStyrene100 Not Detected 1100 Not DetectedBromoform100 Not Detected 520 Not DetectedCumene100 Not Detected 720 Not Detected1,1,2,2-Tetrachloroethane100 Not Detected 520 Not DetectedPropylbenzene100 Not Detected 520 Not Detected4-Ethyltoluene100 Not Detected 520 Not Detected1,3,5-Trimethylbenzene100 Not Detected 520 Not Detected1,2,4-Trimethylbenzene100 Not Detected 630 Not Detected1,3-Dichlorobenzene100 Not Detected 630 Not Detected1,4-Dichlorobenzene100 Not Detected 540 Not Detectedalpha-Chlorotoluene100 Not Detected 630 Not Detected1,2-Dichlorobenzene420 Not Detected 3100 Not Detected1,2,4-Trichlorobenzene420 Not Detected 4500 Not DetectedHexachlorobutadiene420 Not Detected 2200 Not DetectedNaphthalene420 Not Detected 2300 Not DetectedButylbenzene420 Not Detected 2300 Not Detectedsec-Butylbenzene420 2700 1200 8100Isopentane420 450 1000 1100Butane420 Not Detected 1700 Not DetectedMethylcyclohexane
Container Type: 1 Liter Summa Canister (100% Certified)
Limits%RecoverySurrogatesMethod
118 70-1301,2-Dichloroethane-d4102 70-130Toluene-d895 70-1304-Bromofluorobenzene
Page 35 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: Lab Blank
Lab ID#: 0903253A-13A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031306cFile Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 12:17 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 120.50 Not Detected 3.5 Not DetectedFreon 1140.50 Not Detected 1.3 Not DetectedVinyl Chloride0.50 Not Detected 1.9 Not DetectedBromomethane0.50 Not Detected 1.3 Not DetectedChloroethane0.50 Not Detected 2.8 Not DetectedFreon 110.50 Not Detected 2.0 Not Detected1,1-Dichloroethene0.50 Not Detected 3.8 Not DetectedFreon 1130.50 Not Detected 1.7 Not DetectedMethylene Chloride0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene0.50 Not Detected 2.4 Not DetectedChloroform0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride0.50 Not Detected 1.6 Not DetectedBenzene0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane0.50 Not Detected 2.7 Not DetectedTrichloroethene0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene0.50 Not Detected 1.9 Not DetectedToluene0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane0.50 Not Detected 3.4 Not DetectedTetrachloroethene0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)0.50 Not Detected 2.3 Not DetectedChlorobenzene0.50 Not Detected 2.2 Not DetectedEthyl Benzene0.50 Not Detected 2.2 Not Detectedm,p-Xylene0.50 Not Detected 2.2 Not Detectedo-Xylene0.50 Not Detected 2.1 Not DetectedStyrene0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene0.50 Not Detected 1.1 Not Detected1,3-Butadiene0.50 Not Detected 1.8 Not DetectedHexane0.50 Not Detected 1.7 Not DetectedCyclohexane
Page 36 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: Lab Blank
Lab ID#: 0903253A-13A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031306cFile Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 12:17 PM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.0 Not DetectedHeptane0.50 Not Detected 3.4 Not DetectedBromodichloromethane0.50 Not Detected 4.2 Not DetectedDibromochloromethane0.50 Not Detected 2.4 Not DetectedCumene0.50 Not Detected 2.4 Not DetectedPropylbenzene2.0 Not Detected 4.1 Not DetectedChloromethane2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene2.0 Not Detected 21 Not DetectedHexachlorobutadiene2.0 Not Detected 4.8 Not DetectedAcetone
0.50 Not Detected 1.6 Not DetectedCarbon Disulfide2.0 Not Detected 4.9 Not Detected2-Propanol
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene0.50 Not Detected 1.5 Not Detected2-Butanone (Methyl Ethyl Ketone)0.50 Not Detected 1.5 Not DetectedTetrahydrofuran2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone2.0 Not Detected 8.2 Not Detected2-Hexanone
0.50 Not Detected 5.2 Not DetectedBromoform0.50 Not Detected 2.4 Not Detected4-Ethyltoluene2.0 Not Detected 3.8 Not DetectedEthanol
0.50 Not Detected 1.8 Not DetectedMethyl tert-butyl ether2.0 Not Detected 6.3 Not Detected3-Chloropropene
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane2.0 Not Detected 10 Not DetectedNaphthalene2.0 Not Detected 11 Not DetectedButylbenzene2.0 Not Detected 11 Not Detectedsec-Butylbenzene2.0 Not Detected 5.9 Not DetectedIsopentane2.0 Not Detected 4.8 Not DetectedButane2.0 Not Detected 8.0 Not DetectedMethylcyclohexane
Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
98 70-130Toluene-d8106 70-1301,2-Dichloroethane-d496 70-1304-Bromofluorobenzene
Page 37 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: Lab Blank
Lab ID#: 0903253A-13B
MODIFIED EPA METHOD TO-15 GC/MS
b031306aFile Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 10:53 AM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
5.0 Not Detected 25 Not DetectedFreon 125.0 Not Detected 35 Not DetectedFreon 11420 Not Detected 41 Not DetectedChloromethane5.0 Not Detected 13 Not DetectedVinyl Chloride5.0 Not Detected 11 Not Detected1,3-Butadiene5.0 Not Detected 19 Not DetectedBromomethane5.0 Not Detected 13 Not DetectedChloroethane5.0 Not Detected 28 Not DetectedFreon 1120 Not Detected 38 Not DetectedEthanol5.0 Not Detected 38 Not DetectedFreon 1135.0 Not Detected 20 Not Detected1,1-Dichloroethene20 Not Detected 48 Not DetectedAcetone20 Not Detected 49 Not Detected2-Propanol5.0 Not Detected 16 Not DetectedCarbon Disulfide20 Not Detected 63 Not Detected3-Chloropropene5.0 Not Detected 17 Not DetectedMethylene Chloride5.0 Not Detected 18 Not DetectedMethyl tert-butyl ether5.0 Not Detected 20 Not Detectedtrans-1,2-Dichloroethene5.0 Not Detected 18 Not DetectedHexane5.0 Not Detected 20 Not Detected1,1-Dichloroethane5.0 Not Detected 15 Not Detected2-Butanone (Methyl Ethyl Ketone)5.0 Not Detected 20 Not Detectedcis-1,2-Dichloroethene5.0 Not Detected 15 Not DetectedTetrahydrofuran5.0 Not Detected 24 Not DetectedChloroform5.0 Not Detected 27 Not Detected1,1,1-Trichloroethane5.0 Not Detected 17 Not DetectedCyclohexane5.0 Not Detected 31 Not DetectedCarbon Tetrachloride5.0 Not Detected 23 Not Detected2,2,4-Trimethylpentane5.0 Not Detected 16 Not DetectedBenzene5.0 Not Detected 20 Not Detected1,2-Dichloroethane5.0 Not Detected 20 Not DetectedHeptane5.0 Not Detected 27 Not DetectedTrichloroethene5.0 Not Detected 23 Not Detected1,2-Dichloropropane20 Not Detected 72 Not Detected1,4-Dioxane5.0 Not Detected 34 Not DetectedBromodichloromethane5.0 Not Detected 23 Not Detectedcis-1,3-Dichloropropene5.0 Not Detected 20 Not Detected4-Methyl-2-pentanone5.0 Not Detected 19 Not DetectedToluene5.0 Not Detected 23 Not Detectedtrans-1,3-Dichloropropene
Page 38 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: Lab Blank
Lab ID#: 0903253A-13B
MODIFIED EPA METHOD TO-15 GC/MS
b031306aFile Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 10:53 AM
(uG/m3)(uG/m3)(ppbv)(ppbv)CompoundAmountRpt. LimitAmountRpt. Limit
5.0 Not Detected 27 Not Detected1,1,2-Trichloroethane5.0 Not Detected 34 Not DetectedTetrachloroethene20 Not Detected 82 Not Detected2-Hexanone5.0 Not Detected 42 Not DetectedDibromochloromethane5.0 Not Detected 38 Not Detected1,2-Dibromoethane (EDB)5.0 Not Detected 23 Not DetectedChlorobenzene5.0 Not Detected 22 Not DetectedEthyl Benzene5.0 Not Detected 22 Not Detectedm,p-Xylene5.0 Not Detected 22 Not Detectedo-Xylene5.0 Not Detected 21 Not DetectedStyrene5.0 Not Detected 52 Not DetectedBromoform5.0 Not Detected 24 Not DetectedCumene5.0 Not Detected 34 Not Detected1,1,2,2-Tetrachloroethane5.0 Not Detected 24 Not DetectedPropylbenzene5.0 Not Detected 24 Not Detected4-Ethyltoluene5.0 Not Detected 24 Not Detected1,3,5-Trimethylbenzene5.0 Not Detected 24 Not Detected1,2,4-Trimethylbenzene5.0 Not Detected 30 Not Detected1,3-Dichlorobenzene5.0 Not Detected 30 Not Detected1,4-Dichlorobenzene5.0 Not Detected 26 Not Detectedalpha-Chlorotoluene5.0 Not Detected 30 Not Detected1,2-Dichlorobenzene20 Not Detected 150 Not Detected1,2,4-Trichlorobenzene20 Not Detected 210 Not DetectedHexachlorobutadiene20 Not Detected 100 Not DetectedNaphthalene20 Not Detected 110 Not DetectedButylbenzene20 Not Detected 110 Not Detectedsec-Butylbenzene20 Not Detected 59 Not DetectedIsopentane20 Not Detected 48 Not DetectedButane20 Not Detected 80 Not DetectedMethylcyclohexane
Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
95 70-1301,2-Dichloroethane-d4100 70-130Toluene-d894 70-1304-Bromofluorobenzene
Page 39 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: CCV
Lab ID#: 0903253A-14A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031302File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 08:38 AM
%RecoveryCompound
96Freon 1296Freon 11499Vinyl Chloride92Bromomethane87Chloroethane96Freon 11941,1-Dichloroethene91Freon 113103Methylene Chloride921,1-Dichloroethane95cis-1,2-Dichloroethene98Chloroform951,1,1-Trichloroethane96Carbon Tetrachloride98Benzene1001,2-Dichloroethane93Trichloroethene941,2-Dichloropropane96cis-1,3-Dichloropropene95Toluene98trans-1,3-Dichloropropene961,1,2-Trichloroethane96Tetrachloroethene991,2-Dibromoethane (EDB)94Chlorobenzene95Ethyl Benzene94m,p-Xylene93o-Xylene95Styrene931,1,2,2-Tetrachloroethane941,3,5-Trimethylbenzene941,2,4-Trimethylbenzene881,3-Dichlorobenzene891,4-Dichlorobenzene94alpha-Chlorotoluene851,2-Dichlorobenzene1061,3-Butadiene93Hexane90Cyclohexane
Page 40 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: CCV
Lab ID#: 0903253A-14A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031302File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 08:38 AM
%RecoveryCompound
94Heptane97Bromodichloromethane99Dibromochloromethane98Cumene95Propylbenzene106Chloromethane801,2,4-Trichlorobenzene82Hexachlorobutadiene96Acetone91Carbon Disulfide992-Propanol92trans-1,2-Dichloroethene912-Butanone (Methyl Ethyl Ketone)101Tetrahydrofuran921,4-Dioxane924-Methyl-2-pentanone932-Hexanone101Bromoform974-Ethyltoluene102Ethanol91Methyl tert-butyl ether913-Chloropropene962,2,4-Trimethylpentane74Naphthalene93Butylbenzene92sec-Butylbenzene100Isopentane104Butane92Methylcyclohexane
Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
101 70-130Toluene-d8104 70-1301,2-Dichloroethane-d499 70-1304-Bromofluorobenzene
Page 41 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: CCV
Lab ID#: 0903253A-14B
MODIFIED EPA METHOD TO-15 GC/MS
b031302File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 09:21 AM
%RecoveryCompound
97Freon 1297Freon 114100Chloromethane97Vinyl Chloride941,3-Butadiene102Bromomethane96Chloroethane98Freon 11102Ethanol97Freon 113951,1-Dichloroethene90Acetone892-Propanol100Carbon Disulfide943-Chloropropene94Methylene Chloride100Methyl tert-butyl ether100trans-1,2-Dichloroethene94Hexane971,1-Dichloroethane982-Butanone (Methyl Ethyl Ketone)95cis-1,2-Dichloroethene94Tetrahydrofuran99Chloroform951,1,1-Trichloroethane98Cyclohexane95Carbon Tetrachloride952,2,4-Trimethylpentane101Benzene951,2-Dichloroethane101Heptane97Trichloroethene971,2-Dichloropropane961,4-Dioxane97Bromodichloromethane96cis-1,3-Dichloropropene944-Methyl-2-pentanone100Toluene93trans-1,3-Dichloropropene
Page 42 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: CCV
Lab ID#: 0903253A-14B
MODIFIED EPA METHOD TO-15 GC/MS
b031302File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 09:21 AM
%RecoveryCompound
981,1,2-Trichloroethane100Tetrachloroethene902-Hexanone99Dibromochloromethane971,2-Dibromoethane (EDB)97Chlorobenzene97Ethyl Benzene98m,p-Xylene97o-Xylene99Styrene98Bromoform97Cumene961,1,2,2-Tetrachloroethane97Propylbenzene974-Ethyltoluene941,3,5-Trimethylbenzene911,2,4-Trimethylbenzene911,3-Dichlorobenzene901,4-Dichlorobenzene95alpha-Chlorotoluene891,2-Dichlorobenzene961,2,4-Trichlorobenzene100Hexachlorobutadiene93Naphthalene78Butylbenzene85sec-Butylbenzene93Isopentane96Butane101Methylcyclohexane
Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
95 70-1301,2-Dichloroethane-d4102 70-130Toluene-d899 70-1304-Bromofluorobenzene
Page 43 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: LCS
Lab ID#: 0903253A-15A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031303File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 09:11 AM
%RecoveryCompound
94Freon 1294Freon 11494Vinyl Chloride92Bromomethane88Chloroethane97Freon 111071,1-Dichloroethene103Freon 113114Methylene Chloride1001,1-Dichloroethane104cis-1,2-Dichloroethene102Chloroform1001,1,1-Trichloroethane101Carbon Tetrachloride100Benzene1021,2-Dichloroethane97Trichloroethene951,2-Dichloropropane95cis-1,3-Dichloropropene100Toluene98trans-1,3-Dichloropropene981,1,2-Trichloroethane98Tetrachloroethene961,2-Dibromoethane (EDB)95Chlorobenzene95Ethyl Benzene94m,p-Xylene94o-Xylene98Styrene921,1,2,2-Tetrachloroethane951,3,5-Trimethylbenzene941,2,4-Trimethylbenzene881,3-Dichlorobenzene871,4-Dichlorobenzene98alpha-Chlorotoluene831,2-Dichlorobenzene941,3-Butadiene98Hexane95Cyclohexane
Page 44 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: LCS
Lab ID#: 0903253A-15A
MODIFIED EPA METHOD TO-15 GC/MS FULL SCAN
r031303File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 09:11 AM
%RecoveryCompound
97Heptane99Bromodichloromethane100Dibromochloromethane101Cumene98Propylbenzene105Chloromethane791,2,4-Trichlorobenzene78Hexachlorobutadiene102Acetone94Carbon Disulfide1072-Propanol96trans-1,2-Dichloroethene942-Butanone (Methyl Ethyl Ketone)104Tetrahydrofuran921,4-Dioxane944-Methyl-2-pentanone952-Hexanone102Bromoform984-Ethyltoluene80Ethanol96Methyl tert-butyl ether943-Chloropropene992,2,4-Trimethylpentane79Naphthalene
Not SpikedButylbenzeneNot Spikedsec-Butylbenzene
101Isopentane99Butane97Methylcyclohexane
Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
99 70-130Toluene-d8104 70-1301,2-Dichloroethane-d499 70-1304-Bromofluorobenzene
Page 45 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: LCS
Lab ID#: 0903253A-15B
MODIFIED EPA METHOD TO-15 GC/MS
b031304File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 10:00 AM
%RecoveryCompound
84Freon 1285Freon 11477Chloromethane83Vinyl Chloride771,3-Butadiene96Bromomethane83Chloroethane85Freon 1164Ethanol86Freon 113851,1-Dichloroethene77Acetone872-Propanol81Carbon Disulfide773-Chloropropene82Methylene Chloride88Methyl tert-butyl ether79trans-1,2-Dichloroethene75Hexane851,1-Dichloroethane782-Butanone (Methyl Ethyl Ketone)83cis-1,2-Dichloroethene73Tetrahydrofuran86Chloroform841,1,1-Trichloroethane78Cyclohexane86Carbon Tetrachloride752,2,4-Trimethylpentane88Benzene831,2-Dichloroethane78Heptane85Trichloroethene841,2-Dichloropropane761,4-Dioxane78Bromodichloromethane86cis-1,3-Dichloropropene774-Methyl-2-pentanone87Toluene85trans-1,3-Dichloropropene
Page 46 of 47
AN ENVIRONMENTAL ANALYTICAL LABORATORY
Client Sample ID: LCS
Lab ID#: 0903253A-15B
MODIFIED EPA METHOD TO-15 GC/MS
b031304File Name:Dil. Factor: 1.00
Date of Collection: NA Date of Analysis: 3/13/09 10:00 AM
%RecoveryCompound
871,1,2-Trichloroethane85Tetrachloroethene742-Hexanone80Dibromochloromethane871,2-Dibromoethane (EDB)84Chlorobenzene85Ethyl Benzene85m,p-Xylene84o-Xylene89Styrene81Bromoform84Cumene821,1,2,2-Tetrachloroethane75Propylbenzene764-Ethyltoluene791,3,5-Trimethylbenzene801,2,4-Trimethylbenzene771,3-Dichlorobenzene771,4-Dichlorobenzene87alpha-Chlorotoluene731,2-Dichlorobenzene
69 Q1,2,4-Trichlorobenzene72Hexachlorobutadiene81Naphthalene
Not SpikedButylbenzeneNot Spikedsec-Butylbenzene
74Isopentane81Butane78Methylcyclohexane
Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable
Limits%RecoverySurrogatesMethod
95 70-1301,2-Dichloroethane-d4101 70-130Toluene-d899 70-1304-Bromofluorobenzene
Page 47 of 47
