AIM-8800 - Shimadzu · C103-E056F AIM-8800 Infrared Microscope AIM-8800 Printed in Japan...

C103-E056FAIM

Infrared Microscope

AIM-8800

Printed in Japan 3655-06212-30AIT

Company names, product/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation or its affiliates, whether or not they are used with trademark symbol “TM” or “®”.Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services. Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own.

For Research Use Only. Not for use in diagnostic procedures. The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication.

Right on Target...AIM-8800

Complete Control with AIMView®

ATR Objective

ATR-8800M

High Sensitivity, Maintenance-Free MCT DetectorHigh sensitivity—of course! A signal-to-noise ratio of 2600 to 1 is guaranteed in transmission measurement. The high-sensitivity glass dewar type MCT detector eliminates the need to re-evacuate every 1 to 2 years, as required with metallic dewar type MCT detectors.

Abundant OptionsA variety of options are available, including an ATR objective, 32× objective, mapping software, etc.

This intelligent infrared microscope provides convenient control of stage movement, aperture

setting and focusing, all from the PC screen. Supporting analysis using transmission, reflection as

well as ATR methods, the AIM-8800 widens the range of application fields. And in addition to

emphasis on sensitivity for basic performance, ease of operation was also a high design priority.

The AIM-8800 Infrared Microscope advances one step further into the new generation.

Auto X-Y Stage — Simplifies exact sample positioning.

Up to 10 sample positions and 2 background positions can be placed into memory, and the stage can be moved in increments as small as 1µm for finely detailed mapping.

Auto Focus — True focus is only one mouse-click away!

Arduous focusing is unnecessary. Just one click of the mouse automatically brings the image into focus.

Auto Aperture — Maximizes IR illumination on the sample spot.

The aperture is motor-driven, and its size and angle are freely set using mouse operation alone. Simply set the aperture over the sample, and the sampling area is automatically positioned for maximum infrared intensity. The aperture size and angle are always maintained.

Auto Centering — Sample viewing couldn’t be easier!

Double-clicking on any point in the visible observation screen will bring that spot to the center of the viewing area.

(Note : AIMView is the registered trademark of the software used to control the AIM-8800 Shimadzu Infrared Microscope.)

Auto MeasurementMemorized positions are automatically measured.Image of the measured position is also stored in the spectrum.

Right on Target...AIM-8800

Complete Control with AIMView®

ATR Objective

ATR-8800M

High Sensitivity, Maintenance-Free MCT DetectorHigh sensitivity—of course! A signal-to-noise ratio of 2600 to 1 is guaranteed in transmission measurement. The high-sensitivity glass dewar type MCT detector eliminates the need to re-evacuate every 1 to 2 years, as required with metallic dewar type MCT detectors.

Abundant OptionsA variety of options are available, including an ATR objective, 32× objective, mapping software, etc.

This intelligent infrared microscope provides convenient control of stage movement, aperture

setting and focusing, all from the PC screen. Supporting analysis using transmission, reflection as

well as ATR methods, the AIM-8800 widens the range of application fields. And in addition to

emphasis on sensitivity for basic performance, ease of operation was also a high design priority.

The AIM-8800 Infrared Microscope advances one step further into the new generation.

Auto X-Y Stage — Simplifies exact sample positioning.

Up to 10 sample positions and 2 background positions can be placed into memory, and the stage can be moved in increments as small as 1µm for finely detailed mapping.

Auto Focus — True focus is only one mouse-click away!

Arduous focusing is unnecessary. Just one click of the mouse automatically brings the image into focus.

Auto Aperture — Maximizes IR illumination on the sample spot.

The aperture is motor-driven, and its size and angle are freely set using mouse operation alone. Simply set the aperture over the sample, and the sampling area is automatically positioned for maximum infrared intensity. The aperture size and angle are always maintained.

Auto Centering — Sample viewing couldn’t be easier!

Double-clicking on any point in the visible observation screen will bring that spot to the center of the viewing area.

(Note : AIMView is the registered trademark of the software used to control the AIM-8800 Shimadzu Infrared Microscope.)

Auto MeasurementMemorized positions are automatically measured.Image of the measured position is also stored in the spectrum.

Operation is also possible from the AIM-8800 main unit controller.

All operations for controlling the infrared microscope areperformed on the PC screen.

Double-click on any point in the visible observation screen, and that location instantly moves to the center of the viewing area.

Auto X-Y stage X-axis movement

Manual focus adjustment

Auto X-Y stage Y-axis movement

Visible observation screen

Measurement position is moved to right-hand screen

Returns to recordedposition

Maximize display

Aperture Setting screen

Link 1

When mounting the sample stage to the Auto X-Y stage, clicking the position of the displayed opening automatically moves the Auto X-Y stage to the center of the sample stage opening.

Link 2

Auto Centering

Sample Holder

Up to 10 sample positions and 2 background positions can be placed into memory; and at the same time, the aperture size and angle are also recorded.

Link 3

Position Recording

Easy Operation with AIM View

Aperture Setting Click near corner to changethe aperture angle.

Aperture Setting Enter a number to set the size

Auto MeasurementMemorized positions are automatically measured.**) When LabSolutions IR is used.

Auto focusVisual mode - IR mode switching

Transmission mode - reflection mode switching

4 5AIM-8800

Infrared Microscope

Operation is also possible from the AIM-8800 main unit controller.

All operations for controlling the infrared microscope areperformed on the PC screen.

Double-click on any point in the visible observation screen, and that location instantly moves to the center of the viewing area.

Auto X-Y stage X-axis movement

Manual focus adjustment

Auto X-Y stage Y-axis movement

Visible observation screen

Measurement position is moved to right-hand screen

Returns to recordedposition

Maximize display

Aperture Setting screen

Link 1

When mounting the sample stage to the Auto X-Y stage, clicking the position of the displayed opening automatically moves the Auto X-Y stage to the center of the sample stage opening.

Link 2

Auto Centering

Sample Holder

Up to 10 sample positions and 2 background positions can be placed into memory; and at the same time, the aperture size and angle are also recorded.

Link 3

Position Recording

Easy Operation with AIM View

Aperture Setting Click near corner to changethe aperture angle.

Aperture Setting Enter a number to set the size

Auto MeasurementMemorized positions are automatically measured.**) When LabSolutions IR is used.

Auto focusVisual mode - IR mode switching

Transmission mode - reflection mode switching

4 5AIM-8800

Infrared Microscope

Capture microscope images and synthesize a large visual image

Set mapping parameters on the synthesized visual image

Easy microscope operation

Various mapping modes

Manipulation of mapped data

The mapping software captures microscope images and synthesizes a large visual image to determine the mapping area.

Mapping parameters such as mapping area, Aperture setting, scan interval, and so on are set up on the synthesized visual image using a mouse.

Functions to control the AIM-8800 and Mapping operation such as switching the Transmittance/Reflectance mode are short-cut by icons on the screen.

Random (multipoint), Line and Area mapping are available. In addition to general Transmittance/Reflectance mapping, ATR mapping is available (ATR Objective is an option).

Spectra and maps based on specified functional groups are calculated from obtained mapping data. The mapped data is displayed by 3-dimensional (bird's-eye view), Contour or Spectral overlay mode.

The mapping software captures microscope images and synthesizes a large visual image to determine the mapping area.Mapping parameters such as mapping area, Aperture setting, scan interval, and so on are set op on the synthesized visual image by using a mouse.

An area mapping data consists of 4 coordinates-scanned position (x, y), wavenumber and absorbance. Display functions and data manipulation functions of AIM-MAP calculate peak height, peak area or ratio at the scanned position. And AIM-MAP calculates maps based on specified functional groups. Shown data is a map calculated by alkyl group (3050-2750cm-1).The mapped data is displayed by 3-dimensional (bird's-eye view), Contour or Spectral overlay mode.

Spectrum of Film Cross-section

Plots of Additive Peak (1510~1470cm-1)

Various types of additives are applied to materials to impart a variety of characteristics. To ensure uniform product quality, uniform mixing of additives is necessary.Even in general macro measurement, where distribution analysis has been difficult, the infrared microscope enables such analysis.

Distribution analysis is also possible.

Distribution analysis of additives in film

AIM-MAP – Mapping Software

Mapping software allows dimensional analysis of points, lines and surfaces.

6 Infrared MicroscopeAIM-8800

Capture microscope images and synthesize a large visual image

Set mapping parameters on the synthesized visual image

Easy microscope operation

Various mapping modes

Manipulation of mapped data

The mapping software captures microscope images and synthesizes a large visual image to determine the mapping area.

Mapping parameters such as mapping area, Aperture setting, scan interval, and so on are set up on the synthesized visual image using a mouse.

Functions to control the AIM-8800 and Mapping operation such as switching the Transmittance/Reflectance mode are short-cut by icons on the screen.

Random (multipoint), Line and Area mapping are available. In addition to general Transmittance/Reflectance mapping, ATR mapping is available (ATR Objective is an option).

Spectra and maps based on specified functional groups are calculated from obtained mapping data. The mapped data is displayed by 3-dimensional (bird's-eye view), Contour or Spectral overlay mode.

The mapping software captures microscope images and synthesizes a large visual image to determine the mapping area.Mapping parameters such as mapping area, Aperture setting, scan interval, and so on are set op on the synthesized visual image by using a mouse.

An area mapping data consists of 4 coordinates-scanned position (x, y), wavenumber and absorbance. Display functions and data manipulation functions of AIM-MAP calculate peak height, peak area or ratio at the scanned position. And AIM-MAP calculates maps based on specified functional groups. Shown data is a map calculated by alkyl group (3050-2750cm-1).The mapped data is displayed by 3-dimensional (bird's-eye view), Contour or Spectral overlay mode.

Spectrum of Film Cross-section

Plots of Additive Peak (1510~1470cm-1)

Various types of additives are applied to materials to impart a variety of characteristics. To ensure uniform product quality, uniform mixing of additives is necessary.Even in general macro measurement, where distribution analysis has been difficult, the infrared microscope enables such analysis.

Distribution analysis is also possible.

Distribution analysis of additives in film

Mapping software allows dimensional analysis of points, lines and surfaces.

6 Infrared MicroscopeAIM-8800

ATR Objective (sl ide-on type)A magnification of 15×, incident angle of 30°C and single refection are provided with the incorporated 3mm-diameter Ge semicircular prism.The slide-type prism permits switching between the usual observation and infrared measurement modes.The ATR objective can be effectively used to analyze foreign particles on substrates which do not reflect light easily, such as paper or plastic, and to perform surface analysis.

Diamond Cell CThis attachment is used to compress a micro sample into a thin film, which is then analyzed directly by transmission with an infrared microscope. Applications include pharmaceuticals, rubber compounds, plastics and polymers.The C type cell is constructed using artificial diamond, while the B type cell is also available, using natural diamond.

Micro Vice HolderThis holds various types of samples for microscopy. Sample orientation can be selected, or samples can be stretched while being analyzed.

Mapping

Abundant accessories for a wide range ofapplications

Wide-ranging applications possible with an array of optional accessories for the AIM-8800 Infrared Microscope.

Line MappingMeasure data on the line from start to end points.Mapped data is 3-dimensional data consisting of wavenumber, absorbance and position.

8 9AIM-8800

Infrared Microscope

Area MappingMeasure data in the rectangular area specified by start and end points.Mapped data is 4-dimensional data consisting of wavenumber, absorbance and x/y position.

Hair – Microscope Transmission Method

Hair – Microscope ATR Method (Ge prism)

Microscope photograph ofsingle Nylon fiber before compression

Microscope photograph ofsingle Nylon fiber after compression

Black: Infrared spectrum of single Nylon fiber before compressionRed: Infrared spectrum of single Nylon fiber after compression

Transmission Spectrum (upper) and ATR Spectrum (lower) of Hair To obtain good transmission spectra, the sample must be prepared in the form of a thin slice,

such as by using a diamond cell. If the sample is too thick, the peaks become saturated, as

typical in a transmission spectrum, which does not allow obtaining an accurate spectrum. In

contrast, the ATR method allows obtaining sample surface information that is unaffected by

sample thickness or substrate material.

Mapping measurements allow confirming the distribution of components.

Mapping measurement of powdered health food Mapping measurement was performed after flattening out the health food powder using a diamond cell. The photograph below shows the distribution of ascorbic acid (C=O group near 1670 cm-1), starch (O-H group near 3300 cm-1), and also alpha-tocopherol acetate (peak ratio of C=O groups near 1755 cm-1 and 1670 cm-1). As these images show, mapping measurements allow confirming distribution of components in samples.

Microscope photograph of powdered health food

Distribution of Ascorbic Acid (Vitamin C)

Distribution of Starch

Distribution of Alpha-Tocopherol Acetate

C=O (1670cm-1)

O-H (3300cm-1)

C=O (1755cm-1/1670cm-1)

ATR Objective (sl ide-on type)A magnification of 15×, incident angle of 30°C and single refection are provided with the incorporated 3mm-diameter Ge semicircular prism.The slide-type prism permits switching between the usual observation and infrared measurement modes.The ATR objective can be effectively used to analyze foreign particles on substrates which do not reflect light easily, such as paper or plastic, and to perform surface analysis.

Diamond Cell CThis attachment is used to compress a micro sample into a thin film, which is then analyzed directly by transmission with an infrared microscope. Applications include pharmaceuticals, rubber compounds, plastics and polymers.The C type cell is constructed using artificial diamond, while the B type cell is also available, using natural diamond.

Micro Vice HolderThis holds various types of samples for microscopy. Sample orientation can be selected, or samples can be stretched while being analyzed.

Mapping

Abundant accessories for a wide range ofapplications

Wide-ranging applications possible with an array of optional accessories for the AIM-8800 Infrared Microscope.

Line MappingMeasure data on the line from start to end points.Mapped data is 3-dimensional data consisting of wavenumber, absorbance and position.

8 9AIM-8800

Infrared Microscope

Area MappingMeasure data in the rectangular area specified by start and end points.Mapped data is 4-dimensional data consisting of wavenumber, absorbance and x/y position.

Hair – Microscope Transmission Method

Hair – Microscope ATR Method (Ge prism)

Microscope photograph ofsingle Nylon fiber before compression

Microscope photograph ofsingle Nylon fiber after compression

Black: Infrared spectrum of single Nylon fiber before compressionRed: Infrared spectrum of single Nylon fiber after compression

Transmission Spectrum (upper) and ATR Spectrum (lower) of Hair To obtain good transmission spectra, the sample must be prepared in the form of a thin slice,

such as by using a diamond cell. If the sample is too thick, the peaks become saturated, as

typical in a transmission spectrum, which does not allow obtaining an accurate spectrum. In

contrast, the ATR method allows obtaining sample surface information that is unaffected by

sample thickness or substrate material.

Mapping measurements allow confirming the distribution of components.

Mapping measurement of powdered health food Mapping measurement was performed after flattening out the health food powder using a diamond cell. The photograph below shows the distribution of ascorbic acid (C=O group near 1670 cm-1), starch (O-H group near 3300 cm-1), and also alpha-tocopherol acetate (peak ratio of C=O groups near 1755 cm-1 and 1670 cm-1). As these images show, mapping measurements allow confirming distribution of components in samples.

Microscope photograph of powdered health food

Distribution of Ascorbic Acid (Vitamin C)

Distribution of Starch

Distribution of Alpha-Tocopherol Acetate

C=O (1670cm-1)

O-H (3300cm-1)

C=O (1755cm-1/1670cm-1)

Note : When connected to a PC type FTIR-8000 Series, IRAffinity-1, IRPrestige-21, the PC for operating the FTIR main unit is also used for operating the AIM-8800. When connected to a non-PC type FTIR-8000 Series, the PC must be purchased separately.

Auto measurement is available when LabSolutions IR is used.

Optics

MCT detector

Signal-to-noise ratio *

Electrically activated

aperture

Motor-driven X-Y sample

Operation control via main

unit keyboard

Control via PC

Ambient conditions

External dimensions, weight

Power requirements

Options

15 × Cassegrain objective

15 × Cassegrain condenser mirrors

w / inlet for purging

w / liquid nitrogen monitoring system

Wavelength range : Type 1 - 5000 - 720cm-1

Type 2 - 5000 - 650cm-1

Transmission mode, aperture size 50µm, 8cm-1, 60 scans

2600 : 1 or higher (Type 1), 2000 : 1 or higher (Type 2)

* These are the guaranteed signal-to-noise values when connected to the Shimadzu

Fourier Transform Infrared Spectrophotometer

XYθ directional drive. Setting of XY direction increments is 1µm over sample surface, and 1°

increments in θ direction (numerical entry possible).

Minimum setting value : 3µm

Positioning range : X axis : 70mm; Y axis : 30mm

Resolution : 1µm pitch

Sample thickness : Reflection mode - ≤ 40mm

Transmission mode - ≤ 10mm

Measuring mode selection / XY stage operation (speed variable in 4 steps) / manual focusing /

illumination control

Measuring mode selection / XY stage operation / auto centering / manual focusing / auto focusing /

illumination control / aperture setting / aperture preview / measurement position and aperture

setting recording (10 sample positions, 2 background positions)

Auto measurement of memorized positions

Ambient temperature : 15°C ~ 30°C

Ambient humidity : 70% or less

W410mm × D540mm × H520mm, 36kg

AC100 / 120 / 220 / 230 / 240V 125VA

• Ge prism ATR objective

• Diamond ATR objective (Spectra Tech)

• ZnSe ATR objective (Spectra Tech)

• Grazing angle objective (Spectra Tech)

• 32X objective (Spectra Tech, only for reflection mode)

• Visual objective lens (10×, 20×, 40×, 100×)

10 11AIM-8800

Infrared Microscope

Fig. 1 Microscope Photograph of Oily Substance on a Mirror Surface

Fig. 3 Three-Dimensional Graph of Peak Intensity at 1261 cm-1

Fig. 1 Microscope Photograph of Fibrous Foreign Substance (red border indicates area of fibrous substance measured)

Grating (Large)

Fig. 2 Infrared Spectrum of Foreign Substance (Silicone Oil) Fig. 2 Infrared Spectrum of Fibrous Foreign Substance and Membrane Filter Red: Infrared spectrum of fibrous foreign substance (polypropylene) Black: Infrared spectrum of membrane filter (nitrocellulose)

Mapping Oil Adhered to a Mirror SurfaceFig. 1 shows a microscope photograph of an oily substance on a mirror surface. It shows that the substance is about 200 µm wide. This oily substance was mapped using the reflection method. Fig. 2 is an infrared spectrum of a foreign substance, which shows that it is a silicone oil. Fig. 3 is a three dimensional graph with peak intensity near 1261 cm-1 graphed on the Z-axis. This allows determining the distribution status of the silicone oil.

Analysis of Fibrous Foreign Matter byMicroscope ATR Method A membrane filter was used to sample a fibrous foreign substance found in a liquid. A microscope photograph of the substance is shown in Fig. 1. The fibrous substance was then measured using the microscope ATR method. Measurement results are shown in Fig. 2.

Applications Specifications

Optics

MCT detector

aperture

unit keyboard

Control via PC

Ambient conditions

Power requirements

Options

Type 2 - 5000 - 650cm-1

W410mm × D540mm × H520mm, 36kg

AC100 / 120 / 220 / 230 / 240V 125VA

10 11AIM-8800

Infrared Microscope

Grating (Large)

Optics

MCT detector

aperture

unit keyboard

Control via PC

Ambient conditions

Power requirements

Options

Type 2 - 5000 - 650cm-1

W410mm × D540mm × H520mm, 36kg

AC100 / 120 / 220 / 230 / 240V 125VA

10 11AIM-8800

Infrared Microscope

Grating (Large)

Optics

MCT detector

aperture

unit keyboard

Control via PC

Ambient conditions

Power requirements

Options

Type 2 - 5000 - 650cm-1

W410mm × D540mm × H520mm, 36kg

AC100 / 120 / 220 / 230 / 240V 125VA

10 11AIM-8800

Infrared Microscope

Grating (Large)

C103-E056FAIM

Infrared Microscope

AIM-8800

Printed in Japan 3655-06212-30AIT

Company names, product/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation or its affiliates, whether or not they are used with trademark symbol “TM” or “®”.Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services. Shimadzu disclaims any proprietary interest in trademarks and trade names other than its own.

For Research Use Only. Not for use in diagnostic procedures. The contents of this publication are provided to you “as is” without warranty of any kind, and are subject to change without notice. Shimadzu does not assume any responsibility or liability for any damage, whether direct or indirect, relating to the use of this publication.

AIM-8800 - Shimadzu · C103-E056F AIM-8800 Infrared Microscope AIM-8800 Printed in Japan...

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Transcript of AIM-8800 - Shimadzu · C103-E056F AIM-8800 Infrared Microscope AIM-8800 Printed in Japan...