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DEPARTMENT OF APPLIED CHEMISTRY AND CHEMICAL TECHNOLOGY

UNIVERSITY OF KARACHI

SYLLABUS FOR NEW B.S PROGRAM2018-19

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DEPARTMENT OF APPLIED CHEMISTRY AND CHEMICAL TECHNOLOGYUNIVERSITY OF KARACHI

BS (4 YEARS PROGRAMME)COURSE DISTRIBUTION PER SEMESTER

YEARSEMESTE

RCOURSECODE COURSE TITLE

CREDIT

HOURSMARKS PAGE

FIRST I

301 General Chemistry 2+1 80+20

303 Engineering Drawing & Workshop Practice 0+3 100

305 Mathematics (Minor I) 3+0 100

307 Physics (Minor II) 2+1 80+20

309 Islamic Studies (Compulsory) 3+0 100

311 Urdu (Compulsory) 3+0 100

FIRST II

302 Chemical Engineering –I (Stoichiometry) 3+0 100

304 Computer Science – I 2+1 80+20



310 Pakistan Studies (Compulsory) 3+0 100

312 English (Compulsory) 3+0 100

SECOND III

401 Chemical Process Industries – I (Inorganic) 2+1 80+20

403 Chemical Process Principles-I (Thermodynamic) 2+1 80+20

409405 Computer Science – II Analytical Techniques-I 2+1 80+20

407 Physics (Minor-I) 2+1 80+20

409 Mathematics (Minor-II) 3+0 100

SECOND IV

402 Chemical Process Industries – II (Organic) 2+1 80+20

404 Chemical Process Principles-II (Equilibrium) 2+1 80+20

406 Chemical Engineering – II (Fluid Mechanics) 2+1 80+20

408 Mathematics 3+0 100

410 Physics (Minor-I) 2+1 80+20

412 English (Minor-II) 3+0 100

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DEPARTMENT OF APPLIED CHEMISTRY AND CHEMICAL TECHNOLOGYUNIVERSITY OF KARACHI

B. Sc. (Hons) 1 st to 2 nd Year COURSE DISTRIBUTION PER SEMESTER

YEAR SEMESTER COURSE CODE COURSE TITLE CREDIT HOURS MARKS PAGE NO.

FIRST I

301 General Chemistry 2+1 80+20

303 Engineering Drawing & Workshop Practice 0+3 100

Mathematics (Minor I) 3+0 100

Physics (Minor II) 2+1 80+20

Urdu (Compulsory) 3+0 100

311 Islamic Studies (Compulsory) 3+0 100

FIRST II

302 Chemical Engineering –I (Stoichiometry) 3+0 100

304 Computer Science – I 2+1 80+20



310 Pakistan Studies (Compulsory) 3+0 100

312 English (Compulsory) 3+0 100

SECOND

III

401 Chemical Process Industries – I (Inorganic) 2+1 80+20

403 Chemical Process Principles-I (Thermodynamic) 2+1 80+20

409405 Computer Science – II Analytical Techniques-I 2+1 80+20

Mathematics (Minor-II) 2+1 80+20

Physics (Minor-I) 3+0 100

SECOND

IV

402 Chemical Process Industries – II (Organic) 2+1 80+20

404 Chemical Process Principles-II (Equilibrium) 2+1 80+20

406 Chemical Engineering – II (Fluid Mechanics) 2+1 80+20

Mathematics 3+0 100

Physics (Minor-I) 2+1 80+20

English (Minor-II) 3+0 100

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B.Sc.(Hons) 3 rd Year and M. Sc. COURSE DISTRIBUTION PER SEMESTER

YEAR SEMESTER

COURS NUMBER

S

COURSE TITLE CREDIT

HOURS

MARKS

PAGE NUMBER

THIRD V

501 Chemical Process Industries Inorganic-II 2+1 80+20 1503 Polymer Science 2+1 80+20 2505 Chemical Process Industries Organic-II 2+1 80+20 3507 Chemical Engineering-II (Unit Operation) 2+1 80+20 4

511 509Analytical Techniques-I Analytical Techniques-II 2+1 80+20 5

THIRD VI

502 Chemical Process Industries Inorganic-III 2+1 80+20 6504 Textile Processing 2+1 80+20 7506 Chemical Process Industries Organic-III 2+1 80+20 8508 Industrial Economics & Management 3+0 100 9510 Chemical Process Principle III (Dynamics) 2+1 80+20 10512 Communication Skills (English) 3+0 100 10

FOURTH

VII601

Chemical Engineering-III (Heat & Mass Transfer) 2+1 80+20 11

603Chemical Engineering-II (Chemical Reaction Engg.) 3+0 100 11

632 605 Analytical Techniques-II Instrumentation and Process Control 2+1 80+20 12Specialization Courses

607Chemical Process Principles-IV (Solution Thermodynamics & VLE) 2+1 80+20 13

609 Chemical Process Industries Inorganic-I 2+1 80+20 13611 Petroleum and Petrochemicals-I 2+1 80+20 14613 Pharmaceutical Industries-I 2+1 80+20 15615 Polymer Synthesis 2+1 80+20 16

617Textile Processing-I (Colour Matching and Printing Technology) 2+1 80+20 17

619 Food Science & Technology-I 2+1 80+20 17621 Metallurgy & Material Technology - I 2+1 80+20 18

Optional Courses 604 Industrial Pollution 623 Research Project 0+3 100 19625 Electrochemical Industries 2+1 80+20 19627 Polymer Rheology 2+1 80+20 20629 Leather Technology 2+1 80+20 20

631Fuel Technology and Renewable Energy Resource 2+1 80+20 21

FOURTH VIII

602 Chemical Engineering-IV (Plant Design) 2+1 60+40 22638 604 Industrial Pollution Process Simulation 2+1 80+20 23606 Analytical Techniques-III 2+1 80+20 23

Specialization Courses

608Chemical Process Principles-V (Flow Processes & Thermodynamics Cycles) 3+0 100 24

610 Chemical Process Industries Inorganic-II 2+1 80+20 25

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612 Petroleum and Petrochemicals-II 2+1 80+20 25614 Pharmaceutical Industries-II 2+1 80+20 26616 Polymer Physics 3+0 100 27

618Textile Processing-II (Finishing and Quality Assurance) 2+1 80+20 27

620Food Science & Technology-II (Food Engineering) 2+1 80+20 28

622 Metallurgy & Material Technology - II 2+1 80+20 28624 Industrial Training (Compulsory) 0+3 100 29

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MS COURSE DISTRIBUTION PER SEMESTER

YEAR SEMESTERCOURSE NUMBER

COURSE TITLECREDIT HOURS

MARKSPAGE

NUMBER

MS I

701 Advance Analytical Chemistry 3+0 100 1

ASR 701 Research Methodology I 3+0 100

703 Engineering Materials 3+0 100 1

705 Technical Textiles 3+0 100 2

MS II

702Production Control, Project Planning & Risk

Assesment 3+0 100 2

ASRP-702 Research Methodology II

704 Supply Chain Planning 3+0 100 3

706

Chemical Engineering

(Process Modeling, Simulation & Control) 3+0 100 4

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Ph.D COURSE DISTRIBUTION

S.No. Course No. Course Title Cr.Hr

1. ACH-801 Research Seminar (4+0)

2. ACH-802 Colloquiums on Current Advances in the Discipline (4+0)

3. ACH-803 Technical writing Skills in Research (4+0)

4. ACH-804 Development of Research Proposal for Funding Agencies (6+0)

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Course No. 301General Chemistry2+1 Credit hours

PHYSICAL CHEMISTRY: Volumetric Properties of Pure Fluids-- The PVT behavior of pure substances, Equations of State for Gases, the Principle of Corresponding States, gas mixture, mixture of ideal Gases, Generalized correlations for gases and liquids.

INORGANIC CHEMISTRY: Bonds in Solids -- Solid State of Matter, Bonding in Solids, Metallic bonding, Molecular bonding. Complex Compounds -- Chemistry of Transition Elements, Lanthanide and Actinide Series, Characteristics of Transition Metals, Structure of Complex Compounds, Electronic Interpretation of the Structure of Complex Compounds, Isomerism in Complex Compounds. Sources of Metals -- Methods and Techniques of Ore Treatment.

ORGANIC CHEMISTRY: Nomenclature of organic compounds, Interconversion of functional groups, Types of reactions, Reaction Mechanisms.

LAB SAFETY : Introduction to Lab glassware, equipments etc.

Practicals:

1. Calibration of a 5 cc pipette.2. Preparation and standardization of a solution of a secondary standard substance.3. Determination of hydrogen peroxide by iodometric titration.4. Preparation of potash Alum.5. Calcination of lime stone and estimation of calcium oxide.6. Standardization of strong acid solution with anhydrous sodium carbonate.7. Element detection.8. Functional group determination.9. Identification of alcohols, alkane, alkene, aromatic hydrocarbons.10. Preparation of Aspirin.

Recommended Books:

1. J. M Smith, H.C. Van Ness & M.M. Abbott Introduction to Chemical Engineering Thermodynamics, McGraw Hill, 7th Ed., New York, 2004.

2. Silbey, R., R. Alberty, and M. Bawendi. Physical Chemistry. New York, NY: John Wiley & Sons, 2004.3. Srrell, Thosins, Organic Chemistry, Career press. USA, 20044. Vogel, Vogel’s Textbook of Practical Organic Chemistry, 5th Edition 2004.5. Gary L. Miesster, Donald A. Tarr, Inorganic Chemistry, 3rd Edition 2004.6. James E. Huheey, Ellen A. Keiter, Richard L. Keiter, Inorganic Chemistry, Principal of Structure and

Reactivity, 7th Edition 2005.

Course No. 303Engineering Drawing & Workshop Practice

0+3 Credit Hours

BASIC DRAWING TECHNIQUES: Introduction and use of instrument. Planning of drawing sheet. The projection of simple solids in simple positions. The oblige auxiliary planes. Lettering and dimensioning. Requirements of working drawing. Isometric and pictorial projection of solid figure. Freehand sketching.

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WORKSHOP: Use of different types of metal working tools and measuring instruments. Exercise in marking filling and fitting. Use of Lathe Machine. Use of carpenters tools. Preparation of simple jobs. Introduction to forging welding.

Recommended Books:

1. R. P. Kibbe & J. W. Neely “Machine Tool Practice” 2nd Ed. John Wiley & Sons 1982.2. J. S. Dobrovoloy & D. C. O. Bryant Graphics for Engineers: Visulization Communication and design.

2nd Ed. John Wiley & Sons 1984.

Course No. 302Chemical Engineering – I (Stoichiometry)

3+0 Credit hours

Concept of Mole and Avogadro’s Number, Mass Percent Composition from Chemical Formulas, Elemental Analysis, Writing and Balancing Chemical Reactions, Limiting, Reactants. General Principle, liquefaction & vaporization, humidification, equilibrium distribution curve, Material Balance with or without chemical reaction.

Energy and energy balance with and without chemical reaction, Material balance for combustion reactions, Product Separation and Recycle.

Recommended Books:

1. Richard M. Felder, Ronald W. Rousseau, Lisa G. Bullard, Elementary Principles of Chemical Processes, 4th Edition, John Wiley 2016.

2. David M. Himmelblau, James B. Riggs, Basic Principles and Calculations in Chemical Engineering, Eight Edition, Prentice Hall 2012.

3. B. I. Bhatt, S. B. Thakore, Stoichiometry, Fifth Edition, Mc Graw-Hill 2010.4. M. Abbott , M. Swihart, J. M Smith, & H.C. Van Ness, Introduction to Chemical Engineering

Thermodynamics, Eight Edition, McGraw Hill Education 2017.5. Edward V. Thompson, William H. Ceckler, Introduction to Chemical Engineering, Mc Graw-Hill 1985.

Course No. 304Computer and Information System-I

2+1 Credit Hours

The objective of this course is to acquaint the students with computer and its applications. Following topics are covered under this course. Decimal,Binary, Octal & Hexadecimal, conversion from one system to another. Introduction to Operating System, Algorithms, Flow Chart development, Programming languages. How to use MS Office products; MS Word, PowerPoint, MS Access, MS Excel, Internet search, e-mail and other applications.

Programming in C Language: This course is designed to familiarize students with the basic structured programming skills. It emphasizes upon problem analysis, algorithm designing, and program development and testing. The topics to be covered are algorithms and problem solving, development of basic algorithms, introduction to C elementary data types, Input out put, looping, decisions, switch.

Practicals:

Program development related to Chemical Engineering and Mathematical Expressions.

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Recommended Books:

1. Glenn Brooks Hear, Computer Science – An Overview, 3 rd Edition. 2. PK Sinha, Introduction to Computer Science. 3. Deitel and Deitel, C++: How to Program, Prentice-Hall. 4. Gott fried, Programming with C/C++ (Schaum.s Series), McGraw-Hill. 5. Ammeraal, C++ for Programmers, Wiley.6. William M. Fuori and Louis V. Gioia, Computers and Information Systems, Prentice Hall International,

1994. 7. Robert Lafore, C Programming Using Turbo C, 2nd edition Sams Publishing, 1996.

Course No. 401Unit Processes in Inorganic Industries

2+1 Credit hours

SULFUR & SULFURIC ACID: Raw Materials and its Preparation, Process Manufacture, Concentration or Purification, Recycling / Uses, Hazardous & Precaution.

CHLOR ALKALI INDUSTRIES: Raw Materials and its Preparation, Process Manufacture (Mercury & Diaphragm Cell), Concentration or Purification, Recycling / Uses, Merits and Demerits of Electrolytic Cells, Hazardous & Precaution, By Products of Chlorine and Related Industries.

PHOSPHORIC ACID: Raw Materials and its Preparation, Process Manufacture, Concentration or Purification, Merits and Demerits of Dry and Wet Process, Recycling / Uses, Hazardous & Precaution.

FERTILIZERS: Classification of Fertilizers, Minor and Major Ingredients, Raw Materials and its Preparation, Process Manufacture of Nitrogen, Phosphorous and Mixed Fertilizer, Concentration or Purification, Hazardous & Precaution.

INORGANIC PIGMENT: Classification of Pigments, Manufacture of White & Color Pigments, Hazardous & Precaution.

Practicals:

1. Determination of sodium carbonate content in washing soda.2. Estimation of available chlorine in bleaching powder.3. Determination of sulphate as barium sulphate.4. Standardization of sodium thiosulphate against standard potassium dichromate.5. Estimation of phosphate in phosphate fertilizer.6. Estimation of nitrogen in nitrogenous fertilizer.7. Preparation of lead chromate, yellow chrome.8. Estimation of lead as lead chromate.9. Estimation of separate amount of sodium carbonate and bicarbonate.10. Preparation of potassium permanganate.

Recommended Books:

1. K.H. Buchel, H.-H. Moretto, P. Woditsch Industrial Inorganic Chemistry, 2nd Edition, 2000.2. Niir Board, Industrial Chemical Technology, 20003. James E. Huheey, Ellen A. Keiter, Richard L. Keiter, Inorganic Chemistry, Principal of Structure and

Reactivity, 7th Edition 2005.4. G. T. Austin, Chemical Process Industries, 6th Edition, McGraw-Hill, New York,19975. Kirck Othmer, Encyclopedia of Chemical Technology, A Wiley Interscience Publication, 2005.

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Course No. 403Chemical Process Principles-1 (Thermodynamics)

2+1 Credit hours

THE FIRST LAW AND OTHER BASIC CONCEPTS: Internal Energy, Formulation of First Law of Thermodynamics, the Thermodynamic State and State Functions, Enthalpy, the Steady State Flow Process, the Reversible Process, the Heat Capacity and Specific Heat, Thermodynamic identities, Effect of pressure and volume Changes on heat capacities.

THE THERMODYNAMIC PROCESSES: Constant Volume Process, Constant Pressure Process, Constant Temperature Process, Adiabatic Process, Polytropic Processes and their application to ideal and non ideal gases.

HEAT EFFECTS : Heat capacities of gases as function of temperature, specific heats of liquids and solids, Heat Effects accompanying phase changes, the standard heat of reaction, the standard heat of formation, the standard heat of combustion, effect of temperature on the standard heat of reaction, the heat effect of mixing processes.

THE SECOND LAW OF THERMODYNAMICS: Statement of the second Law of Thermodynamics, the Concept of Entropy, and mathematical Statement of the Second Law, Entropy Changes and irreversibility.

THERMODYNAMIC PROPERTIES OF FLUIDS: Relations among Thermodynamic Properties, Thermodynamic Properties of Single phase System, the Two Phase region, Generalized Correlation of Thermodynamic Properties of Gases.

Practicals:

1. Determination of ratio of heat capacities.

2. Determination of heat of neutralization.

3. Determination of integral heat of solution.

4. Determination of solubility at different temperatures and evaluation of differential heat of solution.

5. Determination of molecular radius by viscometer.

6. Determination of solubility at different temperatures and evaluation of enthalpy, entropy and Gibbs energy change of solution.

7. Determination of molar refraction.

8. Determination of surface tension.

Recommended Books:

1. J. M Smith, H.C. Van Ness & M.M. Abbott Introduction to Chemical Engineering Thermodynamics, McGraw Hill, 7th Ed., New York, 2004.

2. P. Atkins and J. de Paula. Physical Chemistry. New York, NY: W.H. Freeman and Company, 2001

3. R. Silbey, R. Alberty, and M. Bawendi. Physical Chemistry. New York, NY: John Wiley & Sons, 2004.

4. Michael J. Moran, Howard N. Shapiro Wiley, Fundamentals of Engineering Thermodynamics;5 edition (June 11, 2003)

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http://www.amazon.com/exec/obidos/search-handle-url/103-2154400-8647864?_encoding=UTF8&search-type=ss&index=books&field-author=Howard%20N.%20Shapiro

http://www.amazon.com/exec/obidos/search-handle-url/103-2154400-8647864?_encoding=UTF8&search-type=ss&index=books&field-author=Michael%20J.%20Moran

Course No. 405Computer and Information System-II

2+1 Credit Hours

Computer Networks and networking, Topology, Hardware used in Networking, Networking Software, Networking Protocols, Development of Local Area Networks(LAN) and Wide Area Network (WAN).

Programming in C Language: This course is designed to familiarize students with the basic structured programming skills. It emphasizes upon the use of Functions, Structures, Files and Arrays in C language for computing chemical engineering problems.

Practicals:

Program development related to Chemical Engineering and Mathematical Expressions.

Recommended Books:

1. Deitel and Deitel, C++: How to Program, Prentice-Hall.

2. Gott fried, Programming with C/C++ (Schaum.s Series), McGraw-Hill.3. Robert Lafore, C Programming Using Turbo C, 2nd edition Sams Publishing, 1996

4. Ammeraal, C++ for Programmers, Wiley.5. Microsoft® Office Home and Student 2007 Step by Step (BPG-step by Step) [Illustrated] (Paperback)

by Joyce Cox and Curtis Frye Joan Preppernau.6. Excel 2003 Bible [Illustrated] (Paperback) by John Walkenbach Excel 2007.7. Formulas (Mr. Spreadsheets Bookshelf) (Paperback) by John Walkenbach.

Course No. 402Unit Processes in Organic Industries

2 +1 (Credit Hours)

UNIT PROCESS IN ORGANIC SYNTHESIS: Thermodynamics, types of chemical reaction, type and shape of reactor.

SULFONATION: Sulfonation and sulfation, types of sulfonation, classification of sulfonates, manufacturing of sulfonates, sulfonating and sulfating agents, comparison between sulfonating agent factor effecting sulfonation, important reactions, thermodynamics and kinetics of sulfonation, preparation of detergent.

NITRATION: Basic definition, mechanism of nitration, physical properties of nitro compounds, reaction of aromatic nitro group types of nitrating agent, important nitration reaction kinetics and thermodynamics, industrial application, manufacturing of TNG.

HYDROLYSIS: Basic definition, mechanism of hydrolysis, types of hydrolyzing agent, Kinetics and thermodynamics, industrial application, manufacturing of Soap.

HYDROGENATION: Basic definition, mechanism of hydrogenation, important hydrogenation reaction kinetics and thermodynamics, industrial application.

HALOGENATION: Basic definition of halogenation, types of halogenation, classification of halogenates, manufacturing of halogenates, important reactions, thermodynamics and kinetics of halogenation, industrial application.

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OXIDATION: Basic definition, mechanism of oxidation, types of oxidizing agents, Kinetics and thermodynamics, industrial application.

AMINATION: Basic definition, mechanism of amination, types of amination, Kinetics and thermodynamics, industrial application.

Practicals

1. Sulfonation2. Nitration3. Halogenation4. Esterfication5. Amination

Recommended Books:

1. P. H Groggins, Unit processes in organic synthesis, 5th edition, Tata McGraw Hills, New York, 2005.2. K. Othmer, Encyclopedia of chemical technology, A. Wiley Intesrscience publication, 1997.3. Bhal, Arun, Bhal, B.S, A textbook of organic Chemistry, 15th Edition, 2000.4. Srrell, Thosins, Organic Chemistry, Career press. USA, 20045. Vogel, Vogel’s Textbook of Practical Organic Chemistry, 5th Edition 2004.6. Wahid U. Malik, G.D. Tuli, R.D. Madan, Selected topics in Inorganic Chemistry, 2001

Course No. 404Chemical Process Principles - II ( Equilibrium)

2+1 Credit hours

Solution thermodynamics: Thermodynamic Properties of Open system, Partial molar Operations, Chemical potential and fugacity. Effect of temperature and pressure on chemical potential and fugacity. Fugacity co–efficient, Applications to pure Component gases and Liquids and gas mixtures, Excess properties of Mixing, Gibb’s Durham equation and it’s co- relation In terms of partial Pressure, fugacity And fugacity coefficient, Determination of fugacity Using residual volume, Compressibility Factor and equation of states.

Chemical Equilibrium: Criteria for Chemical equilibrium, equilibrium constant and its dependence on temperature and pressure. Evaluation of equilibrium constant, equilibrium conversions for single and multiple reactions systems.

Electrochemical Equilibrium: Arrhenius Theory of Electrolysis, Faraday’s Law of Electrolysis, Transport no, Ostwald’s Dilution Law, Strength of Acid and Bases, pH and its measurement, Galvanic Cell, Electrode Potential, Expressions for Electrode Potential, Reference Electrode, applications of Electrode potential.

Practicals:

1. Determination of critical solution temperature of water/phenol system.2. Construct the triangular phase diagram for the ternary system of chloroform, acetic acid and water.3. Determination of partition coefficient of iodine in a water/ carbon tetra chloride system.4. Determination of concentration coefficient of chemical reaction.5. Determination of dissociation constant of benzoic acid by an approximate e.m.f method.6. Study of the variation of conductance of a strong electrolyte and the determination of limiting

equivalent conductance.7. Determination of Faraday’s constant.8. Determination of transport number of an ion by moving boundary method.

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Recommended Books:

1. J.M. Smith, H.C. Van Ness & M.M. Abbott, Introduction to Chemical Engineering Thermodynamics, McGraw Hill International, 7th Ed. New York, 2004

2. K. G. Denbigh, The Principles of Chemical Equilibrium: With Applications in Chemistry and Chemical Engineering, K. G. Denbigh, Cambridge University Press.

3. Physical Chemistry, Ira N. Levine, 2002.

Course No. 406Chemical Engineering – I (Fluid Mechanics)

2+1 Credit Hours

FLUID PROPERTIES & STATISTICS: Density, Specific weight, Specific volume, Viscosity, Types of fluids, Pressure variation in static fluid, Fluid in motion.

CONCEPTS OF IDEAL & REAL FLUID FLOW: Fluid flow rates, Continuity Equation, Bernoulli’s Equation, Friction losses, Mechanical devices, General Energy Equation, Angular motion, Ideal and non-ideal flow, steady and un-steady system, stream line flow, laminar and turbulent flow, Significance of Reynolds number.

FLOW IN PIPES & FLOW MEASUREMENT DEVICES: Pipes and tubing, Interpretation of Bernoulli’s equation, Non-circular cross sections, Enlargement & Contractions, Pitot tube, Orifice meter & Venturimeter.

OPEN CHANNEL FLOW & FLOW MEASUREMENTS DEVICES: Distribution of velocity, Notches & their types, Weirs & Francis formula, Discharge equation, Percentage errors and head measurements, Measurement of velocity in open channel using floats, velocity rods and current meters.

PUMPING FOR CHEMICAL WORKS: Pumping equipment for liquids, rotary pumps, centrifugal pumps, air lift pumps, meter pumps and gas lift pumps.

Practicals:

1. Measurement of pressure head of fluid using a piezometer.2. Study of boundary layer velocity profile using Pitot tube.3. Determination of discharge co-efficient of triangular notches.4. Determination discharge co-efficient of weirs.5. Measurement of head loss for flow between two tanks using General Energy Equation.6. Measurement of friction losses due to fitting and valves in pumping system.7. Determination of discharge co-efficient of venturimeter.8. Determination of discharge co-efficient of orificemeter.9. Reynolds’s experiment for visual verification of laminar and turbulent flow.10. Determination of angular velocity of impeller in vortex flow11. Measurement of friction losses in pipes of different materials of construction12. Determination of discharge coefficient of an orifice fitted in a vessel.

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Recommended Books:

1. J. F., Gasiorek, J. Swaffield, J. Douglas, Fluid Mechanics, Prentice Hall, 6th edition (2011) ASIN: B00GSD7VR8.

2. R. L. Mott, and J. A. Untener, Applied Fluid Mechanics, Pearson, 7th edition (2014) ISBN-10: 9780132558921.

3. Y. A. Cengel and J. M. Cimbala Fluid Mechanics: Fundamentals and Applications, McGraw-Hill, 4th edition (2017) ISBN-10: 9781259696534.

4. J. M. Coulson, J. F. Richardson, Chemical Engineering Vol. 1, Elsevier India, 6th edition, (2014) ISBN-10: 8181473868.

5. W. L. McCabe, J. C. Smith, P. Harriott, Unit Operations of Chemical Engg, Mcgraw-Hill, 7th edition (2005) ASIN: B010TT1VJK.

Course No. 410Computer Aided Drawing

0+1 Credit Hours

INTRODUCTION TO AUTOCAD: User interface, entity selection, setting drawing limits, using the grid and snap, Creating drawing geometry, Modifying drawing geometry, Typed input, using ortho, polar and object tracking, object snapping, screen manipulating, Transformation commands, Layers, Hatching, Properties, Text creation and editing, Dimension creation and editing, Layout / paper space, Plotting.

Recommended Books:

1. Engineering Drawing and Graphic Technology, t.e.French, C. J.Vierk and R. J. Foster, 14th Edition.2. Elementary Engineering Drawing N.D. Bhatt.3. AutoCAD 2002 User’s Guide, George Omura, Autodesk, Mstering AutoCAD 2002

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Course No. 501Chemical Process Industries Inorganic-II

2+1 Credit Hours

NUCLEAR INDUSTRIES: Extraction of uranium and thorium, nuclear fuels, sources and reserve, minning and milling, refining and preparation, isotopes enrichment, nuclear fuel selection, nuclear reactor, fusion reaction and processing nuclear materials.

CEMENT: Type of cements, Manufacture of ordinary Portland Cement, Equipment & Chemical reactions, Merits & demerits of wet & dry processes, setting & hardening of Portland Cement, Different type of special cements and their composition & applications.

GLASS: Type of Glasses, Raw materials & their sources, Chemical reactions during manufacture, Furnaces used, Finishing operations, Special glasses and their composition & applications.

CERAMICS: Production of white-wares, ceramic tiles, pottery, enamels & enameled metal-wares.

Practicals:

1. Detailed Portland Cement analysis i.e. loss on ignition, estimation of total silica, determination of CaO, determination of sesqui oxides (Al2O3 / Fe2O2).

2. Determination of copper in copper sulphate solution using standard sodium thiosulphate solution.3. Determination of calcium by titrating against standard potassium permanganate.4. Determination of iron by titrating against standard potassium dichromate.5. Estimation of Zinc as Zinc pyrophosphate.6. Determination of potassium in potassium chloride solution using anion exchange resin.7. Electroplating on a non-metallic surface.8. Compression testing of cement blocks.9. Estimation of aluminium by complexemetric titration.

Recommended Books:

1. Dinsdale, “Pottery Science: Materials, Processes & Products”, Ellis Horwood Ltd., 1986.2. G. T. Austin, “Chemical Process Industries”, 6th ed., McGraw Hill, New York, 1997.3. K. Othmer, “Encyclopedia of Chemical Technology”, A Wiley Interscience Publication, 1997.4. H. G. Pfaneder, “H. Schroeded, Schott’s Guide to Glass”, Van Nostrand Reinhold Company, New

York, 1990.5. S. S. Dara, “A Text book of Engineering Chemistry” 9th ed 2004.6. G.L. Meissler and Tarr, “Inorganic Chemistry” Prentice Hall 2004.7. Ali, M. F, B.El-Ali and J. Speight, “Hand Book of Industrial Chemistry”, McGraw Hill Companies New

York USA 2005.8. Cotton and Wilkinson, “Advance Inorganic Chemistry”, 7th ed John Wiley 1996.

Course No. 503Polymer Science and Engineering

2+1 Credit Hours

POLYMER CHEMISTRY: Raw materials and synthesis of polymers; monomers, homopolymers, copolymers; basic organic chemistry and applied polymer chemistry;

SYNTHESIS OF POLYMERS & POLYMERIZATION PROCESSES: Types of polymerization, Free radical chain polymerization and ionic polymerization, Kinetics of chain polymerization, Copolymerization and

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kinetics of copolymerization, Reactivity ratio determination of different pair of monomers, Techniques of polymerization -- bulk, solution, suspension and emulsion polymerization processes, ionic and condensation polymerization.

POLYMER CHAINS AND THEIR CHARACTERIZATION: Molecular weight and its distribution, measurement of molecular weight and size of polymer, End, group analysis, Colligative properties measurement, Light scattering, solution viscosity and molecular size, Ultra centrifugation, Poly-electrolytes.

STRUCTURE AND PROPERTIES OF POLYMERS: Structure of crystals, Crystallization and melting, Glass transition.

POLYMER VISCOUS FLOW: Polymer shapes in solutions, dilute solutions and intrinsic viscosity, effect of concentration, molecular weight, Models of non-Newtonian flow, measurement of viscosity, elastic liquids, turbulent flow.

COMMODITY AND SPECIALTY PLASTICS: compositions and fabrication; additives in plastics; commercial manufacturing processes and applications.

Practicals:

1. Preparation of sulfide rubber and examination of its physical and chemical properties2. Determination of the molecular mass of polyvinyl alcohol by viscosity method.3. Preparation of polystyrene by emulsion polymerization and to observe the dependence of

polymerization rate on the concentration of the emulsifier.4. Preparation of Polystyrene with initiator through solution polymerization.5. Preparation of Cross-linked Polystyrene through emulsion polymerization6. Determination of rate of polymerization of polymethyl-methacrylate using a dilatometer.7. Determination of concentration in gm/100 ml of the given polymeric solution by measurement of the

refractive index and plotting of a calibration curve.8. Suspension polymerization of Styrene with Benzoyl Peroxide.

Recommended Books:

1. R.J. Young & P.A. Lovell. Introduction to Polymers, 3rd Ed. CRC Press, 2011. 2. Rodriguez F., C. Cohen, C. K. Ober, and L. A. Archer, “Principles of Polymer Systems”, 5th ed., New

York, London, Taylor & Francis, 2003.3. M. Chanda. Introduction to Polymer Science and Chemistry, 2nd Ed. CRC Press, 2013. 4. J.A. Brydson. Plastic Materials, 7th Ed. Butterworths-Heinemann, 1999. 5. K.K. Kar and A. Hodzic (Editors). Carbon Nanotube Based Nanocomposites: Recent Development.

Research Publishing, Singapore, 2011. 6. J. Cuppoletti, Ed. Nanocomposites Polymers with Analytical methods, INTech, 2011 7. P.C. Painter and M.M. Coalman. Essentials of Polymer Science and Engineering, Destech Publishers,

20098. S.A. Brent. Plastics Materials & Processing, 3rd Ed. Pearson Education Inc., 2006.

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Course No. 505Modified Chemical Process Industries Organic I

2+1 Credit Hours

SUGAR: Introduction -- Types of Carbohydrates, Cane Sugar; Beet Sugar; Properties; Cultivation; Harvesting; Uses; Economics. Cane Sugar processing -- Washing methods, Milling; Extraction of Cane Juice; Impurities in Juice; Liming Methods; Clarification; Filtration of Juice; Concentration; Crystallization; Centrifugation; Types of Centrifuge; Crystallizer working; Construction of Concentrator & Crystallizer; Storage of Sugar. Raw Sugar Refining -- Affination; Melting; Filtration; Carbonation; Phosphatation; Decolorization of Sugar; Packaging.

SOAP & DETERGENT: Introduction to Soaps -- Definition, Types of Soap, Raw material of Soap; Chemistry & Properties. Soap Processing -- Batch & Continuous Methods; Delaval & Monsavan Process, Laundry Soap, Recovery of Glycerin, Drying, Finishing, and Recovery of Fatty Acids from Paper Mill waste. Detergents -- Types; Manufacturing; Additives.

DYES: Introduction -- Definition, Classification of Dyes; Structure; Properties; Chemistry; Application.

Synthesis of Dyes -- Mono Azo Dyes, Dis Azo Dyes, Poly Azo Dyes; Triphenyl Methane Dyes; Anthraquinone Dyes; Vat Dyes.

PAINTS & PIGMENTS: Types of paints; composition of paints, pigments types, properties of pigments, (Hiding power, Tinting strength, Refractive index, Light fastness, Particle size and shape, Bleeding Characteristics ). Binders: types, curing mechanism. Paints additives (fillers, vehicle, etc.) Paint failures. Manufacturing of paints and uses.

PULP & PAPER: Composition of wood. Wood preparation. Definition of pulping. Methods of pulping.Mechanical Pulping: Types, Advantages & disadvantages. Chemical Pulping -- Sulfate (KRAFT) Pulping,

process description, chemicals used, KRAFT liquor cycle, energy cycle in Kraft process. Batch Digester, Continuous Digester. Sulfite Pulping -- Types, process description, chemicals used, advantages & disadvantages. Comparison between mechanical & chemical pulping, pros & cons of both types. Bleaching of Pulp: Bleaching chemistry, bleaching chemicals used for pulp. Bleaching sequences, Assessing lignin content & pulp bleachabily, Manufacturing of Paper.

OILS & FATS: Definition of Oils, fats, lipids, waxes, fatty acids. Composition of vegetable oils (Major & minor components) Physical properties of triglycerides with reference to chain length, unsaturation, branching.

Chemical properties of triglycerides (hydrolysis, methanolysis, inter esterification, hydrogenation, polymerization, auto oxidation reaction, causes, prevention. Processing -- Seeds preparation, Extraction methods (expression, solvent extraction, choice of solvents) Refining -- Degumming, neutralization, bleaching, deodorization, winterization, Quality tests for oils and fats.

PHARMACEUTICALS: Pharmaceutical dosage forms Classification, Types of tablet, manufacturing of tablet, tablet coating, and capsules.

Practicals:

1. Determination of peroxide value of oil.2. Determination of fatty acid value of oil.3. Determination of saponification value of oil4. Preparation of Fluorescence dye.5. Extraction of Mustard oil by Soxhlet apparatus.6. Preparation of raw sugar from Cane Juice.7. Refining of Edible oil.8. Study the effect of surface area on extraction of oil.

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9. Analysis of tablet.10. Determination of pulping quality by Kappa Number.11. Preparation of Soap.12. Preparation of Azo dye.

Recommended Books:

1. V. E Baikow, Manufacture and Refining of Raw Cane Sugar, Revised Edition, Elsevier Science, 2013.2. G.H. Jenkins, Introduction to Cane Sugar Technology, Revised Edition, Elsevier Science, 2013.3. Luis Spitz, Soap Manufacturing Technology, 2nd Edition, Elsevier Science, 2016.4. Pulp and Paper Chemistry and Technology Volume 2, ISBN 978-3-11-021341-6 Edited by Monica Ek,

Göran Gellerstedt,, Gunnar Henriksson, 20095. Handbook of Pulp. Editors(s): Dr. Herbert Sixta. First published: 30 January 2008. Print ISBN:

9783527309993 |Online ISBN: 9783527619887 |DOI:10.1002/9783527619887. Copyright © 2006 WILEY‐VCH Verlag GmbH & Co. KGaA

6. Handbook for Pulp and Paper Technologists (The SMOOK Book), Fourth Edition. Published by TAPPI PRESS 2016.

7. Fats and Oils Handbook (Nahrungsfette und Öle), 1st Edition. Editors: Michael Bockische Book ISBN: 9780128043554, Paperback ISBN: 9780981893600, Imprint: Academic Press and AOCS Press. Published Date: 15th June 1998

8. Edible Oil Processing, Second Edition. Edited by Wolf Hamm, Harpenden, UK. Richard J. Hamilton; Liverpool John, Moores University, Liverpool, UK, Gijs Calliauw, Desmet Ballestra Oils and Fats, Zaventem, Belgium.

9. Shayne Cox, “Pharmaceutical Manufacturing” Hand Book. Production and processes (Pharmaceutical Development series) Edition: March 2008.

10. Ahmet Gurses, Metin, Kubra Gunes, M. Sadi Gurses, Dyes and Pigments, Springer Briefs in Molecular Science, 2016.

11. Arnold R. Lang, Dyes and Pigments: New Research, Nova Science Publishers, 2009.12. Handbook on Soap, Detergents, & Acid Slurry,3rd Revised Edition, NIIR Board, Asia pacific Business

Press, India, 2013.

Course No. 507Chemical Engineering-II (Unit Operations)

2+1 Credit Hours

SIZE REDUCTION OF SOLIDS: Principles of comminution, Basic laws of crushing & grinding (Rittinger's , Kick’s & Bond's law) , Power consumption in size reduction, Size reduction equipments ( Jaw crushers, Ball mills etc.), Particulate solids their properties and handling.

SIZE SEPARATION: Size separation, Screen & size analysis, Material Balance over screen, Standard Mesh sizes, Mean particles size, Capacity and effectiveness of screens, Settling and sedimentation, Application of settling and sedimentation.

Mixing: Theory & types of mixers and agitators, Power requirements, Rate of mixing, Equipment for solid and paste mixing, Application of mixing and agitation in process industries.

DRYING: Principles of drying, Rate of drying, Mechanism of moisture movement, Classification of dryers, Drying equipment and selection criteria.

DISTILLATION: Various types of distillation, Continuous and batch distillation, Constant reflux and constant composition, HETP and lower (McCabe-Thiele's diagram), Efficiencies of different packing.

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Practicals:

1. Size reduction.2. Size separation.3. Mixing of liquids.4. Drying.5. Distillation.

Recommended Books:

1. J.M.Coulson, J.F. Richardson with J.R. Backhurst, J.H. Harker, “Chemical Engineering” Vol. 2 2004.2. W.L. McCabe, J.C. Smith, P. Harriott, “Unit operations of Chemical Engineering”, 5 th Edition, McGraw

Hill, New York, 2004.3. Walter L .Badger & Julius T Banchero, “Introduction to Chemical Engineering”, Mc Graw-Hill 2000.4. Robert H. Perry & Don W.Green, “Perry’s Chemical Engineers Hand book”, 8th Edition, McGraw-Hill

2001.

Course No. 509 511 Analytical Techniques- I II

2+1 Credit Hours

DATA ANALYSIS: Types of errors, accuracy and precession, distribution of random errors, average deviation and standard deviation, variance and confidence limit, Calibration methods, Sampling, techniques of sampling.

POTENTIOMETRY: Modern and classical method of potentiometry, Reference Electrodes, Metal indicator electrodes, Membrane indicator electrodes, Measuring electrodes potential, Techniques and applications,

Conductometry: Introduction, Instrumentation, Applications, Conductometry titration.

ELECTRO ANALYTICAL METHODS BASED ON ELECTROLYSIS: Principles of Electrolysis, Electro Deposition, Coulometry, Amperometry, Polarography.

Practicals:

1. Potentiometric location of end point. 2. Conductometric location of end point. 3. Determination of Phosphate/Nitrate ion in given fertilizer by electro analytical method.4. Determination of vitamin C in given tablet by redox titration / Analysis of pharmaceutical tablet.5. Preparation of different types of buffers of required pH.6. Preparation of different Baume solutions7. Determine the molarity and percent by mass of acetic acid in different types of vinegar.

Recommended Books:

1. D. A. Skoog, F. J. Holler, S. R. Crouch, “Principles of Instrumental Analysis”, 7th ed, Cengage learning, USA, 2016.

2. D. A. Skoog, D. M. West, F. J. Holler and S. R. Crouch, “Fundamental of Analytical Chemistry”, 9 th ed., Thomson Brooks/Cole Pub. (2014).

3. Na Li, John J. Hefferren, Ke'an Li, “Quantitative Chemical Analysis”, world scientific publishing Co. Pte.Ltd, 2013.

4. Daniel C. Harris, Quantitative Chemical Analysis, Macmillan Learning, 2015

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Course No. 509 502 Chemical Process Industries Inorganic-III

2+1 Credit Hours

ELLINGHAM DIAGRAMS & APPLICATIONS IN EXTRACTIVE METALLURGY: Ellingham diagram of oxides, sulfides & chlorides, Role of carbon in metal extraction.

PRODUCTION OF PIG IRON: Reducing agents, Preparation of metallurgical Coke, Blast furnace reactions.

MILD STEEL AND SPECIAL STEELS: Basic oxygen steel making, Electric steel making, HSLA steels, Stainless steel (ferritic, austenitic, martensitic), Tool steel, Maraging Steel.

EXTRACTION OF NON-FERROUS METALS: Source of nickel, Commercial processes for sulfide & oxide ores, Electrolytic nickel refining. Source of titanium, Treatment of Ilmenite concentrate, Production of titanium. Source of magnesium, Electrolytic production, Magnesium reduction process.

STUDY OF FERROUS AND NON-FERROUS ALLOYS: Fe-Ni, Fe-Cr Alloys, Ni-based Alloys, Ti-based Alloys, Mg-based Alloys.

Practicals:

1. Determination of sulphur in iron pyrite using cation exchange resin.2. Dissolution of iron ores & preparation of stock solutions.3. Determination of Nickel as Nickel dimethyl glyoxime.4. Determination of copper and Nickel in Cu – Ni alloy.5. Determination of magnesium by EDTA. 6. Preparation metallurgical specimen for microscopic examination.7. Microscopic examination of microstructure in ferrous alloys (determination of grain size and volume

fraction of pearlite & ferrite phases in a low carbon steel).8. Microscopic examination of non-ferrous alloys.9. Determination of hardness of metal by Brinell hardness tester.10. Spectrophotometric determination of strength of KMnO4 solution.

Recommended Books:

1. “K. Othmer, Encyclopedia of Chemical Technology”, A Wiley Interscience Publication, 2000.2. R. E. Smallman, R. J. Biship, “Metal and Materials, Butterworth-Heinemann Inc.”, 2000.3. W. F. Smith, “Principle of Material Science and Engineering”, 6rd ed., McGraw Hill, New York, 2002.4. G. T. Austin, “Chemical Process Industries”, 6th ed., McGraw Hill, New York, 2000.5. S. S. Dara, “A Text book of Engineering Chemistry” 9th ed 2004.6. G.L. Meissler and Tarr, “Inorganic Chemistry” Prentice Hall 2004.7. Cotton and Wilkinson, “Advance Inorganic Chemistry”, 7th ed John Wiley 2006.

Course No. 504Textile Processing2+1 Credit Hours

INTRODUCTION TO YARN & FABRIC: Textile raw materials, Introduction to Spinning, knitting & Weaving processes, Sizing importance & ingredients, Count & Construction of yarn, Working of Looms.

TEXTILE PRE-TREATMENT: Singeing, Necessity for Desizing and grey preparation, Mechanism of Scouring & important Scouring agents, Bleaching & chemistry of peroxide bleach, mercerization processes.

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DYEING: Classification of dye stuffs according to their chemical structure and specific applications, Elementary theories of dyeing, Dyeing Auxiliaries, Liquor ratio calculation, Classification & working of dyeing machines.

FINISHING: Types of Mechanical & Chemical Finishes, Chemical Finishes application & important finishing machines.

Practicals:

1. Determination and establishing relationship of various yarn count systems of synthetic and natural fibers.

2. Determination of construction of cloths.3. Desizing of cloths.4. Scouring of cloths and fluidity measurement.5. Dyeing of synthetic fibres using different classes of dye stuffs (3 exercises).6. Resin finishing treatment of cotton cloths.

Recommended Books:

1. A. Ormered, “Modern Preparation and Weaving Machinery”, Butterworth, London, 2000.2. Bernard P Corbman, “Textiles Fiber to Fabric”, 6th Edition, Mc Graw-Hill, 2006.3. M. Lowin, S. B. Sellow, “Chemical Processing of Fibres and Fabrics: Fundamentals and Preparation,

Part A & B”, Chemical Publishing, New York, 2005.4. E. R. Trotman, “Dyeing and Chemical Technology of Textile Fibres”, 4th ed., Griffin, London, 2000.5. D. M. Nun, “Dyeing of Synthetic Polymers: Acetate Fibres”, SDC, Bradford, 2000. 6. Clifford Preston., “The Dyeing of Cellulosic fibres”, Dyer Company Publications Trust, 2004.

Course No. 506Chemical Process Industries Organic-III

2+1 Credit Hours

FERMENTATION: Introduction -- Definition, Types of Microorganisms, Factors effecting Microorganisms activity, Isolation of Microorganisms, Types of Fermented products. Citric Acid -- Fermentation Methods, Major Nutrients, Minor Nutrients, Factors effect on Production, Additives, Recovery of Citric Acid. Commercial Ethanol -- Raw material, Microorganism, Factors, Batch & Continuous method, Distillation. Vinegar -- Raw material, Microorganism, Old and New methods of production, Reactions, High quality Vinegar, Defects, Yield.

FOOD & NUTRITION: Introduction -- Major Nutrients & Minor Nutrients. Vitamins -- Fat soluble; Water soluble; Sources; properties; Function; Deficiency; Recommended Intake; Excess Intake. Proteins -- Classification; Structure; Amino Acid Types; Sources; Properties; Function in Human body; Protein Requirement, Deficiency.

FUELS: Introduction -- Definition; Solid; Liquid; Gas. Solid Fuel -- Classification of Coal, Composition, Uses, Coal Pyrolysis; Coal Liquefaction by pyrolysis; Direct Hydro liquefaction; Coal derived liquids; Liquefaction Processes, Coal Gasification; Coal Gasifiers. Liquid Fuel -- Composition, Basic Petroleum Refinery Processes, Products, Uses. Alternative Fuels -- ( non-conventional fuels ). biodiesel, bioalcohol (methanol, ethanol, butanol), refuse-derived fuel, hydrogen, non-fossil methane, non-fossil natural gas, vegetable oil, propane and other biomass sources.

RUBBERS: Pre-requisite of rubber, general properties of rubber. Classification of rubbers. Natural rubbers -- sources, extraction, preservation, coagulation, concentration & drying..Properties of natural rubber, compounding, additives. Vulcanization (cross linking) types, chemicals & process. Synthetic rubbers --SBR &Silicone, Manufacture, types, properties & uses.

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ESSENTIAL OILS: Fragrances & Flavours -- Definition, classification, Bio-synthesis, primary and secondary metabolites, chemical constituents of essential oils. Extraction of Essential Oils -- conventional methods (Enfleurage, expression, dry distillation, hydro diffusion, water & steam distillation, solvent extraction.) Modern methods of extraction, super critical fluids method, Microwave extraction, accelerated solvent extraction & Headspace trapping techniques.

FORMULATING PERFUME: top note, middle note, base note, Concretes, Absolutes, Tinctures, Distilled oils, expressed Oils, vehicle, fixatives.

LEATHER: Composition of hides, Curing of hides. Beam house operations (soaking, unhairing, liming, trimming fleshing, splitting & deliming), Tanyard operations (picking, bating, vegetable tanning, chrome tanning), Post tanning operations (Retanning, Coloring and Fatiliquoring, drying & finishing), Types of Leather.

Practicals:

1. ASTM Distillation of Crude oil.2. Sulfur content in Coal.3. Sterilization of Tomatoes and effects of preservatives.4. Determination of dextrose equivalent in glucose and hydrolysis of Starch.5. Formation of Ethanol by fermentation using Cane Juice.6. Preparation of Disinfectant.7. Determination of Chromium content in Leather.8. Determination of ash, acidity and protein content in Milk.9. Preparation of Banana Flavor.10. Determination of moisture in kerosene.11. Combustion of Renewable & Non-renewable Fuels.12. The Synthesis of Biodiesel from Vegetable Oil.

Recommended Books:

1. Robert W. Hutkins, Microbiology and Technology of Fermented Foods, IFT Press, Blackwell Publishing, USA, 2006.

2. John Oakey, Fuel Flexible Energy Generation: Solid, Liquid and Gaseous Fuels, Elsevier Science, U.K, 2015.

3. James G. Speight, The Chemistry and Technology of Petroleum, 5th Edition, CRC Press, Taylor and Francis Group, 2014.

4. Robert L. Shewfelt, Alicia Orta- Ramirez, Andrew D. Clarke, Introducing Food Science, 2nd Edition, CRC Press, 2015.

5. Vickie A. Vaclavik, Elizabeth W. Christian, Essentials of Food science, 4th Edition, Springer, 2013.6. John M. deMan, John W. Finely, W. Jeffery Hurst, Chang Yong Lee, Principles of Food Chemistry, 4 th

Edition, Springer, 2018.7. The Complete Book on Rubber Processing and Compounding Technology, NIIR Board of Consultants

and Engineers, Asia Pacific Business Press Inc. 2006.8. Natural Rubber Materials: Volume 1: Blends and IPNs, Editors: Sabu Thomas, Chin Han Chan, Laly

Pothen, Rajisha K. R., Hanna Maria, Print ISBN:978-1-84973-610-7, 2013.9. Science and Technology of Rubber, Edited by James E. Mark, Burak Erman and Frederick R. Eirich,

3rd Edition • 200510. Rubber Processing: An Introduction, Peter S. Johnson, 2001.11. Introduction to Natural and Synthetic Rubbers 1st Edition, by D. W. Duke, ISBN-13: 978-0820600956.12. Extraction Technologies for Medicinal and Aromatic Plants. Scientific Editors:: Sukhdev Swami Handa,

Suman Preet Singh Khanuja, Gennaro Longo, Dev Dutt Rakesh. INTERNATIONAL CENTRE FOR SCIENCE AND HIGH TECHNOLOGY, Trieste, 2008

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13. The Chemistry of Fragrances, From Perfumer to Consumer. 2nd Edition, Edited by Charles Sell, Quest International, Ashford, Kent. ISBN-10: 0-85404-824-3.

14. Flavours and Fragrances, Chemistry, Bioprocessing and Sustainability. 2007. ISBN 978-3-540-49338-9 Springer Berlin Heidelberg New York.

Course No. 508Industrial Economics & Management

3+0 Credit Hours

ECONOMICS: Industrial Economics, Break-even analysis & calculation, Benefit cost ratio, Life cycle of Chemical Industry, Selection between Alternatives.

COST ESTIMATION: Types of costs, Capital and production cost, Cost index, Capital investment, Methods for estimating capital investment.

INTEREST AND INVESTMENT COSTS: Simple, compound & continuous interests, Present worth, Future worth, Discount, Annuities & Perpetuities.

DEPRECIATION: Taxes, Straight Line method, Diminishing Balance method, Sinking Fund method, Annuity Charging method, Insurance policy method, Regular Valuation method, Machine Hour Basis method & Sum of Year’s Digits method.

INVESTMENT EVALUATION: Basis for evaluating project profitability, Discount-cash flows, capitalized cost, Pay out period, Rate of return, Return on investment.

MANAGEMENT: Management functions, Management by objective, Marketing & Sales.

PROJECT ANALYSIS AND PLANNING: Network models PERT (Program evaluation and review technique) and CPM (Critical Path method).

Recommended Books:

1. M. S. Peter, K. D. Timmerhous, “Plant Design & Economics for Chemical Engineers”, 4 th ed., McGraw Hill 2001.

2. William G Sullivan, Elin M Wick, James Luxhoj, “Engineering Economy”, 2005.3. C.M.Chang, “Engineering Management”, 2004.4. Philip Kotler, “Marketing Management”, 12th Edition 2006. 5. Clifford F.Gray & Larson,”Project Management, The managerial Process”, McGraw Hill 2000. 6. Donald G. Newnan,”Engineering Economic Analysis”. Oxford University Press, 2007.

Course No. 510Chemical Process Principles – III (Dynamics)

2+1 Credit Hours

CHEMICAL KINETICS: Chemical kinetic fundamentals, Rate equations for non-reversible, reversible and complex reactions, Evaluation of rate equations from laboratory data, Theories of reaction rates.

CATALYSIS: Homogeneous acid-base catalysis, Heterogeneous catalysis, Solid catalysts and their characterization, Rate equations for fluid-solid catalytic reactions.

ELECTRODE KINETICS: Butler-Volmer equation, Tafel slopes, Effect of adsorption, Effect of mass transfer.

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Practicals:

1. Determination of Order of reactions by various techniques (integration, differential and fractional life methods).

2. Activation energies and rate constants.3. To determine exchange current density by Tafel slopes.4. Mobility and transport number of ions.5. Adsorption isotherms

Recommended Books:

1. Ira. N. Levine, Physical Chemistry, McGraw Hill 6th ed., 2009.2. James House, “Principle of Chemical Kinetics” 2nd ed., Elsevier 2007.3. S.K.Upadh yay, “ Chemical Kinetics and Reaction Dynamics” Kluwer Academic Pub. 2007.4. D.W. Green, R.H. Perry. :Reaction Kinetics, Mc Graw Hill. U.S.A. 2007.5. Dimitry Murzin, “Catalytic Kinetics” Elsevier UK 2005.6. R. Aris, “Elementry Chemical reactor analysis” Bover publication 2000. 7. R.W. Missien, C.A. Mims, B.A. Saville. “ Introduction to Chemical Engineering and Kinetics”. John

Wiley & Sons Inc. 1998.8. S.Wronski, R. Pohorceki, J. Siwinsk, “Numerical Problem in Thermodynamics and Kinetics of

Chemical Engineering Processes”. Begell House 1998. 9. P. H. Rieger, “Electrochemistry”, 2nd ed., Chapman and Hall, New York, 1994.10. P. W. Atkins, “Physical Chemistry”, 4th ed., Oxford University Press, Oxford, 1990.11. J. M. Smith, “Chemical Engineering Kinetics”, 3rd ed., McGraw-Hill, New York, 1987.

Course No. 601Chemical Engineering – III (Heat & Mass Transfer)

2+1 Credit Hours

CONDUCTION, CONVECTION & RADIATION: Heat transfer by conduction in steady state cases for one direction, thermal resistances in series. Heat transfer by convection, application of dimensional analysis to heat transfer by convection. Concept of film and over- all heat transfer coefficients. Heat transfer by Introduction to heat transfer by radiation.

HEAT EXCHANGERS: Heat transfer equipments, their types and selection criteria. Design considerations of shell and tube, double pipe heat exchangers.

BOILERS, CONDENSERS & COOLING TOWERS: Working & types of boilers, condensers & cooling towers.

MASS TRANSFER: Introduction to mass transfer, Models in mass transfer operations, Steady state Single & Double stage Solvent Extraction simulation process, Fick’s law of diffusion.

Practicals:

1. Double pipe heat exchanger.2. Heating and cooling in vessels.3. Cooling Towers.4. Mass Transfer. 5. Insulations.

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Recommended Books:

1. Kern. D. Q., “Process Heat transfer” Mc Graw Hill, 2000.2. Coulson, J. M. & Richardson J. F. “Chemical Engg”. Vol – I Pergamon Press, 1999.3. P.S.Ghoshdastidar, “Heat Transfer”, Oxford University Press, India, 2005.4. Treybal R. E. “Mass Transfer Operations”, Mc Graw Hill, 2000.5. Yunus A. Cengel, “Heat Transfer A practical approach”, 2nd Edition, TATA Mc-Graw Hill, 2003.

Course No. 603Chemical Engineering – II (Chemical Reaction Engineering)

3+0 Credit Hours

INTRODUCTION: Classification of Chemical reactors, Fundamentals of Chemical reactor design, Mass balance equation for ideal reactors.

DESIGN OF HOMOGENOUS REACTORS:

1. Isothermal Reactors: Design procedures for stirred tank, and tubular flow reactors.2. Non-isothermal Reactors: Energy balance equations, Design procedures for stirred tank, and tubular

flow reactors.

TRANSPORT PROCESSES IN HETEROGENEOUS CATALYTIC REACTIONS: External transport process in the fixed – bed and the fluidized – bed catalytic reactors, Internal transport process in porous catalytic i.e. Intrapellet mass transfer, Intrapellet heat transfer, Mass transfer with reaction. Mass and heat transfer with reaction, Effect of internal transport on selectivity and poisoning.

INTERPRETATION OF EXPERIMENTAL KINETICS DATA: Interpretation of laboratory kinetic data from

homogeneous and heterogeneous laboratory reactors, Calculation of the global rate.Design of Heterogeneous Catalytic Reactors:1. Fixed – bed Reactors

Design of isothermal and adiabatic fixed – bed reactors, Design of non isothermal – non adiabatic fixed – bed reactors.

2. Fluidised – bed Reactors

Recommended Books:

1. O. Levensreal, “Chemical Reaction Engineering”, John Wiley & Sons, 2000.2. H. Scott Foglar, “Elements of Chemical Reaction Engineering”, Practice Hall, USA, 2004.3. J. M. Smith “Chemical Engineering Kinetics, 4th ed., McGraw Hill, New York, 2000.

Course No. 605Analytical Techniques-II

2+1 Credit Hours

PRINCIPLE AND INSTRUMENT OF SPECTROPHOTOMETRY: Introduction review and atomic molecular energy, absorption and emission of EMR, Instrumentation for measuring absorption of radiation, method and applications of spectrophotometry.

ATOMIC SPECTROSCOPY: Atomic absorption spectroscopy, Flame emission spectroscopy, plasma and electrical discharge emission spectroscopy.

I.R SPECTROSCOPY: Introduction, principle of IR spectroscopy, instrumentation, fundamental modes of vibrations, conditions for IR absorption, I.R regions, sampling techniques, characteristics of IR absorption of common functional groups and application. FTIR spectroscopy.

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X-RAY SPECTROPHOTOMETRY: Introduction & Instrumentation application, Emission, Dispersion and detection of x-rays, Absorption and Diffraction of x-rays, Preparation of Samples, Quantitative X-ray fluorescence analysis.

ELECTRONMICROBE: Introduction, Instrumentation, Applications.

Practicals:

1. Draw the absorption spectra of KMnO4, K2Cr2O7, K2CrO4 2. Multy component mixture analysis by Spectrophotometry.3. Draw the calibration graph of KMnO4, K2Cr2O7, K2CrO4 by Spectrophotometry. 4. To verify Beer-lambarts law and determine the concentration of unknown solution by

spectrophotometry5. Water quality monitoring:

i. sampling and preservationii. Physical Examination: pH, electrical conductivity, turbidity, colour, odour, TDS, TS and TSSiii. Chemical Characterization: Acidity, Alkalinity, Hardness, Sulfate content, chloride content

6. Separation and estimation of Food dyes by Spectrophotometry. 7. Glycerine Analysis.8. Chemical treatment of water.

Recommended Books: 1. J. mendham, R. C. Denney, J. D. barnes, M. Thmoson, B. shivashnakar, “Vogels Textbook Of

Quantitative Chemical Analysis”, 6th ed., Pearson education (2006)2. D. L. Pavia, G. M. Lampman, George S. Kriz, “Intorduction to spectroscopy”, 5th ed., cengage

learning, USA, 20143. Barbara H. Stuart,” Infrared Spectroscopy: Fundamentals and Applications”, John wiley and sons ltd,

2004.4. D. A. Skoog, F. J. Holler, S. R. Crouch, “Principles of Instrumental Analysis”, 7 th ed, Cengage learning,

USA, 2016.

Course No. 607Chemical Process Principles – IV

(Solution Thermodynamics & Vapor Liquid Equilibrium)2+1 Credit Hours

SOLUTION THERMODYNAMICS: Partial properties, Fugacity and fugacity coefficient of pure species, Fugacity and fugacity coefficient for species in solution, Generalized correlations for the fugacity coefficient, Excess properties, Behavior of excess properties of liquid mixtures, Liquid phase properties from Vapor liquid equilibrium (VLE) data, Models for the excess Gibbs energy.

VAPOR LIQUID EQUILIBRIUM (VLE) CALCULATIONS: Dew Point, Bubble Point, and Flash calculations for ideal and non ideal solutions.

Practicals:

1. Measurement of heat of mixing of binary mixtures at different temperature.2. Measurement of volumes of mixing of liquid mixtures.3. Determination of free energy changes.4. Phase Equilibria study (liquid-vapour, liquid-liquid).5. Determination of partial molar quantities.6. Measurement of Equilibrium Constants.7. Study of Phase rule.

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Recommended Books:

1. Yasar Damirel, “Nonequilibrium Thermodynamics”, 2nd ed., Elsevier 2007.2. J. M. Honig, “Thermodynamics”, 3rd ed., Academic Press 2007.3. Eugene Machlin, “An introduction to Aspect of Thermodynamics and Kinetics relevant to Material

Science”, 3rd ed., Elsevier 2007.4. Yoshekata Koga, “Solution thermodynamics and it application to aqueous, solutions”, 2007.5. J. M. Smith, H. C. Van Ness, and M. M. Abbot, “Introduction to Chemical Engineering

Thermodynamics”, 7th Ed., McGraw Hill, New York, 2005.6. H. C. Van Ness, and M. M. Abbot, “Classical Thermodynamics of Non-electrolyte Solution with

Applications to Phase Equilibria”, McGraw Hill, New York, 1982.7. J. M. Prausnitz, R. N. Lichtenthaler, and E. g. be Azevedo, “Molecular Thermodynamics of Fluid

Phase Equilibria”, 2nd ed., Prentice Hall, Englewood Cliffs, NJ, 1986.8. P. Benedek, F. Olti, Computer Aided “Chemical Thermodynamics of Gasses and Liquids: Theory,

Models. Programs”, John Wiley & Sons, New York, 1985.9. R. C. Reid. J. M. Prausnitz, and B. E. Poling, “The Properties of Gasses and Liquids”, 4th ed., McGraw

Hill, New York, 1988.

Course No. Ach – 609Chemical Process Industries Inorganic – I

2+1 Credit Hours

SPECIAL CERAMICS: Technical & Chemical Ceramics, Ceramics in the electrical industry, The ceramics for the new technologies.

COMPOSITE MATERIALS: Properties, Types & different materials.

EXPLOSIVES & PROPELLANTS: Characteristics, Types & applications of explosive & propellants.

FERTILIZER TECHNOLOGY: Recent advancements and process control in the Production of fertilizers, super & triple super phosphate fertilizer, Role of fertilizer in agricultural soil.

SUPER CONDUCING MATERIALS: Theory, types & application of super – conducting materials.

Practicals:

1. Estimation of nitrogen in nitrogenous fertilizers.2. Estimation of phosphate in phosphate fertilizers.3. Preparation of chrome red.4. Purification of copper sulphate.5. Determination of concentration of copper sulphate solution by spectroscopic method.6. Material Testing to be performed from different industries.

Recommended Books:

1. S. S. Dara “A Text book of Engineering Chemistry” 9th ed 20042. NIIR Board “Industrial Chemicals Technology Hand Book”, published Asia Pacific Business Press

Dehli India 2000.3. Donals R. AsReland “The Science & Engineering of Materials” PWS Published 1995.4. Singer & Sonja S. Singer, “Industrial Ceramics Felix” Oxford & IBH Publishing Co PVY-1963.5. G. T. Austin “Shreve’s Chemical Process Industries” 7th edition McGraw Hill 1991.6. Kirk-Othmer “Encyclopedia of Chemical Technology” Joh Viley & Sons. 1997.7. Barnes & Noble “Materials & Technology” Incorporation Longman Group Ltd. 1988.

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8. Akkhavan, “Chemistry of Explosives” J. John Wiley & Sons; Incorp 1998.9. M. E. Pozin, “Fertilizer Manufacture” Mir Publication 1990.10. O.P. Khanna “A text book of Material Science and Metallurgy” Dhanpat Rai Publications 2004.

Course No. 611Petroleum & Petrochemicals – I

2+1 Credit Hours

PETROLEUM PRODUCTION: Introduction to Petroleum, Origin, geological survey, types of drilling equipment. Drilling mud, completion.

PETROLEUM REFINING: Chemistry, Desulphurization, Evaluation of oil stocks. Tube still heaters, tube still heaters performance and design calculation. Distillation towers. Atmospheric and vacuum distillation, calculation of tower dia meter and performance, Stabilization.

CRACKING AND REFORMING: Thermal cracking, catalytic cracking, hydrocracking and catalytic reforming.

CHEMICAL TREATMENT: Treatment techniques of refinery distillation products, testing of petroleum product, natural gas and refinery gases.

TRANSPORTATION: Method of transportation, types of pipelines, pipelines design and construction.

Practicals:

1. Fractional distillation of local crudes.2. Vacuum distillation of topped crude.3. Stabilization of straight run gasoline.4. Air blowing of asphalt. 5. Quality control of oil products.

(i) Percentage of water in oil.(ii) Flash Point.(iii) Carbon residues.(iv) API Gravity.(v) Smoke Point.(vi) Freezing Point of wax.

Recommended Books:

1. Nelson, W. L. Petroleum Refinery Engineering McGraw Hill Ed. IV. 2002.2. Hobson, G. D, “Modern, W. P. Petroleum Technology”, Applied Science Publishers, 2000.3. Mc Ketter J. J. ed. “Advances in Petroleum Chemistry and Refining”. Inter Science Publishers, 2003.4. Parkash, “Refining Processes Hand Book”, Elservier / APP 2003.5. B. K. Bhaskara Rao, “Modern Petroleum Refining Processes”, 2001.6. D.S.J.Jones,”Element of petroleum processing”,1st ed.2000.7. J.P.Waquieer,”Handbook of petroleum refining process” 2001.8. H.K. Abdel, Al. M. A. Fahim, “Petroleum & Gas field processing 2nd ed., 2005.9. Chris Devices, “Industrial utilization of natural gas”, 2000.10. Serge Raseev, “Thermal and catalytic processes in Petroleum refinery”, 2000.

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Course No. 613Pharmaceutical Industries – I

2+1 Credit Hours

DRUG: Introduction of drug, Classification of drug, Administration of drug, Absorption of drug Distribution of drug, Metabolism of drug, Excretion of drug.

BIOAVAILABILITY: Definition of Bioavailability, Factors affecting bioavailability, Half life of drug.

STRUCTURE ACTIVITY RELATIONSHIP WITH FUNCTIONAL GROUP: Structure activity relationship in drug with different functional group (alcohol, aldehyde, carboxylic, ketone etc).

ANTIBIOTIC: Definition, Different types of Antibiotic, Factors affecting antibiotic, Preparation of Antibiotics, Method for preparation of antibiotic.

ANALGESIC: Definition, Types of analgesic, Selection of analgesic, Importance of analgesic some important analgesic.

SULFA DRUG: Introduction of Sulfa drug, Classification of sulfa drug, Selection of sulfa drug, Some important sulfa drug.

Practical:

1. To prepare castor oil emulsion & analyze it.2. To prepare Bismuth Kaolin suspension & analyze it.3. To prepare and analyze Zinc Oxide Ointment.4. To prepare lotion & analyze it.5. To prepare corminative mixture and analyze it.6. To prepare & analyze sulfur Ointment.7. Preparation of pyruric acid.

Recommended Books:

1. Burger, Al fred. Drugs and people “Medications their history and origin and the way they act” Virginia 2002.

2. Greedom Joe “Generic drugs natural substitutes”, Joe Graedon’s new people’s pharmacy Avon 2002.3. Griffth H. Winter “Complete guide to prescription and non prescription drugs” 2004.4. Physician’s Desk Reference Medical Economics Annual Complete information on prescription drugs.

2003.

Course No. 615Polymer Synthesis2+1 Credit Hours

POLYMERIZATION MECHANISM: Polyesters, Polycarbonates, Polyacrylic, Polyamides, Polyaramides, Polyimide, Philips, Ziegler-Natta and Metallocene.

ADVANCE POLYMERIC MATERIALS: Specialty thermoplastics, conducting polymers, biopolymers, ionic polymers: ionomers, ionic cross linking, ion-exchange, ionic polymer-metal composites, applications.

POLYMERS IN TEXTILE FINISHING: Thickeners, binders, functional finishes, anti-microbial coatings, water-repellent and flame-retardant coatings.

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POLYMERS IN CONSTRUCTION: Polymers for concrete reinforcement, polymer as thermal insulators, hydrogels and water absorbing polymers.

CHAIN TRANSFER MECHANISMS: Free Radical chain transfer, Maya method, chain length dependent termination, Determination of chain transfer constant, chain length distribution method, kinetics of chain transfer, pulsed laser Polymerization, Cobalt-based Catalysts for Acrylic polymerizations, CCT for Oligomers, Addition Reaction Fragmentation, CCT for functional acrylates, Determination of chain transfer in CCT, chain transfer cycle for living Polymerization, Block and Graft Copolymer CCT, Catayst efficiency measurements, CCT for emulsion polymerization, molecular weight control.

POLYMER NANOCOMPOSITES: Polymer Nanocomposites: Comparison with conventional composites, matrix materials and nano-particulates, challenges in the production polymer nanocomposites with carbon nanotubes, nanorods, nano fibre and nanoclay, characterization, applications.

Practicals:

1. Bulk polymerization of ∞-aminodecanoic acid and estimation of kinetics of polymerization by end group analysis.

2. Polymerization of methyl methacrylate in the presence and absence of chain transfer agent and observation of time dependence of reaction.

3. Synthesis of biodegradable film of carboxy methyl cellulose and poly vinyl alcohol and testing its transparency, thickness and water solubility.

4. Synthesis of polyaniline (conducting polymer) via interfacial polymerization.5. Synthesis of Polyurethane foam as a construction material for sound insulation.

Recommended Books:

1. Odian G. “Principles of Polymerization”, 4rd Ed. Wiley, 2004.2. Engineering and Specialty Thermoplastics: Water Soluble Polymers, Fink J.K., Wiley & Sons, 2011 3. Biopolymers: Biomedical and Environmental Applications, Kalia S., Avérou L., Wiley & Sons, 2011 4. Developments in ionic polymers, Vol. 1, Wilson A.D., Prosser H.J., Applied Science Pub., 2013 5. Polymers in Construction, Akovali G., Smithers Rapra Press, 2005 6. Degradable Polymers: Principles and Applications, Scott G., Springer, 2nd Ed., 2003. 7. Polymer Composites: From Nano-to-Macro-Scale, Friedrich K., Fakirov S., Zhang Z., Springer, 2005 8. Polymer nanocomposites, Mai Y-W., Yu Z-Z., CRC Press, 2006 9. Characterization Techniques for Polymer Nanocomposites, Mittal V., Wiley-VCH, 201210. J.H. Koo, Polymer nanocomposites: processing, characterization, and applications, McGraw-Hill

Professional, New York, 2006.

Course No. 617Textile Processing – I (Colour Matching & Printing Technology)

2+1 Credit Hours

DATA COLOUR MEASUREMENT: System and numerical measurement of colour and quantity colour mixing difference.

FABRIC HANDLE EVALUATION: Softeners application, Objective parameters of fabric handle, objective and subjective assessment of fabric handle KES of fabric handle.

TEXTILE PRINTING METHODS: Introduction to block printing, roller printing, screen printing, flat screen printing & rotary screen printing.

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ROTARY SCREEN PRINTING MACHINES: Mechanical aspects of rotary printing machine, Design registration, blanket and screen synchronization & printing faults identification.

PRINTING WITH DIFFERENT COLORANTS: Pigment printing, Reactive printing, vat printing & Disperse printing.

Practicals:

1. Colour prediction.2. Colour difference measurements.3. Fabric handle measurements.4. Wet Processing Quality Assurance.

Recommended Books:

1. Tyron, L. Vigo, “Textile Processing and Properties”, Elsewer Amestradem, 2006.2. Colour & Coloumetry Alain Chrisment 3c Canonical France 2006.3. S. Kawabata, “Objective Parameters of Fabric handle”, Textile Machinery Society Japan Kyoto 2000.4. W.C. Mile, “Textile Printing”, Society of Dyers and Colorists, 2003.5. V.A. Shenai,” Technology of Printing”, Society of Dyers and Colorists, 2004.

Course No. 619Food Science & Technology

2+1 Credit Hours

FOOD PROCESSING:

a) Dairy Technology: Composition of milk, Separation of cream from milk, Pasteurization and Equipments, Homogenization, fortification of milk and milk products.

b) Fruits and vegetable canning: Harvesting, Properties of fruits and vegetables, washing techniques, peeling, Trimming, cutting, Blanching, Syrup composition, Filling, sterilization and capping.

c) Tea and Coffee: Types and classification, Fresh leaf composition, Black Tea Manufacturing, Biological activity of Tea, coffee processing.

FOOD MICROBIOLOGY: Classification of microorganisms, Food spoilage, Toxins, food born illness and Chemical Food poisoning.

BAKING TECHNOLOGY: wheat classification, composition, role of ingredients, biscuit types and manufacturing of various types of biscuits.

CONFECTIONARY TECHNOLOGY: Types of candies, types and properties of sugar, Role of ingredients used in confectionary, Gelling agents, manufacturing of various types of confectionary products.

NEUTRACEUTICAL CHEMICALS

Practicals:

1. Salt analysis.2. Dairy products analysis.3. Extraction of caffeine and theobromine from Tea and Coffee.4. Determination of saponification, peroxide, acid, iodine, value of oil.5. Effect of various ingredients in manufacturing of biscuit.

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Recommended Books:

1. Corinne Balog catalodo, Sharon Rady Rolfes, “Understanding Clinical Nutrition” 3rd ed., 2004. 2. Israel Gold berg, Functional Foods (Designer foods pharma foods, Neutracenticals) , 2003.3. Adams M.R and Moss , “Food Microbiology”, Turpin Distribution service Ltd 2000. 4. William-e-Frazier, Westhoff D.C Food Microbiology 4th Ed. Mc Graw Hill, 2002.5. Walstra P. Dairy Technology, Marcel & Dekker Inc, New York 2000.6. Jongen W Fruit and vegetable processing, improving quality, wood head publishing Co. 2002.7. Sanvel A. Matz, Bakery Technology and Engineering. 3rd ed., 2000.8. David A.V. Dendy, Bogdanj, “Cereals and Cereals Product, Technology and Chemistry” 2001.9. HUI. Y.H “Encyclopedia of food science & Technology”. John wiley and sons Inc., New York 2004.10. Jackson E.B, Sugar Confectionary manufacture technology 3rd Ed., Blackie Academic & Professional

2006.

Course No. 621Metallurgy & Materials Technology – I

2+1 Credit Hours

MATERIAL TESTING: Tensile test, Hardness test, Impact test, Fatigue and Creep properties.

METAL WORKING: Rolling, Forging, Deep drawing & extrusion.

FOUNDRY PRACTICE: Pattern and Core making, Runner & Feeder system. Continuous casting. Relationship between cast structure and properties.

POWDER METALLURGY: Production, Compaction and Sintering of powder metal into solid shapes. Application of powder metallurgy.

WELDING, BRAZING AND SOLDERING: Types of welding and defects in weld structure, Brazing & Soldering.

FRACTURE ANALYSIS: Mechanism and characteristics of fractures, Fracture – toughness criteria, Deformation and Dislocation theories.

Practicals:

1. Tensile test – Ferrous & Non Ferrous2. Hardness & Impact test3. Casting of low melting alloy4. Welding, Brazing and Soldering5. Ductile and Brittle fracture study

Recommended Books:

1. Dharmendar Kumar, S. K. Jain, “Foundry Technology”, CBS Publishers, Delhi, 1994.2. L. M. Ground, “Principle of Welding Technology”, English Language Book Society, 1990.3. George E. Dieter, “Mechanical Metallurgy”, Mc Graw Hill Company, 1988.4. V. J. Colengelo, “Analysis of Metallurgical Failure”, John Willy & Sons, 1997.5. R. E. Smallman, R. J. Biship, “Metal and Materials”, Butterworth-Heinemann Inc., 1995.6. W. F. Smith, “Principle of Material Science and Engineering”, 3rd ed., McGraw Hill, New York, 1996.7. P. H. Rieger, “Electrochemistry”, 3rd ed., Chapman and Hall Inc., New York, 1994.

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Course No. 623Research Project0+3 Credit Hours

RESEARCH PROJECT: Students can take a Research project in place of an optional Course under the supervision of Faculty Members. After completion of his / her project, a research report has to be submitted and presentation is to be given in front of Faculty members.

Course No. 625Electrochemical Industries

2+1 Credit Hours

FUNDAMENTAL CONCEPTS: Electron Transfer, Mass Transfer, Adsorption, Electro catalysis, Properties of electrolyte solution, Phase formation in electrode reactions, Basic Electrochemical Engineering.

CHLOR-ALKALI INDUSTRIES: Brine Electrolysis, Chlorine Cell Technologies, Production of KOH.

INORGANIC ELECTROLYTIC PROCESSES: Fluorine, Potassium Permanganate, Potassium dichromate & Chromic acid, Hydrogen peroxide, Peracids and their salts, Synthesis of metal salts via anodic dissolution.

ORGANIC ELECTRO SYNTHESIS: The hydrodimerization of acrylonitrile other commercial electro synthetic process, Indirect electro synthesis.

TREATMENT OF WATER AND EFFLUENTS: Metal ion removal and metal recovery, Electro dialysis, Electrolytic methods of phase separation, Flue gas desulphurization, other electrochemical processes.

METAL FINISHING: Electroplating, Electro less plating, Electrophoretic painting, Conversion coatings, other surface finishing technique.

BATTERIES AND FUEL CELLS: Battery characteristics, Battery specification, Battery components, Fuel cells.

Practicals:

1. Laboratory scale electrochemical synthesis of inorganic and organic compounds.2. Metal Finishing: Electroplating3. The practical study of Anodic behavior of metal4. Differential potentiometer titrations.

Recommended Books:

1. V. S. Bagotsky, “Feul Cells: Problems and solutions”, Wiley, New York 2009.2. W. Plieth, “Electrochemistry for material science”, Elsevier, Oxford UK 2008.3. C.H. Hamann and W. Vielstich, “Electrochemistry” 2nd ed., Wiley – VCH, Weinheim 2007.4. R. Holze, “Electrochemicaly: Electrochemical thermodynamics and kinetics”, Springer, New York

2007.5. N. Kanani, “Electroplating: Basic principles, processes and practice”, Elsevier, Oxford UK. 2004.

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Course No. 627Polymer Rheology2+1 Credit Hours

Introduction to elastic solids and viscous liquids. Flow of polymeric liquids, Material functions. Generalized Newtonian fluid Linear viscoelastic constitutive equations. Non-linear viscoelastic constitutive equations. Single integral Doi – Edwards, KBKZ and Larson – Bell constitutive equations. Fluid dynamics of rheometry, shear and extensional rheometry, rheometer design, rheo – optics.

Practicals:

1. Birefringence in 1-2 plane measurement of orientation angle in a cone-plate geometry.2. Birefringence in 1-3 plane using a slit geometry in a flow cell.3. Flow velocity measurement in v1, v2, v3 direction through a slit die using laser velocimetry.4. Birefringence in 2-3 plane using a capillary apparatus.5. Linear viscoelastic oscillatory shear measurement in a parallel plat geometry at low strains.6. Measurement of relaxation spectrum by linear regression, singular value and non-linear regression

techniques.7. Non-linear viscoelastic step strain measurements in a parallel plate geometry8. Non-linear viscoelastic steady measurement in a parallel plat geometry.9. Numerical solution of Lodge, Maxwell and Wagner’s constitutive equation for the 1-3 plane centre line

streamline and its comparison with experimental results.

Recommended Books:

1. Larson R. G. “Constitutive Equation for Polymeric Melts and Solutions”, Buttorworths, 1989.2. Macosko C. W. Rheology “Principles, Measurements and Applications”, VCH Publishers, New York,

1999.3. Bird R. B. Armstrong R. C., Hassager O, “Dynamics of Polymeric Liquids” Vol. 1 & 2, McGraw Hill,

New York, 1987.4. Roberts, Royston M; Raymond B, and Carraher, Charies E; “Giant Molecules”; John Wiley and Sons

Inc., New York 1990.5. Piau. J. M and Agassant J. F. Rheology for “Polymer Melt Processing”, Elsevier Amsterdam, 1996.6. A. W. Birley, B Haworth and J Batchelor, “Physics of Plastics – Processing Properties and Materials

Engineering” Carl Hanser Verlag (Munich), 1992.

Course No. 629Leather Technology

2+1 Credit Hours

GENERAL INTRODUCTION: General Process in light leather, Leather, industry in Pakistan:

RAW MATERIALS: Raw hides and skin, commercial classification, structure of skin, commercial composition of the skin, curing and disinfection of raw hides and skins. Types of raw material

WATER: Water composition in leather products bating according to the total hardness, water softening.

BEAMHOUSE WORK: Sooking, liming, deliming and bating.

TANNING PROCESS: Chrome tanning, aldehyde tanning, synthetic tanning, masking effect and masking agents.

NEUTRALISATION AND RETAINING: Neutralisation, retannage of various leather.

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DYEING OF CHROME LEATHER: Classification of leather dyes, blending dyes, methods of applying dyes to leather, factor affecting on dyes process, miscellaneous dyeing process.

FINISHING: Polishing, Bottoming, Milling, padding and spraying, drying.

SAFETY AND ENVIRONMENTAL PROTECTION: Waste Water treatment:

Practicals:

1. Microscopic study of leather.2. Tanning and retaining of hides and skin.3. Study cross linking between skin and tanning agents.4. Study the deacidification of leather.5. Study the water repellent treatment of leather.6. Dyeing of leather.7. Recovery of chrome from waste.8. Treatment of dyeing waste water treatment of chrome waste water.

Recommended Books:

1. Sharphouse J.H., “Leather Technician’s Hand book” London Second ed 2000. 2. “Encyclopedia of Chemical Technology”, 3rd edition Wiley Inter Science New York 2000.3. Fred ‘O’ Flaherty William T. Roddy “The Chemistry & Technology of Leather 3rd edition 2004.4. R Norris Shreve, “Chemical Process industries” 5th ed., 2004.5. O Gi Choichi., “A practical guide to light leather processing” Wara 5th ed. 2005.

Course No. 631Fuel Technology & Renewable Energy Resources

2+1 Credit Hours

INTRODUCTION: Sources of Fuel and Energy, Pakistan’s current energy situation

SOLID FUELS: Coal and its products such as coke and briquettes, Coal: Origin, classification, characteristics, test methods and uses.

LIQUID FUELS: Petroleum: origin, composition and characteristics. Refinery products and their test methods. Cracking and reforming.

GASEOUS FUELS: Natural gas, producer gas, water gas, bio gas, blast furnace gas, and coke oven gas.

SOURCES OF RENEWABLE ENERGY: Solar energy, Geothermal, hydro, wind, ocean, hydrogen and energy from biomass.

Practicals:

1. Proximate and ultimate analysis of coal.2. Test methods of petroleum.3. Solar energy equipment operation / study.4. Gaseous fuel equipment operation / study.

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Recommended Books:

1. Bob Brooke, Russell E. Train, “Solar Energy, (Introduction)”, Chelsea House Publishers, 2000.2. D. L. Elliot, C.G. Holladay. W. R. Barchet, H.P Foote, “Wind Energy Resources”, Atlas of the United

States, Wind Books Inc. 2004.3. Karl W. Boer, “Advances in Solar Energy”, Vol. 11, American Solar Energy Society, 2005.4. Wilfrid Francis Martin C. Peters, “Fuels and Fuel Technology”, Franklin Book Company, Inc., 2007.5. Fuels for the year 2000 and beyond, American Chemical Society Division of Fuel Chemis,

2003.

Course No. 602Chemical Engineering – IV (Plant Design)

3+0 Credit Hours

PLANT DESIGN: Introduction to chemical engineering plant design, process studies, scale-up, plant location, site selection, plant layout.

MATERIAL AND ENERGY BALANCE: Basic calculations and industrial stoichiometry material & energy balance.

FLOW SHEET SYNTHESIS AND DEVELOPMENT: Process selection, type of flow diagrams and final process flow sheet presentation, graphics symbols for piping systems and plants.

AUTOMATION AND CONTROL: Agitation, heating and cooling systems, process control and instrumentation, digital control and detail design of reaction vessel.

PROJECT ECONOMICS: Costing and selection between, alternatives, Payback times, Return on investment, discount rates & Cash flow diagram, Life cycle of a chemical plant.

HEALTH, SAFETY AND ENVIRONMENT: Process safety, material handling, operational hazards, health issues and effluent treatment.

EQUIPMENT SELECTION, SPECIFICATION AND DESIGN: Separation processes. Solid – solid, liquid- solid, liquid – liquid, gas – solid separations.

DESIGN PROJECT / PRACTICAL: A design project of 40 marks based on theoretical principles and data collected is to be submitted by each student convening the following: Market survey, Manufacturing cost, Cost of Product, Breakeven analysis, Pay Back period, and Process detail. Materials and energy balance; process flow sheet. Materials of construction, Instrumentation, Mechanical drawing of reaction vessel, Health, safety and environment.

Recommended Books:

1. Coulson. J. M.,& Richardson, J.., Sinnott, R.K., “Chemical Engineering” Vol.,6, Pergamon press. 20002. David M. Himmelblau, “Basic Principles and Calculations in Chemical Engineering”, 6th Edition,

Printence Hall, 2001.3. Peter M.S. & Timmerhaus, K.D.,” Plant Design & Economics for chemical Engineers”, 5 th Ed McGraw

Hill.20034. Martyn S Ray & Martin G. Sneesby, “Chemical Engineering Design Project, A case study Approach”,

2nd Edition, Globe & Breach Science Publishers, 1998.5. W. L. Luyben, “Process Modeling, Simulation and Control for chemical Engineers”, McGraw-Hill 2000.6. JamesWei, “Product Engineering: Molecular Structure and Properties”, Oxford University Press, 2006.

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Course No. 604Industrial Pollution2+1 Credit Hours

INTRODUCTION: Environmental pollution ( Industrial) and sources.

WATER: Quality -- Physical, Chemical & Biological parameters. Purification -- Processes, Waste water treatment methods and applications. Primary, Secondary and Tertiary Treatments. Disposal and reuse. Effluent treatment / recycling -- Chemical process industrial effluent treatment & its recycling.

POLLUTION: Air -- Sources, Air-Pollution control methods in industries. Noise -- Health impact, Measurement and control in industries. Environmental Impact assessment.

ENVIRONMENT QUALITY ASSURANCE: Purposes and designs of environmental sampling, Sample collection and preservation methods. Standard solutions and standard curves. S.I. and derived S.I. units. Analytical techniques for soil, water and plant analysis. Data interpretation for quality control, precision and accuracy. Preparation of Standard solutions and Standard curve. Use of Potentiometery, Conductivitymetry, Titrimetery, Gravimetery, Spectroscopy and Chromatography for the analysis of environmental samples. Determination of chemical characteristics of water and waste water (pH, All Solids, BOD, COD, Fluoride, NO3–N & NH4-N), soil (NPK and organic matter contents, salinity & sodicity).

Practicals:

1. Waster-quality Assessment for 12 NEQS parameters.2. Analysis of Waste-Treatment and disposal methods.3. Analysis of Drinking water.4. BOD Assessment of waste water.5. COD Assessment of waste water.

Recommended Books:

1. Nelson.L.Nemerow, “Industrial Waste Treatment contemporary practice & vision for future”, Butter Worth-Heine Mann published in 2007.

2. Carole Terwilliger Meyers, “Encyclopedia of Environmental Pollution and clean up” (Wiley encyclopedia series in environmental science) 2 volume set, Published by John Wiley & Sons, 2002.

3. Nelson.L.Nemerow, “Strategies of Industrial and Hazardous Waste Management”, 3rd ed., John Wiley & Sons 2004.

4. Franklin Agardy, “Strategies of Industrial and Hazardeous Waste Management”, John Wiley & Sons 2000.

5. Nelson.L.Nemerow, “Industrial Water Pollution Origins, Characteristics and Treatment”, Addison-Wesley 2004.

6. H.F.Lund, “Industrial Pollution Control Handbook” Mc.Graw Hil, 2006. Standard Methods for the Examination of Water & Wastewater.21st Edition. A Greenberg (American Public Health Association), 2005.

Course No. 606 Analytical Techniques - Iii

2+1 Credit Hours

CHROMATOGRAPHY: Introduction Principle of chromatography, classification, theoretical treatment of chromatography, liquid column chromatography, liquid liquid chromatography, HPLC, Gas chromatography.

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NUCLEAR CHEMISTRY: radioactivity, characteristics of radioactive decay, decay kinetic, types of decay, artificial radioactivity, application of radioactivity, nuclear fission and fusion, classification of nuclear reactor, nuclear waste management.

RADIOCHEMICAL METHODS: Neutron activation Analysis Principles of neutron activation analysis, Source of neutron, Capabilities and limitation of neutron activation, Practical consideration in neutron activation.

AUTOMATIC AND PROCESS ANALYZER: Introduction, Sample handling system. Analyzer calibration, Process gas chromatography, Oxygen Analyzers, Moisture analyzers, Calorimetric Analyzers.

Practicals:

1. Preparation of Columns. 2. Selection of mobile phase. 3. Analysis of dye mixture by TLC 4. Examination of dyes in ink by ascending paper chromatography. 5. To separate the mixture of methyl orange and methylene blue by column chromatography.6. Determination of Ion exchange conditioning and capacity.7. Separation of Vitamin 'A' compounds by TLC. 8. Semi quantitative separation of Copper, Cobalt and Nickel on slotted paper strips.

Recommended Books:

1. Francis Rouessac, Annick Rouessac, “Chemical Analysis: Modern Instrumentation Methods and Techniques”, 2nd ed, John wiley and sons ltd, 2013.

2. Mark F. Vitha, “Chromatography: Principles and Instrumentation”, John wiley and sons ltd, 2017.3. Gregory Choppin, Jan-Olov Liljenzin, Jan Rydberg, C. Ekberg,” Radiochemistry and Nuclear

Chemistry”, Elsevier and bookaid, 2013.4. Veronika R. Meyer, “Practical High-Performance Liquid Chromatography”, John wiley and sons ltd,

20135. D. A. Skoog, F. J. Holler, S. R. Crouch, “Principles of Instrumental Analysis”, 7 th ed, Cengage learning,

USA, 2016.

Course No. 608 Chemical Process Principles – V

(Flow Processes & Thermodynamic Cycles)3+0 Credit Hours

THERMODYNAMIC OF FLOW PROCESSES: Mass, energy, and entropy balances, Duct flow of compressible fluids. Expression and Compression processes.

POWER GENERATION: The steam power plant, The Otto engine, The Desel engine, The Gas-Turbine power plant.

REFRIGERATION, HEAT PUMPS, AIR-CONDITIONING AND LIQUEFACATION: The Carnot refrigerator, The Vapour – Compression cycle, Comparison of refrigeration cycles, The choice of refrigerant, Absorption refrigeration, The Heat Pump, Air-conditioning systems, Cooling towers. Liquefaction Processes.

THERMODYNAMIC ANALYSIS OF PROCESSES: Sources of energy supply and energy demands, Combined cycles, Combined heat and power co-generation, Energy management and energy audits, The technology of energy saving, Alternative energy sources.

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Recommended Books:

1. Yasar Damirel, “Nonequilibrium Thermodynamics”, 2nd ed., Elsevier 2007.2. J. M. Honig, “Thermodynamics”, 3rd ed., Academic Press 2007.3. Eugene Machlin, “An introduction to Aspect of Thermodynamics and Kinetics relevant to Material

Science”, 3rd ed., Elsevier 2007.4. Yoshekata Koga, “Solution thermodynamics and it application to aqueous, solutions”, 2007.5. J.M.Smith H.C.,Van Ness, and M.M. Abbot, “Introduction to Chemical Engineering Thermodynamics”,

7th. Ed., McGraw Hill, New York, 2005.

Course No. 610Chemical Process Industries Inorganic – II

2+1 Credit Hours

REFRACTORIES & ALLIED PRODUCTS: Physical forms of a refractory, Manufacture. Properties & application of refractories. Refractory coatings & special refractories.

INORGANIC FIBERS: Glass Fiber, Refractory Fiber

MEASUREMENT & CONTROL OF HIGH TEMPERATURE:

METALLIC CORROSION: Corrosion in general, Reaction mechanism of corrosion, Types & prevention of corrosion.

ELECTRO THERMAL INDUSTRIES: Electro thermal products, Manufacture & Applications, Artificial abrasives, Furnaces used for manufacturing electro – thermal products.

Practicals:

1. Qualitative analysis of refractories.2. Quantitative analysis of refractories.3. Electroplating and study of corrosion resistance.4. Physical testing to be performed in the concerned industries.

Recommended Books:

1. Dr. W. Buchner, Dr. R Schlibs. Dr. G. Winter & Dr. K. H. Buchel, “Industrial Inorganic Chemistry” VCH Publisher, New York, 1989.

2. Alfered B.Searle “Refractory Materials; Their manafacture & Uses” Charles Griffin & Company Ltd. 3 rd

ed. 2001.3. F. H. Norton, “Refractories”, McGraw Hill Book Company, 2002.4. S. S. Dara “A Text book of Engineering Chemistry” 9th ed 20045. Krishan K. Chawla, “Composite Materials Science and Engineering” Springer-Verlag New York Inc. 6. 1997.

Course No. 612Petroleum & Petrochemicals – II

2+1 Credit Hours

GENERAL PETROCHEMICAL INDUSTRIES: Hydrocarbon sources and raw material for petrochemical industries, their examples, production and characterization, Manufacture and purification of acetylene, Olefins and BTX production.

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AMMONIA: Natural gas, desulphurization. Reforming, Shift conversion separation and purification of gas streams Ammonia synthesis.

LUBRICANTS: Types of base oil, additives, refining of base oil.

RECENT TRENDS: Recent trends by research and developments in petroleum and petrochemical industries.

Practicals:

1. Separation and purification of BTX by fractional distillation.2. Test of viscosity index of lubricating oil.3. Test of pour point of oil.4. API gravity test of oil.5. Lovibond color test of oil.6. Determination of Zn content of oil.7. Sulfated ash test of oil.8. Determination of ash content of oil. 9. Acidity test of oil.

Recommended Books:

1. Waddams A. L. “Chemicals from Petroleum”. John Murrcy, 2004.2. Stack, A. V. & James, G.R. Ammonia Mercel Dekker Inc. 2000.3. Samuel Strelzoff, “Technology and manufacture of ammonia”, 2000. 4. Kirk- Othmer “Encyclopedia Chemical Technology” Wiley-Interscience Publishers, 2004.5. R.M. Mortier, “Chemistry and Technology of lubricants 2006.6. Theo Mang and Wilfried Dresel, “Lubricants and Lubrication 2001.7. Sunggyu Lee., “Methane and its Derivatives”, 2004.8. Robert A. Mayers, “Hand Book of petroleum refining processes”, 3rd ed., 2000.

Course No. 614Pharmaceutical Industries – II

2+1 Credit Hours

TABLETS: Classification of tablets, Raw materials for tablet, Methods for production (wet & Dry process), Coating process, Defects of tablet (chipping, cracking etc). Quality control tests.

CAPSULES: Introduction of capsules, Classification of capsules, Raw material of capsule, Manufacturing, Quality control, tests of capsule.

SYRUPS: Introduction of syrups, Types of syrups, Manufacturing of syrup, Quality control tests of syrups, Suspension.

OINTMENTS: Definition, Types of ointments, Ingredients, Manufacturing, Different equipment for filling Ointment, Quality Control test.

INJECTION: Types of injection, Raw materials of injection, Filling of Ampoule, Types of defects after filling, Quality control tests.

STERILIZATION: Introduction, Conditions for sterilization, Methods of sterilization, Factors affecting sterilization.

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QUALITY CONTROL: Different section of Q.C. Instrument use in Q.C Lab, Quality Assurance, Quality Management Validation, GMP (Good Manufacturing Practice).

ENVIRONMENTAL IMPACT OF PHARMACEUTICAL INDUSTRY: Environment Health & Safety, Pharmaceutical Environmental pollution.

Practicals:

1. Note the disintegration time & dissolution time of different tablet and then analyze it.2. Note the disintegration time & dissolution time of different capsule and then analyze it.3. Determination of Ascorbic acid in given tablet.4. Determination of sugar content in syrup (Qualitative & Quantitative).5. Determination of calcium by titrating against potassium permanganate in given tablet.6. Determination of salt content in ORS & tablet.7. Determination of Iron content in tablet using atomic absorption spectroscopy.

Recommended Books:

1. William & Grisuwold. J.B Lippin “A Text Book of Pharmaceutical and Medicinal Chemistry Cot 7 th

edition 2000.2. Alfred Burger “Medicinal Chemistry” Vol I & II Wiley enter. Science 2006.3. Kirk- Othmer “Encyclopedia Chemical Technology” Wiley-Interscience Publishers, 2004.4. Goodman & Gilman, “The Pharmaceutical basis of therapenlx”, Macmiltan publishing 7th edition 2002.5. Dispensing of medication by Hoover Mac Publishing 2006.6. Austin G Shreves “Chemical Process industries” Mc Graw Hill 6th edition 2001.

Course No. 616Polymer Physics2+1 Credit Hours

RHEOLOGY OF COMPLEX FLUIDS: Rheological Principals: Classifications of fluids behavior Viscoelasticity, Linear viscoelasticity, viscoelastic models, relaxation spectrum, methods of measurement, (static and dynamic methods), time-temperature superposition. Introduction to Non-linear Viscoelasticity: Nonlinear phenomena, simple non-linear rheological models. Rheometry: Viscometers and rheometers.

POLYMER STRUCTURE-PROPERTY RELATIONSHIPS: Polymer properties affected by their chemical composition and molecular architecture. Polymer Structures/Morphology: Morphology-processing-property relationships (e.g. injection, blow molding, rotational molding etc.), deformation mechanisms and orientation, study of spherulites; thermodynamics and kinetic forces affecting polymer crystallization, physical techniques for studying crystal structure and morphology of polymers.

Effect of Orientation and Crystallinity on Polymer Properties: Orientation in polymers (shear and tensile deformations).

Molecular and structural requirements of polymers for formation of films, fibers and multiphase systems.

POLYMER CHARACTERIZATION: Introduction and significance of polymer characterisation for property determination. Molecular weight determination: Gel permeation chromatography (GPC), light scattering and viscometry. Thermal Characterization: Differential scanning calorimetry (DSC),

42

thermogravimetric analysis (TGA), dynamic mechanical thermal analysis (DMTA). Microscopy: Optical and electron microscopy, X-ray Diffraction: Wide angle and small angle X-ray diffraction.

Practical:

1. Falling cylinder and falling ball viscometry to establish terminal velocity in Newtonian and viscoelastic fluids.

2. Concentric cylinder rheometry to establish relationship between shear stress and torque and shear rate and angular velocity for a viscoelastic fluid.

3. Measurement of normal stress and effects on secondary flow instabilities for a polymeric fluid in couettee geometry.

4. Measurement of wall shear stress in a capillary rheometer and estimation of apparent viscosity. 5. Wall slip and melt fracture in capillary flow with capillaries of similar length to radius ratios but different

radii.6. Measurement of normal streSses and exit pressure in a slit rheometer and estimation of pressure

pofile.7. Planar elongation flow of polyethylenes of varying levels of branching at constant flow rate in a slit die.

Recommended Books:

1. Non-Newtonian Flow and Applied Rheology, 2nd Ed., Chhabra R.P. and Richardson J.F.; Butterworth-Heinemann, 2008

2. Viscoelastic Properties of Polymers, 41st Ed., Ferry J.D., Isha Books, 2013 3. Introduction to Polymer Viscoelasticity, 1st Ed., Shaw M.T., Wiley, 2013 4. Applied Polymer Rheology, Kontopoulou M., Wiley, 2012

5. Bird R. B, Amstrong R., C, Hassager O, “Dynamics of Polymeric Liquids” Vol I & 2, McGraw Hill, New York, 1999.

6. Rheology: Principles, Measurements and Applications, Macosko C.W.; Wiley-VCH, 19947. Properties of Polymers: their correlations with chemical structure: their numerical estimation and

prediction from additive group contributions, 4th Ed., van Krevelen D.W., te Nijenhuis K., Elsevier, 2009

8. Crystallization of Polymers: Volume 1, Equilibrium Concepts, 2nd Ed., Mandelkern L., Cambridge University Press, 2011

9. Crystallization of Polymers: Volume 2, Kinetics and Mechanisms, 2nd Ed., Mandelkern L., Cambridge University Press, 2012

10. Characterization and Analysis of Polymers, Seidel A., Wiley, 2008.

11. Thermal Analysis of Polymers: Fundamentals and Applications, Menczel J.D. Prime R.B., Wiley, 2009

12. Electron Microscopy of Polymers, Michler G.H., Springer, 2008.

13. Polymer Synthesis and Characterization: A laboratory manual, Sandler S.R., Karo W. Bonesteel J-A, Pearce A.M., Academic Press, 1998.

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Course No. 618Textile Processing – II (Finishing & Quality Assurance)

2+1 Credit Hours

FINISHING: Advances in mechanical & chemical finishing.

SURFACTANTS: Preparation and end uses as softeners, detergents, emulsifiers and other auxiliaries of textile processing.

ENVIRONMENTAL & QUALITY MANAGEMENT SYSTEMS: Quality Assurance, Twenty Elements of ISO 9000 & Introduction to ISO 14000.

ECO LABELING: Textile products classification, Oeko-tex Standard 100.

SOCIAL ACCOUNTABILITY: Introduction to social accountability, Preventions from discriminations, SA-8000 standards.

Practicals:

1. Surfactant synthesis2. Surfactant characterization3. Synthesis of various emulsion polymers.4. Quality assurance.

Recommended Books:

1. Tyron L., Vigo Elsewer Amestradem, “Textile Processing and Properties”, 2006.2. Kenneth J. Lissant. Merceldecker, “Emulsion and Emulsion and Emulsion Technology”, 2005.3. Bernard J Nebel, “Environmental Science-The way the world works”, 2002.4. Gerard Kiely, “Environmental Engineering” 2007.

Course No. 620Food Science & Technology – II (Food Engineering)

2+1 Credit Hours

FOOD PACKAGING:(a) Packaging types, packaging applications, properties and types of plastics used in various food

industries, packaging films, metal foils, Edible films and coatings.(b) Characteristics, advantages, disadvantages and defects of metal, plastic and Glass container.

BEVERAGES: Carbonated and non carbonated drinks. Classification, compositions and processing.

DRYING AND EVAPORATION: Objectives of drying, factors effecting heat and Mass transfer, types of dryers, freeze drying, Industrial freeze dryer, objectives of evaporation, construction and working of evaporators.

FERMENTER DESIGNING: Types of fermenter, energy balance, Material of construction, stirrer glands and bearings, valves, sensor probes and sampling device.

RHEOLOGY OF FOOD: Introduction, Rheological properties of various Food material.

UTILIZATION OF VARIOUS AGRICULTURAL AND FOOD INDUSTRIES WASTES.

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Practicals:

1. Preparation of Food Product by freeze drying.2. Exaction and determination of amino acid (meat protein)3. Determination of saccharin and benzoic acid in soft drink.4. Identification and properties of various types of packaging materials.5. Drying of various Food products.

Recommended Books:

1. J.M.Coulson, “Chemical Enginering”, Vol-I , 2001.2. Animal by products, Mann, Food & agricultural Organization of the United Nation, Italy, 2004.3. James M “Modern Food Microbiology”, 2006.4. Henry e. Vogel, Celeste. C. Todano., Hand Book of Fermentation and Biochemical Engineering,

Principles, Process Design and Equipment 2006. 5. Wilmer. A. Jenkins., Packaging Foods with Plastics 2000.6. T.N. Morris., Principles of Food Preservation 3rd revised ed., 2004.7. Vass. Oreo Poulous, Win Fried Russ., Utilization of by products and treatment of waste in Food

Industry 2007.

Course No. 622Metallurgy and Materials Technology - II

2+1 Credit Hours

X – RAY DIFFRACTION: Principles of X-ray diffraction. Single crystal and powder methods, Interperetation of diffraction data.

PHASE DIAGRAM & APPLICATION: Crystal structure, solid solutions, Interstitial & substitutional solid solutions, Rules for formation of solid solutions, Binary system of alloys, complete solid soluble system, Eutectic transformations with and without terminal solid solubility, Peritectic transformation, Eutecitc transformation, Lever rule, Calculation for composition of phases, Binary system of Cu-Ni, Cu-Zn, Al-Si, Ca-Mg, Fb-Sn & Fe-C.

HEAT TREATMENT OF METALS AND ALLOYS: Annealing, spherodizing and Tempering, Isothermal & Continous cooling, Phase formation products in steel, Hardenability, Case hardening methods, Age hardening of Al alloys, Commercial practice in heat treatment of ferrous and non ferrous alloys.

STRUCTURE PROPERTY RELATION SHIP: Effect of alloy elements in steel, effect of grain size & practicle on properties.

COMPOSITE MATERIALS: Classification of composites, Polymer based Metal based. Refractory based composites, Nano Composites.

Practicals:

1. X-ray diffraction pattern of single crystal and powder specimen.2. Scanning electron microscopy.3. Transmission electron microscopy4. Continuous cooling structure Harden ability test.5. Effect of grain size and precipitate particles.6. Composite methods.

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Recommended Books:

1. Dharmendar Kumar, S. K. Jain, “Foundry Technology”, CBS Publishers, Delhi, 1994.2. L. M. Ground, “Principle of Welding Technology”, English Language Book Society, 1990.3. George E. Dieter, “Mechanical Metallurgy”, Mc Graw Hill Company, 1988.4. V. J. Colengelo, “Analysis of Metallurgical Failure”, John Willy & Sons, 1997.5. R. E. Smallman, R. J. Biship, “Metal and Materials”, Butterworth-Heinemann Inc., 1995.6. W. F. Smith, “Principle of Material Science and Engineering”, McGraw Hill, New York, 1996.

Course No. 624Industrial Training0+3 Credit Hours

INDUSTRIAL TRAINING: Every student of BS 8th Semester has to complete at least 6-8 weeks of industrial training in a particular industry as suggested by the teacher. After completing the training each students has to submit a detailed report and give a presentation in front of Faculty members.

46

Course No. 625 632 New Instrumentation & Process Control

3+1 Credit Hours

INSTRUMENTATION: Principles of measurement of temperature. Pressure level, flow, weight power, speed, position; etc. Study of common sensors, transmitters, controllers, actuators, recorders, switches, etc. Methodolgy for calibration. Fail-Safe modes of operation, alarm, trip and interlock system. Emergency shut-down systems, Fire and gad detection. Pressure relief & venting system.

CONTROL PRACTICE: Terminology signal types and standard ranges interpretation of P & 1 diagram; Servo and regulator operation. Bias and offset auto/manual optimum settings. Ziegler and Nichols formulae. Control strategy: Formulation P & 1 diagrams. Control loop elements, Block diagrams. Control objectives. Industrial Applications. Use of feedback, cascade, ratio, fee forward. Use of analyzer and chromatographs, Modeling: Lumped parameter models to plant, e.g. jacked vessel.

CONTROL THEORY: Use of Laplace transforms. Mathematical modeling of simple lumped parameter systems and their Laplace transforms. Response of First & Second order system. Study of a typical feedback control loop, open and closed loop response to simple input. Stability of a system, frequency response methods, various stability criteria Tuning of PID controllers, criteria, methodologies. Introduction to advance control system, cascade & selective control system.

Practicals:

To be based on the following:1. Study the K & J Type thermocouples.2. Study of control loops.3. Process plant training.

Recommended Books

1. Marlin, T. E. Process Control, 2nd Ed. McGraw Hill Book Co., 20002. Ogunnaike, B. A. et al., Process Dynamics, Modeling and Control Oxford University Press, 1997.3. Process Control Instrumentation Technology, Curtis D. Johnson, Person Education 2003.4. Chemical Process Control, G. Stephanupolos, Prentice Hall 2002.5. Essentials of Process Control, W. L. Luyben McGraw Hill 1997.6. Simith C. A, Corrilpio A. B., Principles and Practice of Automatic Process Control.. Iohn Wiely. 3 'd Ed.

2006

Course No. 626 633 (Optional) New--Food Product Development

3+1 Credit Hours

To provide the opportunity for students to integrate their training in food science and technology courses and related disciplines and to gain experience with the theory and practice of developing food products.

INTRODUCTION: Corporate Organization of Food Companies, Overview of Food Product Development(FPD), Product Development Process, Ideation and Screening Process, FP Marketing and Market Research, Legal and Fiscal, – Test Markets and Launches, Successes and Failure

PRODUCT DEVELOPMENT: Technical Aspects of New Product Development–Dairy, Meat, Poultry, Egg Products, Fish and Shellfish Products

47

PRODUCT DEVELOPMENT: Technical Aspects of New Product Development– Juices and Non‐alcoholic Beverages, Cereals and Grains, Fats and Oils.

PRODUCT DEVELOPMENT: Technical Aspects of New Product Development –Flavors and Flavor Companies, Sugar, Candy and Chocolate.

QUALITY ASPECTS: QC/QA Aspects of Food Product Development, Microbial Aspects of New Product Development, Package Development, Shelf Life of Packaged Foods, Nutrients and Fortification, Labeling and Pertinent Regulations.

Recommended Books

1. Brody, A.L. and Lord, J. 2008. Developing New Food Products for a Changing Marketplace, 2nd Edition. CRC Press, Boca Raton, FL.

2. Campbell‐Platt,G. 2009. Food Science and Technology. Blackwell Publishing Ltd., Oxford, UK.3. Fuller,G.W. 2011. New Food Product Development, 3rd Edition. CRC Press, Boca Raton, FL.4. Moskowitz,H., Saguy, I. S., and Straus, T. 2009. An Integrated Approach to New Food Product

Development. CRC Press, Boca Raton, FL.

Course No. 627 635 (Optional) New Water Technology

3+1 Credit Hours

WATER TECHNOLOGY (Optional for M.Sc.): Water quality parameters - BIS and WHO standards: Determination of alkalinity of water - Hardness - Estimation of hardness by EDTA method,

WATER SOFTENING: Zeolite and Demineralization (Ion - exchangers) processes, Boiler troubles and remedies, Desalination by electrodialysis and reverse osmosis, Treatment of water for domestic use.

MINERAL WATER: TECHNOLOGY: Chemical Constitutions and Microbiology, Collection, treatment and distribution of drinking water supply.

Recommended Books:

1. Handbook of Drinking Water Quality, Second Edition :John De Zuane P.E., First published: 5 December 2007

2. Water Quality, An Introduction. Boyd, Claude E. 20153. Standard Methods for the Examination of Water & Wastewater.21st Edition. A Greenberg (American

Public Health Association), 2005.

Course No. 628 636 (Optional) New Pollution Control Technologies

3+1 Credit Hours

The objective of this course is to acquaint the students with the technological approaches used for control of pollution. The students will become familiar with different technologies and modern techniques for their control and abatement.

Treatment and disposal of municipal and industrial wastewater; Low cost water treatment and sanitation techniques; Solid and hazardous waste management; Cleaner production techniques.

Waste hierarchy (Reduce, re-use and recycling); Waste site investigation and remediation; Air pollution control; Noise pollution control.

48

Recommended Books:

1. Solid Waste Technology and Management, T. Christensen, John Wiley & Sons, 2011. 2. Water Treatment Technologies, B. Salopek, Akademija tehničkih znanosti Hrvatske, 2007. 3. Advanced Air and Noise Pollution Control, L.K. Wang, N.C. Pereira and Y.T. Hung, Humana Press,

2005.4. Preventive Environmental Management, S.R. Asolekar, R. Gopichandran and Centre for Environment

Education, Foundation Books, 2005. 5. Handbook of Solid Waste Management and Waste Minimization Technologies, N.P. Cheremisinoff,

Butterworth-Heinemann, 2003. 6. Municipal solid waste management: strategies and technologies for sustainable solutions, C. Ludwig,

S. Hellweg and S. Stucki, Springer, 2003. 7. Handbook of Water and Wastewater Treatment Technologies, N.P. Cheremisinoff, Butterworth-

Heinemann, 2002. 8. Handbook of Air Pollution Prevention and Control, N.P. Cheremisinoff, Butterworth-Heinemann, 2002.9. Air Pollution Control Technology Handbook, K.B. Schnelle and C.A. Brown, CRC Press, 2002. 10. Basics of solid and hazardous waste management technology, K.L. Shah, Prentice Hall, 2000.

Course No. 628 637(Optional) New Occupational Safety, Health& Environment

3+1 Credit Hours

The course will provide information on occupational health and safety as well as it will review various types of work place hazards, their exposure and effects on the body. Focus will be on hazardous chemicals, carcinogens, effects of chemicals acute and chronic health problems related to work and safe use of chemicals at work. Awareness will also be created about the health and safety laws and enforcement, role of health and safety committees at work etc.

INTRODUCTION TO OCCUPATIONAL HEALTH AND SAFETY: Accidents, Disease, Normal working, Health and safety problems worldwide, Importance of management and training in occupational health and safety.

Common work place associated hazards; biological, chemical, mechanical, physical and psychological hazards and their effects on health and safety, local effects, systemic effects, acute and chronic effects.

Chemicals in the work place, Noise at work, Manual handling,

CONTROLLING HAZARDS: Methods of control, Elimination, Substitution, Engineering controls, Administrative controls, Personal protective equipment (PPE), Cumulative trauma disorder (CTD), Evaluation of job risk factors, Controlling vibration hazards. Male and female reproductive health hazards in the work place, Health and safety for women and children, Labour code of Pakistan.

OCCUPATIONAL HEALTH SAFETY MANAGEMENT SYSTEM: Legislation related to health and safety at work, Check list, Role of health and safety representatives and labour union at work; meetings, reports, training education, negotiation, Role of government, Health and safety committee.

Recommended Books

1. Occupational Health Hazards and Remedies. (2002). Mohapatra, R. Jaypee Brothers Medical Publishers Pvt. Ltd. India.

2. Biosafety Management: Principles and Applications. (2000). Aynor, P. L. Virginia Polytechnic Institute Publications. USA.

3. Hazardous Chemicals Handbook. (2002). 2nded. Carson, P. and Mumford, C. Butterworth Heinemann. Oxford, UK.

49

4. Basic Environmental Health. (2001). 1sted. Yassi, A., Kjellstrom, T., deKok, T. and Guidotti, T. L. Oxford University Press. NY, USA.

5. Risk assessment of chemicals: An Introduction. 2007. Leeuwen, C.J.V. Springer, USA.

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Course No. 628 638 (Optional) New (Incomplete) Process Simulation

3+1 Credit Hours

Process simulators are designed to serve many operating companies in the processing industries and many engineering companies. With such tools users can create rigorous steady state and dynamic models for plant design, performance monitoring, troubleshooting, operational improvement, business planning, and asset management. Through the process simulator’s completely interactive interface, users can easily manipulate process variables and unit operation topology, as well as fully customize their simulation using its customization and extensibility capabilities.

ASPEN HYSYS: Introduction to HYSYS, Simulation Basis Manager, Creating A New Simulation, Adding Components to the Simulation, Selecting A Fluids Package, Selecting Thermodynamics Model, Enter Simulation Environment, Adding Material Streams,

EQUATIONS OF STATE: Equations of State – Mathematical Formulations, Building the Simulation, Accessing HYSYS, Defining the Simulation Basis, Installing a Stream, Defining Necessary Stream, Saving, Preview the Result using Workbook, Analyze the Property using Case Study, Changing the Fluid Package,

COMPRESSORS, PUMPS, PIPELINE: Simulate the behavior of centrifugal compressors by using a single speed curve to calculate outlet pressure and duty consumption or by using multiple speed curves and finding the right speed to reach a desired outlet pressure. The use of centrifugal pumps will be as well explored, using them without curves for a quick duty determination or with available curves to more rigorously simulate the behavior of existing units. The contents of the module will as well help users to define the specifications for solving a pipe segment unit operation and to select the most appropriate correlation for estimating the pressure drop of a pipe line system.

HEAT TRANSFER UNIT OPERATIONS: Use Heaters and Coolers to investigate the duty needs for heating or cooling process streams. Install and converge Shell & Tube Heat Exchangers in Design mode and understand the differences between End Point and Weighted Design Methods. Use the Rating capabilities of the shell & tubes heat exchangers to simulate existing units

REACTION AND REACTORS: Problem Statement, Defining the Simulation Basis, Adding the Reactions, Adding the Reaction Sets, Making Sequential Reactions, Attaching Reaction Set to the Fluid Package, Adding a Feed Stream, Adding the Conversion Reactor, Adding an Equilibrium Reactor, adding a CSTR, Providing Binary Coefficients, Adding an Absorber, adding distillation column, Changing Trays to Packing, Getting the Design Parameters,

DISTILLATION COLUMN: The main objective is to know how the simulator deals with distillation columns: How they are installed, connected and finally, solved. Another objective is to find out how to use the simulator to find alternative operating conditions –using the same column to obtain improved product qualities. how to install columns using the Input Expert simulator wizard

LOGICAL OPERATORS: The Set mathematical operator. The Balance mathematical operator. The Adjust mathematical operator. The Recycle mathematical operator. The Spreadsheet. The Sub flow sheets.

REPORTING: Customize reports in using the Report Manager, Use XML language to create a summary of the input data from a case , Install and run an Excel utility to view data from the workbook

Practicals: ?Recommended Books:?

51

Suggestions by Aleem sb:

BEVERAGE INDUSTRIES ( already a part of Food SP but details missing.)

INTRODUCTION: Definitions and Classifications.

SOFT DRINKS: Carbonated& Non- Carbonated Beverages. Classifications; Compositions; Processing; Production; Bottling and Canning.

FRUIT JUICES: Citrus and Non-Citrus - Definitions; Classifications; Compositions; Processing; Production; Bottling and Canning.

STIMULATING BEVERAGES: Tea & Coffee - Types and Classification, Cultivation, Fresh Leaf Composition; Black Tea Manufacturing; Instant Tea Manufacturing; Biological Activity of Tea, Chemistry of

Coffee; Green Coffee Processing; Conversion of Green Coffee in to Black, De-caffeination of Coffee.

CHOCOLATE BASED DRINKS: Introduction, Agronomy, Technology, Cocoa-Based Beverages; Biological Activity; Chemistry and Microbiology of Cocoa.

Recommended Books:

1. ASHURST, P R. Chemistry and Technology of Soft Drinks and Fruit Juices Oxford Blackwell Publishing Ltd 2005 1-4051-2286-2

Suggestions by Fasiullah sb

COMPUTER AIDED DRAWING: Course No. 303 Engineering Drawing & Workshop Practice may be split into 0+2 and 0+1 portion to contain more or less the same as in course no. 303 the 0+1 portion 0+2 CAD may be introduced after the students have studied computers in 304 and 405. Alternate arrangement could be to shift the whole course to IV semester and CAD may be included.

Suggestions For Pharmaceutical Processing (?)Suggested Addition

Pharmaceutical Processing:

1. MILLING : (3 HRS)

Objectives of comminution factors affecting size reduction, processes of milling, theory of milling and energy requirements, milling rate and types of milling machines, size distribution, determination of size, microscopy, sieving and sedimentation of particles. Pharmaceutical applications of milling

2. MIXING AND HOMOGENISATION: (3 HRS)

Fluid mixing mechanisms and equipment, their classification and feasibility of selection based upon Reynolds, Froude and power numbers; Equipment for solid mixing. Study of following mixers; planetary mixer, agitator, triple roller mill, propellor mixer, Pharmaceutical applications of Mixing.

3. COMPRESSION AND CONSOLIDATION OF PHARMACEUTICAL POWERS: (5 HRS) Definition, angles of repose, Flow rate through tubes and hoppers, mass - volume – force relationship,

granules, compression and consolidation under high loads.

52

Books Recommended: 1. Martin, Physical Pharmacy, 4th Edition, B. I. Waverly Pvt. Ltd., New Delhi (1995). 2. L. Lachman, H.A. Lieberman and J. L. Kanig, Theory and Practice of Industrial Pharmacy, III Eds.

Varghese Publishing House, Bombay (1987). 3. W. Copper and G. Gunn, Dispensing Pharmacy, CBS Publishers & Distributors, Delhi.

Drug Design and Drug Development

1. THE IMPORTANCE OF BIOTECHNOLOGY FOR THE DISCOVERY OF BETTER AND SAFER DRUGS : Introduction, Production of Human Proteins, the First Generation of New Drugs from Recombinant DNA, Natrual Proteins, as leads for structurally modified proteins: The Second Generation of Products from Biotechnology, Examination of the Structure and Function of Proteins as Tools for the Evaluation of Pathological Processes: The Third Generation of Products from Biotechnology. (8Hrs)

2. DESIGNS OF ENZYME INHIBITOR : Mechanism of enzymatic catalysis. Transition state analogs as

enzyme inhibitors. Kinetics of irreversible enzyme inhibition. Design of Reversible and irreversible enzyme inhibitors with following examples: chymotypsin. Subtilison, Elastase. Pepsin. Cholinerterase, Deraminases. Carboxypeptidase. Glutamin synthetase, Trisophosphate isomerase, Aldolase, Enolase, Decarboxylases, Lysozyme and other glycosyl transferring enzymes. Creatine Kinase, adenylate kinases. Asparatate trancarbamolyase. Natural products as enzyme inhibitors. Penicillin, Cephalsporin, Leupeptin. Nojrimycin, Pentastatin, Captopril, Sulphonamids. (8 Hrs)

3. COMPUTER AIDED DRUG DESIGNING : Computer requirement hardware, software, Data base and information retrieval techniques. Graphical description of chemical structure. Molecular interactions and interactive graphics. Modelling in medicinal chemistry-uses and limitations. Logico structural approaches. Activity feature selection within a group of compounds, Activity profile selection. Topological and topographical descriptors. (10 Hrs)

4. SEARCH FOR BETTER AND SAFTER DRUGS: Impact of External Factors- The Social, Financial, and Working Environment: Drug Therapy and Pubic Opinion, Drug Research and Financial Constraints, Working Climate for Innovative Drug Research. (4 Hrs)

Recommended Books:

1. The Organic Chemistry of Drug Design and Drug Action, by R. B. Silverman, Academic Press, 1992. 2. Drug Designs - A Series of Monographs in Medicinal Chemistry Edited by A. J. Ariens. Ist edition, Vol.

I, II, V, VIII & IX (only relevant chapters).3. Comprehensive Medicinal Chemistry. Peragmon Press. 1990, Vol. 4. 4. Modern Drug Research , Paths to Better and Safer Drugs, Medicinal Research Series, Volume 12,

Edited by Yvonne Connolly Martin Eberhard Kutter Vokhard Austel.

53

SYLLABUS FORM.S. PROGRAM

Department of Applied Chemistry and Chemical TechnologyFaculty of Science

University of Karachi

54

ADVANCE ANALYTICAL CHEMISTRYCourse No. ACH-701

(3+0 Cr. Hrs)Gravimetric Analysis:

Scope of gravimetric analysis, combustion analysis, precipitation process, Thermal gravimetric analysis.

Polarimetry:

Optical Rotatory Dispersion and circular Dichroism.

Spectroscopy:

UV and Visible spectroscopy, flame spectroscopy, Atomic Absorption and emission spectroscopy, IR spectroscopy, Electron and ion spectroscopy.

Separation Techniques:

Precipitation

Solvent extraction

Ion exchange separation.

Chromatographic Methods:

HPLC, selecting the mode of separation

Gas chromatography, column, detectors, analytical methods

Books:

1. Kenner, C. T. “Quantitative Analysis”, McMillan Publishing Co., Inc. New York, 2002.

2. Hargis, G. L. “Analytical Chemistry”, Prentice – Hall, Inc, New Jersey, 2004.

3. Fritz J. S., George H. Schenks; “Quantitative Analytical Chemistry”, Fourth Ed., Allyn and Bacon Inc. Bostan, 2000.

4. Day R. A., “Quantitative Analysis”, Prentice-Hall Inter. Ed., 2005.

5. Dong. W. M. “Modern HPLC” A. John Wiley & Sons inc. 2006.

55

ASR-701: Research Methodology ICredit Hours 3+0

Module I

Philosophy of Science: The nature of scientific inquiry

Positivism and the scientific method Positivistic and post-positivistic philosophies of science

Positivistic and post-positivistic research in practice Empiricism and Reductionism

Phenomenological Approach

Literature Review: Sources Primary sources

Secondary sources Objectivity

Objectivity versus subjectivity Delimiting the research problem Seeking the new approaches Avoiding sterile approaches Insight into methods Futurereconunendations

Inventory of Questions Four types of questions

Research Objectives . Identification and specification

Research Approach Inductive and deductive approaches

Technological and simulation approaches

Research Hypotheses \ Real hypothesis I, Use of hypothesis .

Writing and formalizing a hypothesis

Types of Research Methods Experimental Correlation

Natural Observational Survey

Case study

Research Phases Targets

Time-frames and Deadlines

56

Module II

Designing an Investigation: Choice

Aim Conduct

Qualitative and quantitative approach: Internal and external validity Naturalistic and ethnographic perspectives

Exploratory data analysis and interpretation

Design of Experiment: Experiment and size of experiment

Variables and concomitant variables Treatments: cause and effect

Factor and levels Experimental unit Sampling unit Replication Randomization Blocking Degrees of freedom

Identification of Available Technologies and Expertise

Research Proposal Components Research Economics Research budgeting

Significance of research objectives

Reading i

\ I

l. Klee, R. 1997. Introduction to the Philosophy of Science: Cutting Nature at Its Seams.OUP.

2. Creswell, D. J. W. 2003. Research Design: Qualitative, Quantitative and Mixed Method Approaches.

3. Gliner, J. A. and G. A. Morgan. 2000. Research Methods in Applied Settings: An Integrated Approach to Design and Analysis

4. Moustakas, C. 1994. Phenomenological Research Methods. Sage. 5. Newman I. and C.R. Benz. 1998. Qualitative-Quantitative Research

Methodology: Exploring the Interactive Continuum. Southern lllinois University Press.

6. New, C.C. and J. A. Owick. 2003. How to Write a Grant Proposal. Wiley. 7. Bums, R. B. 2000. Introduction to Research Methods. Sage. 8. Hart, C. 1999. Doing a Literature Review. Sage

57

ASRP-702 Research Methodology II Module III

Scientific Record Keeping: Lab notebook

Duplicate record Date

Ownership of Data: Institutional property

Personal rights Patenting

Intellectual property rights Handling of Research Material:

Placement and storage Utilization

DisposalPublic Safety:

Institutional policies Law

Laboratory Safety: Health, safety and environmental affairs Potential hazards Risks Accidents Remedies Laboratory design Gadgets

Environment Conservation: Management of laboratory environment parameters

Humidity Temperature Air quality Illumination Noise

Research Ethics: Informed consent

Confidentiality Deception

De-hoaxing and desensitization Efficient Use of Computers and Internet:

Search engines Digital libraries Archives

58

Module IV

Communication of Science Oral Technical presentation

Keynote address Invited lecture Popular lecture

Written Language, diction and contemporary style

Data presentation and documentation Research Misconduct

Fraudulent research Plagiarism

Retraction and cleansing Legal burdens

Scientific Integrity Precision Reporting Credits Authorship Mentoring

Critical evaluation of research Quality Originality Bias and Distortion

Non-deliberate bias Sampling bias

Publication Paper, audience and journal

Basic structure of research paper Scientific paper

Short communication Notes

Case report Review and case series analysis

Editorial Book review Letter to editor

59

ENGINEERING MATERIALSCourse No. ACH-703

(3+0 Cr. Hrs)

Introduction to Engineering Materials:

Materials for 21st Century, Comparison of Conventional and Emerging Engineering Materials.

Composites:

Composite Materials & Nano Composites.

Engineering Materials Examples:

Polymer based, metal based, photo sensitive materials, ceramic based, properties, uses and economics.

Conductors:

Semi-conductors and super conducting materials.

Books:

1. Kenneth G. Budinski K., “Engineering Materials”, Prentice Hall Publisher 1998.2. Willaium D. Callister “Material Science and Engineering” Wiley John & Sons, Inc. 1999.3. R.E. Smallman, R.J. Bishop, Butterworth-Heincmann, “Modern Physical Metallurgy and Materials Engineering”

2000.

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TECHNICAL TEXTILES

Course No. ACH-705

(3+0 Cr. Hrs)

Introduction to Technical Textile:

Agrotech (Agro-Textiles), Buildtech (Construction Textiles), Clothtech (Clothing Textiles), Geotech (Geo-Textiles), Hometch (Domestic Textiles), Indutech (Industrial Textiles), Medtech (Medical Textiles), Mobiltech (Textiles used in Automobiles, Train and Air Planes), Oekotech or Ecotech (Environmentally – friendly textiles), Packtech (Packaging Textiles), Protech (Protective Textiles), Sporttech (Sports Textiles).

Synthesis:

Oxidative synthesis of Polyanalines in particular the sulphonic and caboaxylic acid derivatives. Solubility and dispersion formation.

Characterization:

Various analytical techniques UV, IR, FAB, MS, NMR and ESR studies to elucidate the structure of polyanalines. Conductometric studies, Thermal Analysis DSC TGA, Dynamic mechanical studies, Gel permeation chromatography MALDI studies SEM TEM. Studies.

Applications:

Conductive fibers, Dispersion and coatings, Sensors, Drug release system, Hydrogells, Micro encapsulation

Books:

1. D. Braun, H. Chedron, M. Rhahn. H. Ritter Springers Berlin “Polymer synthesis Theory and practice”. 2005.

2. Bio Medical Polymers. Mike Jenkins woodhead, publishing Ltd. Cambridge 2007.

3. Horrocks AR and Annand SC “Handbook of Technical textiles” woodhead, publishing Ltd. Cambridge 2004.

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PRODUCTION CONTROL, PROJECT PLANNING & RISK ASSESSMENT Course No. ACH-702

3+0 Credit HoursProduction Control:

Introduction to production planning, Gantt / Bar Chart, Master Scheduling, Plant & Process Layout.

Inventory Control:

Inventory of Chemical Goods, Inventory system, Inventory cost, Economic Order Quantity.

Project Planning:

Work breakdown structure, detail schedules & charts, CPM/PERT, Resource planning

Risk Assessment:

Major Hazards, Basic Concepts of Risks, what if analysis, Hazop.

Books:

1. Fullwood R. R., “Pobabilistic Safety assessment in Chemical and Nuclear Industries”. 1999.2. Richard J. Tensine “Production / Operations Management: Concepts Structure and Analysis” 2003.3. Herold Kerzner, “Project Management: A Systems Approach to Planning, Scheduling and Controlling”, Ninth

Edition, John Wiley & Sons 2006.4. Jay Heizer and Bary Render, “Operations Management”, Fifth Edition, Prentice Hall, 2000.5. Paul Loombo, “Management-A Quantitative perspective, Mc Millan Bublishing, 1998.

SUPPLY CHAIN PLANNINGCourse No. ACH-704

(3+0 Cr. Hrs)Introduction to supply chain.

What is supply chain, What is supply chain planning.

The elements and principles of supply chain planning.

Elements, Demand management, Inventory Management, Production and distribution planning, Principles.

Process industry supply chain benchmarks.

Benefits of modeling approach to supply chain management.

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Demand management.

Order driven, Forecast-Driven, Forecasting, Smoothing methods, Moving averages, Weighted moving averages, Exponential smoothing, Time series decomposition, Trend and cyclical factor.

Inventory management

Finished goods inventory management, Setting safety stock levels, Estimating forwared demands on the plant,

Production and distribution planning.

Planning models for production and distribution, Time discretisation, Degrees of freedom, Resource constraints and availability.

Books:

1. Anderson, D. L., F. E. Britt and D. J. Favre, “The seven principles of supply chain management”, Supply Chain Management Review, www.manufacturing.net/scl/scmr/sevenprinc.htm

2. Arntzen, B. C., G. G. Brown, T. P. Harrison and L. L. Trafton, “Global Supply Chain Management at Digital Equipment Corporation”, Interfaces, 25, 69-93 (1997).

3. Ahmad, M. M. and R. Benson, “Benchmarking in the Process Industries”, IChemE, Rugby (1999).

4. Child, P., R. Diedericks, F. H. Sanders and S. Wisniowski, “The Management of Complexity”, Sloane Management Review, Fall, 73-91 (1991).

5. Davis, T., “Effective Supply Chain Management”, Sloane Management Review, Summer, 35-46 (1993).

6. Evans, G. N., D. R. Towill and M. M. Naim, “Business Process Re-Engineering the Supply Chain”, J. Production Planning and Control, 6, 38-42 (1995).

7. Lewis, C. D., “Scientific Inventory Control”, Elsevier (1970).

8. Makridakis, S. and S. C. Wheelwright, “Forecasting methods for management”, Wiley 1989.

9. Schmidt, J. D., “Achieving the Elusive Integrated Supply Chain”, Proc 2nd Ind. Eng. Res. Conf., 138-141 (1993).

10. Towill, D. R., M. M. Naim and J. Wikner, “Industrial Dynamics Simulation Models in the Design of Supply Chains”, Int J. Phys. Dist. And Logs. Mgt., 22, 3-13 (1992).

11. Vidal, C. J. and M. Goetschalckx, “Strategic Production-Distribution Models”, EJOR, 98, 1-18 (1997).

12. Wikner, J., D. R. Towil l and M. M. Naim, “Smoothing Supply Chain Dynamics”, Int. J. Prod. Econ., 22, 231-248 (1991).

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CHEMICAL ENGINEERING

(PROCESS MODELING, SIMULATION & CONTROL)

Course No. ACH-706

(3+0 Cr. Hrs)

Fundamentals Of Process Control:

Principles & Instrumentation for measurement of temperature, pressure, mass, level, flow, power, speed position etc.

Chemical System Modeling:

Mass transfer operation processes modeling. Fluid mechanics process modeling.

The Laplace Transform:

Definition of the transform, Transform of simple functions, Transform of derivatives, Solution of differential equations, Transform of an integral.

Optimization:

Optimization methods, Numerical techniques for single and multi variable function linear programming.

Simulation:

Introduction to simulation, Coding of simulation software, currently used simulation packages.

Books:

1. J. Inghan, J. Dunn, “Chemical Engineering Dynamics An Introduction to Modeling and Computer Simulation” Willey 2nd ed., 2000.

2. B.V. Babu, “Process Plant Simulation”, Oxford University Press India 2004.3. W.L. Luyben, “Essential of Process Control”, McGraw Hill 1997.4. Edgar T.F. Himmelblau D.M., “Optimization of Chemical Processes”, McGraw Hill 1989.5. User & Tutorial Guides for MSExcel, HYSIS.

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SYLLABUS FOR

Ph.D PROGRAM

Department of Applied Chemistry and Chemical Technology

University of Karachi

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Course Title: Research Seminars

Course No. ACH-801

Credit Hrs. (4+0)

Content:

Each student will be required to deliver two seminars on the topic of his / her research work. One seminar must be presented before completion of first year as proposal defense. Second presentation should be conducted before submission of the thesis as pre-viva. Three senior most members of the Departmental Research Committee (DRC) will evaluate the students. The research supervisor will also be the course In-charge and shall be responsible for final evaluation of the students on basis of DRC recommendations, awarding them grade (A, B or C).

Course Title: Colloquiums on Current Advances in the Discipline

Course No. ACH-802

Credit Hrs. (4+0)

Content:

Each student will be required to give three presentation on current advances in his/her discipline for least of 1 hour duration. Each presentation will be conducted during the second, third and fourth semester of the program. A Course In-charge will be appointed at the beginning of the semester and three senior most members of the Departmental Research Committee will evaluate the students and award them grades A, B or C. The Course In-charge and Research Supervisor shall be responsible for evaluation the students, awarding them grade (A, B or C). The course incharge will submit the result at the end of the semester.

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Course Title: Technical writing Skills in ResearchCourse No. ACH-803

Credit Hrs. (4+0)Content:

Each Ph.D. student will be required to develop the thesis and manuscript writing skills in consultation with the Research Supervisor. The Supervisor may arrange lectures on the above skills. The research supervisor will be the Course Incharge and shall be responsible for evaluating the students, awarding them grades A, B or C and submitting the result at the end of the fourth semester.

Course Title: Development of Research Proposal for Funding Agencies

Course No. ACH-804

Credit Hrs. (6+0)

Content:

Ph.D. students will be required to develop the skills of writing research proposal for national and/ or international funding agency, in consultation with their supervisor. The research supervisor will be the course in-charge and shall be responsible for evaluating the students, awarding them grades A, B or C and submitting the result at the end of fourth semester.

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