0

... To: Ed TQlor, EPA Lib Datt: Slptollbtr 10, 1984

fi'CII: Rob Pal.,.., COM, Inc, ~ Coptea: Dr, R, Hug~to Sub,Jeet: It-solve otte, Clot tz330 Data

Vthdatton RIIIIOrt

All orgentc -lroh waa perf....., b1 llttd ~Chela of Rtsearc~ Trtantlt Park, ltortll Clroltnt, undtr contract - 68-01·67&2 on Januar1 17t~ ~rough Fobrlllr1 t4t~, 1984, 1-gantc -lroh was perf...... b1 vorsar, Jne, of Sprtngfttld, 9frgtnta undor contract .-r 18-01-lnl on olanutr1 Z1at llld Fllbr111r1 1~, 1184,

~~·:~:m.=~~m;d:zt~!: ;:"~~~"an:tr-~·:.:~ !:'~a!',, For orgentc Malroto, 18 ._,-, ...,.. aoa11ztd for tn "" -t-voltttle

:~!!Y:~;.,~ t~~~~-~~!!:1:!:~io~J~o!\':.pe%t~:~ :;t;r"J,:\':,for wore tttan and are ltottd tn Ttblt 1,

~i;~1.::!~t=~ltd~t:,:o.:t,;~:..=:.:~t~nd~a::1:·~~blt z. Ftvt eooaplttt data paekaQtO/boxts -• revt- ..,tc~ eontatntd all per­tt- tnf-tton -•••ar1 to c-et an eeeorato ••••-· Tilt fol­lowing .-ks are 1 result of ~to rovtow:

(1) Surrogate sptkt recowortts for actds wort p- and rangtd fi'CII provhtonal (P) to 11111ccoptablt (U), Alto, - aetd data - ott rt~~orttd duo to utrh tffKto. Thoro .,.ars to bt a ..tria tnttr• ftrtnet tn the ...t.volettlt Malroh for -t ll"'llto. Low to - ­

:::•=.:::t~~r;r.~t~:~·~a~"!.~a~f:!td,.:".!r:tl:::";rdsurrogate reeowertH wM~ tM laboratGrJ ~.. attrtbuttd to ..tr ;, tn­terftrtl'ltti . aeftr to 'Vtrsar, Part 1. Cllt ~r.r Mlrrath•• IK·tt011 A,

(2) Ill tile peottctdt freetton PCI-1254 at 1100 ut/kO and liD IIQ/kg, N· opaettvtlJ, wore tdtnttfttd tn -1• 11211 and l1SS1 wM~ wll a fttld bltnk.

(S) Sl"'llt 1210 wt1 ,.. to eonJundton wtt~ a eontutnattd 1/K blank (atlt~r..-). Ito tnttrftNn.. wtth tM -lt rtllllt wu t¥t-.

(4) 1tot all of tile TCID fraettons _, rwn, Tht proatnct of PCII to tddt­tton to lltgll 1t¥th of voltttlt _..., and polpucltlr arGIItttu eontrtbuttd to llltrh tnttrftrtneH wtt~ TCID dtto..tnottono , and u 1Udl

1 f'K0¥1rt .. lf'l ftoted II •tftHt.,.1URt• •

-(I) High lovell In s'"'o postlcldt fractions roqulrtd dilutions; tlli,.fore,

surrogate reco•tr1 dote Is not co.pltte or ovolloblt for 1 I of tbls fraction. .

(6) On two soporett occoslons conta•lnonts wor.- presont 1,; II~ blonts ,.t there oppoartd to bt no lnttrforonct with 1111plt1 run with thtso bltnks. ·

(7) Saooplt lltl092 wos oot found either this 11111111 WI not 1'1111 or wo 'ust did not recelu. tM liiorglftlc report lot for ltJL .

(ll_ Splkt 11111110 re11ltr tnd ..IICJtt 111111110 retults fot Tnt I Mtth

..... IlK ""' .. QC ..,.rt "'· (t) ,......t recovorln fot s- Tilt I iftd l Mtoh ..,.. oot gl,..,

Tobit ) contJins 1 ro..-.ndttlon .....I'J fot tills ctlt. ,.,. tM ooat portIt oppoors thlt tlli Oftf'lll .,.11t1 cootrol reports woro toOd fot both ltboretorln with tM oxcoptloos u lodlcottd U.We.

If at this tiM 1011 hlvo on1 tddltonol ,..ntlons relltlvt to this ..,.rtlot pltast cootKt • ot Dr. Richerd ~Mo of this offlco.

"' •• c........

,..... TABLE 1

CME 12330 Suoplt s-rJ ..,. '=" lorf Of ,, 'j""l!7 I!e1e 24 Mlts61 • M19584

" ~ . mt7Stell-· ~.m ... - .. um. mn *24 ...a93 • Ml9096SalrfiCt lllttr ~ .

IUH7 • 41271 MltsH • MIH39 11321 . 41336 Mlts41 • MIM43

-*"· "'""'· Mt9540,

llon1tor1tt llolh 18 R!2150·RI2Y . ....,,11 _,313 • MIUII 11318 • ll327 M19090, 11212, ann, 11338 MIH21 • 1119U4

MIMGe • Mltlll Ml9125, MIOM!, ....... MIM49

M19H2 • M19SIIRts1dtftt111 IIllis .l. U240 • 4!2M .1 TOTAL I 74 n

:)

• 1 M19092 VII lost or -.- 1• sM..-ot·

.·

fl) PIC'IIt'" Lib Blanks

Field ll..kl •·

Da(a C.lataoiu

Spectral Parf~~Nt~~ee

SUI'f'OIIta S,lkH

llotrlaJPikH

Lob DupliUtH

Field Dupllutes

lilT£:

TABLE Z

DATA REYIEII PMAIETUS

-· I

· I

A l.rlal 1 Dltl Yolldatlon Wll -rtok.., bind upoo nohotloo of \lie

ollllt ,.,._,.. listed -·

I I I I

Ji~ !rr'llr

1fl

f II I

---

• • • • • • • • • • • • • • • • • • • • • • • •

• • • •

I I I I

'"lrl1 ; :~!\;.~- 1

l,a- ;1TABLE S

') CASE 12330 RECOIIIEDTIONS ~~ril

!Ilk l !!lkl ill. 2 (tiftI!!!I! 11!.1!!1 I !!!! ~l! ! rt!S 1!!!2!1 !

Sedi-U

J

RHidentlll 111111

R1273 AI M A A ·' 1«9561 A A A I Rl274 A M A A 1«9562 A A A ams M M A A M19563 A A A RU76 ,. M A A 1«9564 A A A aun A M A A M19565 A A A §RU71 A M A A 1«9566 A A A RU71 ' A M A A I«K67 A A A ~illRl279 a· M A A I«H68 A...,. A A RUIO M A M 1«9161 A A A "'' Rl281 A A A A 1«9S70 A A A auez AI 1«9S71 A A A ~~• 1«9572 A A ~-~1281 AI A •1«9573 A A A Rl285 A Rl214 AI A

1«9571 A A A RU86 M M 1«9175 A A Rl217 M

..• •••• •1«9176 A A

Rlntl M A 1«9577 A um M :~

••A • 1«9178 •A RUIO M A 1«9579 A Rl211 M M A 1«9580 A A •1«9181 ARlt92 M •1«9181 A RIU2 M Rlt92 M

1«9181 RIZft AI M 1«9181 A A RIZIZ AI 1«9581 A RIZ92 AI 1«9581 A A•= •

•••••••

•••••• RIZ40 · a A -sz A A Rl241 A M A 1«9553 A A A RU42 A A 1«9154 A A A

•••A 1«9555 A ARIZU A A •1«9556 A A ARUM A A • 1«1557 A A ARU45 A A RU46 A

•••• :· 1«9558 A AA A •

dn.

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R· •u

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i

I!·~J IJhJ . ·~l!-.11ll!t I I I I

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'tiOI ... uotf tldloo$ •

y y y liCit~

y y lt06111 y y y 0101111

y y y LUll y y y noAI ' y y y ICIII y y ' ' ' ,y ,y Kill cU06111

tt06111 Ztltl' " ' w w ' , lUll' ' 9t06111 y , ouny' 6(06111 y' 'y ' ft06111 ' ' y ' •nn y' ' ' Lt06111 ' ' .. lUll' y y ' ft06111 ' •w y ,y IIIII' ' y ' w ttl!I' ' K04illl w w (till' ' K- ' ' w y mn' ' y ' ' ' w 'y tNtI ...,.,. ,,.,..,

~(06111 "­' ' '

' !(- ' ., . ' y ' ONtl' ' ' ' 6Nll1)(06111 ' ' ' w

· y INti9106111 ' ' ' ' w ' y ' LIZIIN06111 '' ' ' L~06111 W. tiZII·'' ' ' ' ' W • ,SSZII9106111 ' ' ' ' ' ' ttJU' ' ' ' ' ' y OLZII

61211' ' ' t606111 ' ' •' ' ' ' ' == ' ' INti(606111 ' ' ' . ' w ' ' ' ' mu' ' ' ' ' ' ' ' ' ~ ' ' Ali ' .' ,.,.. illliili lh~ I ijiil 1 ijiil i llWI sna

(P,tU~) ( 311Vl .. c .

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• • •

.. ...... TAIL£ 3 (Cont'd)..,,, ¥06 "" ,.,,, Ink\""""''

llonltarlnt 111111

)

•• 1119090 AR1318 A M A A M A IIIUU ARntt A M

A lllt314 AIUZO A M A M A lllt3U AIf' Mmn, A M A A llltt316 A

IUU ' A M M A liltIOU A IUZ4 A· M M A -21 A

AM A A lllt5U 11326 A M· Mann A

A lllt5U A U327 A A A A lllt5Z4 A IIHO A A A liltIll' •llltt50t AlltZJI M A

lllt510IIZN A A A A •A A llltt511 AUUJ A•llZM A A A A -25 A A llltt54Z Aan» A A A

lllt545 A, M Auna A ..,54,11272 A M A A"'

A • Ottt l<ttPtoblt II Is,

Till£ I

A A A A A A A A A A A A•A A A A A

''" J A A A A A A A A A A A A A A A A A A

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Jrll ...·r•!IL

'ir'f•r11• t I I

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d .5n.

Al A<<tPttd """" but roJo<t -·N •• Atceptlll ovoro11 •lit rtJt<t _._,,_ tMOI'Idt, lls(Z-t:tlle1~1 l plltlollttt. AI • A<<IIPttd -•11 but rtJo<t CS.. M • Surrotote 19lkt rocovorlu ootlldt of OC ll•lts • NJttttd. AI • llltfll 19lkt d""lltiU .......,., OUUidt of 0C llllltl • rt,lttttd. /IIJ • tont•lnoted •link.

• Bot onoi,Jiod for tMs frtttloo.

• S..,lo ttOtZ ••• lost.