915-21 UST Site Assessment Report
Transcript of 915-21 UST Site Assessment Report
UST SYSTEM REMOVAL OSFM SITE ASSESSMENT REPORT
UST SYSTEM REMOVAL
OSFM SITE ASSESSMENT REPORT COMMUNITY CONSOLIDATED SCHOOL DISTRICT 181
THE LANE ELEMENTARY SCHOOL 500 NORTH ELM STREET
HINSDALE, DUPAGE COUNTY, ILLINOIS IES PROJECT NO. 915-21
INTEGRITY ENVIRONMENTAL SERVICES, INC.
1240 IROQUOIS DRIVE SUITE 102
NAPERVILLE, IL 60563
630-718-9133 FAX 630-718-9114
August 8, 2017 C-12250 Mr. Mike Duggan Director of Facilities Community Consolidated School District 181 115 West 55th Street Clarendon Hills, Illinois 60514 Dear Mr. Duggan: UST System Removal Site Assessment Report The Lane Elementary School 500 North Elm Street Hinsdale, Illinois IES No. 915-21 This Report has been prepared based on observations made and documentation gathered or obtained by Integrity Environmental Services, Inc. during and after the above referenced underground storage tank (UST) system Site Assessment project. The results of this Site Assessment work are included in this Report and are intended to satisfy the requirements of the Office of the State Marshal for a UST system removal. If you have any questions, please feel free to contact the undersigned at (630) 718-9133. INTEGRITY ENVIRONMENTAL SERVICES, INC. Benjamin Kelderhouse, P.E. Vice-President, Environmental Division MJR/ks
Results: No Contamination
IEMA #: 20170581
Title: Professional Engineer
Expiration Date: 11/30/2017
Phone Number: (630) 718-9133
OFFICE OF THE ILLINOIS STATE FIRE MARSHAL
Site Assessment Results Report
Owner Name Community ConsolidatedSchool District 181
Address 115 W. 55th St.
Clarendon Hills, IL60514
Contact Person Michael DugganPhone Number (630) 861-4900
Owner - U0038791Facility Name The Lane Elementary
SchoolAddress 500 N. Elm St.
Hinsdale, IL 60514County Du Page
Contact Person Michael DugganPhone Number (630) 861-4900
Facility - 2046398
Tank # Capacity in Gallons Product Date Last Used Status Date Removed/Abandoned1 8000 Heating Oil 12/31/1973 Exempt from registration 07/05/2017
Purpose of the Site Assessment: Tank Removal
Permit Number: 00659-2017REM
Date Release Reported: 07/05/2017
Remarks: All analytical results below TACO Objectives
Under the penalties as provided by law pursuant to Section 1-109 of the Code of Civil Procedure, the undersigned certifiesthat the statements set forth in this instrument are true and correct, except as to matters stated to be on information andbelief and as to such matters the undersigned certifies as aforesaid that he/she verily believes the same to be true.
By checking this box, I certify that the sampling done herein complies with all requirements for the number and location ofsampling pursuant to 35 Ill. Adm. Code 734.210 and, for any soil borings, with 35 Ill. Adm. Code 734.425 and 734.435, asincorporated into the rules and regulations of the Office of the State Fire Marshal as required by 176.330(a)&(b).
Name: Benjamin Kelderhouse
License #: 062182182
Company: Integrity Environmental Services, Inc.
Attached Documents915-21 UST Site Assessment Report.pdf
Submitted Date & Time: 8/8/2017 7:38:13 PM
TABLE OF CONTENTS
UST SYSTEM REMOVAL OSFM SITE ASSESSMENT REPORT
COMMUNITY CONSOLIDATED SCHOOL DISTRICT 181 THE LANE ELEMENTARY SCHOOL
500 NORTH ELM STREET HINSDALE, DUPAGE COUNTY, ILLINOIS
IES PROJECT NO. 915-21
1. PROJECT NARRATIVE 2. EXHIBITS
A. UST AREA/SOIL SAMPLE LOCATION DRAWING
B. OSFM DOCUMENTS
C. SOIL AND LIQUID WASTE MANIFESTS
D. SOIL SAMPLE ANALYTICAL DATA
E. PHOTOGRAPHIC DOCUMENTATION
Integrity Environmental Services, Inc.
Integrity Environmental Services, Inc.
SECTION 1
1
PROJECT NARRATIVE
UST SYSTEM REMOVAL OSFM SITE ASSESSMENT REPORT
COMMUNITY CONSOLIDATED SCHOOL DISTRICT 181 THE LANE ELEMENTARY SCHOOL
500 NORTH ELM STREET HINSDALE, DUPAGE COUNTY, ILLINOIS
IES PROJECT NO. 915-21
The following paragraphs provide a narrative description of the removal of one (1), 8,000-gallon heating oil underground storage tank (UST) system from the above referenced Community Consolidated School District 181 (CCSD 181) Lane Elementary School property, located at 500 North Elm Street, Hinsdale, DuPage County, Illinois. The UST was located near the southwest corner of the school property. Refer to Section 2, Exhibit A for UST Area/Soil Sample Location Drawing. R.W. Collins Company (Collins), a State-registered tank removal contractor, was retained by CCSD 181 to remove the UST. Integrity Environmental Services, Inc. (IES), an environmental consulting and engineering firm, was retained by CCSD 181 to provide environmental services for the UST system removal and to document the environmental condition of the surrounding soils, as required by the regulations of the Office of the State Fire Marshal (OSFM). Refer to Section 2, Exhibit B for the OSFM Removal documents (tank removal permit, tank destruction cert, and notification form). On July 5, 2017, using a back-hoe excavator, Collins begin the tank removal process by exposing the UST in the presence of the OSFM inspector, Mr. Bob Kowalski. The existing UST backfill materials (primarily a sand backfill with silt and clay native material) were stockpiled directly west of the tank excavation area. Once the tank was exposed and prior to its removal from the ground, excess product in the tank was pumped out by HazChem Environmental Corporation, a licensed special liquid waste hauler. A total of 5,500 gallons of product was removed from the UST. Refer to Section 2, Exhibit C for the liquid waste manifest. Prior to disturbing the UST, Collins displaced the oxygen in the tank so the interior could be tested for Lower Explosive Limit (LEL) levels. In the presence of the OSFM inspector, the LEL was recorded to be 0%. After testing and confirming the LEL, the remaining backfill material around the UST was excavated and the UST was lifted from the excavation and temporarily staged to the southwest of the tank excavation pit. The UST was then cut open for access and cleaned by Collins personnel. Once the tank had been cleaned, it was placed in a trailer for off-site disposal.
Integrity Environmental Services, Inc.
500 N Elm Street, Hinsdale, Illinois IES No. 915-21
2
As required, the OSFM inspector and the IES representative inspected the integrity of the 8,000-gallon heating oil UST and its excavation. The OSFM inspector, Mr. Kowalski, indicated that a petroleum release had occurred in association with this tank system due to the presence of petroleum odors in the backfill material. As a result, and as instructed by Mr. Kowalski, the IES representative contacted the Illinois Emergency Management Agency (IEMA) to obtain an incident number. IEMA subsequently assigned Incident No. 2017-0581 to the site and this tank removal. A small amount of backfill material (11.96 tons) from the bottom of the excavation that appeared to have a petroleum odor was loaded onto a small dump truck and sent to Waste Management’s Laraway Landfill in Joliet, Illinois for disposal. Refer to Section 2, Exhibit C for the soil manifest. As required by Title 41 of the Illinois Administrative Code (IAC), Part 176.360 of the OSFM regulations a Site Assessment was performed following the removal of tank by collecting soil samples for laboratory analysis. A total of eight (8) soil samples were obtained from the walls and floor of the excavation in accordance with the Illinois Environmental Protection Agency's (IEPA's) 20-foot grid sampling protocol. The soil samples were also screened with a photoionization detector (PID) for petroleum vapors. No elevated PID readings were detected in any of the soil samples collected. All soil samples were analyzed for Benzene, Toluene, Ethylbenzene, and Total Xylenes (BTEX) and Polynuclear Aromatic Compounds (PNAs) concentrations, the required indicator contaminant analysis for heating oil. The location of these soil samples and their designations can be viewed in Section 2, Exhibit B, UST Area/Soil Sample Location Drawing. The analytical results show several PNA compound concentrations in four (4) of the samples collected that were above the laboratory method detection limits, but all the concentrations were below the IEPA's most stringent Tier 1 Tiered Approach to Corrective Action (TACO) Soil Remediation Objectives (SROs). The analytical results do not support Mr. Kowalski's designation that a UST petroleum release occurred. Refer to Section 2, Exhibit D for the soil sample analytical data. Photographic documentation is included in this Report In Section 2, Exhibit E.
Integrity Environmental Services, Inc.
Integrity Environmental Services, Inc.
SECTION 2
Integrity Environmental Services, Inc.
EXHIBIT A
UST SYSTEM REMOVAL WORKCCSD 181 - THE LANE SCHOOL500 NORTH ELM STREETHINSDALE, ILLINOIS
NORTH
8,000-GALLONHEATING OIL UST
VENT LINE RISER
CONCRETE MANWAYVAULT ABOVE UST
THE LANE SCHOOL
CONCRETE SIDEWALK
F
AH
B
C
DG
E
LARGE OAKTREE
APPROX. EXTENT OFEXCAVATION
THE LANE
MECHANICAL ANDA/C UNIT ENCLOSURE
GRASS
GRASS
Integrity Environmental Services, Inc.
EXHIBIT B
(1) (2)
(a)
(b)
(c)
(d)
(e)
(f)
(3)
(4)
(5)
(6)
cc:
Office of the Illinois State Fire MarshalDivision of Petroleum and Chemical Safety
1035 Stevenson DriveSpringfield, IL 62703
2177851020
FOR OFFICE USE ONLYFacility # 2046398Permit # 00659-2017REMRequest Rec'd 06/08/2017Amended Date Approval Date 6/12/2017 SBPermit Expires 12/12/2017
Permit for REMOVAL of Underground Storage Tank(s) and Piping for Petroleum and Hazardous Substances.Permission to remove underground storage tank(s) or piping is hereby granted. Such removal shall not commence until the contractor the permit wasissued to or an employee of that contractor (this does not include a subcontractor) shall establish a date certain to perform the UST activity bycontacting the Office of the State Fire Marshal, Division of Petroleum and Chemical Safety, at which time the UST activity shall be scheduled. THISPERMIT IS VALID FOR SIX MONTHS FROM THE APPROVAL DATE.
OWNER OF TANKS - Corporation, partnership, or other businessentity:
Community Consolidated School District 181115 W. 55th St.Clarendon Hills, IL 60514
Contact: Michael Duggan (630) 861-4900
FACILITY - name and address where tanks are located:
The Lane Elementary School500 N. Elm St.Hinsdale, IL 60514
Contact: Michael Duggan (630) 861-4900
REMOVAL OF TANKS:
Number and size of tanks being removed: (TK # 1) - 8,000
Description/location of piping being removed:
Product to be stored in each tank: (TK # 1) - Heating Oil
Reason of tanks being removed:
If tank(s) is leaking, indicate IEMA incident number:
Date each tank was last used: (TK # 1) - 12/31/1973
The owner must notify this Office when completion of tank removal has occurred, on the Notification for Underground Storage Tank Form.This form can be obtained at www.sfm.illinois.gov or by calling (217)785-1020. After removal is completed, the owner/operator shall performa site assessment by measuring for the presence of a release where contamination is most likely to be present at the UST site. This is inaccordance with the Illinois Administrative Code 176.360 (a) regulations and 40 CFR Part 280.72 (a) Federal Register Requirement.
SPECIAL CONTINGENCIES :
PERSON, FIRM OR COMPANY PERFORMING WORK:
RW Collins Company7225 West 66th StreetChicago, IL 60638
Contact Person: Mike ZiwerPhone: (708) 458-6868Contractor Registration # IL772 Exp. 2/9/2018
Sincerely,
Shelly Bradley
Storage Tank Safety SpecialistDivision File
Integrity Environmental Services, Inc.
Office of the Illinois State Fire MarshalDivision of Petroleum and Chemical Safety
1035 Stevenson DriveSpringfield, Illinois 62703-4259
Notification Form for Underground Storage Tanks
• A separate form must be used for each site.
• If you have more than five tanks, photocopy pages 1-5 and attach to this notification form.
• Please type, or print in ink; the signature under "certification" (section IX) must be signed in Ink.
II. Location of Tank(s)
Current Owner of TanksDate Purchased
Notification for Underground Storage Tanks OFFICE USE ONLY
Tanks Upgraded/Repaired (Permit # )Tank(s) Removed (Permit # )
Other
Abandonment Notice (Permit # )
Tanks Installed (Permit # )
Tanks Relined (Permit # )
TYPE OF NOTIFICATION
Facility I.D. # (if known)
Amended (Changes/Corrections/Additional Tanks)New Facility
Owner I.D. # (if known)
Mark all that apply:
New Owner Owner Address Change (all facilities owned)
Owner Address Change (this facility only)
I. Ownership of Tank(s)
Owner Name (Corp., Individual., Public Agency or other Entity)
Mailing Address
City State Zip
County
Contact Name (Area Code) Phone Contact Name (Area Code) Phone
County
City State Zip
Street Address or State Road, as applicable (exact address)
Facility Name or Company Site Identifier, as applicable
III. TYPE OF OWNERSHIP (mark all that apply)
Former Owner
Ownership Uncertain
Other
ID NUMBER
DATE RECEIVED
(if same as Section I, Mark box)
IV. TYPE OF FACILITYType of Facility: (Circle correct code)
A. Service Station G. Industrial/Manufacturing M. City/Town S. Port DistrictB. Bulk Plant H. Private Institution N. County T. Utility DistrictC. Petroleum Distributor I. Residence (Non-Farm) O. State U. Fire Dept.D. Convenience Store J. Farm P. Federal (Military) V. Other Special E. Auto Dealer K. Airport Q. Federal (Non-Military) Service DistrictsF. Commercial/Retail L. Marina R. School District W. Other
(Please Specify)
IL
4. Abandoned in PlaceDate tanks filledTank filled with:
Inert materials (sand, etc.)WaterUnknownOther (please specify)
7. Substances Currently or Last Stored:
PetroleumDieselKeroseneGasoline Used oil Other (Please specify)
Petroleum Use (if applicable):Heating oil (consumptive use on premises)Back-up generatorOther (please specify)
Hazardous Substance:Name of principal CERCLA substance
Chemical Abstract Service (CAS No)
V. Description of Underground Storage Tanks (Complete entire column for each tank)
1. Status of Tanks Currently in use
Temporarily out of use(Section 2 must be completed)
Permanently out of use(Section 2 must be completed)
Removed(Section 3 must be completed)
Abandoned in place(Section 4 must be completed)
Tank Identification Number Tank No.Tank No.Tank No.Tank No.Tank No.
2. Tanks Permanently & Temporarily Out of UseEstimated date last used
3. Tanks RemovedDate tank(s) removedEstimated date last used
5. Age of TankDate tank installed Date product placed in tank
6. Estimated Total Capacity (gallons)
Mark all that apply:
Self-Insurance
Commercial Insurance
Risk Retention Group
OATH: I certify the information that is provided in section VII is true to the best of my knowledge, and certify that theinstallation was performed in accordance with all applicable state and federal laws and regulations. (THIS SECTIONMAY ONLY BE COMPLETED BY THE CONTRACTOR. SEPARATE OATH MUST BE SUBMITTED FOR EACH
ACTIVITY PERFORMED BY DIFFERENT CONTRACTOR. )
VII. Certification of Compliance (Complete for all new, upgraded and relined tanks at this location)
Installation (mark all that apply)
Installer certified by tank and piping manufacturers
Installer certified or licensed by implementing agency
Installer registered by implementing agency
Installer is the owner of the tank(s)
Installation inspected by aregistered engineer
Installation inspected & approvedby implementing agency
Manufacturer's installation checklists have been completed
Another method allowed by state agency (please specify)
Name
Permit No.Tank No.
Contractor:Signature (must be original) Date
Position Company
Certificate of Deposit
Trust Fund
Other Method Allowed
Guarantee
Surety Bond
Letter of Credit
(please specify)
I certify under penalty of law that I have personally examined and am familiar with the information submittedin this and all attached documents, and that based on my inquiry of those immediately responsible for
obtaining the information, I believe that the submitted information is true, accurate and complete.
VIII. Financial Responsibility
IX. Certification (Read and sign after completing all sections)
Name and official title of owner orowner's authorized representative
(print)
Date SignedSignature (must be original)
Permit Number 00659-2017REM
Date: 7/14/2017
OFFICE OF THE ILLINOIS STATE FIRE MARSHAL
Certificate of RemovalThis certificate confirms that the tanks listed below were removed on said date.
Owner Name Community ConsolidatedSchool District 181
Address 115 W. 55th St.
Clarendon Hills, IL60514
Contact Person Michael DugganPhone Number (630) 861-4900
Owner - U0038791Facility Name The Lane Elementary
SchoolAddress 500 N. Elm St.
Hinsdale, IL 60514Du Page
Contact Person Michael DugganPhone Number (630) 861-4900
Facility - 2046398
Tank # Capacity in Gallons Product Date Removed1 8000 Heating Oil 07/05/2017
Owner/Operator Name: Community Consolidated School District 181
Owner Operator
Submitted Date & Time: 7/14/2017 3:36:35 PMIntegrity Environmental Services, Inc.
Permit Number 00659-2017REM
Date: 7/14/2017
OFFICE OF THE ILLINOIS STATE FIRE MARSHAL
Certification of Removal
Owner Name Community ConsolidatedSchool District 181
Address 115 W. 55th St.
Clarendon Hills, IL60514
Contact Person Michael DugganPhone Number (630) 861-4900
Owner - U0038791Facility Name The Lane Elementary
SchoolAddress 500 N. Elm St.
Hinsdale, IL 60514Du Page
Contact Person Michael DugganPhone Number (630) 861-4900
Facility - 2046398
Tank # Capacity in Gallons Product Date Removed1 8000 Heating Oil 07/05/2017
Under the penalties as provided by law pursuant to Section 1-109 of the Code of Civil Procedure, the undersigned certifiesthat the statements set forth in this instrument are true and correct, except as to matters stated to be on information andbelief and as to such matters the undersigned certifies as aforesaid that he/she verily believes the same to be true.
By checking this box, I certify that the removal of tanks was conducted in accordance with all applicable rules andregulations of the Office of the State Fire Marshal as required by 415 ILCS 5/57.5(f).
Print Owner/Operator Name: Community Consolidated School District 181
Owner Operator
Submitted Date & Time: 7/14/2017 3:36:35 PMIntegrity Environmental Services, Inc.
Integrity Environmental Services, Inc.
EXHIBIT C
Integrity Environmental Services, Inc.
EXHIBIT D
#=CL#
July 17, 2017
LIMS USE: FR - BEN KELDERHOUSELIMS OBJECT ID: 40152932
40152932Project:Pace Project No.:
RE:
Ben KelderhouseIntegrity Environmental1240 Iroquis DriveSuite 102Naperville, IL 60563
915-21 THE LANE
Dear Ben Kelderhouse:Enclosed are the analytical results for sample(s) received by the laboratory on July 08, 2017. Theresults relate only to the samples included in this report. Results reported herein conform to the mostcurrent, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, whereapplicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Christopher [email protected]
Project Manager(920)469-2436
Enclosures
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 1 of 22Integrity Environmental Services, Inc.
#=CP#
CERTIFICATIONS
Pace Project No.:Project:
40152932915-21 THE LANE
Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky UST Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334New York Certification #: 12064North Dakota Certification #: R-150
Virginia VELAP ID: 460263South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1Wisconsin Certification #: 405132750Wisconsin DATCP Certification #: 105-444USDA Soil Permit #: P330-16-00157Federal Fish & Wildlife Permit #: LE51774A-0
Kansas Certification IDs9608 Loiret Boulevard, Lenexa, KS 66219WY STR Certification #: 2456.01Arkansas Certification #: 15-016-0Illinois Certification #: 003097Iowa Certification #: 118Kansas/NELAP Certification #: E-10116Louisiana Certification #: 03055
Nevada Certification #: KS000212008AOklahoma Certification #: 9205/9935Texas Certification #: T104704407Utah Certification #: KS00021Kansas Field Laboratory Accreditation: # E-92587Missouri Certification: 10070
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 2 of 22Integrity Environmental Services, Inc.
#=SS#
SAMPLE SUMMARY
Pace Project No.:Project:
40152932915-21 THE LANE
Lab ID Sample ID Matrix Date Collected Date Received
40152932001 A Solid 07/05/17 15:00 07/08/17 08:10
40152932002 B Solid 07/05/17 15:05 07/08/17 08:10
40152932003 C Solid 07/05/17 15:10 07/08/17 08:10
40152932004 D Solid 07/05/17 15:15 07/08/17 08:10
40152932005 E Solid 07/05/17 15:20 07/08/17 08:10
40152932006 F Solid 07/05/17 15:25 07/08/17 08:10
40152932007 G Solid 07/05/17 15:30 07/08/17 08:10
40152932008 H Solid 07/05/17 15:35 07/08/17 08:10
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 3 of 22Integrity Environmental Services, Inc.
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:Project:
40152932915-21 THE LANE
Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts
40152932001 A EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GSMT
ASTM D2974-87 1 PASI-GKTS
40152932002 B EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GSMT
ASTM D2974-87 1 PASI-GKTS
40152932003 C EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
40152932004 D EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
40152932005 E EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
40152932006 F EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
40152932007 G EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
40152932008 H EPA 8270 by SIM 18 PASI-KNAW
EPA 8260 7 PASI-GHNW
ASTM D2974-87 1 PASI-GKTS
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 4 of 22Integrity Environmental Services, Inc.
#=HO#
SUMMARY OF DETECTION
Pace Project No.:Project:
40152932915-21 THE LANE
Parameters AnalyzedResultLab Sample ID
Report Limit QualifiersUnitsMethodClient Sample ID
40152932001 ANaphthalene 0.0024J mg/kg 07/13/17 17:14 B0.0036EPA 8270 by SIMPercent Moisture 10.9 % 07/15/17 11:280.10ASTM D2974-87
40152932002 BBenzo(g,h,i)perylene 0.0020J mg/kg 07/13/17 17:330.0036EPA 8270 by SIMPercent Moisture 8.2 % 07/15/17 11:280.10ASTM D2974-87
40152932003 CAcenaphthylene 0.0072 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMAnthracene 0.0045 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMBenzo(a)anthracene 0.0033J mg/kg 07/13/17 17:520.0036EPA 8270 by SIMBenzo(a)pyrene 0.0056 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMBenzo(b)fluoranthene 0.0051 mg/kg 07/13/17 17:52 1q0.0036EPA 8270 by SIMBenzo(g,h,i)perylene 0.047 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMBenzo(k)fluoranthene 0.0023J mg/kg 07/13/17 17:520.0036EPA 8270 by SIMChrysene 0.0069 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMFluoranthene 0.0045 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMFluorene 0.0024J mg/kg 07/13/17 17:520.0036EPA 8270 by SIMIndeno(1,2,3-cd)pyrene 0.0032J mg/kg 07/13/17 17:520.0036EPA 8270 by SIMPhenanthrene 0.0033J mg/kg 07/13/17 17:520.0036EPA 8270 by SIMPyrene 0.0066 mg/kg 07/13/17 17:520.0036EPA 8270 by SIMPercent Moisture 8.8 % 07/15/17 11:280.10ASTM D2974-87
40152932004 DAcenaphthylene 0.022J mg/kg 07/13/17 18:290.038EPA 8270 by SIMBenzo(g,h,i)perylene 0.16 mg/kg 07/13/17 18:290.038EPA 8270 by SIMPercent Moisture 14.5 % 07/15/17 11:280.10ASTM D2974-87
40152932005 EPercent Moisture 12.2 % 07/15/17 11:280.10ASTM D2974-87
40152932006 FPercent Moisture 12.2 % 07/15/17 11:280.10ASTM D2974-87
40152932007 GPercent Moisture 12.6 % 07/15/17 12:350.10ASTM D2974-87
40152932008 HPercent Moisture 15.8 % 07/15/17 11:280.10ASTM D2974-87
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 5 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: A Lab ID: 40152932001 Collected: 07/05/17 15:00 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0018 mg/kg 07/13/17 17:14 83-32-907/12/17 00:000.0036 0.0018 1Acenaphthylene <0.0018 mg/kg 07/13/17 17:14 208-96-807/12/17 00:000.0036 0.0018 1Anthracene <0.0018 mg/kg 07/13/17 17:14 120-12-707/12/17 00:000.0036 0.0018 1Benzo(a)anthracene <0.0018 mg/kg 07/13/17 17:14 56-55-307/12/17 00:000.0036 0.0018 1Benzo(a)pyrene <0.0018 mg/kg 07/13/17 17:14 50-32-807/12/17 00:000.0036 0.0018 1Benzo(b)fluoranthene <0.0018 mg/kg 07/13/17 17:14 205-99-207/12/17 00:000.0036 0.0018 1Benzo(g,h,i)perylene <0.0018 mg/kg 07/13/17 17:14 191-24-207/12/17 00:000.0036 0.0018 1Benzo(k)fluoranthene <0.0018 mg/kg 07/13/17 17:14 207-08-907/12/17 00:000.0036 0.0018 1Chrysene <0.0018 mg/kg 07/13/17 17:14 218-01-907/12/17 00:000.0036 0.0018 1Dibenz(a,h)anthracene <0.0018 mg/kg 07/13/17 17:14 53-70-307/12/17 00:000.0036 0.0018 1Fluoranthene <0.0018 mg/kg 07/13/17 17:14 206-44-007/12/17 00:000.0036 0.0018 1Fluorene <0.0018 mg/kg 07/13/17 17:14 86-73-707/12/17 00:000.0036 0.0018 1Indeno(1,2,3-cd)pyrene <0.0018 mg/kg 07/13/17 17:14 193-39-507/12/17 00:000.0036 0.0018 1Naphthalene 0.0024J mg/kg 07/13/17 17:14 91-20-3 B07/12/17 00:000.0036 0.0018 1Phenanthrene <0.0018 mg/kg 07/13/17 17:14 85-01-807/12/17 00:000.0036 0.0018 1Pyrene <0.0018 mg/kg 07/13/17 17:14 129-00-007/12/17 00:000.0036 0.0018 1Surrogates2-Fluorobiphenyl (S) 78 % 07/13/17 17:14 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 88 % 07/13/17 17:14 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 5035/5030B8260 MSV 5035 Med Level
Benzene <0.010 mg/kg 07/12/17 17:21 71-43-207/12/17 12:300.022 0.010 1Ethylbenzene <0.014 mg/kg 07/12/17 17:21 100-41-407/12/17 12:300.056 0.014 1Toluene <0.013 mg/kg 07/12/17 17:21 108-88-307/12/17 12:300.056 0.013 1Xylene (Total) <0.054 mg/kg 07/12/17 17:21 1330-20-707/12/17 12:300.17 0.054 1SurrogatesDibromofluoromethane (S) 104 % 07/12/17 17:21 1868-53-707/12/17 12:3068-130 1Toluene-d8 (S) 95 % 07/12/17 17:21 2037-26-507/12/17 12:3068-149 14-Bromofluorobenzene (S) 81 % 07/12/17 17:21 460-00-407/12/17 12:3058-141 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 10.9 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 6 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: B Lab ID: 40152932002 Collected: 07/05/17 15:05 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0018 mg/kg 07/13/17 17:33 83-32-907/12/17 00:000.0036 0.0018 1Acenaphthylene <0.0018 mg/kg 07/13/17 17:33 208-96-807/12/17 00:000.0036 0.0018 1Anthracene <0.0018 mg/kg 07/13/17 17:33 120-12-707/12/17 00:000.0036 0.0018 1Benzo(a)anthracene <0.0018 mg/kg 07/13/17 17:33 56-55-307/12/17 00:000.0036 0.0018 1Benzo(a)pyrene <0.0018 mg/kg 07/13/17 17:33 50-32-807/12/17 00:000.0036 0.0018 1Benzo(b)fluoranthene <0.0018 mg/kg 07/13/17 17:33 205-99-207/12/17 00:000.0036 0.0018 1Benzo(g,h,i)perylene 0.0020J mg/kg 07/13/17 17:33 191-24-207/12/17 00:000.0036 0.0018 1Benzo(k)fluoranthene <0.0018 mg/kg 07/13/17 17:33 207-08-907/12/17 00:000.0036 0.0018 1Chrysene <0.0018 mg/kg 07/13/17 17:33 218-01-907/12/17 00:000.0036 0.0018 1Dibenz(a,h)anthracene <0.0018 mg/kg 07/13/17 17:33 53-70-307/12/17 00:000.0036 0.0018 1Fluoranthene <0.0018 mg/kg 07/13/17 17:33 206-44-007/12/17 00:000.0036 0.0018 1Fluorene <0.0018 mg/kg 07/13/17 17:33 86-73-707/12/17 00:000.0036 0.0018 1Indeno(1,2,3-cd)pyrene <0.0018 mg/kg 07/13/17 17:33 193-39-507/12/17 00:000.0036 0.0018 1Naphthalene <0.0018 mg/kg 07/13/17 17:33 91-20-307/12/17 00:000.0036 0.0018 1Phenanthrene <0.0018 mg/kg 07/13/17 17:33 85-01-807/12/17 00:000.0036 0.0018 1Pyrene <0.0018 mg/kg 07/13/17 17:33 129-00-007/12/17 00:000.0036 0.0018 1Surrogates2-Fluorobiphenyl (S) 69 % 07/13/17 17:33 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 78 % 07/13/17 17:33 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 5035/5030B8260 MSV 5035 Med Level
Benzene <0.011 mg/kg 07/12/17 20:03 71-43-207/12/17 12:300.024 0.011 1Ethylbenzene <0.015 mg/kg 07/12/17 20:03 100-41-407/12/17 12:300.061 0.015 1Toluene <0.014 mg/kg 07/12/17 20:03 108-88-307/12/17 12:300.061 0.014 1Xylene (Total) <0.059 mg/kg 07/12/17 20:03 1330-20-707/12/17 12:300.18 0.059 1SurrogatesDibromofluoromethane (S) 86 % 07/12/17 20:03 1868-53-707/12/17 12:3068-130 1Toluene-d8 (S) 96 % 07/12/17 20:03 2037-26-507/12/17 12:3068-149 14-Bromofluorobenzene (S) 81 % 07/12/17 20:03 460-00-407/12/17 12:3058-141 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.2 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 7 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: C Lab ID: 40152932003 Collected: 07/05/17 15:10 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0018 mg/kg 07/13/17 17:52 83-32-907/12/17 00:000.0036 0.0018 1Acenaphthylene 0.0072 mg/kg 07/13/17 17:52 208-96-807/12/17 00:000.0036 0.0018 1Anthracene 0.0045 mg/kg 07/13/17 17:52 120-12-707/12/17 00:000.0036 0.0018 1Benzo(a)anthracene 0.0033J mg/kg 07/13/17 17:52 56-55-307/12/17 00:000.0036 0.0018 1Benzo(a)pyrene 0.0056 mg/kg 07/13/17 17:52 50-32-807/12/17 00:000.0036 0.0018 1Benzo(b)fluoranthene 0.0051 mg/kg 07/13/17 17:52 205-99-2 1q07/12/17 00:000.0036 0.0018 1Benzo(g,h,i)perylene 0.047 mg/kg 07/13/17 17:52 191-24-207/12/17 00:000.0036 0.0018 1Benzo(k)fluoranthene 0.0023J mg/kg 07/13/17 17:52 207-08-907/12/17 00:000.0036 0.0018 1Chrysene 0.0069 mg/kg 07/13/17 17:52 218-01-907/12/17 00:000.0036 0.0018 1Dibenz(a,h)anthracene <0.0018 mg/kg 07/13/17 17:52 53-70-307/12/17 00:000.0036 0.0018 1Fluoranthene 0.0045 mg/kg 07/13/17 17:52 206-44-007/12/17 00:000.0036 0.0018 1Fluorene 0.0024J mg/kg 07/13/17 17:52 86-73-707/12/17 00:000.0036 0.0018 1Indeno(1,2,3-cd)pyrene 0.0032J mg/kg 07/13/17 17:52 193-39-507/12/17 00:000.0036 0.0018 1Naphthalene <0.0018 mg/kg 07/13/17 17:52 91-20-307/12/17 00:000.0036 0.0018 1Phenanthrene 0.0033J mg/kg 07/13/17 17:52 85-01-807/12/17 00:000.0036 0.0018 1Pyrene 0.0066 mg/kg 07/13/17 17:52 129-00-007/12/17 00:000.0036 0.0018 1Surrogates2-Fluorobiphenyl (S) 78 % 07/13/17 17:52 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 86 % 07/13/17 17:52 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0044 mg/kg 07/11/17 18:10 71-43-207/10/17 05:000.015 0.0044 1Ethylbenzene <0.0035 mg/kg 07/11/17 18:10 100-41-407/10/17 05:000.012 0.0035 1Toluene <0.0034 mg/kg 07/11/17 18:10 108-88-307/10/17 05:000.011 0.0034 1Xylene (Total) <0.011 mg/kg 07/11/17 18:10 1330-20-707/10/17 05:000.038 0.011 1SurrogatesDibromofluoromethane (S) 115 % 07/11/17 18:10 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 109 % 07/11/17 18:10 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 88 % 07/11/17 18:10 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.8 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 8 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: D Lab ID: 40152932004 Collected: 07/05/17 15:15 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.019 mg/kg 07/13/17 18:29 83-32-907/12/17 00:000.038 0.019 1Acenaphthylene 0.022J mg/kg 07/13/17 18:29 208-96-807/12/17 00:000.038 0.019 1Anthracene <0.019 mg/kg 07/13/17 18:29 120-12-707/12/17 00:000.038 0.019 1Benzo(a)anthracene <0.019 mg/kg 07/13/17 18:29 56-55-307/12/17 00:000.038 0.019 1Benzo(a)pyrene <0.019 mg/kg 07/13/17 18:29 50-32-807/12/17 00:000.038 0.019 1Benzo(b)fluoranthene <0.019 mg/kg 07/13/17 18:29 205-99-207/12/17 00:000.038 0.019 1Benzo(g,h,i)perylene 0.16 mg/kg 07/13/17 18:29 191-24-207/12/17 00:000.038 0.019 1Benzo(k)fluoranthene <0.019 mg/kg 07/13/17 18:29 207-08-907/12/17 00:000.038 0.019 1Chrysene <0.019 mg/kg 07/13/17 18:29 218-01-907/12/17 00:000.038 0.019 1Dibenz(a,h)anthracene <0.019 mg/kg 07/13/17 18:29 53-70-307/12/17 00:000.038 0.019 1Fluoranthene <0.019 mg/kg 07/13/17 18:29 206-44-007/12/17 00:000.038 0.019 1Fluorene <0.019 mg/kg 07/13/17 18:29 86-73-707/12/17 00:000.038 0.019 1Indeno(1,2,3-cd)pyrene <0.019 mg/kg 07/13/17 18:29 193-39-507/12/17 00:000.038 0.019 1Naphthalene <0.019 mg/kg 07/13/17 18:29 91-20-307/12/17 00:000.038 0.019 1Phenanthrene <0.019 mg/kg 07/13/17 18:29 85-01-807/12/17 00:000.038 0.019 1Pyrene <0.019 mg/kg 07/13/17 18:29 129-00-007/12/17 00:000.038 0.019 1Surrogates2-Fluorobiphenyl (S) 0 % 07/13/17 18:29 321-60-8 P3,S407/12/17 00:0054-93 1Terphenyl-d14 (S) 0 % 07/13/17 18:29 1718-51-0 S407/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0049 mg/kg 07/11/17 18:33 71-43-207/10/17 05:000.016 0.0049 1Ethylbenzene <0.0039 mg/kg 07/11/17 18:33 100-41-407/10/17 05:000.013 0.0039 1Toluene <0.0037 mg/kg 07/11/17 18:33 108-88-307/10/17 05:000.012 0.0037 1Xylene (Total) <0.013 mg/kg 07/11/17 18:33 1330-20-707/10/17 05:000.042 0.013 1SurrogatesDibromofluoromethane (S) 108 % 07/11/17 18:33 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 105 % 07/11/17 18:33 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 82 % 07/11/17 18:33 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.5 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 9 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: E Lab ID: 40152932005 Collected: 07/05/17 15:20 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0019 mg/kg 07/13/17 18:48 83-32-907/12/17 00:000.0037 0.0019 1Acenaphthylene <0.0019 mg/kg 07/13/17 18:48 208-96-807/12/17 00:000.0037 0.0019 1Anthracene <0.0019 mg/kg 07/13/17 18:48 120-12-707/12/17 00:000.0037 0.0019 1Benzo(a)anthracene <0.0019 mg/kg 07/13/17 18:48 56-55-307/12/17 00:000.0037 0.0019 1Benzo(a)pyrene <0.0019 mg/kg 07/13/17 18:48 50-32-807/12/17 00:000.0037 0.0019 1Benzo(b)fluoranthene <0.0019 mg/kg 07/13/17 18:48 205-99-207/12/17 00:000.0037 0.0019 1Benzo(g,h,i)perylene <0.0019 mg/kg 07/13/17 18:48 191-24-207/12/17 00:000.0037 0.0019 1Benzo(k)fluoranthene <0.0019 mg/kg 07/13/17 18:48 207-08-907/12/17 00:000.0037 0.0019 1Chrysene <0.0019 mg/kg 07/13/17 18:48 218-01-907/12/17 00:000.0037 0.0019 1Dibenz(a,h)anthracene <0.0019 mg/kg 07/13/17 18:48 53-70-307/12/17 00:000.0037 0.0019 1Fluoranthene <0.0019 mg/kg 07/13/17 18:48 206-44-007/12/17 00:000.0037 0.0019 1Fluorene <0.0019 mg/kg 07/13/17 18:48 86-73-707/12/17 00:000.0037 0.0019 1Indeno(1,2,3-cd)pyrene <0.0019 mg/kg 07/13/17 18:48 193-39-507/12/17 00:000.0037 0.0019 1Naphthalene <0.0019 mg/kg 07/13/17 18:48 91-20-307/12/17 00:000.0037 0.0019 1Phenanthrene <0.0019 mg/kg 07/13/17 18:48 85-01-807/12/17 00:000.0037 0.0019 1Pyrene <0.0019 mg/kg 07/13/17 18:48 129-00-007/12/17 00:000.0037 0.0019 1Surrogates2-Fluorobiphenyl (S) 78 % 07/13/17 18:48 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 85 % 07/13/17 18:48 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0038 mg/kg 07/11/17 18:56 71-43-207/10/17 05:000.013 0.0038 1Ethylbenzene <0.0031 mg/kg 07/11/17 18:56 100-41-407/10/17 05:000.010 0.0031 1Toluene <0.0029 mg/kg 07/11/17 18:56 108-88-307/10/17 05:000.0097 0.0029 1Xylene (Total) <0.0098 mg/kg 07/11/17 18:56 1330-20-707/10/17 05:000.033 0.0098 1SurrogatesDibromofluoromethane (S) 112 % 07/11/17 18:56 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 101 % 07/11/17 18:56 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 85 % 07/11/17 18:56 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.2 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 10 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: F Lab ID: 40152932006 Collected: 07/05/17 15:25 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0019 mg/kg 07/13/17 19:07 83-32-907/12/17 00:000.0037 0.0019 1Acenaphthylene <0.0019 mg/kg 07/13/17 19:07 208-96-807/12/17 00:000.0037 0.0019 1Anthracene <0.0019 mg/kg 07/13/17 19:07 120-12-707/12/17 00:000.0037 0.0019 1Benzo(a)anthracene <0.0019 mg/kg 07/13/17 19:07 56-55-307/12/17 00:000.0037 0.0019 1Benzo(a)pyrene <0.0019 mg/kg 07/13/17 19:07 50-32-807/12/17 00:000.0037 0.0019 1Benzo(b)fluoranthene <0.0019 mg/kg 07/13/17 19:07 205-99-207/12/17 00:000.0037 0.0019 1Benzo(g,h,i)perylene <0.0019 mg/kg 07/13/17 19:07 191-24-207/12/17 00:000.0037 0.0019 1Benzo(k)fluoranthene <0.0019 mg/kg 07/13/17 19:07 207-08-907/12/17 00:000.0037 0.0019 1Chrysene <0.0019 mg/kg 07/13/17 19:07 218-01-907/12/17 00:000.0037 0.0019 1Dibenz(a,h)anthracene <0.0019 mg/kg 07/13/17 19:07 53-70-307/12/17 00:000.0037 0.0019 1Fluoranthene <0.0019 mg/kg 07/13/17 19:07 206-44-007/12/17 00:000.0037 0.0019 1Fluorene <0.0019 mg/kg 07/13/17 19:07 86-73-707/12/17 00:000.0037 0.0019 1Indeno(1,2,3-cd)pyrene <0.0019 mg/kg 07/13/17 19:07 193-39-507/12/17 00:000.0037 0.0019 1Naphthalene <0.0019 mg/kg 07/13/17 19:07 91-20-307/12/17 00:000.0037 0.0019 1Phenanthrene <0.0019 mg/kg 07/13/17 19:07 85-01-807/12/17 00:000.0037 0.0019 1Pyrene <0.0019 mg/kg 07/13/17 19:07 129-00-007/12/17 00:000.0037 0.0019 1Surrogates2-Fluorobiphenyl (S) 80 % 07/13/17 19:07 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 89 % 07/13/17 19:07 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0042 mg/kg 07/11/17 19:19 71-43-207/10/17 05:000.014 0.0042 1Ethylbenzene <0.0034 mg/kg 07/11/17 19:19 100-41-407/10/17 05:000.011 0.0034 1Toluene <0.0032 mg/kg 07/11/17 19:19 108-88-307/10/17 05:000.011 0.0032 1Xylene (Total) <0.011 mg/kg 07/11/17 19:19 1330-20-707/10/17 05:000.036 0.011 1SurrogatesDibromofluoromethane (S) 110 % 07/11/17 19:19 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 106 % 07/11/17 19:19 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 85 % 07/11/17 19:19 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.2 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
Pace Analytical Services, LLC1241 Bellevue Street - Suite 9
Green Bay, WI 54302(920)469-2436
Page 11 of 22Integrity Environmental Services, Inc.
#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: G Lab ID: 40152932007 Collected: 07/05/17 15:30 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0019 mg/kg 07/13/17 19:25 83-32-907/12/17 00:000.0038 0.0019 1Acenaphthylene <0.0019 mg/kg 07/13/17 19:25 208-96-807/12/17 00:000.0038 0.0019 1Anthracene <0.0019 mg/kg 07/13/17 19:25 120-12-707/12/17 00:000.0038 0.0019 1Benzo(a)anthracene <0.0019 mg/kg 07/13/17 19:25 56-55-307/12/17 00:000.0038 0.0019 1Benzo(a)pyrene <0.0019 mg/kg 07/13/17 19:25 50-32-807/12/17 00:000.0038 0.0019 1Benzo(b)fluoranthene <0.0019 mg/kg 07/13/17 19:25 205-99-207/12/17 00:000.0038 0.0019 1Benzo(g,h,i)perylene <0.0019 mg/kg 07/13/17 19:25 191-24-207/12/17 00:000.0038 0.0019 1Benzo(k)fluoranthene <0.0019 mg/kg 07/13/17 19:25 207-08-907/12/17 00:000.0038 0.0019 1Chrysene <0.0019 mg/kg 07/13/17 19:25 218-01-907/12/17 00:000.0038 0.0019 1Dibenz(a,h)anthracene <0.0019 mg/kg 07/13/17 19:25 53-70-307/12/17 00:000.0038 0.0019 1Fluoranthene <0.0019 mg/kg 07/13/17 19:25 206-44-007/12/17 00:000.0038 0.0019 1Fluorene <0.0019 mg/kg 07/13/17 19:25 86-73-707/12/17 00:000.0038 0.0019 1Indeno(1,2,3-cd)pyrene <0.0019 mg/kg 07/13/17 19:25 193-39-507/12/17 00:000.0038 0.0019 1Naphthalene <0.0019 mg/kg 07/13/17 19:25 91-20-307/12/17 00:000.0038 0.0019 1Phenanthrene <0.0019 mg/kg 07/13/17 19:25 85-01-807/12/17 00:000.0038 0.0019 1Pyrene <0.0019 mg/kg 07/13/17 19:25 129-00-007/12/17 00:000.0038 0.0019 1Surrogates2-Fluorobiphenyl (S) 79 % 07/13/17 19:25 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 83 % 07/13/17 19:25 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0042 mg/kg 07/12/17 08:42 71-43-207/10/17 05:000.014 0.0042 1Ethylbenzene <0.0034 mg/kg 07/12/17 08:42 100-41-407/10/17 05:000.011 0.0034 1Toluene <0.0032 mg/kg 07/12/17 08:42 108-88-307/10/17 05:000.011 0.0032 1Xylene (Total) <0.011 mg/kg 07/12/17 08:42 1330-20-707/10/17 05:000.036 0.011 1SurrogatesDibromofluoromethane (S) 115 % 07/12/17 08:42 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 104 % 07/12/17 08:42 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 82 % 07/12/17 08:42 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.6 % 07/15/17 12:350.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:Project:
40152932915-21 THE LANE
Sample: H Lab ID: 40152932008 Collected: 07/05/17 15:35 Received: 07/08/17 08:10 Matrix: SolidResults reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 8270 by SIM Preparation Method: EPA 35468270 MSSV PAH by SIM
Acenaphthene <0.0020 mg/kg 07/13/17 19:44 83-32-907/12/17 00:000.0039 0.0020 1Acenaphthylene <0.0020 mg/kg 07/13/17 19:44 208-96-807/12/17 00:000.0039 0.0020 1Anthracene <0.0020 mg/kg 07/13/17 19:44 120-12-707/12/17 00:000.0039 0.0020 1Benzo(a)anthracene <0.0020 mg/kg 07/13/17 19:44 56-55-307/12/17 00:000.0039 0.0020 1Benzo(a)pyrene <0.0020 mg/kg 07/13/17 19:44 50-32-807/12/17 00:000.0039 0.0020 1Benzo(b)fluoranthene <0.0020 mg/kg 07/13/17 19:44 205-99-207/12/17 00:000.0039 0.0020 1Benzo(g,h,i)perylene <0.0020 mg/kg 07/13/17 19:44 191-24-207/12/17 00:000.0039 0.0020 1Benzo(k)fluoranthene <0.0020 mg/kg 07/13/17 19:44 207-08-907/12/17 00:000.0039 0.0020 1Chrysene <0.0020 mg/kg 07/13/17 19:44 218-01-907/12/17 00:000.0039 0.0020 1Dibenz(a,h)anthracene <0.0020 mg/kg 07/13/17 19:44 53-70-307/12/17 00:000.0039 0.0020 1Fluoranthene <0.0020 mg/kg 07/13/17 19:44 206-44-007/12/17 00:000.0039 0.0020 1Fluorene <0.0020 mg/kg 07/13/17 19:44 86-73-707/12/17 00:000.0039 0.0020 1Indeno(1,2,3-cd)pyrene <0.0020 mg/kg 07/13/17 19:44 193-39-507/12/17 00:000.0039 0.0020 1Naphthalene <0.0020 mg/kg 07/13/17 19:44 91-20-307/12/17 00:000.0039 0.0020 1Phenanthrene <0.0020 mg/kg 07/13/17 19:44 85-01-807/12/17 00:000.0039 0.0020 1Pyrene <0.0020 mg/kg 07/13/17 19:44 129-00-007/12/17 00:000.0039 0.0020 1Surrogates2-Fluorobiphenyl (S) 80 % 07/13/17 19:44 321-60-807/12/17 00:0054-93 1Terphenyl-d14 (S) 86 % 07/13/17 19:44 1718-51-007/12/17 00:0049-120 1
Analytical Method: EPA 8260 Preparation Method: EPA 82608260 MSV 5035 Low Level
Benzene <0.0045 mg/kg 07/11/17 20:04 71-43-207/10/17 05:000.015 0.0045 1Ethylbenzene <0.0036 mg/kg 07/11/17 20:04 100-41-407/10/17 05:000.012 0.0036 1Toluene <0.0034 mg/kg 07/11/17 20:04 108-88-307/10/17 05:000.011 0.0034 1Xylene (Total) <0.011 mg/kg 07/11/17 20:04 1330-20-707/10/17 05:000.038 0.011 1SurrogatesDibromofluoromethane (S) 113 % 07/11/17 20:04 1868-53-707/10/17 05:0070-130 1Toluene-d8 (S) 105 % 07/11/17 20:04 2037-26-507/10/17 05:0070-130 14-Bromofluorobenzene (S) 86 % 07/11/17 20:04 460-00-407/10/17 05:0070-130 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.8 % 07/15/17 11:280.10 0.10 1
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
40152932915-21 THE LANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
261282EPA 8260
EPA 82608260 MSV Low
Associated Lab Samples: 40152932003, 40152932004, 40152932005, 40152932006, 40152932007, 40152932008
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 1538386Associated Lab Samples: 40152932003, 40152932004, 40152932005, 40152932006, 40152932007, 40152932008
Matrix: Solid
AnalyzedMDL
Benzene mg/kg <0.0047 0.016 07/11/17 13:580.0047Ethylbenzene mg/kg <0.0037 0.012 07/11/17 13:580.0037Toluene mg/kg <0.0036 0.012 07/11/17 13:580.0036Xylene (Total) mg/kg <0.012 0.040 07/11/17 13:580.0124-Bromofluorobenzene (S) % 99 70-130 07/11/17 13:58Dibromofluoromethane (S) % 110 70-130 07/11/17 13:58Toluene-d8 (S) % 99 70-130 07/11/17 13:58
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1538387LABORATORY CONTROL SAMPLE & LCSD:LCSSpike LCSD
% Rec RPDMaxRPD
LCSDResult
1538388
Benzene mg/kg 0.045.05 89 70-129850.042 5 20Ethylbenzene mg/kg 0.046.05 93 80-120920.046 1 21Toluene mg/kg 0.044.05 89 80-120910.045 3 21Xylene (Total) mg/kg 0.14.15 91 70-130900.13 1 204-Bromofluorobenzene (S) % 106 70-130108Dibromofluoromethane (S) % 103 70-130102Toluene-d8 (S) % 102 70-130104
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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Green Bay, WI 54302(920)469-2436
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
40152932915-21 THE LANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
261330EPA 5035/5030B
EPA 82608260 MSV 5035 Med Prep
Associated Lab Samples: 40152932001, 40152932002
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 1538637Associated Lab Samples: 40152932001, 40152932002
Matrix: Solid
AnalyzedMDL
Benzene mg/kg <0.0092 0.020 07/12/17 15:480.0092Ethylbenzene mg/kg <0.012 0.050 07/12/17 15:480.012Toluene mg/kg <0.011 0.050 07/12/17 15:480.011Xylene (Total) mg/kg <0.048 0.15 07/12/17 15:480.0484-Bromofluorobenzene (S) % 94 58-141 07/12/17 15:48Dibromofluoromethane (S) % 104 68-130 07/12/17 15:48Toluene-d8 (S) % 108 68-149 07/12/17 15:48
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1538638LABORATORY CONTROL SAMPLE:LCSSpike
Benzene mg/kg 2.62.5 105 66-130Ethylbenzene mg/kg 2.62.5 102 82-122Toluene mg/kg 2.52.5 102 80-120Xylene (Total) mg/kg 7.87.5 104 70-1304-Bromofluorobenzene (S) % 97 58-141Dibromofluoromethane (S) % 111 68-130Toluene-d8 (S) % 103 68-149
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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Green Bay, WI 54302(920)469-2436
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
40152932915-21 THE LANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
484922EPA 3546
EPA 8270 by SIM8270/3546 MSSV PAH by SIM
Associated Lab Samples: 40152932001, 40152932002, 40152932003, 40152932004, 40152932005, 40152932006, 40152932007,40152932008
Parameter UnitsBlankResult
ReportingLimit Qualifiers
METHOD BLANK: 1986031Associated Lab Samples: 40152932001, 40152932002, 40152932003, 40152932004, 40152932005, 40152932006, 40152932007,
40152932008
Matrix: Solid
AnalyzedMDL
Acenaphthene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Acenaphthylene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Anthracene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Benzo(a)anthracene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Benzo(a)pyrene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Benzo(b)fluoranthene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Benzo(g,h,i)perylene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Benzo(k)fluoranthene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Chrysene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Dibenz(a,h)anthracene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Fluoranthene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Fluorene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Indeno(1,2,3-cd)pyrene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Naphthalene mg/kg 0.0032J 0.0033 07/13/17 16:360.0016Phenanthrene mg/kg <0.0016 0.0033 07/13/17 16:360.0016Pyrene mg/kg <0.0016 0.0033 07/13/17 16:360.00162-Fluorobiphenyl (S) % 85 54-93 07/13/17 16:36Terphenyl-d14 (S) % 99 49-120 07/13/17 16:36
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1986032LABORATORY CONTROL SAMPLE:LCSSpike
Acenaphthene mg/kg 0.031.033 94 64-113Acenaphthylene mg/kg 0.030.033 89 62-112Anthracene mg/kg 0.030.033 90 56-113Benzo(a)anthracene mg/kg 0.029.033 89 62-120Benzo(a)pyrene mg/kg 0.030.033 92 52-119Benzo(b)fluoranthene mg/kg 0.030.033 89 56-128Benzo(g,h,i)perylene mg/kg 0.029.033 89 51-127Benzo(k)fluoranthene mg/kg 0.029.033 88 61-122Chrysene mg/kg 0.032.033 96 54-129Dibenz(a,h)anthracene mg/kg 0.028.033 85 49-130Fluoranthene mg/kg 0.029.033 88 61-120Fluorene mg/kg 0.030.033 90 62-116Indeno(1,2,3-cd)pyrene mg/kg 0.029.033 88 53-123Naphthalene mg/kg 0.031.033 92 63-116Phenanthrene mg/kg 0.030.033 92 62-116Pyrene mg/kg 0.032.033 98 60-127
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
40152932915-21 THE LANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter UnitsLCS
Result% RecLimits Qualifiers% RecConc.
1986032LABORATORY CONTROL SAMPLE:LCSSpike
2-Fluorobiphenyl (S) % 84 54-93Terphenyl-d14 (S) % 94 49-120
Parameter UnitsMS
Result% RecLimits Qual% RecConc.
1986033MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpikeResult
60248277001
1986034
MSDResult
MSD% Rec RPD RPD
MaxMSDMSSpikeConc.
Acenaphthene mg/kg .033 104 10-270103 1 27.032ND 0.034 0.034Acenaphthylene mg/kg .033 102 10-188102 1 29.032ND 0.033 0.033Anthracene mg/kg .033 104 10-184101 3 30.032ND 0.034 0.033Benzo(a)anthracene mg/kg .033 134 10-274122 10 111.032ND 0.044 0.040Benzo(a)pyrene mg/kg .033 120 10-167108 12 63.032ND 0.039 0.035Benzo(b)fluoranthene mg/kg 1q.033 95 10-22682 10 51.032ND 0.045 0.040Benzo(g,h,i)perylene mg/kg .033 138 10-170144 4 54.032ND 0.045 0.047Benzo(k)fluoranthene mg/kg .033 108 10-190101 7 36.032ND 0.035 0.033Chrysene mg/kg .033 140 10-203123 13 42.032ND 0.046 0.040Dibenz(a,h)anthracene mg/kg .033 90 10-19992 35.032ND 0.029J 0.030JFluoranthene mg/kg .033 134 10-273120 12 41.032ND 0.044 0.039Fluorene mg/kg .033 100 10-231100 0 81.032ND 0.033 0.032Indeno(1,2,3-cd)pyrene mg/kg .033 109 10-210114 5 49.032ND 0.035 0.037Naphthalene mg/kg .033 107 10-227107 1 96.032ND 0.035 0.035Phenanthrene mg/kg .033 120 10-295113 7 57.032ND 0.039 0.037Pyrene mg/kg .033 140 10-299127 11 60.032ND 0.046 0.0412-Fluorobiphenyl (S) % P3,S40 54-930Terphenyl-d14 (S) % S40 49-1200
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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Green Bay, WI 54302(920)469-2436
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:Project:
40152932915-21 THE LANE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:QC Batch Method:
Analysis Method:Analysis Description:
261572ASTM D2974-87
ASTM D2974-87Dry Weight/Percent Moisture
Associated Lab Samples: 40152932001, 40152932002, 40152932003, 40152932004, 40152932005, 40152932006, 40152932007,40152932008
Parameter UnitsDup
ResultMaxRPD QualifiersRPDResult
401532660011540427SAMPLE DUPLICATE:
Percent Moisture % 7.8 1 107.9
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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#=QL#
QUALIFIERS
Pace Project No.:Project:
40152932915-21 THE LANE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.TNTC - Too Numerous To CountJ - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - Green BayPASI-GPace Analytical Services - Kansas CityPASI-K
BATCH QUALIFIERS
Batch: 261283A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.[M5]
ANALYTE QUALIFIERSThe methods baseline separation for isomers pairs in the Initial Calibration or Continuing Calibration Verification (CCV)was less than the expected 50% valley to baseline. No further action was taken for this method variation. The twocompounds are still being reported as individual isomers and not a combined total, since there is separation between thetwo isomers.
1q
Analyte was detected in the associated method blank.BSample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.P3Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/17/2017 12:18 PM
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:Project:
40152932915-21 THE LANE
Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch
40152932001 484922 485287A EPA 3546 EPA 8270 by SIM40152932002 484922 485287B EPA 3546 EPA 8270 by SIM40152932003 484922 485287C EPA 3546 EPA 8270 by SIM40152932004 484922 485287D EPA 3546 EPA 8270 by SIM40152932005 484922 485287E EPA 3546 EPA 8270 by SIM40152932006 484922 485287F EPA 3546 EPA 8270 by SIM40152932007 484922 485287G EPA 3546 EPA 8270 by SIM40152932008 484922 485287H EPA 3546 EPA 8270 by SIM
40152932003 261282 261283C EPA 8260 EPA 826040152932004 261282 261283D EPA 8260 EPA 826040152932005 261282 261283E EPA 8260 EPA 826040152932006 261282 261283F EPA 8260 EPA 826040152932007 261282 261283G EPA 8260 EPA 826040152932008 261282 261283H EPA 8260 EPA 8260
40152932001 261330 261337A EPA 5035/5030B EPA 826040152932002 261330 261337B EPA 5035/5030B EPA 8260
40152932001 261572A ASTM D2974-8740152932002 261572B ASTM D2974-8740152932003 261572C ASTM D2974-8740152932004 261572D ASTM D2974-8740152932005 261572E ASTM D2974-8740152932006 261572F ASTM D2974-8740152932007 261572G ASTM D2974-8740152932008 261572H ASTM D2974-87
REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,
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Page 21 of 22
Page 22 of 22
Integrity Environmental Services, Inc.
EXHIBIT E
CCSD 181 The Lane Elementary 500 N Elm Street, Hinsdale, Illinois IES Project No. 915-21 Date: 7/5/17 Description: View of Tank Removal Location Direction: Northwest Photo Number: 1 of 4
CCSD 181 The Lane Elementary 500 N Elm Street, Hinsdale, Illinois IES Project No. 915-21 Date: 7/5/17 Description: View of Tank Excavation Direction: Southeast Photo Number: 2 of 4
INTEGRITY ENVIRONMENTAL SERVICES, INC.
CCSD 181 The Lane Elementary 500 N Elm Street, Hinsdale, Illinois IES Project No. 915-21 Date: 7/5/17 Description: View of Tank Being Cut Open for Cleaning Direction: Northwest Photo Number: 3 of 4
CCSD 181 The Lane Elementary 500 N Elm Street, Hinsdale, Illinois IES Project No. 915-21 Date: 7/5/17 Description: View of Excavation Soil Removal Direction: South Photo Number: 4 of 4
INTEGRITY ENVIRONMENTAL SERVICES, INC.