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.'

Indian StandardBITUMENEMULSIO'N FOR ROADS(CATIONTCTYPE ) ,~.. 'SPEClFICATION

( First Revision)

re s 75.140

P " iJ /( ;. ,j p " ' \ . ~ . ! ;\' )1' ..:l,. ~V(~iV 'J~'''' i;" ." 'I C _ ,~_: l, .' . .. " '. T m . - . ' . t' ! l1 l . ' ~ ' . . , . " " ' . '."!J'l~ ,~".,t"!I"[]'~T"~ ' D ' F '[f.[H1, i , I I ! c i t t~/~;I! r:i,1. r1 " .," .. 1 < 1 " _ . . .,r-

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fndian StandardBITUM'ENEMULSION FOR RO'ADS

( CATIONIC TYPE ) ~ SPECIFIC'ATION( FirstRevision)

B l scoreTili$. $ 't !'i nJ a rd ! c e v-e n t!l~ [ pl h ys .i rn I and . chem !cal re -q~ili~:jnentsof blll,lInen~m~rgiollls(curoo ie ~yp ,~ )1fo r r oa ds ,Z NORi'Il,. '"Tn-'ERE1TERE]\CES;The fol low ing st i ! !J I l "Ja . ll t ls C iH: t t t ii n p rov l st on s w . h i . e n ,l h .wug i IL : re fe renoc f n l j; J ,e l e :- i l. oo l1s~i t l ]u t ; rHO\~.~s.~onsof 1m! ; ; Sl1ll ldard. Al t~ e ti m e OfpUD' .~. i ( :aHOlJ tl'!ee d iH ol1 !S ~ :r ld [c ate ll w e re v alid . .Aj~.Sw.nda rd . s MeSl l .! : Ij e c I t o rev ] : ;fO l l< li J ii .d . pa wesw < lJ~ ] j e e l ]J e [ lt basedO~ ttl.is S~:a l ld. i l l idi areencouraged ~oi~ye$t~:gatethep { ] l S . ' S , i b m , y o f a pp !) in ~, th e .m .O 'S ~c ce m e ( l it ~ o t 1 ! o fm e s ta n da rd s H s . ~ e c lbe l o 'w~

l S N @ . riaera\"~ngbinml!en ( second re .~ ' is io .i 't )Specffi;G.l~ioll f O f . 3 . 3 g . r Jd o ; : :;o n l h r l ar yPQrdilin4~m~~t1t l j (;1 t l71~ ~ " i J : / { l ; ! : t )GJoss ru) ' o .f lleUl~ re.~::iting tob ]t li.! !m e n a nd ta r ( s ( : " c < l t t d le1'hiOl1)TE'SlSic!JesM~!h:ods of t e : \ ' i d n g t a r a . n dp i ~ i U J I l l ! incus rna t erials; : S . :l m : p l ] l i S( j i r . S ! .revlsion)M !ethod:i. fo:r [C & t~!l8 tlf :m d~]M:llll!i Il!OIJ.~ .m : ! :t e r : i J~ ! l. . . .. .. []II.': t e r -nn in :u ion of :p~Ili~tr::uioll (firstw~~:sim)l\:fetho-ds for te:sdf!8 ~~t a!l.dbit1i!m~:nQiiS m(lh~:d'li$ ~ ])eter~mirMl t f iQ~1 (If ~~cdUltrifir:st .nmsicm)M ~lhm ;]!s JDr ]tS[~fI~ ta r ::U~(Ibitumbl lo ! .m m:lI~l"i:l~::;~ D~'ter-~ ' n in : :n le n ' ll fs o l .l !. Ib i] R y j n a rDO ! ;l du~ .u:iphil.lc ofl'l'i{h~l)~o~tftyl~[l(l: ( f l r _ f t1'e'!'Isioli)S p ; C i L : M l " '" H i o ~ l fo r f. l i.~umc[lc n m i s . i o l l l, fm ' r o ;M : lS (an~on!''[~T~')

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3,2 Cl'ltUonieEmtllsiow;. A : n . emt ! ! l s i (ms illw hic h th e c . ' l t ioml o f t he e l 'mJ b i fi e .r1;5.at theieterface whh th e h il ume Jl p , [l rt Ic !e j. a neIm.l~Si()n in wl'lk.~. the p O f qu~mi t.y \ \ 'i sc ; , i s m~.e lyto effect or harden the reski L i ~ bi lt L I [i 1! 1 ": 1 1b~rl)nd~heJ bn Hs s pe >c if i 'tI u n( l r 8 1.No. (i.'~)o f T

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t~)W!):~ thCtfHllaililcr w,rr:d fro f t " :. 0 p~riDtiof:2 !(I 3 m in u re s, S ! ; I C l . " t ' . ' l S J . < e : l y inr~ ] 1 ' po s i tedirtc[jon, a"ow! fig ~t rCO:l.~'[ fi'.I(l reve Itit~or.s~)I' t fi e OOi l l , ta incr iii e ac h , t ! i ir~(:lUOI1! ~ H U . l ~ 1 ' J en\ LP - f .HHiung the con'[;lh' lcr ~hmtllgll! tw or~~v (lIIlH o]l ,~[irst in one direclion ~!lid then . in( !: li e o p p o s H e di.~ect.iol1.

b) FtOtli Bulk ~ Where practfcable, bu]kd~.iiv{~r,Yof bitl,llTlerliem ~.d$!OIlsJl.'3U :bea_gflilitedb}' forced d ir (;lld < J , e ~ c r H o ~ o l y . rne thoos .refcfIoJ ~ r j l in T a b f, ;: : 1 1 .

".lEmch C Q ! 1 J t" .i n e t s h ,d J : be .k:gfb.ly ~Jlld jnddib[y.marked W J lh the foJrawing,a ) 1m d.ic a.tiQ .1 ),hhe soeree of iiJJ;m,lfabl1llre;l !l) Moruh a n(l y ea r of man I ! ! . r a c u . l r e ; 'It) Type;d) Bateh nUli t l lbe:r ;.8]1!1e} D a te of~]'liry.

9J i . .i l B IS C m fj ic at io n.: M o .t kin gThe oO l l lM ine r .may also be l!'Iltlrl\;ed with theS r t a n d < l T I ! l : Ma r k .9 ,. 1 .1 ., 1 T il e u s e (If d ~ ; e S t < l I 1 !c 1 @ 1 r d :a rk i s , g Q \ l e r ! l : o o .b y (hep!:Olcisioruof Bu~~~of lndlfi/tSfanda:m$ A rt ,~ 98 6J.n d th .e Ru le :s; [In c! Reg~]~MO!1$ U l , a : 4 e there-uli:doe:t.nce de, l~Qn(C' : l ! f ion i :c 'fyp~}(Cfl l t l :s~:r . : " 1 . 2 , 6.land 8)

Md~IiID" Qo~'[':~$1:,R J ~ i IT I ~ 'o .

R : : l :{l) (2) (3)i) R~id'~~ o m ~"Ittlkrnli 0,05

IS .s~e\'e(Il"=f(~!l~b ;v !D l

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1 11

ANNEX C(Table]) .,

J ! , ' IE "H rOn FOR n E ~.r ER ],''H ; ;,o \T lON O F COA (j u tid'] o N o r 1~;\~OJ,s[ONSl\,TLOW ' j ' : i ! . " . . . . I \ . ~~>E.RI\TUREc"~AI 'PA]" {ATl1Sc.r.i G .la ss B oH .u ng T l:.lh .- .l.5 0 m m BQ l l i g s .n - ~.,5 G , lm . s : IhHls- \ \ \ ' h h name imlisth,:d'Mdi5,6..4nuu in dL~~m:I~'r~ I H H : l r/~ :~]Imin~cn,gt,.

Do - l. 6 O ! l'e 1 1 ~ . T h e :r tlr ll l) :: ;~ a t~ c a .I J! ,I ' COillJu'o][@d.. - . - . . ' _ " - - - .~ p a b le Q fm o iFilul in i~ g ~ ,cmp ~ ] 1 ! l ! , i r e o f 163 .2.~C.1 )-1 P RO C EDURE

I\OZ.!S.rb ' l!g lh ~ :b jtIJJr n mI emuls lcn U) :mmn1icn]r'[au~n.'l(2l W 27"'q.P:klce . : I i SODbn~ltr~pm.sCn~Ol~~\jl!~ m . i ? l e in c , : u : ' n of~h.e ~.VI~!!.! :'$:! iC . J ' ~ i ~ i J e . r s .StopE l c r Ihc t:yl in!.!i l :fS ~l:'Id ~l[~tl\:\lU~iI'llll.~ o SIj[i!1!~Ull!"dis;l'urol..':d. Jl k~.bDr1nory::llr tem r H ~ F : I l ! . m : : : {2 1 t. O27"c]~k~t14hm~rs.AJ~,~':rSHmd i ,n~ for this pc'ri(~d.r em o v e ~ P ' l l I : O ' X ] m 1 l i ~ , c i y55 ' ~~~1m l ! ~ ~U~ !Cll)~.l' o r th ec ~~~ , d s ] o nby lHC '. :l rl lSo f d l. cP ll CHc 'O !! '$ } i' Pl 'I o u \\'ith,()'I)! ldis~l:Imi~k:~i i l ce. les t . Tl lOf 'O l l !g [ ] ] ymixe 'J iCln. ~lonil)l].])-2:.2 Wl~igh:50~o.l g of le!lch samp , l c inl~)s f .p . 1 ltm l d y \ \'I c t~ g h l t't I 6~ J 'lH [ (NJOnt[ g , ras~ I lt 'a ken ; ,

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d~"dl I'l~;'l~ ~ ~ r fw v iIJ ~ p~{_:l;'i;< J . < ; J ' } I f : l o i . ' ' ( ; : : : '. W d , ~ J i ~d ..i~!~~Ih~ H.!;I% rml (f(;,(l ~J,Lf;): Adjust the~tJ~pt:~ a ti.J'Co l ~J~tl 0'.'(:11 ~() IG_1:: : -"1, :F,"C 1 1 1 ( ; ] ] p ia re m e b e a kti~m:~nl~d~]!~ghc wd!~ ..md ~a!~~p,lei,~he 0\",)]1Jf ) f2 l ' i m ' u 11j ,. i\ .:l t h~ end {)f lM~ F'C:ficd ~ c :m (N ,e C O jC i lb~~r~.nd thoro 1I gti. ly st i . 1 I illi~J'Csid uc, Rcp[,lcc in~h d oven for] hour., Hl c r n r emove th e b eak ers [m mt l~ c o ' i. 'e n , i d lOw 10 c o (t~ to m om il{;:mperai[!HC, a n d ', rdgiJ, wi~~]ile rO Os (see No ! e ) ,!'H.:r[J:.-C~~t:"~i1iil.tJ~.d;C!!1.0r~mu r . t . ~ o } , [ b~I'I!I~i:::~rl~mIh~ be~~~.rILl:lr'OO,~1'l'D.amt~ser ~pMl~r~i Gri:1Nh. F(~ '1 I1 i :$,1\"~~i'I, 1 o o o ~ m ~ o c ; ! Jk ~ !I~r,~Oli'l.mf:j)::red ..Al~a',~ht':P~2d'i ~ - E ,o f be~~!'::rnli l;t{! ,~mllt~ict; .~rnpJ~ i l i l . 1 ! . cord or ".,..,tII 'O'\ie'JiI,;l(~'~ ~ja~il'l~~! i l ~Q1 , "e1 : l < l 0 l c ' > i ~~mpleip ~(l.~ iti.mpcr~m~1l:,(iflcJ;)"'C 'I(l.gc~ . e t ~ ~ . p= ,i~~ib lie , ~I rr~f~.rr~~i p~.I.i!:I! ~m;.~ '~pil[rJli0~ OQw,; jH:~ r InO l lyo.:l!I!xQ~PJ~'"i&iI~c,a r~lll~ rn,~.

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Itild g~3:)i'or otner s.~J.L~~b!cg. ia~S. .h $h~dl h~Cl'Ig.r i l "~C J II !) '! : ! cllOlmdlcd at ~t',eha c k .anti prQvklcd\ c t ,; j ~h :It'!i cxpall~inn 1 : 1 ' 1 , 1 mJ)(~r'~'1 d g!'IS. 1 e r 't h e M ' !m p l e .F~3 Sj\,~[[!,lET h sa m p'l~ s fiJ l H be rep re sen t a t i v e o f tn ,e bi~u m e nen:Uj]si{l'~ lo:t;e tC$ ted .F ~ Ji'ltO C EUUU:E , FOR T h"'S T \\"lUI MTA Ge :R EG AT EF ~ .L C a l l)' Oilt. t h . e t e s t a r 2 4 : : i t : 5 . 5C .F.:j.2\Velgh. 460 g o f t b > l i : : i f r dri~d!gr.: l!Qi~dUn,cstOiAe~ ~ : r e g ; H f s i l l ! Ult: J n i : : ' r . ' : im g p a : n .~ '. 4.3W e j ,g l~ 4 0 g o r 000) ,uw;t in the ! 1 i I i ~ ! J j g .fl~l'n~nd ml"! win~ Ihe 460g { ' ] i f [l~greg;J~~~Or

< ;I p pw ; - ; ; im M c ry O H ( ; . U"lirLtllt: Ily meilitf. of 1 1 n:d:dng~}iarleInob.[,rd~] unfiir;;rtl f ~ J m of ( Jt l:; C on Ut{;.~ J g g r c g . o : : se p,a .rUdCli . .. Thr;: tOi~1 ; , '< " ( : : r g h l o r 3 gg.c ga [CshaH be 4(~~.F . to t P lp ~;U e 93rnl (j,lw,HCf to ~hc aggregate a ndQlCi03 diUSl mi:n~reinto HIemWtig p~~andrnkt hO!1( )l lgh ly ]0 o b t a i l ! D IJ ] 1 i f o T r n w . e t U r a g . F~ .5 W eiJ J:h 3 5 g oC tJ Hl]m e 'Il e m uls ie n lnto U: tC-f : ! g g m g a t t ]iI1 l~ p a :n a m ( l m I x v i ! ! ( ) r l ) ! J L s ~ . JW i th U tem o o fl!g o .l i!d e for;5 m iJ ilU te s b y.a b a c k i 1 ! 1C i l Forthm O l I o f i m ,1 ! leUi lH. ica] paU l ! o f r n ,e m i x i ~ , g b]; i ideo.rspoon, A~ ~lle:eJ i idof ihe m L l l n : g . p e r i o ( l , tUllhe p ~ . ! ' 1a~d ,permi[ aElY !e~s f:['J;l1l!$](ln not 0]) llhej' tes rs ~i[!iboth d ry a nd W~[ :agf l J [eg. l [e5,F'S.l A[ d le end ot the m : b d I D l . g p e r - t o " record (h eC ( l 1 i f ~ . ~ I l ! 1 : of the to~a!~ggrc:ga[C: s u r f J ! r e O ! r ~ o : J : h y I h eb ]u l if f ii fl n em V:~~o l ila s e

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A .N NJi:X G(Table 1)

S TA nU :,JTY T O M ~X JN G wrrn CE'' ' ' ll '~N'ft;,l AI'P,!'\I~ATUSG .L 1 S j , e ~ 1 e $ ~ A lAO lBm IS S iev e a p r ro ; rim ~ ~ c J ;yn O D m m In d f a : m e w r and 4 1 0 m m :in h e jg h t i lndj iSH"mfc r rD l l ~S Si,evc appm:dmat:ely200' mm i : 1 l{!f~mc,te;r.G , . ~ ., Z ,M t: u d .ms t. . ~ . A : f(.1li i lld: ;Mtto'med! Jt i ( l :~o : i ]~[~!f'!ICnfapproJ~mate,ly 5 T . l i l ) " t m t l ~racity.G.1.,J S~!e~~Rl')d~ A St.ee] rod w:I[]noll.l.I1dad eads :13 r o m In ( Ifame ,te r.G ~AB;}]3]1re - 250 g c a P ' l !l ~ jt y a c c ;u r a te (0 0 , . 1 g .CA .. 5 , G r ' ; !! d I L H l l i e o d Cylini~er~ o f lOOm.] c apachy ,ChV6 Sh~!!m;t P~n ~ o r JiOOm m diameter ,and ofabcmt ~ijmlcap'i i lc i ty10 [U iUO! ] $ p e r

minute. Ad th e ~rld o f c n e -m i nu te rn.i:dllgperi:odadd , r S U I m l ( r c sM y b o i l e d d]~tHk:dwater a l IQOm! c .l it lJ p e r a tu r e a n d ! ~(HlUll:~~MJu.ing for 3 mlnuies,Ma lllta in tl",e jngmdiCrll:S ata tcmp>cwnl [cof~p"p : !' o x i m . a t e :J y 2 5 C d ur .i ng m b :ililg . P'OtiF th e m ix ru relhrou~h the 'Wt:.i~ed l,IW mm ]$ S ] , , - e (iln4r i t ! s ~wkh . c : H S l m c J W9l[,(ii'. Plac (he sieve hi the " , ,' e: jgh.ed!pal:l ,heal i l l l the ovenat 1l0"Cll~lf] d ry 3:l1d....ejghto nearest 0.1 g(W2) .G4 CALCULATION

, _. _, ,_ W~- r \ vi.Oo.ag l ! J .~a l lOI JJV

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ANN~~X J(Claases 6..2;.G~4 and Table] )

ME'HWD H ..H~nETEHM1NA'nOoN (}1"Hl~SiPUI nYEVA]~OJh\'noN';r.~ Ali~AR"'lTUSJt.IGhl.ss .]j:'ea kers .~ low form of 1 OOO~m Ic a p a c it y m r lt ! C . ( ; I f il{}i'osniG'lH~gh"l~~.J.1 .2 G la s5 Ro~.'i .~ W i th fl.~ ,m .e pD lb hc d 6.4 mrn[a d~i~iW}~t:f~ll~. 1 7 1 . j mm Ifl iel]gdl.J.L 3 Ik l!l . ..~(:e ~ of 5 00g a lp 3!c Hy ~ ]1 jd;aCC~J:-ne](1oJg,

J

J 4 . 4 O v e . 1 Q !. ~ Th-e.rItlQSl;jl ~ C i i ! H y cot! ~!:.o ll(id a t at empe : r~~ : tl [e o f . 1 63 H l"CJ.~~~RO.cEDUR.EW eig h 5 0 . : i l : : i()J.gof~horQl;lgl'!lJmi'{.ed o f i l m . u J I S ] O I lin to ea ch of : th r~(l ;beake j: 'S .ad t (. 1 f " " ~ r u c l lh as p .r (l'...io'!I:~lJhee:~ \ '! , -e~g1 ' ledw~~t l~~e la ss rod, P J a.(:c th eb:.( lk t r< l i~of lg ' . . th i t h e : r ro , j lJ l t h eove .n , : :HhB 2$"C[ Q r " 2 f~Oil!f$. AJ the e n d o ft h is pedDd! r emove e a ! C 1 ~ .beaker aadstir thE;!.esil l l ! le thoroiUghly. Re :p ll lc ( ) I nlite o~'.e;nor , ! U I O l n e , r o n ' ( ' ! n o u t lh~:n l '~Q\i\~.::a!JJ(lc ool . a t r oom hlmpenHure , w dgh the b ea k ers alon~Whfl the [00$,

J-3.n Reskille, p e r e en t = = 2 (A ~ B) V::; -~ --.~ot I' ~'C-where . . ~ c -AB ."" m a s s o t be e ke r, TiO~ and I : "csudue : 1 ; ; ~nd:= {..: :m~s:sof bea kera ndrod, g.. ] 1 . 3 . 2 Tate l~~ , n 1 e r a , g , e Qf t h r ce w a l l : ( ' : S ob ta i n ed ! f o rlesiclue~percent. vJ.4 T:'ESTS ON .RESmlJJ~.4.1 .P-eIJ!~~mHO\~ - De,~eImi. l1!epenetrat ion O}l. :a :sa rn ri e of th e [ c. sjJ ue ] [ J J aceordaaee with ]$ l2 !03 ,191:tJ.4.2 .l)udiUty ~De:ter~i:l1e the dh. lC1H~[y on atepr6csen:tath-eportron bEthe residue in aecordaneew ith ]S ]200 : 197&J.~. SO]llIbH~lyi.!l'f:;kh[Qt'(!ed1~'Ie;i~e.~. Deter-mine the sO]lJibiHty in tJkhloroethyiene on arepreseIu.:at~!,,'es

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Contaia Nmlnlbers lBII'TeamGSHP 1...5

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