804 Ti Stand

Manual8.804.8001EN

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 01info@metrohm.comwww.metrohm.com

804 Ti Stand

Manual

8.804.8001EN 06.2010 ek

TeachwareMetrohm AGCH-9101 Herisauteachware@metrohm.com

This documentation is protected by copyright. All rights reserved.

Although all the information given in this documentation has beenchecked with great care, errors cannot be entirely excluded. Should younotice any mistakes please send us your comments using the addressgiven above.

Documentation in additional languages can be found onhttp://products.metrohm.com under Literature/Technical documenta-tion.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents

804 Ti Stand ￭￭￭￭￭￭￭￭ III

Table of contents

1 Introduction 1

1.1 Instrument description ......................................................... 1

1.2 About the documentation ................................................... 11.2.1 Symbols and conventions ........................................................ 1

1.3 Safety instructions ................................................................ 21.3.1 General notes on safety ........................................................... 21.3.2 Electrical safety ........................................................................ 21.3.3 Working with liquids ................................................................ 31.3.4 Flammable solvents and chemicals ........................................... 31.3.5 Recycling and disposal ............................................................. 4

2 Device overview 5

3 Installation 6

3.1 Setting up the instrument .................................................... 63.1.1 Packaging ................................................................................ 63.1.2 Checks .................................................................................... 63.1.3 Location .................................................................................. 6

3.2 Mounting the 804 Ti Stand ................................................. 7

3.3 Connecting the 804 Ti Stand ............................................. 10

4 Technical specifications 12

4.1 Rotational speed 804 Ti Stand .......................................... 12

4.2 Power supply ...................................................................... 12

4.3 Safety specifications ........................................................... 12

4.4 Electromagnetic compatibility (EMC) ................................ 12

4.5 Ambient temperature ......................................................... 13

4.6 Dimensions .......................................................................... 13

5 Conformity and warranty 14

5.1 Declaration of Conformity ................................................. 14

5.2 Quality Management Principles ........................................ 15

5.3 Warranty (guarantee) ......................................................... 16

6 Accessories 17

6.1 Scope of delivery ................................................................ 176.1.1 804 Ti Stand without stand 2.804.0010 ................................. 176.1.2 804 Ti Stand with stand 2.801.0040 ...................................... 17

Table of contents ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

IV ￭￭￭￭￭￭￭￭ 804 Ti Stand

6.2 Optional accessories ........................................................... 196.2.1 804 Ti Stand 2.804.0010, 2.804.0040 ................................... 19

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804 Ti Stand ￭￭￭￭￭￭￭￭ V

Table of figures

Figure 1 Front 804 Ti Stand ............................................................................. 5Figure 2 Rear 804 Ti Stand .............................................................................. 5Figure 3 Connecting the 804 Ti Stand ........................................................... 11Figure 4 Connecting the Dosino to the 804 Ti Stand ..................................... 11

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804 Ti Stand ￭￭￭￭￭￭￭￭ 1

1 Introduction

1.1 Instrument description

The 804 Ti Stand is a titration stand and controller for the propeller stirrer802 Stirrer.

The titration stand is directly connected to an analysis device via an MSBconnection cable.

1.2 About the documentation

Caution

Please read through this documentation carefully before putting theinstrument into operation. The documentation contains informationand warnings which the user must follow in order to ensure safe opera-tion of the instrument.

1.2.1 Symbols and conventionsThe following symbols and styles are used in this documentation:

Cross-reference to figure legend

The first number refers to the figure number, thesecond to the instrument part in the figure.

Instruction step

Carry out these steps in the sequence shown.

Warning

This symbol draws attention to a possible life hazardor risk of injury.

Warning

This symbol draws attention to a possible hazard dueto electrical current.

Warning

This symbol draws attention to a possible hazard dueto heat or hot instrument parts.

1.3 Safety instructions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

2 ￭￭￭￭￭￭￭￭ 804 Ti Stand

Warning

This symbol draws attention to a possible biologicalhazard.

Caution

This symbol draws attention to a possible damage ofinstruments or instrument parts.

Note

This symbol marks additional information and tips.

1.3 Safety instructions

1.3.1 General notes on safety

Warning

This instrument may only be operated in accordance with the specifica-tions in this documentation.

This instrument has left the factory in a flawless state in terms of technicalsafety. To maintain this state and ensure non-hazardous operation of theinstrument, the following instructions must be observed carefully.

1.3.2 Electrical safetyThe electrical safety when working with the instrument is ensured as partof the international standard IEC 61010.

Warning

Only personnel qualified by Metrohm are authorized to carry out servicework on electronic components.

Warning

Never open the housing of the instrument. The instrument could bedamaged by this. There is also a risk of serious injury if live componentsare touched.

There are no parts inside the housing which can be serviced or replacedby the user.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 3

Mains voltage

Warning

An incorrect mains voltage can damage the instrument.

Only operate this instrument with a mains voltage specified for it (seerear panel of the instrument).

Protection against electrostatic charges

Warning

Electronic components are sensitive to electrostatic charges and can bedestroyed by discharges.

Always pull the mains cable out of the mains connection socket beforeconnecting or disconnecting electrical appliances on the rear panel ofthe instrument.

1.3.3 Working with liquids

Caution

Periodically check all system connections for leaks. Observe the relevantregulations in respect to working with flammable and/or toxic fluidsand their disposal.

1.3.4 Flammable solvents and chemicals

Warning

All relevant safety measures are to be observed when working withflammable solvents and chemicals.

￭ Set up the instrument in a well-ventilated location (e.g. laboratoryflue).

￭ Keep all sources of flame far from the workplace.￭ Clean up spilled fluids and solids immediately.￭ Follow the safety instructions of the chemical manufacturer.

1.3 Safety instructions ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

4 ￭￭￭￭￭￭￭￭ 804 Ti Stand

1.3.5 Recycling and disposalThis product is covered by European Directive 2002/96/EC, WEEE – Wastefrom Electrical and Electronic Equipment.

The correct disposal of your old equipment will help to prevent negativeeffects on the environment and public health.

More details about the disposal of your old equipment can be obtainedfrom your local authorities, from waste disposal companies or from yourlocal dealer.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 5

2 Device overview

1

Figure 1 Front 804 Ti Stand

1 LED function displayLights up, when the stirrer is switched on.

3.804.300x

MSB

1

2

3

4

Figure 2 Rear 804 Ti Stand

1 MSB connectorMetrohm Serial Bus.

For connecting additional devices

2 Clamping screwFor fixing the positioning height or theswing position of the magnetic stirrer.

3 MSB connection cableFor connecting to a control device.

4 Propeller stirrer connectorFor connecting the 802 Stirrer

3.1 Setting up the instrument ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

6 ￭￭￭￭￭￭￭￭ 804 Ti Stand

3 Installation

3.1 Setting up the instrument

3.1.1 PackagingThe instrument is supplied in highly protective special packaging togetherwith the separately packed accessories. Keep this packaging, as only thisensures safe transportation of the instrument.

3.1.2 ChecksImmediately after receipt, check whether the shipment has arrived com-plete and without damage by comparing it with the delivery note.

3.1.3 LocationThe instrument has been developed for operation indoors and may not beused in explosive environments.

Place the instrument in a location of the laboratory which is suitable foroperation, free of vibrations, protected from corrosive atmosphere, andcontamination by chemicals.

The instrument should be protected against excessive temperature fluctu-ations and direct sunlight.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 7

3.2 Mounting the 804 Ti Stand

Mounting the stand

6.2001.060

6.2016.070

1

2

Mount the stand as follows:

1 Screw the 6.2001.060 stand plate with the accompanying fourscrews tightly to the bottom of the instrument.

2 Screw the 6.2016.070 stand plate with the hexagon screw (hexagonkey supplied) firmly to the stand plate.

3.2 Mounting the 804 Ti Stand ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

8 ￭￭￭￭￭￭￭￭ 804 Ti Stand

Fastening the titration stand

2

1

Fasten the titration stand as follows:

1 Attach the titration stand on the support rod and push it down-wards.

2 With the clamping screw, fix the positioning height or the swingposition of the titration stand.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 9

Attaching the clamping ring and the electrode holder

6.2021.020

6.2013.010

Fasten the clamping ring and the electrode holder as follows:

1 Push the 6.2013.010 clamping ring onto the support rod.

2 Attach the 6.2021.020 electrode holder on the support rod.

3 Keep the red button pressed down and push the electrode holderdownwards to the required height.

4 Fix the position of the electrode holder with the aid of the clampingring.

3.3 Connecting the 804 Ti Stand ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

10 ￭￭￭￭￭￭￭￭ 804 Ti Stand

Mounting the propeller stirrer

1

2

Mounting the propeller stirrer as follows:

1 Insert the propeller stirrer 802 Stirrer without the stirring propellerfrom above into the center opening of the electrode holder.

2 Plug the stirring propeller from below to the propeller stirrer.

3.3 Connecting the 804 Ti Stand

Connect the titration stand as follows:

1 Exit the control software.

2 Connect the connection cable of the titration stand to one of thesockets marked with MSB on the rear of the control device.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 11

Figure 3 Connecting the 804 Ti Stand

3 Connecting an additional device (e.g. Dosimat or Dosino) to the MSBconnector of the titration stand.

MSB

3.804.300X

Figure 4 Connecting the Dosino to the 804 Ti Stand

4 Start the control software.

4.1 Rotational speed 804 Ti Stand ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

12 ￭￭￭￭￭￭￭￭ 804 Ti Stand

4 Technical specifications

4.1 Rotational speed 804 Ti Stand

Maximum rota-tional speed

±1700...1900 U/min

Setting of therotational speed

±15 steps

Increase of rota-tional speed perstep

±115...125 U/min

4.2 Power supply

Voltage +12 V, -12 V, +5 V

Power consump-tion

4 W

Fuse Electronic overload protection

4.3 Safety specifications

Design and testing ￭ EN/IEC 61010-1:2001￭ UL 61010-1: 2004￭ CSA-C22.2 No. 61010-1: 2004￭ Degree of protection IP40￭ Protection class III

4.4 Electromagnetic compatibility (EMC)

Emission Standards fulfilled:￭ EN/IEC 61326-1:2006￭ EN/IEC 61000-6-3: 2006￭ EN 55011 / CISPR 11: 2007

Immunity Standards fulfilled:￭ EN/IEC 61326-1:2006￭ EN/IEC 61000-6-2: 2005￭ EN/IEC 61000-4-2: 2001￭ EN/IEC 61000-4-3: 2006￭ EN/IEC 61000-4-4: 2004￭ EN/IEC 61000-4-5: 2001

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804 Ti Stand ￭￭￭￭￭￭￭￭ 13

￭ EN/IEC 61000-4-6: 2001￭ EN/IEC 61000-4-11: 2004￭ EN/IEC 61000-4-14: 2004￭ NAMUR:2004

4.5 Ambient temperature

Nominal functionrange

+5…+45 °C(at a maximum of 85% humidity)

Storage –20…+60 °C

Transport –40…+60 °C

4.6 Dimensions

Width 90 mm

Height (withoutstand)

70 mm

Height (withstand)

430 mm

Depth 140 mm

Weight 330 g

5.1 Declaration of Conformity ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

14 ￭￭￭￭￭￭￭￭ 804 Ti Stand

5 Conformity and warranty

5.1 Declaration of Conformity

This is to certify the conformity to the standard specifications for electricalappliances and accessories, as well as to the standard specifications forsecurity and to system validation issued by the manufacturing company.

Name of commodity 804 Ti Stand

Titration stand and controller for 802 Stirrer.

This instrument has been built and has undergone final type testingaccording to the standards:

Electromagneticcompatibility

Emission: EN/IEC 61326-1: 2006, EN/IEC 61000-6-3: 2006,EN 55011 / CISPR 11: 2007

Immunity: EN/IEC 61326-1: 2006, EN/IEC 61000-6-2: 2005,EN/IEC 61000-4-2: 2001,EN/IEC 61000-4-3: 2006,EN/IEC 61000-4-4: 2004,EN/IEC 61000-4-5: 2001,EN/IEC 61000-4-6: 2001,EN/IEC 61000-4-11: 2004,EN/IEC 61000-4-14: 2004, NAMUR: 2004

Safety specifications EN/IEC 61010-1: 2001, UL 61010-1: 2004,CSA-C22.2 No. 61010-1: 2004, degree of protection IP40, protectionclass III

This instrument meets the requirements of the CE mark as contained inthe EU directives 2006/95/EC (LVD), 2004/108/EC (EMC). It fulfils the fol-lowing specifications:

EN 61326-1 Electrical equipment for measurement, controland laboratory use – EMC requirements

EN 61010-1 Safety requirements for electrical equipment formeasurement, control and laboratory use

Manufacturer Metrohm Ltd., CH-9101 Herisau/Switzerland

Metrohm Ltd. is holder of the SQS certificate ISO 9001:2000 Quality man-agement system for development, production and sales of instrumentsand accessories for ion analysis.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 15

Herisau, 6 January, 2009

D. Strohm

Vice President, Head of R&D

A. Dellenbach

Head of Quality Management

5.2 Quality Management Principles

Metrohm Ltd. holds the ISO 9001:2000 Certificate, registration number10872-02, issued by SQS (Swiss Association for Quality and ManagementSystems). Internal and external audits are carried out periodically to assurethat the standards defined by Metrohm’s QM Manual are maintained.

The steps involved in the design, manufacture and servicing of instrumentsare fully documented and the resulting reports are archived for ten years.The development of software for PCs and instruments is also duly docu-mented and the documents and source codes are archived. Both remainthe possession of Metrohm. A non-disclosure agreement may be asked tobe provided by those requiring access to them.

The implementation of the ISO 9001:2000 quality management system isdescribed in Metrohm’s QM Manual, which comprises detailed instruc-tions on the following fields of activity:

Instrument development

The organization of the instrument design, its planning and the intermedi-ate controls are fully documented and traceable. Laboratory testingaccompanies all phases of instrument development.

Software development

Software development occurs in terms of the software life cycle. Tests areperformed to detect programming errors and to assess the program’sfunctionality in a laboratory environment.

Components

All components used in the Metrohm instruments have to satisfy the qual-ity standards that are defined and implemented for our products. Suppli-ers of components are audited by Metrohm as the need arises.

Manufacture

The measures put into practice in the production of our instruments guar-antee a constant quality standard. Production planning and manufacturingprocedures, maintenance of production means and testing of compo-nents, intermediate and finished products are prescribed.

5.3 Warranty (guarantee) ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

16 ￭￭￭￭￭￭￭￭ 804 Ti Stand

Customer support and service

Customer support involves all phases of instrument acquisition and use bythe customer, i.e. consulting to define the adequate equipment for theanalytical problem at hand, delivery of the equipment, user manuals, train-ing, after-sales service and processing of customer complaints. TheMetrohm service organization is equipped to support customers in imple-menting standards such as GLP, GMP, ISO 900X, in performing Opera-tional Qualification and Performance Verification of the system compo-nents or in carrying out the System Validation for the quantitative determi-nation of a substance in a given matrix.

5.3 Warranty (guarantee)

Metrohm guarantees that the deliveries and services it provides are freefrom material, design or manufacturing errors. The warranty period is 36months from the day of delivery; for day and night operation it is 18months. The warranty remains valid on condition that the service is provi-ded by an authorized Metrohm service organization.

Glass breakage is excluded from the warranty for electrodes and otherglassware. The warranty for the accuracy corresponds to the technicalspecifications given in this manual. For components from third parties thatmake up a considerable part of our instrument, the manufacturer's war-ranty provisions apply. Warranty claims cannot be pursued if the Customerhas not complied with the obligations to make payment on time.

During the warranty period Metrohm undertakes, at its own choice, toeither repair at its own premises, free of charge, any instruments that canbe shown to be faulty or to replace them. Transport costs are to the Cus-tomer's account.

Faults arising from circumstances that are not the responsibility ofMetrohm, such as improper storage or improper use, etc. are expresslyexcluded from the warranty.

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804 Ti Stand ￭￭￭￭￭￭￭￭ 17

6 Accessories

6.1 Scope of delivery

Note

Subject to change without notice.

6.1.1 804 Ti Stand without stand 2.804.0010

Qty. Order no. Description

1 1.804.0010 804 Ti Stand

Titration stand with permanently attached cable for MSB (MetrohmSerial Bus).

1 8.804.8001ML Manual 804 Ti Stand

6.1.2 804 Ti Stand with stand 2.801.0040

Qty. Order no. Description

1 1.804.0010 804 Ti Stand

Titration stand with permanently attached cable for MSB (MetrohmSerial Bus).

1 6.2001.060 Stand plate without support rod

For mounting the 801, 804, 803 stirrers on a Titrando, Titrino plus,Dosimat plus and on the 856 and 867 measuring modules.

6.1 Scope of delivery ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭

18 ￭￭￭￭￭￭￭￭ 804 Ti Stand

Qty. Order no. Description

1 6.2013.010 Clamping ring

For support rods with a diameter of 10 mm

Material: Metal

Width (mm): 20

Height (mm): 16

1 6.2016.070 Support rod / 400 mm

Material: Steel, stainless 18/8

Outer diameter (mm): 10

Length (mm): 400

1 6.2021.020 Electrode holder

Electrode holder for 4 electrodes and 2 buret tips

Material: Plastic

1 6.2621.070 Hexagon key 5 mm

Length (mm): 80

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804 Ti Stand ￭￭￭￭￭￭￭￭ 19

Qty. Order no. Description

1 6.2621.130 Hexagon key 2 mm

Length (mm): 50

1 8.804.8001ML Manual 804 Ti Stand

6.2 Optional accessories

6.2.1 804 Ti Stand 2.804.0010, 2.804.0040

Order no. Description

6.2001.090 Base plate two-sided

Double stand plate for fixing two 801, 803, 804 stirrers and a Titrando

6.2151.010 Cable MSB plug / socket

Extension cable for MSB connections and for Touch Control - Titrando. Mini DINsocket - Mini DIN plug

Length (m): 2