50 Years Achievements of 3MV Van de Graaff ion accelerator ...
Transcript of 50 Years Achievements of 3MV Van de Graaff ion accelerator ...
50 Years Achievements of 3MV Van de Graaff ion accelerator in Tehran: A
brief historyMohammad Lamehi-Rachti,
Omidreza Kakuee
Physics and Accelerators Research School, Nuclear Science and
Technology Research Institute, Tehran, Iran
Ion beamlines established at the 3 MV Van De Graaff accelerator, in Tehran
From left to right – Nuclear Microprobe, NRA, External & K-edge contrast
Imaging, IBMM, Conventional IBA analysis, RBS-channeling, PIGE which
are shown separately in the next slides
K-edge contrast Imaging
PIGE
External PIXE
Continued
PIGE
NRA
Omidreza Kakuee, Vahid Fathollahi,
Mohammad Lamehi-Rachti,
Development of a versatile user-friendly
IBA experimental chamber, Nucl. Instr.
and Meth. B371 (2016)156-160.
15
Ionoluminescence spectroscopy in nuclear microprobe system
Fiber
optic
Collection lenz
CCD
Cooled pack
Termome
ter
Laboratory
Cooler
Opt. Mic.
Color: red
Ca: host
Yb: luminescent element
Color: white
Si: host
Eu: luminescent element
Color: bright blue
Zn: host
Cu: luminescent element
T. Nikbakht , O. Kakuee, M. Lamehi-Rachti, Ionoluminescence spectroscopy and microscopy of lapis
lazuli, Journal of Luminescence, 181 (2017) 246–251
T. Nikbakht, O. Kakuee, M. Lamehi-Rachti, Study of the ionoluminescence behavior of the gemstones:
Beryl (aquamarine variety), opal, and topaz, Journal of Luminescence, 171 (2016) 154-158.
Formula: Na6Ca2Al6Si6O24[(SO4); S;Cl; (OH)]2
PIXE analysis of patients liver
1
10
100
1000
10000
0 2 4 6 8 10 12
Co
un
ts
Energy(KeV)
Normal
Thalasemia
Cl
K(Kα)
Ca(Kα)
Ca(Kß)
Fe(K
Fe(K
Cu
Zn(K
Zn(K
Cu(K
(b)
Development of a reaction chamber to study
radiation damage by energetic ion beam
A reaction chamber to study radiation damage by energetic ion beam
By bombarding the test materials in irradiation facilities:•One could quickly test different materials,
•Study the effects from different sources individually,
•Explore the science behind the observed behavior
• The thin part of the chamber could be inserted in tube furnace
• Heating the sample up to about 1000° C
• Electrically isolating for ion beam monitoring
• Evacuation down to about 10-5 Torr
Ion irradiation chamber
Viewer
To uniformly irradiate the sample with ions, the beam must be reasonably
uniform. A visual beam viewer was installed in the beamline just prior to the
reaction chamber to roughly measure the beam profile
tube furnace
reaction chamber
water-cooled coil
JUMO dTRON Compact Controller
Beam viewer
phase angle controller
Research activities of group via publications since 1972
The number of publications exceeds 350, categorized as follows:
Fundamental ResearchEnvironmental researchMaterial ScienceHuman health Archaeology
Fundamental Research
AuthorsTitlesPublication
S.Farrokhi , D.Moghemi ,
R.Nahavande , M.Pichevar ,
B.Delaunay
Le Van de Graaff de 3 MeV du
Centre Nucléaire de Téhéran
Juillet-Aout ,No. 172, 1972
M.R Khan , A.G Hopkins, D
Crumpoton , (Aston Univ)
Proton induced LX-ray cross-
sections for In ,Sn,Nd,Dy,Pt
and Au
Zeitschrift-fuer-Physik,-A(1978),
Vol.288(2) Page133-137.
Md.R.Khan and M.KarimiKβ/Kα Ratios in Energy
dispersive X-Ray Emission
X-ray Spectrometry,
Vol.9,No.1,1980
F. Shokouhi, S. Fazinic, I.
Bogdanovic, M. Jaksic, V.
Valkovic, H. Afarideh
M-Shell X-ray production
Cross sections of Tb, Ho, Tm
and Lu for protons of Energy
2-6 MeV
Nuclear instruments and Methods
in Physic Research B (1996)15-
18
A.Amirabadi ,
H.Afarideh,S.M.Haji-Saeid ,
F.Shokouhi and H.Peyrovan
L subshell and total M shell x-
ray production cross sections
of Hg for protons of energy
0.7-2.9 MeV
J. Phys. B:At. Mol. Opt.
Phys.30(1997)863-872 .
M.Goudarzi , F.Shokouhi,
M.Lamehi-Rachti, P.Oliaiy
L-sub shell and total M-shell
X-ray production cross
sections of Ta, W, Pt, Au, Pb
and Bi by 0.7-2.4 MeV protons
Nuclear Instruments and
Methods in Physics Research B
247 (2006) 217-222
Measured differential cross section Reactions
23Na(p,p/γ)23Na 16O(d,p0,1)17O
23Na(p,αγ)20Ne 28Si(p,p/γ)28Si 16O(d,d0)16O
24Mg(p,p/γ)24Mg 29Si(p,p/γ)29Si natMg(d,d0)natMg
25Mg(p,p/γ)25Mg 31P(p,p/γ)31P 24Mg(d,p0,1,2,3,4)25Mg
27Al(p,p/γ)27Al 27Al(p,αγ)24Mg 35Cl(d,p0,1,2,3,4-5)35Cl
1) A. Jokar, O. Kakuee, V. Fathollahi, M. Lamehi-Rachti, N. Sharifzadeh, Measurement of deuteroninduced gamma-ray emission cross sections on nitrogen for analytical applications, NIMB,431(2018)25.
2) A. Jokar, O. Kakuee, M. Lamehi-Rachti, V. Fathollahi, Thick target yields of proton induced gamma-rayemission from Al, Si and P, NIMB, 394 (2017) 28-32.
3) A. Jokar, O. Kakuee, M. Lamehi-Rachti, Differential cross sections measurement of 31P(p,pγ1)31Preaction for PIGE applications, NIMB, 383 (2017) 152-155.
4) M. Chiari, et al., Measurement of proton induced γ-ray emission cross sections on Na from 1.0 to4.1MeV, NIMB, doi.org/10.1016/j.nimb.2017.01.043
5) A. Jokar, O. Kakuee, M. Lamehi-Rachti, “Measurement of deuteron induced gamma-ray emissiondifferential cross sections on natCl from 1.0 to 2.0 MeV”, NIMB, 377 (2016) 37-42.
6) H. Rafi-kheiri, O. Kakuee, M. Lamehi-Rachti, “Differential cross section measurement of the natO(d,d0)reaction at energies and angles relevant to EBS”, NIMB, 373 (2016) 40-43.
7) H. Rafi-kheiri, O. Kakuee, M. Lamehi-Rachti, “Measurements of the 24Mg(d,p0,1,2,3,4) and natMg(d,d0)reactions cross sections in the energy range of 1.2–2 MeV for NRA and EBS applications”, NIMB, 373(2016) 63-69.
8) N. Sharifzadeh, O. Kakuee, S. Mohammadi, “Measurements of proton induced γ-ray emission cross-sections on Mg from 1.0 to 3.0 MeV” , NIMB, 372 (2016)109-113.
9) A. Jokar, O. Kakuee, M. Lamehi-Rachti, “Differential cross sections measurement of 28Si(p,pγ)28Si and29Si(p,pγ)29Si reactions for PIGE applications”, NIMB, 371 (2016)37-40.
10) H. Rafi-kheiri, O. Kakuee, M. Lamehi-Rachti, “Differential cross section measurement of 16O(d,p0,1)reactions at energies and angles relevant to NRA”, NIMB, 371 (2016) 46-49.
11) A. Jokar, O. Kakuee, M. Lamehi-Rachti, N. Sharifzadeh, V. Fathollahi, “Differential cross sectionmeasurements of 27Al(p,p/γ)27Al and 27Al(p,αγ)24Mg reactions in the energy range of 1.6–3.0 MeV”,NIMB 362 (2015)138-141.
Recent VDG Lab. publications regarding Nuclear Data
Environmental researchAuthorsTitlesPublication
P.Sioshansi , A.S.Lodhi
and H.Payrovan
Proton Induced X-ray
Analysis of drinking water
samples
Nuclear Instruments and
Methods 142 (1977) 285-287
A. Gharib ;H. Rahimi,
H. Peyrovan, H.N.J
Raofei, H.Taherpour
The Study of trace elements
in milk by nuclear analytical
techniques
Scientific Bulletin of the
Atomic Energy Organization
of Iran (sum1983).
(no.4)p.65-81
A. Gharib, H. Rahimi, H.
Peyrovan, N. J. Raoffi,H.
Taherpoor
Study of trace elements in
milk by nuclear analytical
techniques Al, Co, Cr, Cu,
Fe, Hg, Mg, Mn, Ni, Pb, Rb,
Sb, Se,V, Zn.
Journal of Radio analytical
and Nuclear-Chemistry
articles .(Mar1985).V89(1)
Page31-44.
M.Kasrai
,L.Fozoonmayeh and
H.Peyrovan
Quantitative determination
of gold in ore using energy –
dispersive XRF
Spectrometry
X-Ray Spectrometry, Vol .
17,219-222 (1988)
Environmental research- continued
AuthorsTitlesPublication
H.Peyrovan ,
A.Amirabadi
Heterogeneity measurement
of trace elements
distribution in sheep liver
using the PIXE method
Nuclear Instrument and
Methods in Physics Research
B 109/110 (1996)309-311
H.Peyrovan,
A.R.Karbassi,
F.Shokouhi, P.Oliaiy
Analysis of sediments from
the central part of the
Persian Gulf using PIXE
symposium on harmonization
of health related
environmental, IAEA, 1997,
Page 567-570.
D. Agha-Aligol, S.
Ghorbanzdeh,Mashkani,
P. TajerMohammad
Ghazvini, M. Lamehi-
Rachti, P. Oliaiy, A.
Baghizadeh, F. Shokouhi
Application of Micro-PIXE
for measurement of metals
bioaccumulation by new
strain bacteria
18th International Conference
on Ion Beam Analysis ,
IBA2007 ( Sep. 23rd -28th )
J. Rahighi, P. Oliay, F.
Shokouhi, A. Aghaii, M-
Al-R. Hadjzadeh
The Impact of
Hypothyroidism on mineral
elements in rat's Tissues
using PIXE
International Journal of PIXE
Vol. 17 (2007) 99-106.
Material ScienceAuthorsTitlesPublication
A.Baghizadeh, D.Aligol ,
D.Fathy , H.Ghaforian
Shallow Junction Formation
by Steam Oxidation of As
Implanted Si
International conference on
Physics, 2004, Tehran, Page
305-310
A. Baghizadeh, D. Agha-
Aligol, M. Lamehi-Rachti,
D. Fathy
Formation of enriched As
layer by steam oxidation of
As+ implanted Si
18th International Conference
on Ion Beam Analysis ,
IBA2007 ( Sep. 23rd -28th )
M. Torkiha, M. Lamehi –
Rachti, D. Agha-Aligol , F.
Razi
Microbeam analysis of lateral
inhomogeneity in depth
penetration of Pd in porous
silicon
Nuclear Instruments and
Methods in Physics Research
B266(2008)1507-1510.
A. Baghizadeh, D. Agha -
Aligol, D. Fathy, M.
Lamehi-Rachti, M.
Moradi
Formation of As enriched
layer by steam oxidation of
As+-implanted Si
Applied Surface Science 255
(2009) 5857 -5860
R. Sahraei, G. Motedayen
Aval, A. Baghizadeh, M.
Lamehi-Rachti, A.
Goudarzi, M. H. Majles
Ara
Investigation of the effect of
temperature on growth
mechanism of
nanocrystalline ZnS thin
films
Materials Letters
62(2008)4345-4347
Material Science: Continued
AuthorsTitlesPublication
R. Sahraei, G. Motedayen
Aval, A. Baghizadeh, M.
Lamehi-Rachti
RBS and AFM investigation
of growth mechanism of
nanocrystalline chemical bath
deposited ZnS thin films
Iran – India joint conference in
Nano-Technology, Tehran
(April 2008)
R. Sahraei, G. Motedayen
Aval, A. Baghizadeh, M.
Lamehi-Rachti, A.
Goudarzi, M. H. Majles
Ara
Investigation of the effect of
temperature on growth
mechanism of
nanocrystalline ZnS thin
films
Proceeding of the 2nd
conference on nanostuctures
held in Kish university, 2008
L. Aghli-Moghadam, A.
Baghizadeh, G. Nabiyouni,
A. Farashiani,
A. Zendehman
Zn-diffused LiNbO3
waveguides fabricated by DC
magnetron sputtering
Appl. Phys A (2009)97:805-
810.
O. R. Kakuee, V.
Fathollahi, D. Agha-Aligol,
P. Oliaiy, M. Lamehi-
Rachti, M. Torkiha
Evaluating Refurbishment
quality of hot components in
gas turbines using IBA
analysis techniques
19th International conference on
Ion Beam Analysis, Sep. 2009,
UK
Human HealthA.S.Lodhi,
MD.Rashiduzzaman Khan
Trace element analysis of
whole blood and urine
samples of Diabetic patients
Journal of Radioanalytical
Chemistry , Vol . 49, No . 1 ,
(1979) 89-94
A. Aframian ,H. Shakiba,
A. Housseiney
Trace element analysis of
human hair by proton
induced X-ray excitation
PIXE.
International conference on
nuclear methods in environments
and energy research, Columbia,
1980, page 442-448.
S.Mousavi-Yeganeh ,
F.Ebrahimy-Fakhar and
F.Enayati
Analysis of Addicted and
Normal Blood Samples Form
Humans by PIXE
Nuclear Instrument and
Methods in Physics Research
B3 (1984) 364-367
A.A.Hosseini ,
A.Amirabadi , H.Afarideh
S.M.Haii-saeid,
A.H.Behrozi
Determination of toxic and
non-toxic hair trace elements
in tobacco smokers using
PIXE and NAA techniques
Nuclear Instrument and
Methods in Physics Research B
109/110 (1996)239-242
P.Hatami, H.Peyrovan and
H.Afarideh
Determination of trace
elements in human saliva by
PIXE technique
International journal of PIXE ,
Vol . (1996) 273-276
H.Peyrovan , P.Hatami,
N.Mansourian and
F.Shokouhi
Analysis of liver biopsy
samples for Fe,Cu and Zn
using PIXE
International journal of PIXE
Vol.6,Nos.1&2 (1996) 269-272
Human Health: Continued 1
S.Vatankhah , K.Moosavi
,J.Salimi , L.Geranpayeh
,H.Peyrovan
A PIXE analysis for
measuring the trace elements
concentration in breast tissue
of Iranian women
Iran.J. Radiat.Res .,2003
;1(1):23-27
J.Salimi, K.Moosavi,
S.Vatankhah
The concentration of heavy
trace elements in pigment and
cholesterol human gallstones
:Comparative studies by
PIXE analysis
Iran.J.Radiat .Res.,2003 ;
1(2):93-97
S.Vatankhah ,K.Moosavi,
H.Peyrovan
Comparative Studies of trace
element in two kinds of
human gallstones
International journal of PIXE ,
Vol.13, Nos.3&4(2003) 97-106
J.Salimi , K.Moosavi,
S.Vatankhah, A.Yaghoobi
Investigation of heavy trace
elements in neoplastic and
non-neoplastic human thyroid
tissue : A study by PIXE
Iran.J.Radiat.Res.,2004;1(4):21
1-216
K. Moosavi, S.Vatankhah,
J. Salimi
Measurement of trace metals
in Thyroid nodules in Iran by
PIXE
International journal of PIXE
Vol.16 ,Nos .1&2 (2006) 39-46
Human Health: Continued 2
S.Vatankhah , K.Moosavi
,J.Salimi , L.Geranpayeh
,H.Peyrovan
A PIXE analysis for
measuring the trace elements
concentration in breast tissue
of Iranian women
Iran.J. Radiat.Res .,2003
;1(1):23-27
K. Moosavi, S.Vatankhah,
J. Salimi
Relative measurement of
heavy elements in the bile,
gallbladder and gallston
Iran. J. Radiat. Res. , 2006;
3(4): 195-198
S. Vatankhah, K. Moosavi,
J. Salimi, M. Lamehi and
M. Farmahini Farahani
Study the deficiency of
potassium , Manganese,
cupper and zinc concentration
in the abdominal aortic
aneurism by PIXE analysis
International Journal of PIXE
Volume 17 (2007) 107-112
N Gholizadeh, Z Kabiri, O
Kakuee, M Saleh-
Kotahi, V Changizi, V
Fathollahi, P Oliaiy, R
Omranipour
Feasibility of breast cancer
screening by PIXE analysis
of hair
Biol Trace Elem Res,
153(2013)105-10.
ArcheologyAuthorsTitlesPublication
P.Oliaiy ,F.Shokouhi,
M.Lamehi-Rashti,
J.Rahighi
Application of PIXE to study
ancient Iranian silver coins
International journal of PIXE
Vol.9,Nos3&4 (1999)495-500
A.Hasssanzadeh ,
M.LamehiI-Rashti,
P.Oliaiy, J.Rahighi and
F.Shokouhi
External PIXE analysis of old
inks and papers
International journal of PIXE
Vol.9,Nos.3&8 (1999) 481-485
S.Durali , P.Oliaiy,
F.Shokouhi, M.Lamehi-
Rashti and J.Rahighi
Evolution of the tilework of
Masjid jumah in Isfahan,
based on glaze analysis
Fiftieth Anniversary
Symposium on Scientific
Research in the Field of Asian
Art ,September 27 - 29, 2001,
Washington, D.C.
M.Lamehi-rashti , P.Oliaiy ,
J.Rahighi , F.Shokouhi ,
M.Fakhrai
Application of PIXE in the
analysis of archaeological
glazed tiles
Nuclear Instrument and
Methods in Physics Research B
184 (2001)430-436
F.Shokouhi, P.Oliaiy,
J.Rahighi , M.Lamehi-
Rachti
Elemental Analysis of ancient
Iranian Luster Decorated
Pottery
International journal of PIXE
,Vol .12, Nos.3&4 (2002)253-
258
Archeology: continued 1
P.Oliaiy , F.Shokouhi,
J.Rahighi, M.Lamehi-Rachti
Evaluation of glazed and Body
Composition in Ancient
Iranian Pottery
International journal of PIXE ,
Vol.12, Nos.3&4 (2002) 245-251
I.Bogia , B.Brunetti, A.Giulvl,
A.sgamellottim,
F.,shokouhi,P.oliaiy,J. Rahighi,
M.Lamehi-Rachti, M.Mellini,C.viti
Characterisation of decorations
on Iranian (10th-13th
century)Lustreware
Appl.Phys.A79,257-261 (2004)
S.Ahmadi, F.Shokouhi,
P.Oliaiy, M.Lamehi-Rachti
and J.Rahighi
Characterization of the Wall
Painting Pigments of
Baghcheh Joogh Castle by
PIXE
International journal of PIXE
Vol.15.Nos3&4 (2005)
S. Padovani, D. Puzzovio, C. Sada,
P. Mazzoldi, I. Borgia, L.Cartechini,
A. Sgamellotti, B.G. Brunetti, F.
Shokouhi, P. Oliaiy, J. Rahighi, M.
Lamehi-Rachti,
F.Acapito,C.Maurizio, E.Pantos
XAFS study of copper and
silver nanoparticles in glazes
of medieval middle-east
Iustreware (10th – 13th
Century)
Appl.Physic.A.83,512-528(2006)
D. Agha-Aligol, F. Jalai
Farshi, M. Lamehi-Rachti,
P. Oliaiy, F. Shokouhi
Provenance study of “Nader-
Tepe Aslanduz “ Obsidian
using PIXE method by
multivariate statistical analysis
18th International Conference on
Ion Beam Analysis , IBA2007 (
Sep. 23rd -28th )
Archeology: continued 2D. Agha Aligol, N. Javidnia,
M. Lamehi-Rachti, P. Oliaiy,
A. Baghizadeh, F. Shokouhi
Micro-PIXE analysis of a 240-
year old colored garment
18th International Conference on
Ion Beam Analysis , IBA2007 (
Sep. 23rd -28th )
D. Agha-Aligol, F.
Khosravi, M. Lamehi-
Rachti, P. Oliaiy, F.
Shokouhi
Analysis of 18th- 19th century's
historical samples of Iranian
ink and paper belonging to the
Qajar dynasty
Appl. Phys. A89, 799-805 (2007)
M. Hajivaliei, Y.
Mohammadifar, K. Ghiyasi,
B. Jaleh, M. Lamehi-Rachti,
P. Oliaiy
Application of PIXE to study
ancient Iranian silver coins
Nuclear Instruments and Methods
in Physics Research B266(2008)
1578-1582.
Davoud Agha-Aligol, Parvin
Oliaiy, Mohammad
Mohsenian, Mohammad
Lamehi-Rachti,
FarahShokouhi
Provenance study of ancient
Iranian luster pottery using
PIXE multivariate statistical
analysis
Journal of Cultural heritage
10(2009)487-492
P. Oliaiy, D. Agha-Aligol, F.
Shokouhi and M. Lamehi-
Rachti
Analysis of Iranian postage
stamps belonging to the Qajar
dynasty (18th – 20th Century’s)
X-ray Spectrometry, 2009, 38,
479-486.
Handicraft Raytheon Cup
External PIXE analysis results
External PIXE Analysis Report
Concentration (%) Element
95.9Ag
4.1%Cu
1 µm (Thickness)Au coatingNet Weight: 700 g
PIXE
Omidreza Kakuee, V. Fathollahi, P. Oliaiy, M. Lamehi-
Rachti, R. Taheri, H.A. Jafarian, External PIXE analysis
of an Iranian 15th century poetry book, Nucl. Instr. and
Meth. B273(2012)178-181.
• The characterization of Persian miniature of the Joseph and Zulaikha created in the 15th-16th century in the Bokhara school.
• The required information for preservation, restoration, and authenticity of the masterpiece, the elemental composition of the applied pigments in the miniature paintings as well as the elemental composition of the employed ink and paper was analyzed by external PIXE.
PIXE Analysis of Persian Miniature Used in 16th
Century Poetry Manuscript
O. Kakuee · V. Fathollahi · P. Oliaiy · [...] · M.B. Kasiri
May 2014 · Acta Physica Polonica Series a
Figure shows a vaghf document belonging to the Timurid period (1485 A.D) preserved by the heirs in their private collection. The document includes 11 pices with the total length of the document is about 547 cm when flattened
Artwork
Painted cloth belonging to Zandieh era (r. 1751-1779)
Holy cloth decorated with prayer
that contains 1001 names
and attributes of God
Pigments investigated by microPIXE
The Safavid period (1499-1722 AD), antique carpets
Are known for their: Artistic beauty High quality raw materials Various colors Sometimes decorated by golden threads Hand-woven in the royal carpet workshops
Omidreza Kakuee, Vahid Fathollahi, Parvin Oliaiy, Shokoufeh Mesbahi, Investigation of mordants for dyeing of yarns in ancient Persian carpets (15th–17th century) by IBA methods, NIMB, 450 (2019) 294-298.
• Scholar practitioner
• Capacity building
• PhD Thesis 50
• MSc thesis 170
• Initiating Archaeometry in Country
• International Scientific journal Publications >250
• National Scientific journal Publications >100
summary
Challenges:
The accelerator is no longer able to produce beam with reasonable emittance,
C-RBS and proton microscopy cannot be performed under normal operating
conditions of the machine.
The machine is a 64-year-old, working with this machine is time consuming.
The spare parts are not readily available.
Acknowledge
I would like to thank the IAEA, High Voltage
Engineering Europa BV, and colleagues from IBA
society, sneapers and my pioneers colleagues for their
support.
Thank you very much for your Attention
Persepolis in Shiraz(Takht-e Jamshid)