348E Seventh Generation Natural Dishwasher … Environmental and Compliance, INC. Dear Client:...

Oilfield Environmental and Compliance INC

Dear Client

Enclosed is an analytical report for the above referenced project The samples included in this report were received on 01-Dec-15 1115 and analyzed in accordance with the attached chain-of-custody

Unless otherwise noted all analytical testing was accomplished in accordance with the guidelines established in our Quality Assurance Manual applicable standard operating procedures and other related documentation The results in this analytical report are limited to the samples tested and any reproduction thereof must be made in its entirety

If you have any questions regarding this report please do not hesitate to contact the undersigned

Sincerely

Work Order 1505053

25 January 2016

Project Manager

Meredith Sprister

Heidi DAgostino

301 2nd Street

Woodland CA 95695

RE Consumer Products Bioassay Testing

Yolo County District Attorney

307 Roemer Way Suite 300 Santa Maria CA 93454

TEL (805) 922-4772

FAX (805) 925-3376wwwoecusacom

Project

Project Number

Project Manager

Reported


301 2nd Street [none]

Heidi DAgostino

Consumer Products Bioassay Testing

25-Jan-16 1450Woodland CA 95695


Sample ID Laboratory ID Matrix Date Sampled

ANALYTICAL REPORT FOR SAMPLES

Date Received

348E Seventh Generation Natural Dishwasher D1505053-01 25-Nov-15 1030 01-Dec-15 1115Product

349E ForceField FireGuard Flame Retardant for1505053-02 25-Nov-15 1030 01-Dec-15 1115Product

350E Armorall Leather Wipes 20 Wipes 1505053-03 25-Nov-15 1030 01-Dec-15 1115Product

351E Armorall Glass Wipes 25 Wipes 1505053-04 25-Nov-15 1030 01-Dec-15 1115Product

352E Prestone 5050 Prediluted AntifreezeCoola1505053-05 25-Nov-15 1030 01-Dec-15 1115Product

353E Prestone Concentrate AntifreezeCoolant 11505053-06 25-Nov-15 1030 01-Dec-15 1115Product

354E Argan Oil Hair Color Very Black 3 fl oz 1505053-07 25-Nov-15 1030 01-Dec-15 1115Product

355E Febreze Scented Oil Refill 175 oz 1505053-08 25-Nov-15 1030 01-Dec-15 1115Product

356E Ion Color-Preserving Masque for color tre1505053-09 25-Nov-15 1030 01-Dec-15 1115Product

357E Mane n Tail Shampoo 12 fl oz 1505053-10 25-Nov-15 1030 01-Dec-15 1115Product

358E Mane n Tail Conditioner 12 fl oz 1505053-11 25-Nov-15 1030 01-Dec-15 1115Product

359E Loreal Preference Permanent Haircolor M1505053-12 25-Nov-15 1030 01-Dec-15 1115Product

360E Wella Permanent Liquid Hair Toner T28 N1505053-13 25-Nov-15 1030 01-Dec-15 1115Product

361E Clairol Professional Soy4Plex Haircolor 31505053-14 25-Nov-15 1030 01-Dec-15 1115Product

362E Ion Color Brilliance Temporary Color Mas1505053-15 25-Nov-15 1030 01-Dec-15 1115Product

Oilfield Environmental and Compliance The results in this report apply to the samples analyzed in accordance with the chain of custody document This analytical report must be reproduced in its entirety

Page 2 of 19

307 Roemer Way Suite 300 Santa Maria CA 93454TEL (805) 922-4772FAX (805) 925-3376wwwoecusacom

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit

BatchReporting Prepared Analyzed Method Notes DilutionUnits

348E Seventh Generation Natural Dishwasher Detergent Gel 42 oz1505053-01 (Product)

Oilfield Environmental and Compliance

Microbiological Parameters by CA Dept of Fish and Game

Fail Polisini amp Miller

(CDFG 1988)

05-Dec-15 05-Dec-15PassFail B5L01621Bioassay 96 Hour Screen LC50

00 Fish Mortality Total of 20 750ppm 96-Hr00 Mortality Total of 20 750ppm 72-Hr00 Mortality Total of 20 750ppm 48-Hr

20 Mortality Total of 20 750ppm 24-Hr

00 Mortality Total of 20 400ppm 96-Hr00 Mortality Total of 20 400ppm 72-Hr00 Mortality Total of 20 400ppm 48-Hr


Polisini amp Miller

(CDFG 1988)

602 B6A0005 02-Jan-16 02-Jan-16mgL 1Definitive Bioassay LC50 LC50

Hazardous LC50


Page 3 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


349E ForceField FireGuard Flame Retardant for Fabrics amp Upholstery 22 fl oz1505053-02 (Product)



Pass Polisini amp Miller

(CDFG 1988)


00 Fish Mortality Total of 20 750ppm 96-Hr00 Mortality Total of 20 750ppm 72-Hr00 Mortality Total of 20 750ppm 48-Hr00 Mortality Total of 20 750ppm 24-Hr00 Mortality Total of 20 400ppm 96-Hr00 Mortality Total of 20 400ppm 72-Hr00 Mortality Total of 20 400ppm 48-Hr00 Mortality Total of 20 400ppm 24-Hr

ResultAnalyteLimit


350E Armorall Leather Wipes 20 Wipes1505053-03 (Product)




(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 4 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


351E Armorall Glass Wipes 25 Wipes1505053-04 (Product)




(CDFG 1988)



ResultAnalyteLimit


352E Prestone 5050 Prediluted AntifreezeCoolant 1 gal1505053-05 (Product)




(CDFG 1988)


00 Fish Mortality Total of 20 750ppm 96-Hr00 Mortality Total of 20 750ppm 72-Hr00 Mortality Total of 20 750ppm 48-Hr00 Mortality Total of 20 750ppm 24-Hr




Page 5 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


353E Prestone Concentrate AntifreezeCoolant 1 gal1505053-06 (Product)




(CDFG 1988)


10 Fish Mortality Total of 20 750ppm 96-Hr

00 Mortality Total of 20 750ppm 72-Hr00 Mortality Total of 20 750ppm 48-Hr00 Mortality Total of 20 750ppm 24-Hr00 Mortality Total of 20 400ppm 96-Hr00 Mortality Total of 20 400ppm 72-Hr00 Mortality Total of 20 400ppm 48-Hr00 Mortality Total of 20 400ppm 24-Hr

ResultAnalyteLimit


354E Argan Oil Hair Color Very Black 3 fl oz1505053-07 (Product)




(CDFG 1988)






Page 6 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


355E Febreze Scented Oil Refill 175 oz1505053-08 (Product)




(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


356E Ion Color-Preserving Masque for color treated hair 6 fl oz1505053-09 (Product)




(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


357E Mane n Tail Shampoo 12 fl oz1505053-10 (Product)




(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


358E Mane n Tail Conditioner 12 fl oz1505053-11 (Product)




(CDFG 1988)


00 Fish Mortality Total of 20 750ppm 96-Hr70 Mortality Total of 20 750ppm

72-Hr80 Mortality Total of 20 750ppm





48-Hr00 Mortality Total of 20 400ppm 24-Hr

Polisini amp Miller

(CDFG 1988)


Hazardous LC50


0 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


359E Loreal Preference Permanent Haircolor Medium Brown 5 2 fl oz1505053-12 (Product)




(CDFG 1988)






lt 20 Polisini amp Miller

(CDFG 1988)

06-Jan-16 06-Jan-16mgL B6A01041Definitive Bioassay LC50 LC50

Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


360E Wella Permanent Liquid Hair Toner T28 Natural Blonde 14 fl oz1505053-13 (Product)




(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


361E Clairol Professional Soy4Plex Haircolor 3RN Medium Red-Neutral Brown 2 oz1505053-14 (Product)




(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit


362E Ion Color Brilliance Temporary Color Masque Golden Blonde 15 oz1505053-15 (Product)




(CDFG 1988)


00 Fish Mortality Total of 20 750ppm 96-Hr00 Mortality Total of 20 750ppm 72-Hr00 Mortality Total of 20 750ppm 48-Hr00 Mortality Total of 20 750ppm 24-Hr00 Mortality Total of 20 400ppm 96-Hr00 Mortality Total of 20 400ppm 72-Hr




Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




Result LimitReporting

Units LevelSpike

ResultSource

RECRECLimits RPD

RPDLimit Notes Analyte

Microbiological Parameters by CA Dept of Fish and Game - Quality Control

Batch B5L0162 - BioMicro Prep

Blank (B5L0162-BLK1) Prepared amp Analyzed 05-Dec-15Bioassay 96 Hour Screen PassFailPass LC50

Mortality Total of 20 750ppm 96-Hr Fish00

Mortality Total of 20 750ppm 72-Hr 00



























Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD













Batch B6A0005 - BioMicro Prep

Blank (B6A0005-BLK1) Prepared amp Analyzed 02-Jan-16Definitive Bioassay LC50 mgLND LC50

LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD


Microbiological Parameters by CA Dept of Fish and Game - Definitive - Quality Control



LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




Notes and Definitions

Z-01a ND

Z-01 lt 20

Non-Haz Non-Hazardous

LC50 State of CA limit for Non-Hazardous Designation LC50 gt 500 mgL Pass Screen lt40 dead in 750 mgL (LC50 gt 750 mgL) Fail Screen gt40 dead in 750mgL (Definitive Recommended)Fail Screen [CA Haz] gt60 dead in 400mgL (LC50 lt 400mgL)

Haz Hazardous

_Pass Pass

_Fail Fail

Sample results reported on a dry weight basis

Relative Percent DifferenceRPD

dry

Not ReportedNR

Analyte NOT DETECTED at or above the reporting limitND

Analyte DETECTEDDET


Page 19 of 19


---------------------- Bioassay Definitive Test ~OD OEC-Oilfield Environmental amp Compliance Inc

Polisini and Miller CA Fish amp Game Lab 1988

Hardness EDTA Titrimetric Method SM 2340 C (20th ed)

End point Eriochrome Black indicator solution from pink to blue

Sample Vol (ml) Initial pH pH (100-1001) EDTA Vol (ml) CaC03 mgL

Method Blank 25 Sj~ j () b

LCS (90-110) Crl 10 ~O

Control Initial 15- LQ C)

Control Final ~I - middot0 40 4tx)ppWl Initial lbL t --0 tOJPGM Final - - - 8 V 4U

Calculate as follows Hardness as CaC03 mgL =(mL 001m EDTA used)(CaC03 equivalent to 1mL EDTA) (1000) mL sample

Total Alkalinity as Calcium Carbonate

SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------

LC50 Result oD Z 0 mgL

Chlorine Negative Positive

Hardness

LCS ID -(fb040Y LCS exp 1~b Spike Vol ~o mL

Alkalinity

LCS ID S1oi~ LCS exp ((Jlb Spike Vol 25 mL -

Fish Averages

weigbfo=o---shyLength (mm)

O~middotImiddotmiddotSO 5middot C11~

Sample Vol (ml) Initial pH Normality Stand Titrant Vol to pH 45 CaC03 mgL

Method Blank 2S ~b 010 00 2 LCS (80-120) 9 Y2 22~Lf

Control Initial J)L[ ()~l L~

Control Final ~I 0middot if 1(Slt6 iO()n~ Initial t-bl C)b 52 4Woo(f Final -L - B~ lt 1 lt0

-~lmiddotOY~~3middot rNAf f~l 4lmiddot rI ~

~Y Itlta ~~-O middot12 ~t J 0middot1~1f1middot ~

Omiddotl~l- o lttSSomiddot

SOmiddot i middotbl~ shy

Calculate as follows Alkalinity a CaC03 mgL =(mL standard acid used)(normality standard acid)(50000) mL sample ( j 0middot91 Averages

0

$0 0middotlt64shy

bull shy ~

---- oiL Reviewed and Date_cI _0 II~10

_~~~ushy~i~_ l-~~

~

Definitive Haz Toxicity BATCH Bbmiddotccc6 OEC-Oilfield Environmental amp Compliance SAMPLE 10 505053-() Hazardous Material Bioassay (Static) Sample Received Izcntottj

Polisini and Miller 1988 Start Bioassay ) 02 t Sample Description SOLID I AQ ~D~ End Bioassay (gt ob b

~OO -J _ w~ _ _

ylnitial Readout (i) 24-Hr

-et 1 eM - ()e~ JrvI H I ij il)Readouts

pH DO Temp pH DO Temp M

Control 14 f6~ lb 1middot 5middot1 201 0

lOc) ppm IS ltg~b 03 ) Smiddot1 20) 10

400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to

~oO ppm 76 01 lK3 1 1middot) l1) to

200 JS q~ ~b 1018 1middot1 r~middotDppm

00 ppm 7S lt1~ ~7 11 1middot4shy lormiddot 10

00 ppm J~ Q1 0

lmiddotamp l(p j J tD

SO ppm 5 AmiddotLt ~6 1- IQmiddotO middot3 I

SO rzS qO ~~ smiddotp ferS 1shyppm

20 175 M ~9 1-1 bO 11 0 ppm

20 ImiddotS Fr I~~ 1middot lq bull Imiddot~ 0

ppm

Air Control 11 $0 wmiddot3 0 -

48-Hr

()oL JNl 130 pH DO Temp M

1middotls Smiddot$ 1iJz 0

1 ~middotO l1 -lshy 0

5 5middotl 11middotltb 1

~1 Zmiddot14 9middot1 0

8-1shy yentl WmiddotD ()

) 1 1-04 0

72-Hr 96-Hr

Oiltf5 JtmiddotH 4 30 Oct JM i1 ~1J) pH DO Temp M pH DO Temp M Total M

IS Smiddot1 UHq 0 j 5middot3 tomiddot 0 0

fo

0

10

to

tD

to

81 lt6l 20-0 0 ~ 2shy eg middotif 1middot4 0 I

81shy middot1 1 0 82shy i~ t~) 0 3

8middot1 ~4 100 0 2 ~middotl 11middot1 0 0

8middot2 ~middot3 101 0 tmiddot2 l($ imiddotgshy 0 01

lt1

1 1middot 20~ 0 imiddotO ~ 0 0 JMI il 1)middot2

Comments

Start taking data the

day air is added to

~tanks

95 Confidence IntefYal Method Parameters

Upper 0t lt Z mgL Sample Extraction Mechanical Shaker wI 01 H20

LC50= 0 Z 0 mgL Lower ~Z 3 mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method Graphical I Probit I Spearman-Karber Eed-S~ Control Water Hardness 40-48 mgL CaC03

Feeding None

Temperature Range 18 - 22degC Initial

Day 1 Hardness Alkalinity

Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL

Final Day5 Hardness Alkalinity

Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [

Fish Data Avg Min Max

Length (mm)

50middot llmiddot 5~middot

Weight (g) Omiddot~q 0middot11shy -0

Test Organism Pimephales promelas

Source Anderson Farms

Photoperiod 16hr LighU 8hr Dark

Test Chamber Volume 10L

Number of Replicates 2

Fish per Chamber 10

Tanks aerated None I ~ Aeration Source Outside Air

Aeration Rate (Maintain ~Ogt 4ppm)

Aeration Method narrow glass bore

Test Endpoints Survival at 96 hours

)

)Bioassay Definitive Test Batch Ow AO 104

Sample ID 5()$053 - 03 OEC-Oilfield Environmental amp Compliance Inc PoJisini and Miller CA Fish amp Game Lab 1988 Analyst d M H

Start Date lIiD II (P

LC50 Result Ze-rqi mgL Hardness EDTA Titrimetric Method SM 2340 C (20th ed) ~


CaC03 mgLSample Vol (ml) Initial pH pH (100-1001) EDTA Vol (ml)

1-SlYiethod Blank -lt1 0 0 -1 102LCS (90-110) 301middot0

Control Initial UqI I4l

Control Final Vshy ltis 401middot0- v 5lP ttOOm Initial I 4shymiddotU V y753 JbLtOO rJtrfl Final

~alculate as follows Hardness as CaC03 mgL = (mL 001 m EDTA used)(CaC03 equivalent to 1 mL EDTA) (1000) I mL sample ~-


SM 2320 B (20th ed)

End point pH =45

Chlorine(Negati~ I Positive

Hardness

LCSID 14 D~OIf04 LCS exp - 29 I (p

Spike Vol 2middot0 mL

Alkalinity

LCSID 51101 Y LCS exp IR to middotliP Spike Vol lS mL


Method Blank 1-5 lt- 0middot0 O-Oj 1shyLCS (80-120) 120 1231 14l12 Contra Initial gt 1 0middot11 144shyControl Final - ~ Omiddot(p ~2

UO()pIrn Initial 1middot11 Omiddot Sshy 0 1+00 IIrolYl Fina) I lt53 o~ gO rtO

Fish Averages

Length (mm) Weight (g)

4yenmiddot O-lL s) Omiddot~ flo 1lt( o fu gt Mn

lltiS OmiddotQfp

SOmiddot Omiddot~q pound0

0middot153 5middot omiddot~1

Stmiddot 0middot81

Stmiddot o~O 51 NiD- Omiddot 1 mo~

Averages

SOmiddot Omiddot ltgO

Calculate as follows Alk~jfity as CaC03 mgL (mL standard acid used)(normality standard acid)(50fJJO) I mL sample

l shyReviewed and Date~~ 11(II

------~--- shy

Definitive Haz Toxicity BATCH BfJ 0 1D1I OECmiddotOilfield Environmental amp Compliance SAMPLE 10 r~D)O S 3 - D3 Hazardous Material Bioassay (Static) Sample Received 12-1 1)

Polisini and Miller 1988 Start Bioassay 1 lP 1 ~ Sample Description SOLID I AQ I ~ODU0 End Bioassay l I I 0 [till

Analyst J M H Initial Readout 24-Hr 3 S

Readouts lIP JM H 1500 1 edd 4 pH DO Temp pH DO Temp M

Control 3 9middot3 t1middot 7middot3 54 gb 0

too ppm 1middot3 8-3 1middot 13 44 ro4 2

400 ppm 3 1middot0 ni J4 6 20( 10

1e)O ppm 1middot ~I nmiddotS-4 b 206 0

1pound)0 ppm ~ to-t nmiddot -5 576 ZD~ )

IlOO middot3 1- 3 14 D~4 207 0

middot1ppm

00 14 4~ 20lt6 I ~ ppm 16 1middot)( nmiddot4

S 0 ppm 13 1middot1 11lt JLt JO 20~ 0

so 74 Lt9 lo7 01JJ ppm 13 1 yen t1~S

U) ppm 1middot3 1middot0 nmiddot L 7-f SC) qq 0

fC6 ed4~tr i2S

1middot4 rl q~ 0 ~ 1 q 1J) ppm middot3 Y nmiddoto

Air Control ~middot3 qf nmiddot3 7middot3 56 qt () =

pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~

jq e(~Hr r~ 96-Hr tHo JNH 930

pH DO Temp M pH DO Temp M Total M Comments

7~y 4~ 205 0 3 -I-r 11middot2 0 0 rq 1middot9 216 0 l$l

middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0

11-0 ~middotiv 22S t --

bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0

~2 6[ 2(7 e ~I ~1 middot2middotr 0 0

tlt2 6~7 2LO 0 a 08-t yenO it =6 3Q 20Q 0 0 0

t

js3 ~3 ~i2 ~

6L X)I 0 z Start taking t~ the lt[I ~ lt I tt17 0 0 day air is addeg tel

~samiJCIIlgt C

~

1~ u f c

lt

95 Confidence Interval Method Parameters

Upper ~ mgL Sample Extraction Mechanical Shaker wI 01 H20

LC50= 257 1 mgL Lower l5 tgt mgL Control Water Source Soft Water with Filter for-Chloramine Rmv

LC50 Method Graphical ~I Spearman-Karber I Trimmed-SK Control Water Hardness 40-48 mgL CaC03

Feeding None

Initial Temperature Range 18 - 22degC

Dav 1 Hardness

Control

O ppm

mgL

Stu mgL

IFiSh ID e Z015 15 mgL

bull mgL Fish Data Avg Min Max

Photoperiod 16hr Light 8hr Dark



Fish per Chamber 10

Length (mm) Final Tanks aerated None ~ GOmiddot 4-lu S2middotDay 5 Hardness Alkalinity Aeration Source Outside Air

Aeration Rate (Maintain DO gt 4ppm)

Weight (g)

Control 1-0 mgL l52 mgL

400 ppm -5~ mgL lgO mgL Aeration Method narrow glass bore o~jOlo300 Test Endpoints SUNival at 96 hours

Test Organism Pmephaes promeas


Temperature fluctuations due to extreme temperature drops in the past week I do not believe the

temperature biased test results in either direction Control tanks were set up along-side the test tanks

and there were no mortalities

La)c~ Y (~Je1

~1~ +tolo

----- ---

---

t5atch tUQssay uennmve I est

Sample ID (~

OEC-Oilfield Environmental amp Compliance Inc Polisinj and Miller CA Fish amp Game Lab 1988 Analyst

Start Date

Le50 Result Hardness EDTA Titrimetric Method SM 2340 C (20th ed)

End point Eriochrome Btack indicator solution from pink to blue

Sample Vol (ml) Initial pH pH (100-1001) EDT A Vol (ml) CaC03 mgL

Method Blank -z-S lt11 0 0 102LCS (90-110) 1middot0 00 Control Initial 1middot4~ I I U~

Control Final V -0 4-0lmiddot~ - 3(Ptt-QOtl3fYl Initial Omiddot orOmiddot4) v 010

--shy

ilGl S~t-O O)(JJfI Final ___shy

Calculate as follows Hardness as CaC03 mgL = (mL O01m EDTA used)(CaC03 equivalent to 1mL EDTA) (1 ODD) I mL sample


SM 2320 B (20th eel

End point pH = 45 Sample Vol (ml) Initial pH Normality Stand Titrant Vol to pH 45 CaC03 mgL

-

l-S 0middot0Method Blank 0middot01SII 1shyt 1 31LCS (80-120) 11middot20 241R 2

t1-i 0middot11Control Initial 44shy - umiddot- to

--shy

Control Final 1f~ tS-1 Omiddot to i 3lptJOOpIrn Initial middot4~ I

IYq 012 14L( IiJOO QIOM Final

Calculate as follows Alkalinty as CaC03 mgL standard acid used)(normality standard acid(50jJO) I mLsampe

~

J

Reviewed and - ~ lll Ii lt

DP PI U 1 UJ4L-____ ~OSOS - 0 l( d t1 H I I (j) l (p

I ~3 mgl

Chlorine~ega~ Positive

Hardness

LCS ID UO~OtfO U LCS exp 1 2lt1middot I tp


Alkalinity

LCS ID 5 I 1b I - Y LCS exp LR tomiddot III Spike Vol t-S ~

Fish Averages ___

Length (mm) Weight (g) _J 4-lt6 0middot11

r---~--~---~~ ~

somiddot omiddot 214 I L+tI hA 0 P 3 1111 ityen omiddot Iv

lt0 0middot64shy~Q p 3 ~ D~l Sl O~1

C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~

Definitive Haz Toxicity

DEC-Oilfield Environmental amp Compliance

Hazardous Material Bioassay (Static)

Polisini and Miller 1988

Sample Descrlption SOLID I AQ I EODUsP

Initial Readout 24-Hr

Readouts Itt oM~ ~iO - 3 4S evld pH DO Temp pH DO Temp M

) ry j cr 0Control 13 ~-o 1 )

qoo ppm 1Z laquo1 i 72 [0 105 0

fro ppm 1middot) g~ nmiddotll 7middot2 ilo 106 Iegt

200 ppm 1middot3 ~D 11middot I 7lt3 (2 201 10 12 -5 210 1014)0 1 l1middot L

I ppm 3

too I 1Io 2or6 I ppm 1middot3 omiddot~ tlmiddot 4

) Lt 2 107 01100 1middot3 amp S 1middot1 -I ppm

I 72 Lt~ ~ ()Iso 3 ~ ~ 11middot2gtppm

I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0

ppm 1middot3 11-1shy

w 13 8middot4 1middot2 YJ 2() 0 I ppm 1- J

Air Control -Z rs~ middotiq~ 0)

1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66

eamprr ~2lt 0 DO Temp M pH

5 )(lltt 0 14

61 213 S Iq

lq 214 5 1middot9 lt62 LS () bO

11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0

Temp M pH DO Temp M Total M

C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0

2-L~ 0 8middot3 ~(p 0 to 2~1 () 0 0 ~middot3 20-0 I lo

0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~

0 ~2 imiddot) itmiddot D 0 0

20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks

BATCH 13 (Q AOIOLishySAMPLE 10 I 50Sos 3- 0

Sample Received 121 I I) Start Bioassay iR Illp End Bioassay ItO Ill

JMH

sri hi) )


Upper get 1- mgL Sample Extraction Mechanical Shaker wi 01 H20

LC50= middotB3 mgL Lower s~ is mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method Graphical 181Spearman-Karber I Trimmed-SK Control Water Hardness 40-48 mgL CaC03

Feeding None


o - ---- --____ - Photoperiod 16hr Ughtl8hr Dark- -------- - --I

Control 44 mgL 44 mgL

ppm 30 mgL l3p mgL

- C [IFiSh ID lt 1cC 7 Test Chamber Volume 10L


Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot

~eight (g) O~Q O~3 O~4

Tanks aerated None I All Tanks

Day 5 Hardness Alkalinity Aeration Source Outside Air

Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)

Bioassay Definitive Test

OEC-Oilfield Environmental amp Compliance Inc Polisini and Miller CA Fish ampGame Lab 1988

Hardness EDT A Titrimetric Method SM 2340 C (20th ed)


Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~

53 -H+lmiddoti3 middot4q 1 $5

pH (100-1001)

V 1

v V

1

EDTA Vol (ml)

0 1-Q 0 lmiddotO to ()

CaCOs mgL

0

8)

LiQ tiD

fO U()

Calculate as follows Hardness as CaC03 mgL = (mL 001m EDTA used)(CaC03 equivalent to 1mL EDTA) (1000) I mL sample


SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10

Titrant Vol to pH 45

lt)0 L1 O~C1 Omiddot (p2

051 ObS

Calculate as follows Alkalinity as CaC03 mgL = (mL standard aiid used)(normality standard aCid)(50000) I mL sample

Reviewed and Date ~18 to

CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy

Analyst =ED=D_________

Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL

Chlorine ~egati~ I Positive

Hardness

LCS ID UIOOlt J

LCS exp 2Cfl~ Spike Vol 1--D mL

Alkalinity

LCS ID S 11-011 8 LCS exp 6lolllP Spike Vol zS mL

Fish Averages

Weight (g)

SOmiddot Length (mm)

Omiddot(Sshy5S - fN1tt Omiddot 1 ~

0-13 SOmiddot 53middot

0-10 (Jgsomiddot

4Cfmiddot 0middot(0 S 6 t- omiddotgO41 (Ct omiddot S I rri1

0-52shy4~ 54middot Omiddot 1 i

Averages

o-pSmiddot -

v

Definitive Haz Toxicity BATCH 86A0320

OEC-Oilfield Environmental amp Compliance SAMPLE 10 1505053-09

Hazardous Material Bioassay (Static) Sample Received 12012015

Polisini and Miller 1988 Start Bioassay 01142016

Sample Description End Bioassay 01182016SOLID 1 AQ 1e~ Analyst EDD -

Initial Readout 24-Hr l-e fl 11416 edd 1 IS 11516 -eM gt)

Readouts pH DO Temp pH DO Temp M

Control 3 Q7 b51 14 b2 Iq~ I

I) Rmiddot9 1(1 ~) ~Omiddot fq~ 6750 ppm

)~ qi~ )bq IS rl~ 201 lD 750 ppm

h~ Qmiddot7 bR -~~i 20 ~ 10 500 ppm

IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm

11) 1middot3 1 C1 iIS 61 2tgt~a b 150 ppm

t) Ot7 i 6lt1 IS I 2oJ) L[150 ppm

48-Hr ~

11616 ~ki 5)1 pH DO Temp M

7L t~~3 1)0 0

~

1S LC 2CJO 3 lt ~SJ oJJ Y

l~ (17 Ib~ 111 IbLf 20J I~ --2 ~oC I 75 ppm

J3 eLI )b~ 7middot3 b1 202 6 16 731~O 0 75 ppm

Air Control 14 64 ~9 ) fSrG ~3 10lt J 0

72-Hr 96-Hr

11716 J M H 1 ) 0 11816 J Mt+ 10 0 pH DO Temp_ M pH DO Temp M Total M Comments

1middotlt ijQ 11middot 3 0 1middot4shy Ifmiddot) 2l~ 0 I

0

lO

U)

ID

10

ID

1middot) 1middot0 2(middotL I 10

lc) Ifmiddot1 21 1shy 10

1- l8) Umiddot~ 1 T6 10 2Ho I 4shy

1-1 1- 2t~ 2 lAgshy 71 1middot J 3 Start taking data the

~7 g-l 1S 0 -0 gmiddotr 7bull1-0 0 0 day air is added to

sample tanks


Upper tJ A mgL Sample Extraction Mechanical Shaker wI 01 H20

LC50= ~ bull~ mgL ~ Lower WA mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method Graphical I Probit Spearman-Karber Control Water Hardness 40-48 mgL CaC03~ Feeding None


IFiSh ID


Length (mm) 5 41middot GSmiddot

iWeight (g) ol~ omiddotS 0middot94


I Test Chamber Volume 10L


Fish per Chamber 10

Tanks aerated None I Oay5 Hardness Alkalinity

Final Aeration Source Outside Air




ITest Organism Pimephafes promefas


Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL

Bioassay Definitive Test Batch B6A0356

OEC-Oilfield Environmental amp Compliance Inc Polisini and Miller CA Fish amp Game Lab 1988



Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()

Control Initial 16 V LCJ O Control Final lmiddotOjij V tmiddot 44

~It))Qj V Initial tlL v )middot0 40 ooo~)M Final 10shy 1middot~O 1 L 41

Calculate as follows Hardness as CaC03 mgl = (ml OOlm EDTA used)(CaC03 equivalent to 1ml EDTA) (1000) I ml sample

~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________

LC50 Result it b 2 mgL

Chlorine Negative I Positive

Hardness

LCS 10 L- O(J t

LCS exp i 2 ttb Spike Vol 1-0 mL

Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45

CaC03 mgLInitial pH Normality Stand Titrant Vol to pH 45Sample Vol (ml)

)1 2 L00O-ltJMethod Blank

220L1 LQ~ LOLCS (80-120)

Fish Averages


51 b ~t 41 omiddotID~

5 3middot WlAv omiddot~1 tM)C

SOmiddot O~

53 Omiddot~2 Y v I ( OmiddotS2 w

53middot 0middotamplaquo _+1

bmiddot$4

40ft 0)3 4-17middot D(Pb

Averages

bO- I anl

-0_1 l2ieblControl Initial

1middot Yshy O-VlP i 32shyControl Final 2-2172 O blLtooppV Initial _

JLQ)OOl Final 2lt6Omiddotb~~ill Calculate as follows Alkalinity as CaC03mgll = (mLiitandard acid used)(normality standard acid)(50OOO) I mL sample

Reviewed and Date til 11 ((

Definitive Haz Toxicity BATCH B6A0356

OEC-Oilfield Environmental amp Compliance SAMPLE 10 1505053-10 Hazardous Material Bioassay (Static) Sample Received 1212015


Sample Description End Bioassay 1192016SOLID I AQ I EOD~ Initial Readout I 24-Hr

11516 Qdd b)O 11616 edtA r~)OReadouts


Control I~ ql 7~ 14 bS ~O Q

h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm

hy qO il 7l rsmiddot6 (CO 0 200 ppm

200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm

50 ppm 7middot3 qQ lbg ~ SCf l6 0 7

hy lt10 fbD) II~ b~ S 50 ppm

13 Q2 Ibq tIS bb ~ () 20 ppm

rgtl qr 1l1 75 bS 1 - 0 20 ppm

Air Control 1middotQ ipq ~middotO i Ishy

Analyst EDD-48-Hr 72-Hr 96-Hr

117116 j tH rl lO 11816 J M H to1K 1119116 JM)o q r pH DO Temp M pH DO Temp M pH DO Temp M Total M Comments I

middotr Smiddot lIU () 1middot (qmiddotO 1J 0 1middotl 5middot4 Ltmiddot) 0 0 0

- to

D

LU

()

0

lmiddot~ (p~ 1tmiddotq 3 10

1 1middot0 11middot) 1 1o

middot1 1middot~ 21-S 0 i j imiddot3 2J~ 0 yenmiddotI ~(p llD 0 0

~middoti gmiddot2 21middot 0 8middot i yenS 21middot9 0 middot2 imiddot1 Umiddotl 0 0


~ t ~middot2 11) 0 ~ ~-1 tHo 0 bull 21S e J day air is added to

- sample tanks


Upper tJA mgL Sample Extraction Mechanical Shaker wI 01 H20

LC50= t 02 mgL Lower (l r mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

lC50 Method Graphical I Probit I Spearman-Karber I~n~~V Control Water Hardness 40-48 mgL CaC03

Feeding None

Temperature Range 18 - 22degC Initial a_ ____

Control 40 mgL

IFiSh ID 6010182 IFish Data Avg Min Max

Length (mm) SO 4tu ~3

Weight (g) 011shy OmiddotS2 O~

Photoperiod 16hr Light 8hr Dark --J bull ------- bullbull -1

11 mgL Test Chamber Volume 10L

400 ppm t1L- mgL Number of Replicates 2

Fish per Chamber 10

vt0 mgL

Final Tanks aerated None e Aeration Source Outside Air






Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL

C)Bioassay Definitive Test

OEC-Oilfield Environmental ampCompliance Inc Polisini and Miller CA Fish amp Game Lab 1988



Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______

Analyst EOO_________

Start Date 1152016________

LC50 Result ZJ S3 mgL

CaC03 mgLSample Vol (ml) Initial pH pH (100-1001) EOTA Vol (ml)

ltg 1 V 0 025Method Blank V~O~~ ~OLCS (90-110) 2middot0 V 07middotb Control Initial l-tO V I - 4Control Final 44 v 1[0ISb 0-rfo(JIVl Initial

shy v1)OWM Final ~ 10 Imiddot 0 ~O

Chlorine Negative

Hardness

LCSIO qtAgtV LCS exp [2e b Spike Vol 7-0

Alkalinity

LCS 10 Slo-n LCS exp G 0 t Spike Vol 2S

Positive

mL

mLCalculate as follows Hardness as CaC03 mgL 001 m EDTA used)(CaC03 equivalent to 1 mL EDTA) (1000) I mL sample


SM 2320 B (20th ed)

End point pH =45

CaC03 mgLSample Vol (ml) Initial pH Normality Stand Titrant Vol to pH 45

~) 000010 lt2Method Blank S 10 2202 LOg LCS (80-120)

Oltif 12Control Initial

omiddot (pp1- 9 4Control Final 32 156 2~J)O~(1m Initial 061

i8 (0 Qmiddotl$l ~~9VM Final-- $0---shy

Calculate 2~ rollows Alkalinity as CaC03 mgL = (mL standard acid used)(normality tdndard acid)(50000) I mL sample

Reviewed and Date ljAh-

Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~

4middot Omiddotii 53 Wloyenshy o ~i ((WIJ

sn O~3 53middot O~i-4~ NI (J S2 Myen

S~middot 6iW 41 0middot54 4~middot 0$ 4yenmiddot Omiddot(QO

Averages

SOmiddot I QmiddotIt




Sample Description SOLID 1 AQ I~D~ End Bioassay 1192016

Analyst EDD

Initial Readout ~ r bull 3SV 11516 ~kJ b)() 116116 e lmiddot


Control 7 3 RIi 1SlY 63 ~b 0

qs 72 1J3 ~ )lt60 ylmiddotY 750 ppm

hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I

500 ppm Jy ftl 13 t2 S~ 1-b2 b

~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm

JLt middot3 SJJ Itzql 1~O 0 150 ppm

74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm

Air Control -I bLI ltamp0 I

-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M

1middotlt) ~- 2middotltJ 0

1middot1 19middot0 21-1- fq

middotlI SmiddotO Umiddot3 ltg

lmiddotgshy (psshy 21~ S

1middotgshy 1-0 2Xq p

~middoto rmiddoto 2 2 l

1middotCj - 21middot)

8middot g- ~H-t 0

SmiddotO 1C 2middot2 0

Itgt 0 1S wmiddotj 0

~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr

11816 J M H to 30 11916 J M ~ ~ s-o pH DO Temp M pH DO Temp M Total M Comments

iQ 0

~ ~ 2HpO 1~ t~ llmiddot 0 0 1MoI 1Isshy

10

n 10

1middot1 fpyen 21middot 1shy 1~ 1middot~ Itmiddotj 9 ) t 11middot( ~ 10

~

~ lt

1middot~ 1middotS 2J 4 OJ 1middot1 1middot1 0

7middoti hmiddottp 21middotrshy 1 ~middoto ~2 1lt) 2 (p ~

~ I 8 1 0 ~ g-1 2( ~ I 8middot0 ~ 1 ij 0 8middot1 5gtmiddot4 lV~ I

8middot0 ~S Umiddotf D 55 middot1 ~middotS 11-2 0 0

~iS ~middot1 2lS 0 8middot1 g- 2middot c) 0


~I g1 1) 0 day air is added togmiddott rmiddot7 2J-lP 0 sample tanks


Upper 301 D mgL Sample Extraction Mechanical Shaker wI DI H20

LC50= 1~ 5 e mgL Lower ZOZt8 mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method Graphical e Spearman-Karber I Trimmed-SK Control Water Hardness 40-48 CaC03

Feeding None


IFiSh 10 6010182 Fish Data Avg Min Max

Length (mm)

50middot 4(0middot 53middot

lWeight (g) 0-11 0)2 O~

~ ----

I Photoperiod 16hr Lightl8hr Dark



Fish per Chamber 10

Oay 1 Hardness Alkalinity

Control -10 750 ppm V0

mgL

---mgL

11 mgL

l22 mgL

Tanks aerated None I~ Oay5 Hardness Alkalinity




Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL



Isource Anderson Farms





Batch

Sample 10

Analyst

Start Date

lC50 Result

CaCOs mgLEDTA Vol (ml) pH (100-1001)Sample Vol (ml) Initial pH

Z-S Method Blan k lt11 0 0 v 1)0202LCS (90-110) 1middot0- Control Initial 1middot4~ Uu1middot1 ifControl Final middot0 U-D 1f -~ilq Omiddot~OLl-OOjfV Initial 31 V~pSl 32____0 IlL LtOO Jsrn Final -

A ==-J

1SoSOS3 - It

--------- shy

zD mgL

Chlorine(Negat~ Positive

Hardness

LCS ID t( O~)4() II LCS exp 29middot IIP Spike Vol 1middot0 mL

Alkalinity

LCSID 512011 Y

LCS exp Iemiddottomiddotlip Spike Vol 1) mLCalculate as follows Hardness as CaC03 mgL (mL 001m EDTA used)(CaC03 equivalent to 1mL EDTA) (1000) I mL sample

Fish Averages


SM 2320 B (20th 00)

End point pH = 45

Calculate as follows Alkalil1ly as CaC03 mgL (mL standard acid used)(normality standard acid)(50jvO) I mL sample

Sample Vol (ml) I initial pH I Normality Stand ITitrant Vol to pH 45

___un Blank I 1- S I S-T1 0-01 0-01 LCS (80-120) II 20 I 2 31

Control Initial I W t 0 middot11 ~~

l1s 0 middotllP I s-l

Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J

Definitive Haz Toxicity BATCH f (0 TO lOll-shyOEC-Oilfield Environmental amp Compliance SAMPLE 10 -1 S OS 0 ) 3 - t1 Hazardous Material Bioassay Sample Received 11 f I fie Polisini and Miller 1988 Start Bioassay IlP If (0

Sample Description SOLID I AQ I OD~ End Bioassay t ( I0 I lIP Analyst J HH

Initial Readout

1 24-Hr

11gtReadouts

tfJJ JHH ISW ed ~middotmiddot4S pH DO Temp pH DO Temp M pH

Control 1middot3 3 1middot I) s( qmiddotb 0 15

4-00 ppm 1f(p 9middot3 11middot S tb2 f)) )1 ()

~OO ppm i-(P ~l llmiddotS ~~4 11 ~6 10

LOO ppm amp0 ~( lT3 ilq 7 19 10 10

)JJO ppm 80 ~ D r IT Ji ~l (11 ()

100 ppm lmiddotlfJ ~ n4shy lt 61 Q2 10

wo 3 l1-5 Ibmiddot I qS iO(pppm

amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm

50 ~r 1middot3 11middot lmiddotb iS Q2 10 ppm

20middot ppm lmiddotLt -3 t71 IS 11 lQ2 Lt r

7) b~ q~ Lf 71 1J TmiddottJ ~~ [I

prm

dJr Ifeuro gt - IrCgtt DO Temp M pH

rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr

eel l~~) ItO lnH 0-0 DO Temp M pH DO Temp M Total M

L-tlt6 lOS 0 -3 4middot) 1middot2 D0 10

iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)

Air Control 1- ~lt In3 73 q lltt~ 0 ~O [~ q~ 0 6 F6lj Q 0 1lh

ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I


Iday air is added to

sample tanks fyeno

llO


Upper NA- mgL Sample Extraction Mechanical Shaker wI DI H20

lC50= t 20 Lower VA Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method(dffipF~ Probit I Spearman-Karber I Trimmed-SK Control Water Hardness 40-48 mgL CaC03

Feeding None

Temperature Range 18 22degCInitial

IFiSh ID 6LoS tS Fish Data

Length (mm)

Avg Min Max bull

50middot ltlo S2middot

Weight (g) OmiddotgO Olo3 0middot61




Fish per Chamber 10

Final Tanks aerated None IG Aeration Source Outside Air

Control 1~2 _4QOppm ~)

Aeration Rate (Maintain DOgt 4ppm)



Oay5 Hardness Alkalinity



400ppm 2gt2 mgL Lt(P mgL



----------------------Batch B6A0445

Sample ID _1__ ____ ______----__505053_-1_3 OEC-Oilfield Environmental amp Compliance Inc

Analyst _JM_H____________Polisini and Miller CA Fish amp Game Lab 1988

Start Date 011916 ~-----------------

LC50 Result L ~D mgL Hardness EDTA Titrimetric Method SM 2340 C (20th ed)



0LtMethod Blank 05middot~S 1- 0LCS (90-110)) l)S R-O

Control Initial v I f ~Umiddot1lP 10(0~~ LOControl Final 0vi

~4-DLoQ Initial 1middot~l middot0~

1 lO)Q Final --_ _ __ shy-middot8~ 4QshyCalculate as follows Hardness as CaC03 mgL = (mL 001 m EDTA used)(CaC03 equivalent to 1 mL EDTA) (1000) I mL sample


SM 2320 B (20th ed)

End point pH =45 SampllVol (ml) Initial pH Normality Stand Titrant Vol to pH 45 CaC03 mgL

Method Blank t~ Smiddot~5 0 () OD 2

LCS (80-120) H 1 11middot40 L4SD Control Initial 21 I Dmiddot 12lt0shy1- ~ Control Final -cto 0 sy

i rCO Initial 1middot~1 012shy ~- UOU Final 1middot~3 I shy 0middot1 tp S2

Positive

Hardness

LCSID lfO ) ltb IJ LCS exp f2- lJo Spike Vol 2~O mL

LCSID

LCS exp

Spike Vol mL

Fish Averages

Length (mm) Weioht (0)

5middot 0middot10 UX o iJt1

50 O1~ ll-1 I)middotif Somiddot 0middot15 1) ri( omiddot(ot~

41middot 0middot(0)

SOmiddot Omiddot~~ 50shy O~f

SQmiddotmiddot ~ omiddot91 ~ Averages

lq l bmiddot14

Calculate as follows Alkalinity as CaC03 mgL = (mL stanqard acid used)(normality standard acid)(60000) I mL sample

Reviewed and Date h-t ishy

~

----------------

---

if

Definitive Haz Toxicity BATCH B6A0445 --------------~

DEC-Oilfield Environmental amp Complial1ce SAMPLE 10 1505053-13

Hazardous Material Bioassay (Static) Sample Received 1 I II f Polisini and Miller 1988 Start Bioassay 1 1 1 I lip

Sample Description SOLID AQ ~V End Bioassay 113 iI Analvst- j M H

Initial Readout 24-Hr 72-Hr~Hr u 2-3 ~ 2~20f ~ 11 euu I ~O JMM ~U U) JMtt qSSshy 1Readouts

Total M pH DO Temp pH DO Temp M pH DO Temp pH DO Temp M pH DO Temp M CommentsM

1smiddot1 ~1tS) 2tt~ 1152 It 0 0204 0Control ~4ltS$ )j~ 0 IfSmiddotO~

If)11 2J1tshy~middotlf tgmiddot(1middoti400 ppm 0 10 fOltjyt~r middot1middot1 1l8a~4-00ppm

tbg to~S- 1)1middot S- umiddotOj100 ppm 8 b to11-S 21-0200 ppm 1~middot1 1) fr

-ISshya to(gamptoo ~3 10imiddot0 10-ppm ~middot2 IMh IflJl

T 10) S 102raquo1(00 ppm lLIimiddot1middot4 101O~101middot4shyt~middot)11 10B 150 ppm

(gqfmiddot3 101Dl8middot3 lO1middot~Yfmiddot2sO ppm

10(0) U)~1-3 loftmiddot iP 13middot2ppm ~

f 10lO1middottIt- tol1middotf2f) ppm tu

2- hmiddot4 Start taking data the

3 ~2 ~I~U Lo~ 0 ()I~t~~~ LoI~J 06 to day air is added toAir Control If i 2DY 9 4 samola tanks

10

to


Upper AFA mgL Sample Extraction Mechanical Shaker wI DI H20

LC50= ~ 20 mgL Lower JJ It mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

LC50 Method~ Probit I Spearman-Karber I Trimmed-SK Control Water Hardness 40-48 mglL CaC03

Feeding None


Da 1 Hardness Alkalini IFiSh ID ~()Ol 0 Fish Data Avg Max

Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL

00 ppm ~ mgL l(Lf mglL

Final Tanks aerated None I ~ Day5 Hardness Alkalinity Aeration Source Outside Air

Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL





bource Anderson Farms


OEC-Oilfield Environmental amp Compliance Inc Pofisini and Miffer CA Fish amp Game Lab 1988



Sample Vol (ml) Initial pH pH (100-1001) EOTA Vol (ml) CaC03 mgL

Method Blank ~) poundgSshy 0 0 LCS (90-110) 1- 0) f)o 80 ContraInitial 21P I WI Control Final - etQ Id) 40 400 Initial -00 I 44 I )0 Final

I shy S -02 (middot2 Lamp Calculate as follows Hardness as CaC03 mgfL = (mL 001m EDTA used)(CaC03 equivalent to 1mL EDTA) (1000) I mL sample


SM 2320 B (20th ed)

End pointpH =45


Method Blank l) 5middot1$~ (J (0 Omiddot 0 t 1shy

LCS (80-120) 1ImiddotlP l tmiddot u 0 7U it Contra Initial 1lP OmiddotiPcamp 3 Control Final J~~() C)bl ~Y

4)O Initial ~middotOO o~1- ltL

regO Final 8middot02 0-14 ~~

Calculate as follows Alkalinity as CaC03 mgfLt== (mL standard acid used)(nonnality standard acid)(50000) f mL sample-

Reviewed and Date rf i(0

Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------

LC50 Result L Z 0 mgL

I

Chlorine reurogati~ Positive

Hardness

LCS 10 40 0lj 0U LCS exp middot29 HI Spike Vol lmiddota mL

Alkalinity

LCSIO ~1DlY LCS exp iJ)9 Spike Vol 1~ 0 mL

Fish Averages


b~ 0 l ~ b

middot~iOmiddot ~l l l) Olyen

l) ~14shynil)6b

4shy Dw j () iI) itfnlllmiddot 111

O8ij SDmiddot 50middot

o~r Smiddot M~ O1~tl~

Averages

lq 0-1

----------------Definitive Haz Toxicity BATCH B6A0445


Hazardous Material Bioassay (Static) Sample Received (21 II~

Sample Description SOLID IAQ I ~O~~ End Bioassay 230 II V

Poisini and Miller 1988 Start Bioassay l I

JM - Initial Readout 24-Hr 48-Hr 72-Hr - -- - -- 9S-Hr

Readouts fl~ JMH ~l(O 10 JIH ~f)oS- 1-ecld OSO 11 middote-Jd IOO n2~~ 220 pH DO Temp pH 00 Temp M pH DO Temp M pH DO Temp M pH DO Temp M Total M Comments

Control 1-1 I~ i 80 1gt 10) 10 S () FjS rsit 104 6 IS J2 2U~~ -6 I ~ 2 ct1 0 0

100 ppm middot1 1middot1 ~l OJ 1middot 2-1middot 0 10

WO ppm 1middot ~1 (middot3 1 1middot 3 Itmiddot1 to 10 WJ ~ppm 1middot 5 8middot2 ~~ (0 1 2l to 10

100 ppm 1middot) 0-0 middot4 middotlJ 1-1 1l 10 10

100 ppmh ~ 0 Wmiddot$ 1 S 1middoty 2middot3 0 (0

tO ppmhmiddot ~ 8~ 1middot 11middot) 11 1))11 3 7 b ~ )Cl~ 7 to- to

toO ppm 1middot4 ~ b 8middot~ 1-(0 21middot2 to 10

1JMI-I

50 ppm lt3 g j )0 1middot lI1 21)middot3 1 lmiddotb H~- tG6 rB lO

1)) ppm 1middot 3 ~1 imiddotO lr (p 1J)y 0 17~ ~i lq~ IS [8J t~ 2u~ 36middot Lr3J lQ2 0 ~

W ppm 1 middot0 l~oO lr jg 20 0 11 1~ IClC) is ~O ~x) 2us 2 ~2 60 1C5 b I ~ 1~4 10~ () ~ r 10 Qt ~ - Start taking data the

Air Control 13 g1 1)Y 0 10 10 0 l ~t bull iq~ 0 ) day air is added to l samole tanks

95 Confidence tntelVat Method Parameters

Upper JJ A mgL Sample Extraction Mechanical Shaker wi DI H20

LC50= L to mgL Lower -AI~ mgL Control Water Source Soft Water with Filter for Chloramine Rmvl

lC50 Method Graphical I Probit I Spearman-Karber I E~ Control Water Hardness 40-48 mgL CaC03

Feeding None


Control 4) mgL mgL

400 ppm ~~ 111gIL -- -shy mgL

IFiSh 10 (Q~~tl


Length (mm) r~kmiddot4151 Weight (g)

~ light 79 65 99 I

Photoperiod 1eurohr Light 8hr Dark


Alkalinit

JCp mgLI ~n mgL

j mgL 6j mgL Number of Replicates 2

Fish per Chamber 10

Tanks aerated None iAlI Tanks


Final Aeration Source OutSide Air




Test Organism Pimephaies promeias


bull OFFICE OF THE DISTRICT ATTORNEY Please send results to

YOLO COUNTY Name Investigator Heidi DAgostino

301 2nd Street Email heididagostinoyolocountyorg

Woodland California 95695 Fax 530-666-81a5 -------shy -~ Telephone (530) 666-3424 Fax (530) 666-S423

-----------

Testing Facility sa~I~i~~ner 0

Facility name Oilfield Environmental amp Compliance Inc = li

~ ~Facility address 307 Roemer Way S E z CHAIN OF CUSTODY RECORD ~ 12 iSanta Maria CA 93454 ~ ji= e 0 8

Facility contact Meredith Sprister Project Manager Q) gtshy

ig shy 4i Egt ~ ~ ~~ Ii Q

E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5

II o 0 01 eshy ~jiDescrlptlon J 0 W 2 sample Number

Manufacturer UPC Quantlty Main Ingredient I Or Usage I NOTES S S ~~ ~l 0 _ shy I ltgt ~ ( ~ 0

c F 2 8 Seventh Generation Natural DIShwasher

IS-COlti~___348E __~~eIJ42oz Sevent GeneratJ~ryII)_~ 732913221714 1 liquid ~(201S 1030 AM na 200gimin) P N N X ForceFleld FireGuard~Aam-e -Repoundardant for Fabrics

349E_ amp Upholstery 22 f1 02 Shield Industries Inc~~ 609052130224 1 liquid 2A 112520l 1030 AM na 200gimin) P N N X The Armor AIlSTP

------c-I---

350E Armoral L~a~~~~~~ipe$ 20 wipes Products Co 070612108814 1 solid 3t~ 11252015 1030 AM na 200g(minl P N N The Armor AIISTP

~ ____ 3_51E Armoral Glass Wipes~ 25 wipes Products Co 070612108654 1 solid lA 11252015 1030 AM na 200giminl P N N X Prestone 5050 Prediluted AntifreezeCoolant 1 Prestone Products

352E al Corporation 797496871671 1 liquid I5A 11252015 1030 AM na 200gimin) P N N X Prestone Products

353E Prestone Concentrate AntifreezeCoolant 19a1 Corporation 797496871572 1 liquid (QA p252015 1030 AM ofa 200gimin) p N N X-shy --~~-~~

3S4E Argan OLtt~ir Color Very Black 3 fl OZ One-nOny 074108258342 1 liquid 1A 11l25~ 1030 AM ~ 200g(min) C N N _X --~-~-- ~~~~

355E Febreze Scented Oil Refill 175 02 Proctor amp Gamble 037000461036 2 Ilquid EA-B 1125f201_5~ ecce lO30AM ~ 200g(min) C N N X Ion Coor~Prese~rving Masque for color treated

-shy

356E hair 6 fl 02 Ion Professional Products 033102833349 1 liquid OJ 1l252015 1030 AM na 200gimln) P N N X ----shy

Straight Arrow Producis~~~ ---shy

PIlt357E Mane n Tail Shampoo 121102 Inc 071409543214 1 liquid 11252015 1030 AM na 200gJmin) P N N X -shy --~-~-

Straight Arrow Products

358E Mane to Tail Conditionerp 12 fI OZ Inc 071409543221 1 liquid IIAshy 1l252015 1030 AM nJ 200gimin) P N N Xc-------shy loreal Preference Permanent Hairc~oror Medium

359E Brown 5 2 fl 01 Loreal USA Inc 657201010255 2 liquid i~A-6 112Sz015 1030 AM na 200gimin) P N N X Wella Permanent Liquid HairToner T28 Natural

I3A-lt360E Blonde 14 fl 02 T~~_~~~~~rDoration 070018066909 3 liquid 11252015 1030 AM na 200gimin) C N N X --Claiml Professional Soy4Plex Haircolor 3RN

361E Medium Red-Neutra18ro~~J ~ ~~_~_~__ ___ ~~~~~ Proctor ampGamble -shy 381519024153 2 iquid ltA-6 11252015 1030 AM ~~OOJ1imi~) C N N X Ion Color BriUianceTemporary Cofor Masque~

__~E Golden Blonde 1501 ~~f~~si~_~~I_~~~~_~~ ~821605 2 liquid V i) A-igt 11252015 1030 AM na 200g(min) C N N X ---~-

na -~~-

200g (min) N N X ---shy ----shy

na 200gimin) N N X ~~~~~

i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X

NOTE All Samples were taken at 3012nd St Woodland CA 95695

re Time Remarks ~~ mi Relinquihedmiddot ~~~lSecr~~ 12s1ts lC-3Q AM Received by

Relinquished by tl p) () f( ISshy~-~~=ti==-shy 6ceshy)~IrG t~Ui(flI(ftJ firReceived by

Relinquished by ______---_________

Received by

CLIENT D Lc ~ -oA WORK ORDER tSODS TEMPERATURE 13(0 q degC SAMPLE RECEIPT Acceptable Range OmiddotC to 6middotC [see exception notes below]

CDC RECEIVED DATEfTIME (tlotll~ IllS- LOGIN DATEfTIME I01 fry II 51 REFRIGERATOR(S) r3

SAMPLE TRANSPORT SAMPLE RECEIPT CONDITION PRESERVATION YES NO NlA (J OEC PRES ID

o OEC CourierSampler o Samples Received Outside Temperature Range [Acceptable] COC Document(s) Received With Samples ~ D 0 o Delivery (Other than OEC) o Direct from Field on Ice Correct Container(s) for Analysis Requested IKl 0 0 o After-Hours Outside Drop-Off [Brought Insiele] o Ambient Air or Filter Matrix Container(s) Intact and in Good CondHion IZl 0 0

InitialsiDatelTime o Received Ambient Placed on Ice for Transport Container Label(s) ConSistent with COC ~ 0 0

00 Shipment Carrier lAPS o Sample Temperature Acceptable for Analysis Requested Proper Preservation on Sample Label(s) 0 0 [1J

Tracking 1tIY1 Sw 03 c83 3lc 28 lEI Samples Received Outside Temperature Range [Exception] OEC Preservative Added 0 0 ~

CUSTODY SEALS o None Present o See Problem Chain VOA Containers Free of Headspace 0 0 t9 Cooler(s) 0 Present Intact 0 Present Not Intact 0 None ~ Insufficient Ice or Unknown Cause Tedlar Bag(s) Free of Condensation 0 Omiddot ~ Sample(s) OPresent Intact 0 Present Not Intact 0 None o Expedited PM Notification [lnitlDatelTime] () PROBLEM CHAIN FORM REQUIRED

CONTAINERS COC CHANGES ANDOR CORRECTIONS OEC

CONTAINER DESCRIPTION CHECKS

MATRIX COMMENTS INITIALS CONTAINER ID

PRESERVATIVE cr S amplor pH

1Ashy r- i I- h L-V ( -12 0-2 PtMri(Ji517ipound P CJeiGNklshy fl-tJ)ampU1 CblfjftzlJ6e

ZAshy (72( lt 5f2tUl-1 jTTlI)

3 -YA ~ lIc Dlle6)Stgt rJ 5loft lmiddot~~IJlw-tA~ PoW 6tshy -1fT 12-5 Mi- fa Lv (qb ~l-iLvBe

SA-B 2 pLfjTf( BAamps (2- 2pj( ~Fl)) - r-

C(A ( EH ftJJj

6 ~I ~ shy 25b 1gtIv~ftJLY ~A 6sS l f37~ - r-~

12A- )3 2- Go ML fbGj ~

13A-( 3- S() I L hLYf (N$IOG ox )

itA-8 2- 20 tshy Po~Y7 (21 TCASB)

~Ir-B 2- 4z foi-y ( s lt TlA8e-) V V

Rev 0912512015

RECEIPT LOGIN BY ~ RECEIPT REVIEWED BY 0 Page ---l of

-- -- - --- ---- -

--

bull Testing Facility

Facility mime Oilfield Environmental amp Compliancel Inc

Facility address 307 Roemer Way

Santa Maria CA 93454 FacUity contact Meredith Spristerl Project Manager

OFFICE OF THE DISTRICT ATTORNEY YOLO COUNTY

30I 2nd Slreel Woodland California 95695

Telepbone (530) 666-8424 Fax (530) 666-8423

CHAIN OF CUSTODY RECORD

ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description

seventh Generation Natural Dishwasher

Manufacturer UPC Quantity Main Ingredient I Or Usage I NOTES

348E Dete ent Get 42 oz Sevent Generation Inc I shy __C ForceFleld FireGuard~ Flame Retardant for Fabrics

~ _ amp Uholsterv 22 fI oz Shield Industries Inc The Armor AIISTP

350E IArmorall Leather Wipes 20 wipe Products Co 10706121088JA---1_ The Armor AII7$TP

solid

35iE

952E

353E

354E

355E

356E

357E

358E

rn=~~~~~~~~~-=~~=C~lt1~=~2~ct=n~~~~~dUct-s-- 070~1_2_1_08_6_54_~__-=_ solid

Prestone Concentrate AntifreezeCooJant~ 1 gal

Argan 011 Hair9gtIor Very Black Sf oz

Febrez Scented Oil Refill 175 oz Ion CoTOr-Preserving Masquefor colortreated hair6 fl OZ

Mane In Tail Shampoo 12 fI 01

~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~

Corporation 7974968Tl572 liquid

OnelnOnJv 074108258342 liquid

Proctor amp Gamble 037000461036

Ion Profsslonal Products 1033102833349 1 Straight Arrow Products

r---~----

Straight Arrow Products --~-

Mane n Tail Conditioner 12 II oz _ __ Inc 071409543221 liquid

Inc 071409543214 IiqUldiO~11252015

loreal Preference Permanent Haircolor Medium

Brown 5 2ft oz Lore1 USA Inc 657201010255 liquid -----EA-fgt3S9E

360E Walla Permanent Liquid HairToner~ T28 Natural

Blonde 14 fI oz The Well Corporation 07001806(909 3__ liquid __

361E

362E

Clairol Professional Soy4Plex HaircolorJ 3RN Medium Red-NeutralSrown 2 OZ Proctor amp Gam~_ 381519024153 2 Ii uid lonColorBriliianceTemporaryCo[orMasquEl

Golden Blonde 150 Ion ProlossionalProducts 033102821605 2 liquid Y

1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-

Please send results to

Name Investigator Heidi D1Agostino

Email heidLdagostinoy6locountyorg

Fax 530-666-8185 p S

~ ~ ~ ~ ~ ~ middotI~ E Z 11~~ ~ ~ (i ~0 ~=a~ u 88 8z ~ euroE Q~ u -i - ~ ei ~sect ~ l ~ 8 0-8 ~~ amp-s8 02 ~~ ~ C05 ~g ~cr ~i ~ ltJ f) a _ tl

na f 200g (min ~P tN I NI X

I ~

-----I=_1-20Oirlmin) P N N X I u

n 200g(mi1 X W~ I PIN Imiddot~ 11252Q15 ___ 1030 AM nfa 200g(min) N N X

N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p

A11252015 200g (minl_t C juNjuNt ~X_~ ltA~ _illl~015 200 (min) N N X

1030 AM na 2DOg (mio) P N N X b-- --- --~ -- - -- --~

11 1030 AM n 200 (min) P N N X It

103QAM n~a 200g (min N N X D 13A-c 1112512015 1030 AM na 200g (min) C N N X I

I I 1 I lA -e 1030 AM 0 200 (min C N N X I I----I - shy -~ () A-6 i 1030 AM na 200g (min) _ C N ___N X

--InLa~200g (min I I N N X

--il------- --- _~g(mlnLl_ I N I N I

f=--rIllrrgti11Lf-+~~~ N N X

na 200g(minl x NOTE All Samples were laken at 3012nd St Woodland CA 95695

~~ Title re Time Remarks bocd fJYl l21qll~ Relinquished ~~~(d secretAry 12~ iQ-30 AM Received by

Relinquished by Vt p () ( ISshy-==~~~=jjj==----shy 66c-shyReceived by 5tM-IA Z~fVfIIlb Ifltr

Relinquished by ____________________

Received by

bull OFFICE OF THE DISTRICT ATTORNEY

YOLO COUNTY 301 2nd Street

California 95695 Fax (530) 666-8423

Testing Facility

Facility name Oilfield Environmental amp Compliance Inc


CHAIN OF CUSTODY RECORDSanta Maria CA 93454 Fadlitv contact Meredith Spristert Project Manager

Ll Description Manufacturer

Sample Number UPC Quantity Main Ingredient I Or Usage I NOTES

Seventh Generation Natural Dishwasher 348E Detent Gel 420z Sevent Generation Inc 732913221714 1 Hquid IS-G SoSl- i A

ForeeField FireGllard Flame Retardant for Fabrics 349E amp Upholstery22fLo_ ____________________________ Shield Industries Inc 609052130224 1 liquid 2A

The Armor AIistP-shy -----shy

350E Armorall Leather Wipes 20 wipes Products Co 070612108814 1 solid 3 The Armor AIISTP

351E Ar-moral Glass Wipes 25 wipes Products Co 070612108654 1 solid ~A Prestone 5050 Prediluted AntifreezeCoolant 1 Prestone Products

352E gal Corporation 797496871671 1 liquid 15A Prestone Products

353E Prmone Concentrate AntifreezeCoolant 1 gal Corporation 797496871572 1 liquid 1lt2 A

354E Argan Oil Hair Color Very Black 3 f OZ One nOnly 074108258342 1 liquid 11

355E Febreze Scented Oil Refill 175 oz Proctor amp Gamble 037000461036 2 liquid bA-B Ion Color-Preserving Masque for color treated

~A356E hair6 fI oz Ion Professional Products 033102833349 1 Ii uid Straight Arrow Products

357E Mane n Tail Shampoo 12 fl oz Inc 071409543214 1 liquid iCPlt Stra Ight Arrow Products

358E Mane n Tail Conditioner~ 12 fI oz Inc 071409543221 1 liquid ill loreal Preference Permanent Haircolor~ Medium

359E Brown 5 2 II OZ Loreal USA Inc 657201010255 2 liquid iZk6 Wella Permanent liquid Hair Toner T2B Natural

fM-c360E Blonde 14 II oz The Wella Corporation 0700l8066909 3 liquid Ctafrol Professional SO-v4Pfex Halrcotor 3RN

f I-e361E Medfum Red~Neutral Brown 2 oz Proctor amp Gamble 381519024153 2 liquid Ion Color BriilfanceTemporary Color Masque

362lt Golden Blonde 1S 02 Ion Professional Products 033102821605 2 liquid Y is A-fgt


Name Investigator Heidi DAgostino

Email heididagostinoy6locountyorg

Fax 530-666-8185 Sple

- t]II ili r 5 EaDpound ~ aog

c to 0 ]i~ Q 88 ~u

~g shy it ~

cshy~~ 0 -gtshya a EV shy

O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N

112Sizo15 1030 AM na 200g (min) P N N

11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N

nta 2()degltjmin) N N

nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6

NOTE AI Samples were taken at 3012nd St Woodland GIl 95695

Remarks (~ Relinquishedb ~~ lO3pound) AM~~teg~l s1crefary l[2s1 IS

Time

Received by

Relinquished by ll p) () e IS-Received by -~-~~-i~--_-)i=--- 5ttMIAf ZfFUfWItlfi Ifrr 6Ecshy

Relinquished by ________________

Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




Sample ID Laboratory ID Matrix Date Sampled

ANALYTICAL REPORT FOR SAMPLES

Date Received

348E Seventh Generation Natural Dishwasher D1505053-01 25-Nov-15 1030 01-Dec-15 1115Product

349E ForceField FireGuard Flame Retardant for1505053-02 25-Nov-15 1030 01-Dec-15 1115Product

350E Armorall Leather Wipes 20 Wipes 1505053-03 25-Nov-15 1030 01-Dec-15 1115Product

351E Armorall Glass Wipes 25 Wipes 1505053-04 25-Nov-15 1030 01-Dec-15 1115Product

352E Prestone 5050 Prediluted AntifreezeCoola1505053-05 25-Nov-15 1030 01-Dec-15 1115Product

353E Prestone Concentrate AntifreezeCoolant 11505053-06 25-Nov-15 1030 01-Dec-15 1115Product

354E Argan Oil Hair Color Very Black 3 fl oz 1505053-07 25-Nov-15 1030 01-Dec-15 1115Product

355E Febreze Scented Oil Refill 175 oz 1505053-08 25-Nov-15 1030 01-Dec-15 1115Product

356E Ion Color-Preserving Masque for color tre1505053-09 25-Nov-15 1030 01-Dec-15 1115Product

357E Mane n Tail Shampoo 12 fl oz 1505053-10 25-Nov-15 1030 01-Dec-15 1115Product

358E Mane n Tail Conditioner 12 fl oz 1505053-11 25-Nov-15 1030 01-Dec-15 1115Product

359E Loreal Preference Permanent Haircolor M1505053-12 25-Nov-15 1030 01-Dec-15 1115Product

360E Wella Permanent Liquid Hair Toner T28 N1505053-13 25-Nov-15 1030 01-Dec-15 1115Product

361E Clairol Professional Soy4Plex Haircolor 31505053-14 25-Nov-15 1030 01-Dec-15 1115Product

362E Ion Color Brilliance Temporary Color Mas1505053-15 25-Nov-15 1030 01-Dec-15 1115Product


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 3 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 4 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Page 5 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)




ResultAnalyteLimit






(CDFG 1988)






Page 6 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 4 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Page 5 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)




ResultAnalyteLimit






(CDFG 1988)






Page 6 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






Page 5 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)




ResultAnalyteLimit






(CDFG 1988)






Page 6 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)



ResultAnalyteLimit






(CDFG 1988)






of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)




ResultAnalyteLimit






(CDFG 1988)






Page 6 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)




ResultAnalyteLimit






(CDFG 1988)






of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 7 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 8 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)










Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 9 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


Page 10 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)









Polisini amp Miller

(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 11 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 12 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


Page 13 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)







(CDFG 1988)


Hazardous LC50


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






Page 14 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino




ResultAnalyteLimit






(CDFG 1988)






of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































Page 15 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD

































of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 16 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD















LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


Page 17 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


LC50 Non-Hazardous



LC50 Non-Hazardous


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


Page 18 of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino





Units LevelSpike

ResultSource

RECRECLimits RPD





LC50 Non-Hazardous


of 19


Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


Page 19 of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

Project

Project Number

Project Manager

Reported



Heidi DAgostino





Z-01a ND

Z-01 lt 20



Haz Hazardous

_Pass Pass

_Fail Fail



dry

Not ReportedNR


Analyte DETECTEDDET


of 19








LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by







LCS (90-110) Crl 10 ~O





SM 2320 B (20th ed)

End point pH = 45

Batch B6A0005

Sample 10 --1=505-=053--01_______________

Analyst -=E=D-=-D__________

Start Date 01022015 ~~~~-------



Hardness


Alkalinity


Fish Averages












0

$0 0middotlt64shy

bull shy ~


_~~~ushy~i~_ l-~~

~



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by



~OO -J _ w~ _ _






400 ppm 75 ~7 Icg3

11 1middot 2JJ~ to




00 ppm J~ Q1 0




20 175 M ~9 1-1 bO 11 0 ppm


ppm


48-Hr







) 1 1-04 0

72-Hr 96-Hr



fo

0

10

to

tD

to





lt1


Comments


day air is added to

~tanks





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None



Control

~()) ppm

l() mgL

Lt mgL

1lt mgL

S2shy mgL


Control -

100 ppm

O mgL

4pound1 mgL

lttgte mgfL

1-~o mgL

[FiSh 10 5110S IS [


Length (mm)








Fish per Chamber 10





)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

)












SM 2320 B (20th ed)

End point pH =45


Hardness



Alkalinity





Fish Averages



lltiS OmiddotQfp



Stmiddot 0middot81


Averages




------~--- shy







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by







400 ppm 3 1middot0 ni J4 6 20( 10



IlOO middot3 1- 3 14 D~4 207 0

middot1ppm





fC6 ed4~tr i2S



pH DO Temp M

7S ~ qt 0

7 ( l20 C

1lt1 Iq 2tb ()

~O ~3 2LO e ~1 Cf 210 0

~ () lt6~2 2tO 0

~J ~~ 1-09 0

~l ~S 20~ 0

202 0

ltbO ~g q~ 0 ~




middot9 j~ 21-2 0 2-

D I

1()

~ 1 ~y 2~ 0 9-0 0 I22-2 ~$O lt6b 2J( 0


bO 71J tL( 0 1- i~ uS 0 I

DQ O~b 2L7 () 5 0 21middot1p~q 0 0



t

js3 ~3 ~i2 ~


~samiJCIIlgt C

~

1~ u f c

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

lt





Feeding None


Dav 1 Hardness

Control

O ppm

mgL

Stu mgL






Fish per Chamber 10



Weight (g)








La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by




La)c~ Y (~Je1

~1~ +tolo

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

----- ---

---


Sample ID (~


Start Date






--shy




SM 2320 B (20th eel


-



--shy




~

J



I ~3 mgl


Hardness



Alkalinity


Fish Averages ___


r---~--~---~~ ~



C3 0 80 02middot (MA~ 0 1$4 JV~

Averages

5D 0 ~_O___~~~












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by












I ppm 3




I 1 ~ S 209~lt 00 ppm -3 ~q 12shy

10 gg 12 bD LtO 0




1middot3 1-) l1J- ~

~ pH

tes

~

71 J6 7q

middotl~

1middot9 lt9 lt66


5 )(lltt 0 14

61 213 S Iq


11 2Lt S 15J)

lt6i~ 209gt 0 6Q

~3 201 0 ~n

~~ JC1g 6 fbj

eJd2 -H r

DO

t~

IS

~ ~S ttl

~vmiddotO

tJ 6L 12~~

Ollt

~~-- -I--~

96-Hr IrSb 10 Jr-1t1 4-0


C1tlti( 0 middot3 4-) 12 0 0

0

it)

eO 0


0 1 9middot0 20-0 0 0

V C 0 I

8middot0 ~2 ~

Ltl 0 1lt(-2 0 0g-2 ~


20 1 0 zZ 0g ~t l-H 0

Comments

e


day air is added to

sample tanks



JMH

sri hi) )





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None




ppm 30 mgL l3p mgL



Fish per Chamber 10

Final

IFish Data i

Avg Min Max

Length (mm)

50 lJlP 62middot




Control 40 mgL

ppm mgL









La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by




La)c~ Y (~Je1

~1~ +tolo

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

---------

-)





Method Blank

LCS (90~110)

Control Initial

Control Final

lSdegP9VaI Initial

IltOPOVA Final

Sample Vol (ml)

lS

J-

Initial pH

ltmiddot~b ~~


pH (100-1001)

V 1

v V

1

EDTA Vol (ml)


CaCOs mgL

0

8)

LiQ tiD

fO U()



SM 2320 B (20th ed)

End pointpH =45

Method Blank

LCS (80-120)

Control Initial

Control Final

JS)DP~ Initial

i50PV~1

Sample VOl (ml)

TS

-I shy

Initial pH

S~1)lta ~O 15 ) ~3

lmiddot4Ot 7S)

Normality Stand

()10



051 ObS



CaCOs mgL

~ tZ2d 16 t14 y sQ

Batch B6A0320 ~~~---------------

Sample ID 1505053-09______---shy


Start Date 1142016

LC50 Result ~~~-----------

QO11 mgfL


Hardness

LCS ID UIOOlt J


Alkalinity


Fish Averages

Weight (g)




0-10 (Jgsomiddot



Averages

o-pSmiddot -

v












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by












IJ~ Q7 61 IS Cb 202 D 500 ppm

5 G7 ~bl) IS ~j 20~ to 300 ppm

3 ~l 7 I~b fi5 L20S 0 300 ppm



48-Hr ~


7L t~~3 1)0 0

~





72-Hr 96-Hr



0

lO

U)

ID

10

ID






sample tanks






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by






IFiSh ID







Fish per Chamber 10








Oay 1

Control

fo ppm

Hardness

40 mgL

40 mgL

Alkalinity

lt mgL

y mgL

Control

150 ppm

40 mgL

mgL

114shy mgL

mgL





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Method Blank

LCS (90-110)


0 ~D

25 5 203

V 1

CmiddotOO

~()




~~~------------------------------------Sample I D 1~50=5~05=3--10_______________________________

Analyst -=EDD_________________________________________

Start Date 115=2016____________________________



Hardness

LCS 10 L- O(J t


Alkalinity

LCSIO Y2C)I~ I

LCS exp b () I

Spike Vol ltLS mL I


SM 2320 B (20th ed)

End point pH =45



220L1 LQ~ LOLCS (80-120)

Fish Averages




SOmiddot O~



bmiddot$4


Averages

bO- I anl












h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by








h4 ~S I~S 113 ~D ltt 0 )0400 ppm

1 fi$ 12[72 llO 60 to 400 ppm


200 ppm I1J-t Q2 tI h) 40 1Q 10

h1( f6 q 10 72 lO 1) I 0 100 ppm

14 ~9 16 L ~l g1 0 100 ppm









- to

D

LU

()

0







- sample tanks





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None


Control 40 mgL







Fish per Chamber 10

vt0 mgL







Day 5

Control

400 ppm

Hardness

Lq mgL

ViC mgL

Alkalinity

-2 mgL

2 mgL





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Batch -=B6AO356=--_______

Sample ID 150~5~053-11_______


Start Date 1152016________





Chlorine Negative

Hardness


Alkalinity


Positive

mL



SM 2320 B (20th ed)

End point pH =45








Fish Averages

Length (mm)

Stmiddot Weight (g)

omiddot~




Averages






Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Analyst EDD





hY ql 72 71 40 ~ (J ~ 750 ppm

lY 11 112 500 ppm

17 LjQ rtJ I


~1 1Y 17~3 s) 1~3 67middot4 300 ppm

)1 11 tL 73 SS i~3 0 300 ppm


74 q) 11() 73 ~~q YiJ 6 150 ppm

4 91 11lt0rt) b) $1gt 0 75 ppm

1 ql iI 1 1~ h-O t) 0 75 ppm


-shy ~L

48-Hr

11716 J~H 121 ( pH DO Temp M








8middot g- ~H-t 0



~ 8) Ltmiddot 0

g 8middot2 21Sshy 0

72-Hr 96-Hr


iQ 0


10

n 10


~

~ lt












Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None



Length (mm)


lWeight (g) 0-11 0)2 O~

~ ----




Fish per Chamber 10



mgL

---mgL

11 mgL

l22 mgL





Control

750 ppm

44 40 mgL ISD mgL

mgL l2 mgL








Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Batch

Sample 10

Analyst

Start Date

lC50 Result



A ==-J

1SoSOS3 - It

--------- shy

zD mgL


Hardness


Alkalinity

LCSID 512011 Y


Fish Averages


SM 2320 B (20th 00)

End point pH = 45






Final ~~(+-I g~~~ )l~~ ~

~ Reviewed and

O~l middot~1

O1sD 0middot34

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

4J



Initial Readout

1 24-Hr

11gtReadouts






)JJO ppm 80 ~ D r IT Ji ~l (11 ()



amp0 1middot) ] 11 S ~~ 17 lCt 110

ppm




prm


rs1 )q$ ro ~4

bull

bl I~l b

bJ Q7 b

7~Hr 96-Hr



iD

lO

i()

itgt

Q

to iO

-

ishy f

0

it)


ltj( g ~ 0 0 ~amp ~-

I

Comments

I

I



sample tanks fyeno

llO





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None



Length (mm)

Avg Min Max bull






Fish per Chamber 10












----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

----------------------Batch B6A0445



Start Date 011916 ~-----------------









SM 2320 B (20th ed)





Positive

Hardness


LCSID

LCS exp

Spike Vol mL

Fish Averages




41middot 0middot(0)



lq l bmiddot14



~

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

----------------

---

if

















10

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

to





Feeding None



Length (mm)

eight (g)




Fish per Chamber 10

Control mgL 1 mgL



Control 40 mgL

4-J PPITI LtO _mgL

~L mgL

l 2- mgL














SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by









SM 2320 B (20th ed)

End pointpH =45








Batch B6A0445 ~--------------------

Sample 10 _1505053-_14---_________--shy

Analyst J_M_H___________________

Start Date 011916~=~----------------


I


Hardness


Alkalinity


Fish Averages


b~ 0 l ~ b


l) ~14shynil)6b




Averages

lq 0-1















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by















1JMI-I









Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





Feeding None


Control 4) mgL mgL


IFiSh 10 (Q~~tl



~ light 79 65 99 I



Alkalinit

JCp mgLI ~n mgL


Fish per Chamber 10













-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by





-----------






E shy~Ii - ll ~

-------shy ~ E 0 m ~ e li~ ~ o~ 5






------c-I---







-shy










na -~~-



i na 200gimin) N N X --~~~-~~

na 200gimin) N N

na 200g(min) N N X





Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

















C(A ( EH ftJJj


12A- )3 2- Go ML fbGj ~




Rev 0912512015


-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

-- -- - --- ---- -

--







Telepbone (530) 666-8424 Fax (530) 666-8423


ltAj riA

ii2A

1A

eA-B~

U Sample Number

Description






solid

35iE

952E

353E

354E

355E

356E

357E

358E






~~~i~oouctS 79749687-1f7-1----1-_---_--r=--_______~





r---~----



Inc 071409543214 IiqUldiO~11252015





361E

362E



1----- -----I----------------1-----+shy

I -

__ L---- --L-___

~ L-g~ ~ m l G

~ ~ _ _ _ ~ ____

11252015 1030 AM

-




Fax 530-666-8185 p S



I ~



N N X

11252015 _1030 AM n 200g (lLj_ C I N I N I X

11252015 1------=10e3~0~A~M~_f=-i_=-=--t_ p



11 1030 AM n 200 (min) P N N X It




--il------- --- _~g(mlnLl_ I N I N I





Relinquished by ____________________

Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by



California 95695 Fax (530) 666-8423

Testing Facility

























Fax 530-666-8185 Sple


c to 0 ]i~ Q 88 ~u

~g shy it ~


O~ ll E E

i~l -g sect on ~~ 8

i O-g Qo rshy

liZll i E ~g shy e~

to ~cr ~ 0

c 8 =shy Q - ~ 8

11252015 IO30AM na 200g(mln) p N N

11252015 1030 AM na 200qminJ p N N~~~~

V 11252015 1030 AM na 200~(rnin) P N N

11252015 1030 AM na 200lttrnin) p N N

11252015 ~30AM na 200g[min) p N N

11252015 1030 AM na 200lmin) N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM na 200g(min) C N N

11252015 1030 AM nfa 200glminl p N N

11252015 1030 AM na 200g(mln) P N N

11252015 1030 AM na 200g(min) p N N


11252015 1030 AM ____ nra 200g (min) C N N

11252015 1030 AM nfa 200g(minL C N N

11252015 1030 AM nfa 200g(minL C N N

na 200g(min) N N

na 2002 (mini N N

na 200g(min) N N


nta 200gmin) N N

Required

analvsis

gtshy~ 2

-= ~

Q ~ u X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

X

-f)

ffP E

j

b

b

1 IrlS

6 J 6 6



Time

Received by



Received by

348E Seventh Generation Natural Dishwasher … Environmental and Compliance, INC. Dear Client:...

Documents

Transcript of 348E Seventh Generation Natural Dishwasher … Environmental and Compliance, INC. Dear Client:...