1 ISM Document and Training Roadmap · 2013-01-24 · ISM Document and Training Roadmap: Field...
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ISM Document and Training Roadmap
Plan
Principles
Systematic PlanningStatistical
Design
ImplementField
ImplementationLab
Processing
Assess Making Decisions
Introduction Challenges/Opportunities
Application
Part 1
Part 2
Section 2
Section 3
Section 4
Section 5
Section 7
Section 8
Section 6
ISM DocumentTraining Module
ISMOpportunities
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1. REPORT DATE MAR 2012 2. REPORT TYPE
3. DATES COVERED 00-00-2012 to 00-00-2012
4. TITLE AND SUBTITLE ISM Document and Training Roadmap: Field Implementation Learning Objectives
5a. CONTRACT NUMBER
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7. PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) Interstate Technology and Regulatory Council (ITRC),50 F Street NWSte 350,Washington,DC,20001
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13. SUPPLEMENTARY NOTES Presented at the 9th Annual DoD Environmental Monitoring and Data Quality (EDMQ) Workshop Held26-29 March 2012 in La Jolla, CA. U.S. Government or Federal Rights License
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2 Field Implementation Learning Objectives
Learn how to: Collect an ISM sample
• Understand the similarities and differences between surface and subsurface ISM sampling
ITRC, ISM-1, Section 5
• Consider issues specific to non-volatile and volatile ISM sampling
• Implement and collect ISM replicate samples
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Key Presentation Topics
Sampling design Sampling tools ISM surface/subsurface sampling
• Cores and subsampling Specific contaminant of
concern (COC) considerations• Non-volatile and volatile
ISM replicates
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ISM Field Sampling Implementation
ITRC, ISM-1, Section 5.1, Figure 5-1
Separate Sample Contai ner for %
Moisture Determ ination
ISM Field Sampling Implementation
v .....
Subsampling on-site Determine Number &
Mass of Soi l
Yes
No
Processing inField?
No
Sample Containerized, Packaged and Shipped to Lab
Yes
Hand Operated Coring Devices
Yes
No DHp Sample or Subsurface ISM
Sampling Collection Methods Needed
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Sample Collection Components
Decision Unit (DU) sampling design • Simple random sampling• Random sampling within a grid • Systematic random sampling
Sampling tools• Core shaped• Adequate diameter
Mass• Increment mass• Sample mass
ITRC, ISM-1, Section 4.3.4.2
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Sampling Designs
Simple Random Random within Grids
Systematic Random
Increments
ITRC, ISM-1, Section 4.3.4.2 & Section 5.3.1, Appendix A1
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7 Florida Case Study: Decision Unit (DU) Identification
Identify DU in the field• Use typical environmental site investigation procedures• Examples
Survey GPS Swing ties
ITRC, ISM-1, Section 9.3 & Appendix C, Section C.3
Decision Unit(~1/4 acre)
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Increment Locations
Identify increment locations in field• Utilize similar site investigation tools
ITRC, ISM-1, Section 5.3.1
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9 Florida Case Study: Increment Field Determination
c:::::::;.
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Sampling Tool Considerations
Criteria - shape• Cylindrical or core shaped increments • Minimum diameter required – based on particle
size (soil fraction) of interest
e.g., core diameter >16 mm
ITRC, ISM-1, Section 5.2
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Additional Considerations
Decontamination• Not necessary within DU (including replicates)
Sampling tool• Appropriate for matrix and contaminant of interest
ITRC, ISM-1, Section 5.2
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Sampling Tool Examples
Soft Surface Soil
Source: Courtesy http://www.jmcsoil.com/index.htmlhttp://fieldenvironmental.com/evc-incremental-sampler.php
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Alternate Sampling Tools
Hard Surface Soil
ITRC, ISM-1, Section 5.2; Figure 5-2b
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14 Florida Case Study:Field Sampling
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15 Florida Case Study:“Low Tech” Sampling Tools
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Adequate Sample Mass
Criteria – mass (non-volatile)• Recommended mass per increment: 20-60 grams• Final ISM samples: generally 600-2,500 grams
Ms = • n • Ds • • (q / 2)2
Ms – targeted mass of sample (g)Ds – increment length (cm)n – number of increments - soil or sediment density (g/cm3)q - diameter of sample core (cm)
ITRC, ISM-1, Section 5.3.1
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Individual core samples combined to prepare an ISM sample for each DU
Subsurface Decision Units (DU)
-1.5’
-0.5’
-3.0’
-5.0’
-10’
DU-1
DU-2
DU-3
DU-4
30 Borings (minimum recommended)Core Increments
not to scale
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Preferred increment – entire core interval Core subsampling alternatives
1. Core wedge2. Core slice
Subsurface Sampling Considerations
ITRC, ISM-1, Section 5.3.2
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Core Wedge
Continuous wedge removed from entire length of targeted DU interval for 100% coverage
ITRC, ISM-1, Section 5.3.2.1
e.g., wedge width >16 mm
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Core Slice
Core Slice removed from randomly selected interval length of targeted DU depth
ITRC, ISM-1, Section 5.3.2.1
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Field Processing for Non-Volatiles
ISM sample processing in a controlled laboratory environment is recommended to reduce error
Field processing may be applicable if project specific DQOs can be met
ITRC, ISM-1, Section 5.4.1
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22 Florida Case Study: Non-Volatile ISM Sample Logistics
Final ISM samples: typically 600-2,500 grams or more• Containers, storage, shipping
Laboratory• Facilities and equipment for correct
processing and subsampling
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ISM Volatile Sampling Tools
Core type sampler Typical for VOC soil sampling per SW846 5035A
ITRC, ISM-1, Section 5.4.2 Source: Courtesy www.ennovativetech.com
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ISM Volatile Samples – Subsurface
Numerous increments collected across core/depth interval
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Methanol
Soil
VOC preservation and analysis• Increments are extruded from sampler directly into
volume of appropriate container with predetermined methanol
• Methanol preserved sample submitted to laboratory
• Note shipping restrictions/ requirements
ISM Volatile Sample Logistics
ITRC, ISM-1, Section 5.4.2, Figure 5-11
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Replicates Recommended
Increments collected from alternate random locations• Independent samples, not “splits”
Minimum 3 replicate set for statistical evaluations Additional replicates may be necessary
depending on contaminant heterogeneity and project specific DQOs
ITRC, ISM-1, Section 5.3.5
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Replicate Spacing and Collection
Decision Unit
Replicate Increment Spacing
Decision Unit
Sample Collection
R1 R2 R3Replicate 1Replicate 2Replicate 3ITRC, ISM-1, Section 5.3.5
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Field Replicates – Simple Example
Replicate 3
Replicate 2
Replicate 1
Collecting the Samples
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Replicate/Sampling Reminders
Replicates • What type• How many• Where/when will they be collected• How will they be evaluated
“Homogenizing” or mixing not necessary• Laboratory processing and subsampling (following
module) designed to attain representative analytical sample
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Field Implementation Summary
Determined during Systematic Planning• Sampling design• Adequate sampling tools• ISM surface/subsurface sampling logistics
Subsurface cores and subsampling
• Specific contaminant of concern (COC) considerations
• Non-volatile and volatile
• ISM replicates
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ISM Document and Training Roadmap
Plan
Principles
Systematic PlanningStatistical
Design
ImplementField
ImplementationLab
Processing
Assess Making Decisions
Introduction Challenges/Opportunities
Application
Part 1
Part 2
Section 2
Section 3
Section 4
Section 5
Section 7
Section 8
Section 6
ISM DocumentTraining Module
ISMOpportunities