19january2017snapshot.epa.gov · A , , ' ACCURA ANALYTICAL LADORA TORY, INC. (AAL) 6017 Financial...

Lab. Work Order # : 12740

WRS Infrastructure & Environment, Inc.

Project Manager: Rodney Swiney

Project Name : Circle Environmental I

October 18, 2007

ACCURA Analytical Laboratory, Inc.6017 Financial Drive Norcross, GA 30071Phone: 770-449-8800 Fax: 770-449-5477

Analytical Report for:

Project ID : Region 4 ERRS

Project Location : Georgia

A ,

,

'

ACCURA ANALYTICAL LADORA TORY, INC. (AAL) 6017 Financial Drive, Norcross, GA 30071, Phone: (770) 449-8800

FL Certification #E87429 • NC Certification #483 ' SC Certification #980 15 • Utah Certification # AALI 1 ,

" USACE Approved Case Narrative

---------.~------

AAL Work Order# 12740

Client Project: Circle Environmental I I Region 4 ERRS

Accura Analytical Laboratory Inc. certifies that the results meet all requirements of the NELAC Standards.

The data package includes a total of 178 pages including: Cover Page, Case Narrative, Chain of Custody, Analytical Report pages, subcontract laboratory report pages and a list of common EPA qualifier codes and abbreviations used by AAL

The following items were noted concerning this work order:

Project Manager's Notations:

1. The following analysis was performed by Analysts, Inc., 3075 Corners North Court, Norcross, GA 30071: Water Content KF by Method D6304. The lab contact person at Analysts, Inc is Marian Kiley at 770-448-5235.

2. The following analyses were performed by Xenco Laboratories, 5757 NW 1581h Street,

Miami Lakes, FL 33014: TCLP Metals by SW846 Methods 1311/6020 and 6020. The lab contact person at Xenco Laboratories is Mark Masino at 305-823-8500

Project Manager

tions have been generated, reviewed, and edited by:

Octo6er 18, 2007

Date

This report may not be reproduced, except in full, without written approval from Accura Analytical Laboratory, Inc. NELAP Accredited Certificate #-E87429- Effective 7/01/07, Expires 6/30/08

Pagel of! WO 12740CN

U.S. ENVIRONMENTAL PROTECTION AGENCY

REGION4 ~.~/?~

PROJ. NO. en a: w z :;( ... z 0 u u. 0

CHAIN OF CUSTODY RECORD

CJrcletadd Parameters DeSired ( ) ~ lndiCBIBS

Separate Conta1ners

DISTRIBUTION Ong•nal and P'lnk cop•es accompany sample sh•pment to laboratory, P1nk copy retamed by labmatory, Yellow copy re1a1ned by .amplers, Blue copy e•tra copy .u neede<l

W'R6 J: fl. 6fr14~ r ~,.. ... ,. ... • • • • • • · llr~ l.f C¥1AOP~MEIIJ I At SEAOICES Dlt'ISIOM-

Remarks

111T-6

CuttEG'E-STA+ImJ RENm' ~0613

REMARKS/TAG NUMBERS

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ll

Jt

wee---k

T4- 8024

Certificate of Analytical Results

Page 1

12740

*

WRS Infrastructure & Environment, Inc., Norcross, GA Circle Environmental I

1.045 Version:

Sep-26-07 16:20

Date Received:% Moisture:

Sep-19-07 12:00 Date Collected: 12740-001 Lab Sample Id:LIQUID Matrix: CEI-S01 Sample Id:

TAL Metals by SW6020 Analytical Method:

Oct-16-07 16:10 Date Analyzed: MCJ01 Analyst:

SW3050B Prep Method:

Oct-01-07 10:00 Date Prep: MSN01 Tech:

Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Lead Magnesium Manganese Nickel Potassium Silver Sodium Thallium Tin Vanadium Zinc

Parameter

2762.034.15

0.8490.6131.0894.33.633.213.213.3036.0

0.8493.2593.4

0.5192821.841.133.111.04

Result

4724.724.724.721.422.364724.724.724.724.724724.724.724724.724724.7223.64.7247.2

Rep Limit Flag

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRL10.8BRLBRLBRL7.17BRL49.6BRLBRL9.95BRLBRLBRLBRLBRLBRLBRL181

37812 Seq Number:

Sample Depth:


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Parameter

2872.114.31

0.8820.6371.1398.03.773.333.333.4337.4

0.8823.3897.1

0.5392931.911.183.241.08

Result

4904.904.904.901.472.454904.904.904.904.904904.904.904904.904904.9024.54.9049.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRL8.82BRLBRLBRL6.23BRL11017.5BRL14.834.3BRLBRL525

BRLBRLBRL718

37812 Seq Number:

Sample Depth:


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Sep-19-07 12:00 Date Collected: 12740-003 Lab Sample Id:SOLID Matrix: CEI-S03 Sample Id:






Parameter

2922.144.39

0.8970.6481.1599.73.843.393.393.4938.0

0.8973.4498.7

0.5482981.941.203.291.10

Result

4994.994.994.991.502.494994.994.994.994.994994.994.994994.994994.9924.94.9949.9

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

625120

BRL3040BRLBRL18007.58BRL5.98BRLBRL17.0BRLBRLBRLBRLBRL39.5BRL70.1

37811 Seq Number:

Sample Depth:


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Parameter

2792.054.19

0.8570.6191.1095.23.673.243.243.3336.3

0.8573.2994.3

0.5242851.861.143.141.05

Result

4764.764.764.761.432.384764.764.764.764.764764.764.764764.764764.7623.84.7647.6

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRL138

BRL7.38BRLBRLBRLBRL6.33BRLBRLBRL8.33BRLBRLBRLBRLBRLBRLBRLBRL

37811 Seq Number:

Sample Depth:


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Parameter

2932.154.40

0.9000.6501.151003.853.403.403.5038.2

0.9003.4599.0

0.5502991.951.203.301.10

Result

5005.005.005.001.502.505005.005.005.005.005005.005.005005.005005.0025.05.0050.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRL21.8BRLBRL28009.85BRL24.7BRLBRL67.45.40BRLBRL1640BRLBRLBRL139

37811 Seq Number:

Sample Depth:


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Parameter

2792.054.19

0.8570.6191.1095.23.673.243.243.3336.3

0.8573.2994.3

0.5242851.861.143.141.05

Result

4764.764.764.761.432.384764.764.764.764.764764.764.764764.764764.7623.84.7647.6

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

3480BRLBRL24.7BRLBRL909022.3BRL86.5763

402096.714.4947

BRLBRLBRLBRL32.4132

37811 Seq Number:

Sample Depth:


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Parameter

2872.114.31

0.8820.6371.1398.03.773.333.333.4337.4

0.8823.3897.1

0.5392931.911.183.241.08

Result

4904.904.904.901.472.454904.904.904.904.904904.904.904904.904904.9024.54.9049.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRL66.7BRL682

BRLBRL1490BRL7.2512.4BRLBRLBRL9.17BRLBRLBRLBRLBRLBRLBRL

37811 Seq Number:

Sample Depth:


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Parameter

2932.154.40

0.9000.6501.151003.853.403.403.5038.2

0.9003.4599.0

0.5502991.951.203.301.10

Result

5005.005.005.001.502.505005.005.005.005.005005.005.005005.005005.0025.05.0050.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRL92.0BRL42.3BRLBRL60208.75BRL9.2012.4BRLBRLBRLBRLBRLBRLBRLBRL5.50446

37811 Seq Number:

Sample Depth:


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SW3005A Prep Method:


Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Lead Magnesium Manganese Molybdenum Nickel Potassium Silver Sodium Thallium Vanadium Zinc

Parameter

0.04300.00490.00200.00120.00150.00030.08600.00240.00020.00050.00040.01120.00310.00440.00220.07500.00090.05300.00100.00120.0064

Result

0.500.100.100.100.100.100.500.100.100.100.100.500.100.100.100.500.100.500.100.100.10

Rep Limit Flag

mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L

Units

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7439-98-7 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6

MDL

BRLBRLBRLBRLBRLBRL1.41BRLBRLBRLBRLBRLBRLBRLBRL2.07BRL8.69BRLBRL1.20

37810 Seq Number:

Sample Depth:


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Parameter

0.04300.00490.00200.00120.00150.00030.08600.00240.00020.00050.00040.01120.00310.00440.00220.07500.00090.05300.00100.00120.0064

Result

0.500.100.100.100.100.100.500.100.100.100.100.500.100.100.100.500.100.500.100.100.10

Rep Limit Flag

mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L

Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7439-98-7 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6

MDL

BRLBRLBRL

0.102BRLBRL3.53BRLBRL

0.122BRL1.46

0.3210.242

0.05557.24BRL38.9BRLBRL

0.488

37810 Seq Number:

Sample Depth:


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1.045 Version:

Sep-26-07 16:20


Sep-25-07 15:00 Date Collected: 12740-011 Lab Sample Id:SLUDGE Matrix: CEI-S11 Sample Id:






Parameter

2872.114.31

0.8820.6371.1398.03.773.333.333.4337.4

0.8823.3897.1

0.5392931.911.183.241.08

Result

4904.904.904.901.472.454904.904.904.904.904904.904.904904.904904.9024.54.9049.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRL8.48BRLBRLBRLBRLBRL84.319.0BRL6.27BRLBRLBRLBRLBRLBRLBRL739

37812 Seq Number:

Sample Depth:


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1.045 Version:

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Sep-25-07 15:00 Date Collected: 12740-012 Lab Sample Id:SLUDGE Matrix: CEI-S12 Sample Id:






Parameter

2711.994.07

0.8330.6021.0692.63.563.153.153.2435.3

0.8333.1991.7

0.5092771.811.113.061.02

Result

4634.634.634.631.392.314634.634.634.634.634634.634.634634.634634.6323.14.6346.3

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRL1240BRLBRLBRL11.515.628.367.0201019.118.0BRL6.34699

BRLBRLBRL

24800

37812 Seq Number:

Sample Depth:


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1.045 Version:


Date Collected: 303886 BLK Lab Sample Id:SOIL Matrix: 303886 BLK Sample Id:






Parameter

2932.154.40

0.9000.6501.151003.853.403.403.5038.2

0.9003.4599.0

0.5502991.951.203.301.10

Result

50025.025.025.01.502.5050025.05.0025.025.050025.025.050025.05005.0025.05.0050.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37812 Seq Number:

Sample Depth:


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1.043 Version:


Date Collected: 303884 BLK Lab Sample Id:WATER Matrix: 303884 BLK Sample Id:





Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Lead Magnesium Manganese Nickel Potassium Silver Sodium Thallium Vanadium Zinc

Parameter

0.04300.00490.00200.00120.00150.00030.08600.00240.00020.00050.00040.01120.00310.00220.07500.00090.05300.00100.00120.0064

Result

0.500.100.100.100.100.100.500.100.100.100.100.500.100.100.500.100.500.100.100.10

Rep Limit Flag

mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L mg/L

Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-62-2 7440-66-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37810 Seq Number:

Sample Depth:


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1.044 Version:


Date Collected: 303885 BLK Lab Sample Id:SOIL Matrix: 303885 BLK Sample Id:






Parameter

2932.154.40

0.9000.6501.151003.853.403.403.5038.2

0.9003.4599.0

0.5502991.951.203.301.10

Result

5005.005.005.001.502.505005.005.005.005.005005.005.005005.005005.0025.05.0050.0

Rep Limit Flag


Units

5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5

Dil Cas Number

7429-90-5 7440-36-0 7440-38-2 7440-39-3 7440-41-7 7440-43-9 7440-70-2 7440-47-3 7440-48-4 7440-50-8 7439-92-1 7439-95-4 7439-96-5 7440-02-0 7440-09-7 7440-22-4 7440-23-5 7440-28-0 7440-31-5 7440-62-2 7440-66-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37811 Seq Number:

Sample Depth:


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WRS Infrastructure & Environment, Inc., Norcross, GACircle Environmental I

1.042Version:

Sep-26-07 16:20 Date Received:% Moisture:

Sep-19-07 12:00 Date Collected: 12740-001Lab Sample Id:LIQUIDMatrix: CEI-S01 Sample Id:

Flash Point (Closed Cup) by SW1010

PCBs by SW8082

Reactive Cyanide/Sulfide by SW846 Sec. 7.3

TAL Mercury by SW7471A

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 19:10

Oct-02-07 16:00

Oct-03-07 13:31

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 13:35

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Flash Point

Aroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260

Reactive SulfideCyanide, Reactive

Mercury

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

650.020

0.010

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1001.0

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Deg F

mg/kgmg/kgmg/kgmg/kgmg/kgmg/kgmg/kg

mg/Lmg/L

mg/kg

Units

Units

Units

Units

1

1111111

11

1

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

>140

BRLBRLBRLBRLBRLBRLBRL

BRLBRL

BRL

37620

37663

37605

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:



TCL SVOCs by SW8270CAnalytical Method:

Oct-02-07 19:45 Date Analyzed: CTP01Analyst:

SW3580APrep Method:

Oct-02-07 12:30 Date Prep: BPR01Tech:

1,2,4-Trichlorobenzene1,2-Dichlorobenzene1,3-Dichlorobenzene1,4-Dichlorobenzene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2,4-Dichlorophenol2,4-Dimethylphenol2,4-Dinitrophenol2,4-Dinitrotoluene2,6-Dinitrotoluene2-Chloronaphthalene2-Chlorophenol2-Methylnaphthalene2-Methylphenol2-Nitroaniline2-Nitrophenol3,3-Dichlorobenzidine3,4-Methylphenol3-Nitroaniline4,6-Dinitro-2-methylphenol4-Bromophenyl-phenylether4-Chloro-3-methylphenol4-Chloroaniline4-Chlorophenyl-phenylether4-Nitroaniline4-NitrophenolAcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Butylbenzylphthalatebis(2-Chloroethoxy)methanebis(2-chloroethyl)etherbis(2-Ethylhexyl)phthalateCarbazoleChryseneDibenz(a,h)anthracene DibenzofuranDiethylphthalateDimethylphthalate

Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:


di-n-Butylphthalate di-n-Octylphthalate FluorantheneFluoreneHexachlorobenzeneHexachlorobutadieneHexachlorocyclopentadieneHexachloroethaneIndeno(1,2,3-c,d)pyreneIsophoroneNaphthaleneNitrobenzeneN-Nitroso-di-n-propylamineN-NitrosodiphenylaminePentachlorophenolPhenanthrenePhenolPyrene

Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag

ug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kgug/kg

Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37606Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260BAnalytical Method:

Oct-01-07 14:49 Date Analyzed: MJL01Analyst:

SW5030BPrep Method:

Oct-01-07 09:31 Date Prep: MJL01Tech:

1,1,1-Trichloroethane1,1,2,2-Tetrachloroethane1,1,2-Trichloro-1,2,2-trifluoroethane1,1,2-Trichloroethane1,1-Dichloroethane1,1-Dichloroethene1,2,4-Trichlorobenzene1,2-Dibromo-3-Chloropropane1,2-Dibromoethane (Ethylene Dibromide)1,2-Dichlorobenzene1,2-Dichloroethane1,2-Dichloroethene (total)1,2-Dichloropropane1,3-Dichlorobenzene1,4-Dichlorobenzene2-Butanone2-Hexanone4-Methyl-2-PentanoneAcetoneBenzeneBromodichloromethaneBromoformBromomethaneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethanecis-1,2-Dichloroethene cis-1,3-Dichloropropene CyclohexaneDibromochloromethaneDichlorodifluoromethaneEthylbenzeneIsopropylbenzeneMethyl AcetateMethyl tert-butyl etherMethylcyclohexaneMethylene ChlorideStyreneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene

Parameter

190300280170200290220400220320150200230250170

2300280810

1700130130240610360190140610180570170130240250290140190240170270540190

1300000150190170

Result

120012001200120012001200120012001200120012001200120012001200

120001200012000120001200120012001200120012002500120012001200120012001200120012001200120012001200120012001200

6200000120012001200

Rep Limit Flag


Units

5050505050505050505050505050505050505050505050505050505050505050505050505050505050

*****505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

60000000BRLBRLBRL

37631Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260B

pH by SW9040B

Analytical Method:

Analytical Method:

Oct-01-07 14:49

Oct-01-07 15:30

Date Analyzed:

Date Analyzed:

MJL01

AJI01

Analyst:

Analyst:

SW5030BPrep Method:

Prep Method:

Oct-01-07 09:31 Date Prep:

Date Prep:

MJL01

AJI01

Tech:

Tech:

TrichloroetheneTrichlorofluoromethaneVinyl ChlorideXylenes, Total

pH

Parameter

Parameter

180880500460

N/A

Result

Result

1200120012003700

N/A

Rep Limit

Rep Limit

Flag

Flag

ug/kgug/kgug/kgug/kg

pH

Units

Units

50505050

1

Dil

Dil

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

12408-02-5

MDL

MDL

5900BRLBRLBRL

5.8

37631

37628

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:




PCBs by SW8082



Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 19:33

Oct-02-07 16:00

Oct-03-07 13:35

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 13:35

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Flash Point



Mercury

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

650.020

0.011

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1001.0

0.050

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Deg F


mg/Lmg/L

mg/kg

Units

Units

Units

Units

1

1111111

11

1

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

>140


BRLBRL

BRL

37620

37663

37605

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

9200140001400082009800

140001100020000110001600073009700

11000120008300

11000014000390008400062006100

12000300001800090007000

300009000

2800081006600

12000120001400069009200

120008400

13000260009000

1300000720095008200

Result

610006100061000610006100061000610006100061000610006100061000610006100061000

610000610000610000610000610006100061000610006100061000

120000610006100061000610006100061000610006100061000610006100061000610006100061000

6100000610006100061000

Rep Limit Flag


Units

25002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500250025002500

*****250025002500

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

10000000BRLBRLBRL

37631Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260B

pH by SW9040B

Analytical Method:

Analytical Method:

Oct-01-07 15:20

Oct-01-07 15:30

Date Analyzed:

Date Analyzed:

MJL01

AJI01

Analyst:

Analyst:

SW5030BPrep Method:

Prep Method:


Date Prep:

MJL01

AJI01

Tech:

Tech:


pH

Parameter

Parameter

8600430002400023000

N/A

Result

Result

610006100061000

180000

N/A

Rep Limit

Rep Limit

Flag

Flag


pH

Units

Units

2500250025002500

1

Dil

Dil

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

12408-02-5

MDL

MDL

BRLBRLBRLBRL

6.3

37631

37628

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:


Sep-19-07 12:00 Date Collected: 12740-003Lab Sample Id:SOLIDMatrix: CEI-S03 Sample Id:


PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 19:55

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 13:16

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

126


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

75012001100670800

1200870

1600860

1300590800920990680

900011003200

34000510500950

24001400740580

2400740

2300660540940990

1200560750940690

11002200740

1000580780670

Result

500050005000500050005000500050005000500050005000500050005000

500005000050000

25000050005000500050005000500099005000500050005000500050005000500050005000500050005000500050005000500050005000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100500100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


730000BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

2600015000

BRLBRLBRLBRLBRL9300BRLBRLBRL

37631Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260B

TCLP Herbicides by SW1311/8151A

TCLP Mercury by SW1311/7470A

TCLP Metals by SW1311/6020

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 16:49

Oct-03-07 17:08

Oct-02-07 17:03

Oct-01-07 13:10

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:


2,4,5-TP (Silvex)2,4-D

Mercury

ArsenicBariumCadmiumChromiumLeadSeleniumSilver

Parameter

Parameter

Parameter

Parameter

700350020001800

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

500050005000

15000

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Units

Units

Units

Units

100100100100

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

110000

BRLBRL

BRL


37631

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:



TCLP Pesticides by SW1311/8081A

TCLP SVOCs by SW1311/8270C

TCLP VOCs by SW1311/8260B

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 22:49

Oct-01-07 17:00

Sep-28-07 12:28

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:

ChlordaneEndrinGamma-BHC (Lindane) HeptachlorHeptachlor EpoxideMethoxychlorToxaphene

1,4-Dichlorobenzene2,4,5-Trichlorophenol2,4,6-Trichlorophenol2,4-Dinitrotoluene2-Methylphenol3 & 4-MethylphenolHexachlorobenzeneHexachlorobutadieneHexachloroethaneNitrobenzenePentachlorophenolPyridine

1,1-Dichloroethene1,2-Dichloroethane2-ButanoneBenzeneCarbon TetrachlorideChlorobenzeneChloroformTetrachloroethyleneTrichloroetheneVinyl Chloride

Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag


mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL


BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37603

37594

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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pH by SW9045CAnalytical Method:

Oct-01-07 16:15 Date Analyzed: AJI01Analyst:

Prep Method:

Date Prep: AJI01Tech:

pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

6.30

37627Seq Number:

Sample Depth:


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1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 20:18

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 13:39

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

130


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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SW5030BPrep Method:



Parameter

350550510310370540400750400600280370430460320

4200520

150032000

240230440

1100670340270

1100340

1100310250440460550260350440320500

1000340480270360310

Result

230023002300230023002300230023002300230023002300230023002300

230002300023000

23000023002300230023002300230046002300230023002300230023002300230023002300230023002300230023002300230023002300

Rep Limit Flag


Units

5050505050505050505050505050505050505005050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


1000000BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL5500BRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37631Seq Number:

Sample Depth:


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TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 18:40

Oct-03-07 17:39

Oct-02-07 17:26

Oct-01-07 13:17

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

3301600930860

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

2300230023006900

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

50505050

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

28000

BRLBRL

BRL


37631

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 23:08

Oct-01-07 22:50

Sep-28-07 18:00

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

6.05

37627Seq Number:

Sample Depth:


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1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 20:41

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 13:51

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

>140


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

68011001000610720

1000790

1500780

1200540720840900620

8200100029006200460450870

22001300670520

2200670

2100600490850900

1100510690850630980

2000670940530700610

Result

450045004500450045004500450045004500450045004500450045004500

4500045000450004500045004500450045004500450090004500450045004500450045004500450045004500450045004500450045004500450045004500

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL5400BRLBRLBRL

37633Seq Number:

Sample Depth:


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TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 15:24

Oct-03-07 18:09

Oct-02-07 17:30

Oct-01-07 13:36

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 11:20

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

640320018001700

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

450045004500

14000

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

100100100100

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRLBRL

BRLBRL

BRL


37633

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 23:27

Oct-01-07 23:19

Sep-28-07 16:37

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

6.22

37627Seq Number:

Sample Depth:


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1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 21:04

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 13:55

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

>140


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 33 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


Page 34 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


Page 35 of 97

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1.042Version:





SW5030BPrep Method:



Parameter

180280260160190280210390210310140190220240160

2200270770

1600120120230590350180140580180550160130230240280130180230170260520180250140190160

Result

120012001200120012001200120012001200120012001200120012001200

1200012000120001200012001200120012001200120024001200120012001200120012001200120012001200120012001200120012001200120012001200

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL62007400BRLBRL5500BRLBRL2400BRLBRLBRL

37631Seq Number:

Sample Depth:


Page 36 of 97

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1.042Version:



TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 19:07

Oct-03-07 18:39

Oct-02-07 17:34

Oct-01-07 13:43

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

170840480440

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

1200120012003600

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

50505050

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

47000

BRLBRL

BRL


37631

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 37 of 97

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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 23:46

Oct-01-07 23:48

Sep-28-07 17:05

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

5.43

37627Seq Number:

Sample Depth:


Page 39 of 97

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1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 21:27

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 13:59

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

128


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 40 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

13000000

37606Seq Number:

Sample Depth:


Page 41 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRL

64000000BRLBRLBRLBRLBRLBRLBRLBRL

37606Seq Number:

Sample Depth:


Page 42 of 97

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1.042Version:





SW5030BPrep Method:



Parameter

370590550330400580430800430640300400460490340

4500560

160068000

250250480

1200720370290

1200370

1100330270470490590280

7500470340540

1100370510290390330

Result

250025002500250025002500250025002500250025002500250025002500

250002500025000

5000002500250025002500250025005000250025002500250025002500250025002500

50000250025002500250025002500250025002500

Rep Limit Flag


Units

505050505050505050505050505050505050

100050505050505050505050505050505050

1000505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL



34000220000

BRLBRLBRLBRLBRLBRL

20000BRLBRL

37631Seq Number:

Sample Depth:


Page 43 of 97

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1.042Version:



TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 19:35

Oct-03-07 19:10

Oct-02-07 17:38

Oct-01-07 13:49

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

35017001000

18000

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

250025002500

150000

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

505050

1000

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

640000

BRLBRL

BRL


37631

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 44 of 97

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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 00:05

Oct-02-07 00:17

Sep-28-07 17:32

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 45 of 97

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1.042Version:





Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

4.43

37627Seq Number:

Sample Depth:


Page 46 of 97

12740

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1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 21:49

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 14:02

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.011

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.050

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

>140


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 47 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


Page 48 of 97

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*


1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


Page 49 of 97

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1.042Version:





SW5030BPrep Method:



Parameter

350550510310370530400750400590270370430460310

4200520

150013000

240230440

1100670340270

1100340

1100300250430460540

5200350440320500

1000340480270360310

Result

230023002300230023002300230023002300230023002300230023002300

23000230002300092000230023002300230023002300460023002300230023002300230023002300

460002300230023002300230023002300230023002300

Rep Limit Flag


Units

505050505050505050505050505050505050200505050505050505050505050505050

100050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL



5500005700BRLBRLBRLBRLBRLBRL3400BRLBRL

37631Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 20:03

Oct-03-07 19:40

Oct-02-07 17:42

Oct-01-07 13:55

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

3301600920

17000

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

230023002300

140000

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

505050

1000

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

2400000

BRLBRL

BRL


37631

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 00:24

Oct-02-07 15:22

Oct-02-07 20:41

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Oct-02-07 11:20

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37632

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

5.80

37627Seq Number:

Sample Depth:


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1.042Version:




PCBs by SW8082



TAL - Mercury by SW7470A

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 22:12

Oct-02-07 16:00

Oct-02-07 20:00

Oct-02-07 16:44

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7470A_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-01-07 14:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.0025

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.013

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/L

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

< 65


BRL

BRL

BRL

37623

37663

37616

37611

37608

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:


1,1,1-Trichloroethane1,1,2,2-Tetrachloroethane1,1,2-Trichloro-1,2,2-trifluoroethane1,1,2-Trichloroethane1,1-Dichloroethane1,1-Dichloroethene1,2,4-Trichlorobenzene1,2-Dibromo-3-Chloropropane1,2-Dibromoethane (Ethylene Dibromide) 1,2-Dichlorobenzene1,2-Dichloroethane1,2-Dichloroethene (total)1,2-Dichloropropane1,3-Dichlorobenzene1,4-Dichlorobenzene2-Butanone2-Hexanone4-Methyl-2-PentanoneAcetoneBenzeneBromodichloromethaneBromoformBromomethaneCarbon DisulfideCarbon TetrachlorideChlorobenzeneChloroethaneChloroformChloromethanecis-1,2-Dichloroethene cis-1,3-Dichloropropene CyclohexaneDibromochloromethaneDichlorodifluoromethaneEthylbenzeneIsopropylbenzeneMethyl AcetateMethyl tert-butyl etherMethylcyclohexaneMethylene ChlorideStyreneTetrachloroetheneToluenetrans-1,2-Dichloroethenetrans-1,3-Dichloropropene

Parameter

360990490440370490640

1400400370410410410370300640

13001100

34000340480680

1400370450300

1100690610400380500400370

33000500

3200310380460280

8800340370420

Result

250025002500250025002500250025002500250025002500250025002500

250002500025000

1300000250025002500250025002500250025002500250025002500250025002500

250000250050002500250025002500

25000250025002500

Rep Limit Flag

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

Units

500500500500500500500500500500500500500500500500500500

25000500500500500500500500500500500500500500500500

500005005005005005005005000500500500

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

49000BRLBRL


140000055000

BRLBRLBRLBRLBRL

1700007200BRLBRL

37637Seq Number:

Sample Depth:


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1.042Version:



TCL VOCs by 8260B

pH by SW9040B

Analytical Method:

Analytical Method:

Oct-02-07 19:46

Oct-01-07 15:30

Date Analyzed:

Date Analyzed:

MJL01

AJI01

Analyst:

Analyst:

SW5030BPrep Method:

Prep Method:


Date Prep:

MJL01

AJI01

Tech:

Tech:


pH

Parameter

Parameter

360430530

45000

N/A

Result

Result

250025001000

380000

N/A

Rep Limit

Rep Limit

Flag

Flag

ug/Lug/Lug/Lug/L

pH

Units

Units

500500500

25000

1

Dil

Dil

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

12408-02-5

MDL

MDL

BRLBRLBRL

510000

8.2

37637

37628

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:


Sep-25-07 15:00 Date Collected: 12740-010Lab Sample Id:WATERMatrix: CEI-S10 Sample Id:

Anions by SW9056


PCBs by SW8082



Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-05-07 00:46

Oct-02-07 13:10

Oct-04-07 22:35

Oct-02-07 16:00

Oct-02-07 16:48

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

LJB01

AJI01

SK001

NV01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7470A_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 13:35

Oct-01-07 14:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

LJB01

AJI01

BPR01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

ChlorideFluorideNitrateSulfate

Flash Point



Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

0.0620.0240.0270.062

N/A

0.110.100.100.110.110.110.13

650.020

0.0025

Result

Result

Result

Result

Result

1.00.100.101.0

65.0

1.01.01.01.01.01.01.0

1001.0

0.013

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

mg/Lmg/Lmg/Lmg/L

Deg F


mg/Lmg/L

mg/L

Units

Units

Units

Units

Units

1111

1

1111111

11

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

16887-00-616984-48-814797-55-814808-79-8

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

17BRLBRL

3.7

>140


BRLBRL

BRL

37656

37620

37663

37605

37608

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

360990490440370490640

1400400370410410410370300640

13001100690340480680

1400370450300

1100690610400380500400370330500

3200310380460280880340370420

Result

250025002500250025002500250025002500250025002500250025002500

2500025000250002500025002500250025002500250025002500250025002500250025002500250025002500500025002500250025002500250025002500

Rep Limit Flag


Units

500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500500

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


320000BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

37637Seq Number:

Sample Depth:


Page 62 of 97

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1.042Version:



TCL VOCs by 8260B

pH by SW9040B

Analytical Method:

Analytical Method:

Oct-02-07 20:13

Oct-01-07 15:30

Date Analyzed:

Date Analyzed:

MJL01

AJI01

Analyst:

Analyst:

SW5030BPrep Method:

Prep Method:


Date Prep:

MJL01

AJI01

Tech:

Tech:


pH

Parameter

Parameter

360430530900

N/A

Result

Result

2500250010007500

N/A

Rep Limit

Rep Limit

Flag

Flag

ug/Lug/Lug/Lug/L

pH

Units

Units

500500500500

1

Dil

Dil

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

12408-02-5

MDL

MDL

BRLBRLBRL

11000

8.2

37637

37628

Seq Number:

Seq Number:

Sample Depth:


Page 63 of 97

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1.042Version:


Sep-25-07 15:00 Date Collected: 12740-011Lab Sample Id:SLUDGEMatrix: CEI-S11 Sample Id:


PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 22:58

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 14:06

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

120


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 64 of 97

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*


1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


Page 65 of 97

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*


1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

370580540330390570430790420630290390450490330

4400550

16003400250240470

1200710360280

1200360

1100320260460480580280370460340530

1100360500290380330

Result

240024002400240024002400240024002400240024002400240024002400

2400024000240002400024002400240024002400240049002400240024002400240024002400240024002400240024002400240024002400240024002400

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

26000BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

240000BRLBRLBRLBRL6000BRLBRLBRL

37646Seq Number:

Sample Depth:


Page 67 of 97

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*


1.042Version:



TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-03-07 17:00

Oct-03-07 20:10

Oct-02-07 17:46

Oct-01-07 14:08

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-03-07 11:24

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

3401700980910

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

2400240024007300

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

50505050

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL8100

BRLBRL

BRL


37646

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 68 of 97

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*


1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 00:43

Oct-02-07 16:20

Oct-02-07 21:09

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Oct-02-07 11:20

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37632

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


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1.042Version:





Prep Method:


pH

Parameter

N/A

Result

N/A

Rep Limit Flag

pH

Units

1

DilCas Number

12408-02-5

MDL

8.37

37627Seq Number:

Sample Depth:


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*


1.042Version:




PCBs by SW8082




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 13:10

Oct-04-07 23:21

Oct-02-07 16:00

Oct-02-07 20:00

Oct-03-07 14:10

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

SK001

NV01

CW01

MSN01

Analyst:

Analyst:

Analyst:

Analyst:

Analyst:

SW3580A

SW7.3

SW7.3

SW7471_DIG

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 14:00

Oct-02-07 11:00

Oct-02-07 15:00

Oct-02-07 09:30

Date Prep:

Date Prep:

Date Prep:

Date Prep:

Date Prep:

AJI01

BPR01

NV01

NV01

MSN01

Tech:

Tech:

Tech:

Tech:

Tech:

Flash Point


Reactive Cyanide

Reactive Sulfide

Mercury

Parameter

Parameter

Parameter

Parameter

Parameter

N/A

0.110.100.100.110.110.110.13

0.020

2.0

0.010

Result

Result

Result

Result

Result

65.0

1.01.01.01.01.01.01.0

1.0

100

0.049

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

Flag

Deg F


mg/kg

mg/kg

mg/kg

Units

Units

Units

Units

Units

1

1111111

1

1

1

Dil

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

Cas Number

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

57-12-5

7439-97-6

MDL

MDL

MDL

MDL

MDL

>140


BRL

BRL

BRL

37623

37663

37616

37611

37653

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 71 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180000016000001600000160000018000001900000130000018000001600000160000013000001800000180000015000001400000130000013000001500000300000014000001700000170000014000001700000190000015000001200000140000017000001500000160000015000001600000170000017000001500000120000014000001600000170000013000001900000130000016000001500000

Result

100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000100000001000000010000000200000001000000020000000200000002000000020000000100000001000000010000000100000002000000020000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100100

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


Page 72 of 97

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*


1.042Version:





SW3580APrep Method:



Parameter

180000017000001300000120000017000001100000170000016000001800000100000016000001800000140000021000001800000170000014000001700000

Result

100000001000000010000000100000001000000010000000100000001000000010000000100000001000000010000000100000001000000020000000100000001000000010000000

Rep Limit Flag


Units

100100100100100100100100100100100100100100100100100100

DilCas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

MDL


37606Seq Number:

Sample Depth:


Page 73 of 97

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*


1.042Version:





SW5030BPrep Method:



Parameter

370590550330400570430800430640300400460490340

4500560

16003400250250480

1200720370290

1200370

1100330270470490580280380470340540

1100370510290390330

Result

250025002500250025002500250025002500250025002500250025002500

2500025000250002500025002500250025002500250050002500250025002500250025002500250025002500250025002500250025002500250025002500

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL

BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRL

11000BRLBRLBRL8100BRLBRL

580002600BRLBRL

37646Seq Number:

Sample Depth:


Page 74 of 97

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*


1.042Version:



TCL VOCs by 8260B




Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-03-07 17:25

Oct-03-07 20:40

Oct-02-07 17:49

Oct-01-07 14:15

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

SK001

MSN01

MCJ01

Analyst:

Analyst:

Analyst:

Analyst:

SW5030B

EXT_SW8151

SW7470A_DIG

SW3005A

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-03-07 11:24

Oct-02-07 13:00

Oct-01-07 10:00

Sep-27-07 09:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

MJL01

VHB01

MSN01

MSN01

Tech:

Tech:

Tech:

Tech:



Mercury


Parameter

Parameter

Parameter

Parameter

35017001000920

0.00150.0024

0.000260

0.0008730.0005650.0001780.00172

0.0005030.00809

0.000570

Result

Result

Result

Result

2500250025007400

0.00500.0050

0.0200

1.001.001.001.001.001.001.00

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag


mg/Lmg/L

mg/L


Units

Units

Units

Units

50505050

11

1

1111111

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

93-72-194-75-7

7439-97-6

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

MDL

MDL

MDL

MDL

BRLBRLBRL

50000

BRLBRL

BRL


37646

37640

37610

37592

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 75 of 97

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1.042Version:






Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 01:02

Oct-02-07 16:49

Oct-02-07 14:56

Date Analyzed:

Date Analyzed:

Date Analyzed:

SK001

CTP01

MJL01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 14:00

Sep-28-07 11:30

Oct-02-07 11:20

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MJL01

Tech:

Tech:

Tech:




Parameter

Parameter

Parameter

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

0.00500.0010

0.000500.000500.000500.00500.020

0.100.100.100.100.100.200.100.100.100.100.200.10

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag




Units

Units

Units

1111111

111111111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL




37603

37594

37632

Seq Number:

Seq Number:

Seq Number:

Sample Depth:


Page 76 of 97

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*


1.042Version:

Sep-26-07 16:20 Date Received:

Date Received:

Date Received:

% Moisture:

% Moisture:

% Moisture:

Sep-25-07 15:00 Date Collected:

Date Collected:

Date Collected:

12740-012

303858 BLK

303876 BLK

Lab Sample Id:

Lab Sample Id:

Lab Sample Id:

SLUDGE

SOIL

SOIL

Matrix:

Matrix:

Matrix:

CEI-S12

303858 BLK

303876 BLK

Sample Id:

Sample Id:

Sample Id:

pH by SW9045C



Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 16:15

Oct-01-07 12:19

Sep-28-07 10:38

Date Analyzed:

Date Analyzed:

Date Analyzed:

AJI01

MCJ01

MJL01

Analyst:

Analyst:

Analyst:

SW3005A

SW5030B

Prep Method:

Prep Method:

Prep Method:

Sep-27-07 09:00

Sep-28-07 07:59

Date Prep:

Date Prep:

Date Prep:

AJI01

MSN01

MJL01

Tech:

Tech:

Tech:

pH



Parameter

Parameter

Parameter

N/A

0.0003940.000240

0.00006800.000474

0.00007400.0009200.000176

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

Result

Result

N/A

1.001.001.001.001.001.001.00

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

pH



Units

Units

Units

1

1111111

10101010101010101010

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

12408-02-5

7440-38-27440-39-37440-43-97440-47-37439-92-17782-49-27440-22-4

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL

MDL

MDL

9.94

BRLBRLBRLBRLBRL

0.0680BRL


37627

37592

37572

Seq Number:

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:

Sample Depth:


Page 77 of 97

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1.042Version:

Date Received:

Date Received:

Date Received:

% Moisture:

% Moisture:

% Moisture:

Date Collected:

Date Collected:

Date Collected:

303877 BLK

303878 BLK

303894 BLK

Lab Sample Id:

Lab Sample Id:

Lab Sample Id:

SOIL

SOIL

WATER

Matrix:

Matrix:

Matrix:

303877 BLK

303878 BLK

303894 BLK

Sample Id:

Sample Id:

Sample Id:




Analytical Method:

Analytical Method:

Analytical Method:

Oct-01-07 14:39

Oct-01-07 21:32

Oct-02-07 15:50

Date Analyzed:

Date Analyzed:

Date Analyzed:

CTP01

SK001

MSN01

Analyst:

Analyst:

Analyst:

SW3510C

SW3510C

SW7470A_DIG

Prep Method:

Prep Method:

Prep Method:

Sep-28-07 11:30

Sep-28-07 14:00

Oct-01-07 14:00

Date Prep:

Date Prep:

Date Prep:

BPR01

BPR01

MSN01

Tech:

Tech:

Tech:



Mercury

Parameter

Parameter

Parameter

0.00810.0240.0180.0120.0200.0220.0180.0120.013

0.00850.0480.025

0.00130.0000570.0000250.0000340.0000260.000290.0094

0.00010

Result

Result

Result

0.100.100.100.100.100.200.100.100.100.100.200.10

0.00500.0010

0.000500.000500.000500.00500.020

0.0020

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag



mg/L

Units

Units

Units

111111111111

1111111

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

106-46-795-95-488-06-2121-14-295-48-7108-39-4118-74-187-68-367-72-198-95-387-86-5110-86-1

57-74-972-20-858-89-976-44-81024-57-372-43-58001-35-2

7439-97-6

MDL

MDL

MDL



BRL

37594

37603

37608

Seq Number:

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:

Sample Depth:


Page 78 of 97

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1.042Version:


Date Collected: 303895 BLKLab Sample Id:SOILMatrix: 303895 BLK Sample Id:

TCLP Mercury by SW1311/7470AAnalytical Method:

Oct-02-07 16:52 Date Analyzed: MSN01Analyst:

SW7470A_DIGPrep Method:

Oct-01-07 10:00 Date Prep: MSN01Tech:

Mercury

Parameter

0.000260

Result

0.0200

Rep Limit Flag

mg/L

Units

1

DilCas Number

7439-97-6

MDL

BRL

37610Seq Number:

Sample Depth:


Page 79 of 97

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1.042Version:





SW5030BPrep Method:



Parameter

385956344058448143653040465034

46056

160340262548

120733729

12037

12033274750592838473555

1103752293934

Result

250250250250250250250250250250250250250250250

2500250025002500250250250250250250500250250250250250250250250250250250250250250250250250250250

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37631Seq Number:

Sample Depth:


Page 80 of 97

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1.042Version:

Date Received:

Date Received:

% Moisture:

% Moisture:

Date Collected:

Date Collected:

303899 BLK

303901 BLK

Lab Sample Id:

Lab Sample Id:

SOIL

SOIL

Matrix:

Matrix:

303899 BLK

303901 BLK

Sample Id:

Sample Id:

TCL VOCs by 8260B


Analytical Method:

Analytical Method:

Oct-01-07 12:47

Oct-03-07 13:05

Date Analyzed:

Date Analyzed:

MJL01

MSN01

Analyst:

Analyst:

SW5030B

SW7471_DIG

Prep Method:

Prep Method:

Oct-01-07 09:31

Oct-02-07 09:30

Date Prep:

Date Prep:

MJL01

MSN01

Tech:

Tech:


Mercury

Parameter

Parameter

3518010093

0.011

Result

Result

250250250750

0.050

Rep Limit

Rep Limit

Flag

Flag


mg/kg

Units

Units

50505050

1

Dil

Dil

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

7439-97-6

MDL

MDL

BRLBRLBRLBRL

BRL

37631

37653

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:


Page 81 of 97

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1.042Version:





SW3580APrep Method:



Parameter

180001600016000160001800019000130001800016000160001300018000180001500014000130001300015000300001400017000170001400017000190001500012000140001700015000160001500016000170001700015000120001400016000170001300019000130001600015000

Result

100000100000100000100000100000100000100000100000200000100000100000100000100000100000100000200000100000200000200000200000200000100000100000100000100000200000200000100000100000100000100000100000100000100000100000100000100000100000100000100000100000100000100000100000100000

Rep Limit Flag


Units

111111111111111111111111111111111111111111111

DilCas Number

120-82-195-50-1541-73-1106-46-795-95-488-06-2120-83-2105-67-951-28-5121-14-2606-20-291-58-795-57-891-57-695-48-788-74-488-75-591-94-1108-39-499-09-2534-52-1101-55-359-50-7106-47-87005-72-3100-01-6100-02-783-32-9208-96-8120-12-756-55-350-32-8205-99-2191-24-2207-08-985-68-7111-91-1111-44-4117-81-786-74-8218-01-953-70-3132-64-984-66-2131-11-3

MDL


37606Seq Number:

Sample Depth:


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1.042Version:

Date Received:

Date Received:

% Moisture:

% Moisture:

Date Collected:

Date Collected:

303904 BLK

303907 BLK

Lab Sample Id:

Lab Sample Id:

SOIL

NONAQUEOUS

Matrix:

Matrix:

303904 BLK

303907 BLK

Sample Id:

Sample Id:

TCL SVOCs by SW8270C

PCBs by SW8082

Analytical Method:

Analytical Method:

Oct-02-07 17:19

Oct-04-07 17:39

Date Analyzed:

Date Analyzed:

CTP01

SK001

Analyst:

Analyst:

SW3580A

SW3580A

Prep Method:

Prep Method:

Oct-02-07 12:30

Oct-02-07 14:00

Date Prep:

Date Prep:

BPR01

BPR01

Tech:

Tech:



Parameter

Parameter

180001700013000120001700011000170001600018000100001600018000140002100018000170001400017000

0.110.100.100.110.110.110.13

Result

Result

100000100000100000100000100000100000100000100000100000100000100000100000100000100000200000100000100000100000

1.01.01.01.01.01.01.0

Rep Limit

Rep Limit

Flag

Flag



Units

Units

111111111111111111

1111111

Dil

Dil

Cas Number

Cas Number

84-74-2117-84-0206-44-086-73-7118-74-187-68-377-47-467-72-1193-39-578-59-191-20-398-95-3621-64-786-30-687-86-585-01-8108-95-2129-00-0

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

MDL

MDL



37606

37663

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:


Page 83 of 97

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1.042Version:

Date Received:

Date Received:

Date Received:

Date Received:

% Moisture:

% Moisture:

% Moisture:

% Moisture:

Date Collected:

Date Collected:

Date Collected:

Date Collected:

303909 BLK

303911 BLK

303915 BLK

303922 BLK

Lab Sample Id:

Lab Sample Id:

Lab Sample Id:

Lab Sample Id:

NONAQUEOUS

SOIL

SOIL

SOIL

Matrix:

Matrix:

Matrix:

Matrix:

303909 BLK

303911 BLK

303915 BLK

303922 BLK

Sample Id:

Sample Id:

Sample Id:

Sample Id:





Analytical Method:

Analytical Method:

Analytical Method:

Analytical Method:

Oct-02-07 16:00

Oct-02-07 20:00

Oct-02-07 16:00

Oct-03-07 15:07

Date Analyzed:

Date Analyzed:

Date Analyzed:

Date Analyzed:

NV01

CW01

NV01

SK001

Analyst:

Analyst:

Analyst:

Analyst:

SW7.3

SW7.3

SW7.3

EXT_SW8151

Prep Method:

Prep Method:

Prep Method:

Prep Method:

Oct-02-07 13:35

Oct-02-07 15:00

Oct-02-07 11:00

Oct-02-07 13:00

Date Prep:

Date Prep:

Date Prep:

Date Prep:

NV01

NV01

NV01

VHB01

Tech:

Tech:

Tech:

Tech:


Reactive Cyanide Reactive Sulfide

Reactive Cyanide


Parameter

Parameter

Parameter

Parameter

650.020

0.0202.0

0.020

0.00150.0024

Result

Result

Result

Result

1001.0

1.0100

1.0

0.00500.0050

Rep Limit

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag

Flag

mg/Lmg/L

mg/kgmg/kg

mg/kg

mg/Lmg/L

Units

Units

Units

Units

11

11

1

11

Dil

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

Cas Number

57-12-5

57-12-5

57-12-5

93-72-194-75-7

MDL

MDL

MDL

MDL

BRLBRL

BRLBRL

BRL

BRLBRL

37605

37611

37616

37640

Seq Number:

Seq Number:

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:

Sample Depth:

Sample Depth:


Page 84 of 97

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1.042Version:



TCLP VOCs by SW1311/8260BAnalytical Method:


SW5030BPrep Method:



Parameter

0.0150.0130.0220.0100.0120.0170.0110.0120.0110.014

Result

0.0500.0500.45

0.0500.0500.0500.0500.0500.0500.020

Rep Limit Flag


Units

10101010101010101010

DilCas Number

75-35-4107-06-278-93-371-43-256-23-5108-90-767-66-3127-18-479-01-675-01-4

MDL


37632Seq Number:

Sample Depth:


Page 85 of 97

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*


1.042Version:





SW5030BPrep Method:



Parameter

385956344058448143653040465034

46056

160340262548

120733729

12037

12033274750592838473555

1103752293934

Result

250250250250250250250250250250250250250250250

2500250025002500250250250250250250500250250250250250250250250250250250250250250250250250250250

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37633Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

3518010093

Result

250250250750

Rep Limit Flag


Units

50505050

DilCas Number

79-01-675-69-475-01-41330-20-7

MDL

BRLBRLBRLBRL

37633Seq Number:

Sample Depth:


Page 87 of 97

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1.042Version:


Date Collected: 303929 BLKLab Sample Id:WATERMatrix: 303929 BLK Sample Id:



SW5030BPrep Method:



Parameter

0.712.0

0.970.880.740.981.32.8

0.790.730.820.820.810.740.591.32.52.21.4

0.670.961.42.7

0.730.890.592.21.41.2

0.800.760.990.790.730.661.06.4

0.620.760.920.561.8

0.680.730.84

Result

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0505050505.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0105.05.05.05.05.05.05.05.0

Rep Limit Flag


Units

111111111111111111111111111111111111111111111

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37637Seq Number:

Sample Depth:


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1.042Version:





SW5030BPrep Method:



Parameter

0.720.851.11.8

Result

5.05.02.015

Rep Limit Flag

ug/Lug/Lug/Lug/L

Units

1111

DilCas Number

79-01-675-69-475-01-41330-20-7

MDL

BRLBRLBRLBRL

37637Seq Number:

Sample Depth:


Page 89 of 97

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*


1.042Version:





SW5030BPrep Method:



Parameter

385956344058448143653040465034

46056

160340262548

120733729

12037

12033274750592838473555

1103752293934

Result

250250250250250250250250250250250250250250250

2500250025002500250250250250250250500250250250250250250250250250250250250250250250250250250250

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37646Seq Number:

Sample Depth:


Page 90 of 97

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*


1.042Version:





SW5030BPrep Method:



Parameter

3518010093

Result

250250250750

Rep Limit Flag


Units

50505050

DilCas Number

79-01-675-69-475-01-41330-20-7

MDL

BRLBRLBRLBRL

37646Seq Number:

Sample Depth:


Page 91 of 97

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*


1.042Version:




Oct-03-07 13:27 Date Analyzed: MDS01Analyst:

SW5030BPrep Method:



Parameter

0.712.0

0.970.880.740.981.32.8

0.790.730.820.820.810.740.591.32.52.21.4

0.670.961.42.7

0.730.890.592.21.41.2

0.800.760.990.790.730.661.06.4

0.620.760.920.561.8

0.680.730.84

Result

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0505050505.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0105.05.05.05.05.05.05.05.0

Rep Limit Flag


Units

111111111111111111111111111111111111111111111

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37654Seq Number:

Sample Depth:


Page 92 of 97

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*


1.042Version:




Oct-03-07 13:27 Date Analyzed: MDS01Analyst:

SW5030BPrep Method:



Parameter

0.720.851.11.8

Result

5.05.02.015

Rep Limit Flag

ug/Lug/Lug/Lug/L

Units

1111

DilCas Number

79-01-675-69-475-01-41330-20-7

MDL

BRLBRLBRLBRL

37654Seq Number:

Sample Depth:


Page 93 of 97

12740

*


1.042Version:





SW5030BPrep Method:



Parameter

0.712.0

0.970.880.740.981.32.8

0.790.730.820.820.810.740.591.32.52.21.4

0.670.961.42.7

0.730.890.592.21.41.2

0.800.760.990.790.730.661.06.4

0.620.760.920.561.8

0.680.730.84

Result

5.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0505050505.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0105.05.05.05.05.05.05.05.0

Rep Limit Flag


Units

111111111111111111111111111111111111111111111

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37655Seq Number:

Sample Depth:


Page 94 of 97

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*


1.042Version:





SW5030BPrep Method:



Parameter

0.720.851.11.8

Result

5.05.02.015

Rep Limit Flag

ug/Lug/Lug/Lug/L

Units

1111

DilCas Number

79-01-675-69-475-01-41330-20-7

MDL

BRLBRLBRLBRL

37655Seq Number:

Sample Depth:


Page 95 of 97

12740

*


1.042Version:





SW5030BPrep Method:



Parameter

385956344058448143653040465034

46056

160340262548

120733729

12037

12033274750592838473555

1103752293934

Result

250250250250250250250250250250250250250250250

2500250025002500250250250250250250500250250250250250250250250250250250250250250250250250250250

Rep Limit Flag


Units

505050505050505050505050505050505050505050505050505050505050505050505050505050505050505050

DilCas Number

71-55-679-34-576-13-179-00-575-34-375-35-4120-82-196-12-8106-93-495-50-1107-06-2540-59-078-87-5541-73-1106-46-778-93-3591-78-6108-10-167-64-171-43-275-27-475-25-274-83-975-15-056-23-5108-90-775-00-367-66-374-87-3156-59-210061-01-5110-82-7124-48-175-71-8100-41-498-82-879-20-91634-04-4108-87-275-09-2100-42-5127-18-4108-88-3156-60-510061-02-6

MDL


37659Seq Number:

Sample Depth:


Page 96 of 97

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*


1.042Version:

Date Received:

Date Received:

Date Received:

% Moisture:

% Moisture:

% Moisture:

Date Collected:

Date Collected:

Date Collected:

303944 BLK

37620 BLK

37623 BLK

Lab Sample Id:

Lab Sample Id:

Lab Sample Id:

SOIL

NONAQUEOUS

SOLID

Matrix:

Matrix:

Matrix:

303944 BLK

37620 BLK

37623 BLK

Sample Id:

Sample Id:

Sample Id:

TCL VOCs by 8260B



Analytical Method:

Analytical Method:

Analytical Method:

Oct-04-07 10:18

Oct-02-07 13:10

Oct-02-07 13:10

Date Analyzed:

Date Analyzed:

Date Analyzed:

MJL01

AJI01

AJI01

Analyst:

Analyst:

Analyst:

SW5030BPrep Method:

Prep Method:

Prep Method:


Date Prep:

Date Prep:

MJL01

AJI01

AJI01

Tech:

Tech:

Tech:


Flash Point

Flash Point

Parameter

Parameter

Parameter

3518010093

N/A

N/A

Result

Result

Result

250250250750

65.0

65.0

Rep Limit

Rep Limit

Rep Limit

Flag

Flag

Flag


Deg F

Deg F

Units

Units

Units

50505050

1

1

Dil

Dil

Dil

Cas Number

Cas Number

Cas Number

79-01-675-69-475-01-41330-20-7

MDL

MDL

MDL

BRLBRLBRLBRL

>140

>140

37659

37620

37623

Seq Number:

Seq Number:

Seq Number:

Sample Depth:

Sample Depth:

Sample Depth:


Page 97 of 97

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*


1.042Version:



Anions by SW9056Analytical Method:

Oct-04-07 17:32 Date Analyzed: LJB01Analyst:

Prep Method:

Date Prep: LJB01Tech:

ChlorideFluorideNitrateSulfate

Parameter

0.0620.0240.0270.062

Result

1.00.100.101.0

Rep Limit Flag

mg/Lmg/Lmg/Lmg/L

Units

1111

DilCas Number

16887-00-616984-48-814797-55-814808-79-8

MDL

BRLBRLBRLBRL

37656Seq Number:

Sample Depth:

Region 4 ERRS

Circle Environmental IProject Name:

Project ID:

Surrogate Recovery [D] = 100 * A / BAll results are based on MDL and validated for QC purposes.

Form 2 - Surrogate Recoveries

12740Work Order #:

* Surrogate outside of Laboratory QC limits** Surrogates outside limits; data and surrogates confirmed by reanalysis*** Poor recoveries due to dilution

Z = Surrogate Recovery exceeded the Labortatory QC limits

10/18/07 13:35Report Date:

1.%Version:

Page 1 of 31

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

Decachlorobiphenyl

Tetrachloro-m-xylene

Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0

1.2

0

1.2

0

1.4

0

1.3

0.725

0.71

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

Z

Z

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

0

240

0

240

0

280

0

260

145

142

SURROGATE RECOVERY STUDY





Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37663

37663

37663

37663

L

L

L

L

L

12740-001 / SMP

12740-001 / SMP

12740-002 / SMP

12740-002 / SMP

12740-003 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 2 of 31

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.575

0.63

0.751

0.72

0.673

0.66

0.619

0.31

0.556

0.52

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

115

126

150

144

135

132

124

62

111

104






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37663

37663

37663

37663

L

L

L

L

L

12740-003 / SMP

12740-004 / SMP

12740-004 / SMP

12740-005 / SMP

12740-005 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 3 of 31

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.602

0.59

0.538

0.51

0.610

0.55

0.586

0.46

0.607

0.56

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

120

118

108

102

122

110

117

92

121

112






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37663

37663

37663

37663

L

L

L

L

L

12740-006 / SMP

12740-006 / SMP

12740-007 / SMP

12740-007 / SMP

12740-008 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 4 of 31

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.546

0.51

0.745

0.68

0.686

0.56

0.738

0.72

0.661

0.66

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

109

102

149

136

137

112

148

144

132

132






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37663

37663

37663

37663

L

L

L

L

L

12740-008 / SMP

12740-009 / SMP

12740-009 / SMP

12740-010 / SMP

12740-010 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 5 of 31

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

PCBs by SW8082

Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.293

0.33

0.265

0.26

0.603

0.53

0.577

0.44

0.000638

0.00054

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

0.500

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

19-203

19-191

19-203

19-191

19-203

19-191

19-203

19-191

61-152

19-191

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

59

66

53

52

121

106

115

88

128

108






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/kg

mg/kg

mg/kg

mg/kg

mg/kg

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37663

37663

37663

37663

L

L

L

L

L

12740-011 / SMP

12740-011 / SMP

12740-012 / SMP

12740-012 / SMP

303907 BLK / BLK

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 6 of 31

PCBs by SW8082



Decachlorobiphenyl


2,4,6-Tribromophenol

2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0.000602

0.00048

0

0

0

0

0

0

0

0

0

0

0

0

0.500

0.50

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

61-152

19-191

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

ControlLimits %R

ControlLimits %R

ControlLimits %R

120

96

0

0

0

0

0

0

0

0

0

0

0

0




Matrix:

Matrix:

Matrix:

mg/kg

ug/kg

ug/kg

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37663

37606

37606

L

S

S

303907 BLK / BLK

12740-001 / SMP

12740-002 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 7 of 31





2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

ControlLimits %R

ControlLimits %R

ControlLimits %R

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0




Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37606

37606

37606

S

S

S

12740-003 / SMP

12740-004 / SMP

12740-005 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 8 of 31





2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

ControlLimits %R

ControlLimits %R

ControlLimits %R

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0




Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37606

37606

37606

S

S

S

12740-006 / SMP

12740-007 / SMP

12740-008 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 9 of 31





2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

33-112

19-105

23-100

12-105

25-100

20-138

ControlLimits %R

ControlLimits %R

ControlLimits %R

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0




Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37606

37606

37606

S

S

S

12740-009 / SMP

12740-010 / SMP

12740-011 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 10 of 31



TCL VOCs by 8260B


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

1,2-Dichloroethane-d4

4-Bromofluorobenzene

Toluene-d8

0

0

0

0

0

0

868100

422500

921400

393400

819400

405100

60.54

59.76

56.10

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

1000000

500000

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

Z

Z

Z

Z

33-112

19-105

23-100

12-105

25-100

20-138

37-93

41-94

33-100

29-105

35-100

47-107

53-135

53-175

56-126

ControlLimits %R

ControlLimits %R

ControlLimits %R

0

0

0

0

0

0

87

85

92

79

82

81

121

120

112




Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37606

37606

37631

S

S

S

12740-012 / SMP

303904 BLK / BLK

12740-001 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 11 of 31

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Toluene-d8



Toluene-d8



Toluene-d8



Toluene-d8

59.86

59.57

55.83

59.33

58.43

55.16

56.81

59.57

56.11

55.21

67.06

56.47

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-135

53-175

56-126

53-135

53-175

56-126

53-135

53-175

56-126

53-135

53-175

56-126

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

120

119

112

119

117

110

114

119

112

110

134

113





Matrix:

Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37631

37631

37631

37631

S

S

S

S

12740-002 / SMP

12740-003 / SMP

12740-004 / SMP

12740-006 / SMP

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 12 of 31

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Toluene-d8



Toluene-d8



Toluene-d8



Toluene-d8

54.02

57.03

53.92

50.14

56.49

55.23

59.93

59.57

52.47

56.35

57.72

53.83

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-135

53-175

56-126

53-135

53-175

56-126

58-128

47-166

68-120

53-135

53-175

56-126

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

108

114

108

100

113

110

120

119

105

113

115

108





Matrix:

Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37631

37631

37631

37633

S

S

S

S

12740-007 / SMP

12740-008 / SMP

303899 BLK / BLK

12740-003 DL / DIL

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 13 of 31

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Toluene-d8



Toluene-d8



Toluene-d8



Toluene-d8

55.62

58.38

54.13

56.00

62.37

55.10

49.55

57.63

55.40

57.01

57.16

54.50

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-135

53-175

56-126

53-135

53-175

56-126

53-135

53-175

56-126

58-128

47-166

68-120

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

111

117

108

112

125

110

99

115

111

114

114

109





Matrix:

Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37633

37633

37633

37633

S

S

S

S

12740-004 DL / DIL

12740-005 / SMP

12740-006 DL / DIL

303927 BLK / BLK

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 14 of 31

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B


Bromofluorobenzene

Toluene-d8


Bromofluorobenzene

Toluene-d8


Bromofluorobenzene

Toluene-d8



Toluene-d8

55.86

55.95

55.58

55.04

56.72

54.64

57.01

57.16

54.50

46.51

59.45

49.06

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-159

30-186

83-136

53-159

30-186

83-136

64-136

66-148

86-127

53-135

53-175

56-126

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

112

112

111

110

113

109

114

114

109

93

119

98





Matrix:

Matrix:

Matrix:

Matrix:

ug/L

ug/L

ug/L

ug/kg

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37637

37637

37637

37646

W

W

W

S

12740-009 / SMP

12740-010 / SMP

303929 BLK / BLK

12740-001 DL / DIL

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Toluene-d8



Toluene-d8



Toluene-d8



Toluene-d8

47.28

59.01

49.63

50.38

47.12

49.37

45.57

57.20

48.84

47.02

57.77

49.83

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-135

53-175

56-126

53-135

53-175

56-126

53-135

53-175

56-126

53-135

53-175

56-126

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

95

118

99

101

94

99

91

114

98

94

116

100





Matrix:

Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

ug/kg

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37646

37646

37646

37646

S

S

S

S

12740-002 DL / DIL

12740-007 DL / DIL

12740-007 DL2 / DIL

12740-008 DL / DIL

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Toluene-d8



Toluene-d8



Toluene-d8


Bromofluorobenzene

Toluene-d8

48.44

58.38

50.40

47.51

57.79

50.35

50.29

56.49

49.89

45.11

59.52

50.61

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-135

53-175

56-126

53-135

53-175

56-126

58-128

47-166

68-120

53-159

30-186

83-136

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

97

117

101

95

116

101

101

113

100

90

119

101





Matrix:

Matrix:

Matrix:

Matrix:

ug/kg

ug/kg

ug/kg

ug/L

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37646

37646

37646

37654

S

S

S

W

12740-011 / SMP

12740-012 / SMP

303933 BLK / BLK

12740-009 DL / DIL

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B


Bromofluorobenzene

Toluene-d8


Bromofluorobenzene

Toluene-d8


Bromofluorobenzene

Toluene-d8


Bromofluorobenzene

Toluene-d8

44.75

58.91

48.43

44.57

58.68

48.91

50.29

56.49

49.89

37.82

45.90

46.75

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

53-159

30-186

83-136

53-159

30-186

83-136

64-136

66-148

86-127

53-159

30-186

83-136

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

90

118

97

89

117

98

101

113

100

76

92

94





Matrix:

Matrix:

Matrix:

Matrix:

ug/L

ug/L

ug/L

ug/L

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37654

37654

37654

37655

W

W

W

W

12740-009 DL3 / DIL

12740-010 DL / DIL

303942 BLK / BLK

12740-009 DL2 / DIL

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B



Bromofluorobenzene

Toluene-d8



Toluene-d8



Toluene-d8

2,4-Dichlorophenylacetic Acid

37.49

46.89

47.09

38.66

43.85

47.36

37.49

46.89

47.09

0.72

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

50.00

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

64-136

66-148

86-127

53-135

53-175

56-126

58-128

47-166

68-120

6-127

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

75

94

94

77

88

95

75

94

94

144





Matrix:

Matrix:

Matrix:

Matrix:

ug/L

ug/kg

ug/kg

mg/L

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37655

37659

37659

37640

W

S

S

S

303943 BLK / BLK

12740-008 DL2 / DIL

303944 BLK / BLK

12740-003 / SMP

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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0.44

0.45

0.39

0.43

0.36

0.50

0.50

0.50

0.50

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

6-127

6-127

6-127

6-127

6-127

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

88

90

78

86

72






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37640

37640

37640

37640

37640

S

S

S

S

S

12740-003 / SMP

12740-004 / SMP

12740-004 / SMP

12740-005 / SMP

12740-005 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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0.27

0.26

16

2.4

0.50

0.50

0.50

0.50

0.50

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

6-127

6-127

6-127

6-127

6-127

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

54

52

3200

480

100






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37640

37640

37640

37640

37640

S

S

S

S

S

12740-006 / SMP

12740-006 / SMP

12740-007 / SMP

12740-007 / SMP

12740-008 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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0.32

0.36

0.37

0.32

0.21

0.50

0.50

0.50

0.50

0.50

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

6-127

6-127

6-127

6-127

6-127

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

64

72

74

64

42






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37640

37640

37640

37640

37640

S

S

S

S

S

12740-008 / SMP

12740-011 / SMP

12740-011 / SMP

12740-012 / SMP

12740-012 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.000096

0.00013

0.005294

0.004110

0.005337

0.004383

0.005211

0.003519

0.50

0.50

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

11-98

11-98

0-128

20-110

0-128

20-110

0-128

20-110

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

19

26

106

82

107

88

104

70






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37640

37640

37603

37603

37603

S

S

S

S

S

303922 BLK / BLK

303922 BLK / BLK

12740-003 / SMP

12740-003 / SMP

12740-004 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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1.%Version:

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Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.005226

0.003821

0.004428

0.003585

0.004861

0.003077

0.003276

0.001496

0.003256

0.001545

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

0-128

20-110

0-128

20-110

0-128

20-110

0-128

20-110

0-128

20-110

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

105

76

89

72

97

62

66

30

65

31






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37603

37603

37603

37603

37603

S

S

S

S

S

12740-004 / SMP

12740-005 / SMP

12740-005 / SMP

12740-006 / SMP

12740-006 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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1.%Version:

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Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.004717

0.005220

0.004902

0.005638

0.004802

0.003544

0.005117

0.004785

0.004813

0.003523

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

0-128

20-110

0-128

20-110

0-128

20-110

0-128

20-110

0-128

20-110

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

94

104

98

113

96

71

102

96

96

70






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37603

37603

37603

37603

37603

S

S

S

S

S

12740-007 / SMP

12740-007 / SMP

12740-008 / SMP

12740-008 / SMP

12740-011 / SMP

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


Decachlorobiphenyl


0.004795

0.003779

0.005835

0.003761

0.005865

0.004732

0.000005600

0.000005000

0.000005600

0.000005100

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

0.005000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

0-128

20-110

0-128

20-110

0-128

20-110

39-127

32-107

39-127

32-107

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

96

76

117

75

117

95

113

100

111

102






Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37603

37603

37603

37603

37603

S

S

S

S

S

12740-011 / SMP

12740-012 / SMP

12740-012 / SMP

303878 BLK / BLK

303878 BLK / BLK

Sample:

Sample:

Sample:

Sample:

Sample:

1

1

1

1

1

Batch:

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



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2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0.6545

0.2951

0.5056

0.2672

0.4435

0.3068

0.5893

0.2586

0.4460

0.2271

0.4642

0.2993

0.5857

0.2455

0.3901

0.2131

0.4020

0.2663

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

ControlLimits %R

ControlLimits %R

ControlLimits %R

65

59

51

53

44

61

59

52

45

45

46

60

59

49

39

43

40

53




Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37594

37594

37594

S

S

S

12740-003 / SMP

12740-004 / SMP

12740-005 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 27 of 31





2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0.5974

0.2689

0.4705

0.2386

0.4463

0.2926

0.5027

0.2131

0.01766

0.2887

0.0004050

0.2523

0.5989

0.2642

0.5052

0.2526

0.4589

0.2896

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Z

Z

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

ControlLimits %R

ControlLimits %R

ControlLimits %R

60

54

47

48

45

59

50

43

2

58

0

50

60

53

51

51

46

58




Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37594

37594

37594

S

S

S

12740-006 / SMP

12740-007 / SMP

12740-008 / SMP

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 28 of 31





2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14


2-Fluorobiphenyl

2-Fluorophenol

Nitrobenzene-d5

Phenol-d5

p-Terphenyl-d14

0.5124

0.2371

0.4486

0.2069

0.4121

0.2428

0.5274

0.2316

0.3834

0.2099

0.3544

0.2818

0.6084

0.3017

0.5262

0.2648

0.4882

0.3390

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

1.000

0.5000

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

35-101

23-106

18-100

20-102

18-95

40-111

ControlLimits %R

ControlLimits %R

ControlLimits %R

51

47

45

41

41

49

53

46

38

42

35

56

61

60

53

53

49

68




Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37594

37594

37594

S

S

S

12740-011 / SMP

12740-012 / SMP

303877 BLK / BLK

Sample:

Sample:

Sample:

1

1

1

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 29 of 31





1,2-Dichloroethane-D4


Toluene-D8



Toluene-D8



Toluene-D8



Toluene-D8

0.0395

0.0449

0.0479

0.0393

0.0473

0.0486

0.0397

0.0463

0.0481

0.0397

0.0457

0.0490

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

72-129

72-126

81-116

72-129

72-126

81-116

72-129

72-126

81-116

72-129

72-126

81-116

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

79

90

96

79

95

97

79

93

96

79

91

98





Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37572

37572

37572

37572

S

S

S

S

12740-003 / SMP

12740-004 / SMP

12740-005 / SMP

12740-006 / SMP

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 30 of 31







Toluene-D8



Toluene-D8



Toluene-D8



Toluene-D8

0.0403

0.0437

0.0482

0.0387

0.0468

0.0485

0.0551

0.0571

0.0544

0.0557

0.0585

0.0546

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

Recovery%R[D]

72-129

72-126

81-116

72-129

77-127

84-114

72-129

72-126

81-116

72-129

72-126

81-116

ControlLimits %R

ControlLimits %R

ControlLimits %R

ControlLimits %R

81

87

96

77

94

97

110

114

109

111

117

109





Matrix:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

mg/L

Units:

Units:

Units:

Units:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37572

37572

37632

37632

S

S

S

S

12740-007 / SMP

303876 BLK / BLK

12740-008 / SMP

12740-011 / SMP

Sample:

Sample:

Sample:

Sample:

1

1

1

1

Batch:

Batch:

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Flags

Flags

Analytes

Analytes

Analytes

Analytes

Region 4 ERRS


Project ID:



12740Work Order #:



10/18/07 13:35Report Date:

1.%Version:

Page 31 of 31





Toluene-D8



Toluene-D8

0.0563

0.0590

0.0553

0.0570

0.0572

0.0545

0.0500

0.0500

0.0500

0.0500

0.0500

0.0500

TrueAmount

[B]

TrueAmount

[B]

Recovery%R[D]

Recovery%R[D]

72-129

72-126

81-116

72-129

77-127

84-114

ControlLimits %R

ControlLimits %R

113

118

111

114

114

109



Matrix:

Matrix:

mg/L

mg/L

Units:

Units:

Lab Batch #:

Lab Batch #:

37632

37632

S

S

12740-012 / SMP

303926 BLK / BLK

Sample:

Sample:

1

1

Batch:

Batch:

AmountFound

[A]

AmountFound

[A]

Flags

Flags

Analytes

Analytes

Region 4 ERRS


Project ID:

Blank Spike Recovery [D] = 100*[C]/[B]All results are based on MDL and validated for QC purposes.

Blank Spike Recovery

12740Work Order #:

ND = Not Detected, J = Present Below Reporting Limit, B = Present in Blank, NR = Not Requested, I = Interference, NA = NotApplicableN = See Narrative, EQL = Estimated Quantitation Limit

10/18/07 13:35Report Date:

Anions by SW9056


TCL VOCs by 8260B

Chloride

Fluoride

Nitrate

Sulfate

1,2,4-Trichlorobenzene

1,4-Dichlorobenzene

2,4-Dinitrotoluene

2-Chlorophenol

4-Chloro-3-methylphenol

4-Nitrophenol

Acenaphthene

N-Nitroso-di-n-propylamine

Pentachlorophenol

Phenol

Pyrene

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

<1.0

<0.10

<0.10

<1.0

<100000

<100000

<100000

<100000

<100000

<200000

<100000

<100000

<200000

<100000

<100000

<250

<250

<500

<250

<250

10

0.50

5.0

10

500000

500000

500000

1000000

1000000

1000000

500000

500000

1000000

1000000

500000

2500

2500

2500

2500

2500

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

Z

71-121

85-116

85-119

81-114

41-86

41-77

42-103

43-79

43-97

10-106

49-90

43-99

18-100

39-77

48-103

47-166

56-155

36-184

43-177

44-168

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

97

104

108

98

80

76

82

84

85

73

74

92

67

75

70

116

88

92

96

88

9.7

0.52

5.4

9.8

400000

380000

410000

840000

850000

730000

370000

460000

670000

750000

350000

2900

2200

2300

2400

2200

BLANK /BLANK SPIKE RECOVERY STUDY



Lab Batch #:

Lab Batch #:

Lab Batch #:

Matrix:

Matrix:

Matrix:

mg/L

ug/kg

ug/kg

Reporting Units:

Reporting Units:

Reporting Units:

37656

37606

37631

W

S

S

BlankResult

[A]

BlankResult

[A]

BlankResult

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

37656 BKS

303904 BKS

303899 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

Region 4 ERRS


Project ID:



12740Work Order #:


10/18/07 13:35Report Date:

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene

Methyl tert-butyl ether

Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

<250

<250

<500

<250

<250

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<250

<250

<500

<250

<250

2500

2500

2500

2500

2500

50

50

50

100

50

50

2500

2500

2500

2500

2500

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

47-166

56-155

36-184

43-177

44-168

74-127

72-122

74-122

50-150

77-121

66-119

47-166

56-155

36-184

43-177

44-168

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

124

100

104

108

96

122

96

102

100

104

90

108

104

104

112

100

3100

2500

2600

2700

2400

61

48

51

100

52

45

2700

2600

2600

2800

2500




Lab Batch #:

Lab Batch #:

Lab Batch #:

Matrix:

Matrix:

Matrix:

ug/kg

ug/L

ug/kg

Reporting Units:

Reporting Units:

Reporting Units:

37633

37637

37646

S

W

S

BlankResult

[A]

BlankResult

[A]

BlankResult

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

303927 BKS

303929 BKS

303933 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

Region 4 ERRS


Project ID:



12740Work Order #:


10/18/07 13:35Report Date:

TCL VOCs by 8260B

TCL VOCs by 8260B

TCL VOCs by 8260B

1,1-Dichloroethene

Benzene

Chlorobenzene


Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene


Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

<250

<250

<500

<250

<250

50

50

50

100

50

50

50

50

50

100

50

50

2500

2500

2500

2500

2500

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

74-127

72-122

74-122

50-150

77-121

66-119

74-127

72-122

74-122

50-150

77-121

66-119

47-166

56-155

36-184

43-177

44-168

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

106

104

104

120

112

100

96

94

104

79

96

98

96

92

104

96

100

53

52

52

120

56

50

48

47

52

79

48

49

2400

2300

2600

2400

2500




Lab Batch #:

Lab Batch #:

Lab Batch #:

Matrix:

Matrix:

Matrix:

ug/L

ug/L

ug/kg

Reporting Units:

Reporting Units:

Reporting Units:

37654

37655

37659

W

W

S

BlankResult

[A]

BlankResult

[A]

BlankResult

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

303942 BKS

303943 BKS

303944 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

Region 4 ERRS


Project ID:



12740Work Order #:


10/18/07 13:35Report Date:




2,4,5-TP (Silvex)

2,4-D

Endrin

Gamma-BHC (Lindane)

Heptachlor

Heptachlor Epoxide

Methoxychlor

1,4-Dichlorobenzene

2,4,5-Trichlorophenol


2,4-Dinitrotoluene

2-Methylphenol

3 & 4-Methylphenol

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene

Pentachlorophenol

Pyridine

<0.0050

<0.0050

<0.0010

<0.00050

<0.00050

<0.00050

<0.0050

<0.10

<0.10

<0.10

<0.10

<0.10

<0.20

<0.10

<0.10

<0.10

<0.10

<0.20

<0.10

0.050

0.050

0.0050

0.0050

0.0050

0.0050

0.015

1.0

1.0

1.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

Z

Z

Z

13-117

11-136

34-140

36-122

33-120

63-111

43-136

16-100

29-106

33-99

27-96

35-98

31-105

43-105

14-106

13-100

32-106

33-104

6-96

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

200

94

140

122

118

138

153

76

70

79

76

80

80

58

78

77

75

61

52

0.10

0.047

0.0070

0.0061

0.0059

0.0069

0.023

0.76

0.70

0.79

0.76

0.80

1.6

0.58

0.78

0.77

0.75

0.61

0.52




Lab Batch #:

Lab Batch #:

Lab Batch #:

Matrix:

Matrix:

Matrix:

mg/L

mg/L

mg/L

Reporting Units:

Reporting Units:

Reporting Units:

37640

37603

37594

S

S

S

BlankResult

[A]

BlankResult

[A]

BlankResult

[A]

Flags

Flags

Flags

Analytes

Analytes

Analytes

303922 BKS

303878 BKS

303877 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

Region 4 ERRS


Project ID:



12740Work Order #:


10/18/07 13:35Report Date:



1,1-Dichloroethene

1,2-Dichloroethane

2-Butanone

Benzene

Carbon Tetrachloride

Chlorobenzene

Chloroform

Tetrachloroethylene

Trichloroethene

Vinyl Chloride

1,1-Dichloroethene

1,2-Dichloroethane

2-Butanone

Benzene


Chlorobenzene

Chloroform

Tetrachloroethylene

Trichloroethene

Vinyl Chloride

<0.050

<0.050

<0.45

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.020

<0.050

<0.050

<0.45

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.020

0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

SpikeAdded

[B]

SpikeAdded

[B]

BlankSpike%R[D]

BlankSpike%R[D]

Z

70-130

70-131

69-134

76-121

72-125

70-130

75-124

78-127

70-130

57-135

70-130

70-131

69-134

76-121

72-125

70-130

75-124

78-127

70-130

57-135

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

106

90

72

104

108

114

100

98

102

116

124

96

81

100

112

106

106

132

96

96

0.53

0.45

0.72

0.52

0.54

0.57

0.50

0.49

0.51

0.58

0.62

0.48

0.81

0.50

0.56

0.53

0.53

0.66

0.48

0.48



Lab Batch #:

Lab Batch #:

Matrix:

Matrix:

mg/L

mg/L

Reporting Units:

Reporting Units:

37572

37632

S

S

BlankResult

[A]

BlankResult

[A]

Flags

Flags

Analytes

Analytes

303876 BKS

303926 BKS

Sample:

Sample:

1

1

Batch #:

Batch #:

BS / BSD Recoveries

12740 Region 4 ERRS


Project ID:

Relative Percent Difference RPD = 200*|(D-G)/(D+G)|Blank Spike Recovery [D] = 100*(C)/[B]Blank Spike Duplicate Recovery [G] = 100*(F)/[E]All results are based on MDL and Validated for QC Purposes

Work Order #:

F = RPD exceeded the laboratory control limits

1.%Version:

10/18/07 13:35Report Date




Flash Point

Flash Point

Reactive Sulfide

Cyanide, Reactive

>140

>140

<100

<1.0

81

81

3100

5.0

99

99

97

90

0

0

0

2

30

20

30

30

70-130

70-130

79-122

65-113

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

99

99

97

92

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

RPD%

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

Flag

Flag

Flag

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

Blk. Spk Dup.%R[G]

Blk. Spk Dup.%R[G]

Blk. Spk Dup.%R[G]

BlankSpike

DuplicateResult [F]

BlankSpike

DuplicateResult [F]

BlankSpike

DuplicateResult [F]

80

80

3000

4.6

80

80

3000

4.5

37620

37623

37605

Lab Batch ID:

Lab Batch ID:

Lab Batch ID:

Matrix:

Matrix:

Matrix:

L

Sd

L

BLANK /BLANK SPIKE / BLANK SPIKE DUPLICATE RECOVERY STUDY



Deg F

Deg F

mg/L

Units:

Units:

Units:

37620 BKS

37623 BKS

303909 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

81

81

3100

5.0

SpikeAdded

[E]

SpikeAdded

[E]

SpikeAdded

[E]

Blank Sample Result

[A]

Blank Sample Result

[A]

Blank Sample Result

[A]

Analytes

Analytes

Analytes

BS / BSD Recoveries

12740 Region 4 ERRS


Project ID:


Work Order #:


1.%Version:





Reactive Sulfide

Reactive Cyanide

Mercury

<100

<1.0

<0.0020

3100

5.0

0.0030

97

90

103

0

2

0

30

30

20

79-122

65-113

85-115

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

97

92

103

BlankSpike%R[D]

BlankSpike%R[D]

BlankSpike%R[D]

RPD%

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

Flag

Flag

Flag

ControlLimits %R

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

BlankSpike

Result[C]

Blk. Spk Dup.%R[G]

Blk. Spk Dup.%R[G]

Blk. Spk Dup.%R[G]

BlankSpike

DuplicateResult [F]

BlankSpike

DuplicateResult [F]

BlankSpike

DuplicateResult [F]

3000

4.6

0.0031

3000

4.5

0.0031

37611

37616

37608

Lab Batch ID:

Lab Batch ID:

Lab Batch ID:

Matrix:

Matrix:

Matrix:

S

S

W




mg/kg

mg/kg

mg/L

Units:

Units:

Units:

303911 BKS

303915 BKS

303894 BKS

Sample:

Sample:

Sample:

1

1

1

Batch #:

Batch #:

Batch #:

3100

5.0

0.0030

SpikeAdded

[E]

SpikeAdded

[E]

SpikeAdded

[E]

Blank Sample Result

[A]

Blank Sample Result

[A]

Blank Sample Result

[A]

Analytes

Analytes

Analytes

BS / BSD Recoveries

12740 Region 4 ERRS


Project ID:


Work Order #:


1.%Version:




Mercury

Mercury

<0.050

<0.0200

0.50

0.0250

104

105

0

1

20

20

85-115

85-115

SpikeAdded

[B]

SpikeAdded

[B]

104

104

BlankSpike%R[D]

BlankSpike%R[D]

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

Flag

Flag

ControlLimits %R

ControlLimits %R

BlankSpike

Result[C]

BlankSpike

Result[C]

Blk. Spk Dup.%R[G]

Blk. Spk Dup.%R[G]

BlankSpike

DuplicateResult [F]

BlankSpike

DuplicateResult [F]

0.52

0.0260

0.52

0.0263

37653

37610

Lab Batch ID:

Lab Batch ID:

Matrix:

Matrix:

S

S



mg/kg

mg/L

Units:

Units:

303901 BKS

303895 BKS

Sample:

Sample:

1

1

Batch #:

Batch #:

0.50

0.0250

SpikeAdded

[E]

SpikeAdded

[E]

Blank Sample Result

[A]

Blank Sample Result

[A]

Analytes

Analytes

BS / BSD Recoveries

12740 Region 4 ERRS

Circle Environmental I Project Name:

Project ID:

Relative Percent Difference RPD = 200*|(D-G)/(D+G)| Blank Spike Recovery [D] = 100*(C)/[B] Blank Spike Duplicate Recovery [G] = 100*(F)/[E] All results are based on MDL and Validated for QC Purposes

Work Order #:


1.043 Version:

Report Date

TAL Metals by SW6020


<0.50 <0.10 <0.10 <0.10 <0.10 <0.10 <0.50 <0.10 <0.10 <0.10 <0.10 <0.50 <0.10 <0.10 <0.50 <0.10 <0.50 <0.10 <0.10 <0.10

0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

103 120 118 117 146 120 106 108 109 110 115 113 110 107 100 101 96 112 101 444

15 5 3 7 5 4

15 3 3 7 4

14 3 4 5 0

11 4 3 5

25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25

Z

Z Z

Z

Z

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

120 126 122 126 153 125 123 111 112 118 120 130 113 111 105 101 107 117 104 469

Blank Spike

%R [D]

RPD

%

Control Limits %RPD

Flag

Control Limits

%R

Blank Spike

Result [C]

Blk. Spk Dup. %R [G]

Blank Spike

Duplicate Result [F]

1.08 0.126 0.122 0.126 0.153 0.125 1.11

0.111 0.112 0.118 0.120 1.17

0.113 0.111 1.89

0.101 0.961 0.117 0.104 0.469

0.930 0.120 0.118 0.117 0.146 0.120 0.954 0.108 0.109 0.110 0.115 1.02

0.110 0.107 1.80

0.101 0.865 0.112 0.101 0.444

37810 Lab Batch ID: Matrix: W

BLANK /BLANK SPIKE / BLANK SPIKE DUPLICATE RECOVERY STUDY mg/L Units:

303884 BKS Sample: 1 Batch #:

0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

Spike Added

[E]

Blank Sample Result

[A] Analytes

BS / BSD Recoveries

12740 Region 4 ERRS


Project ID:


Work Order #:


1.045 Version:

Report Date



<293 <2.15 <4.40 <0.90 <0.65 <1.15 <100 <3.85 <3.40 <3.40 <3.50 <38.2 <0.90 <3.45 <99.0 <0.55 <299 <1.95 <1.20 <3.30 <1.10

900 100 100 100 100 100 900 100 100 100 100 900 100 100

1800 100 900 100

1000 100 100

93 110 107 102 125 102 103 105 105 104 107 99 105 104 88 109 97 106 102 103 103

1 1 0 2 0 1 0 1 1 1 1 2 1 2 0 2 2 1 1 0 0

20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

94 111 107 100 125 103 103 104 104 103 106 101 104 102 88 111 95 105 103 103 103

Blank Spike

%R [D]

RPD

%

Control Limits %RPD

Flag

Control Limits

%R

Blank Spike

Result [C]


Blank Spike


844 111 107 99.9 125 103 928 104 104 103 106 907 104 102

1580 111 855 105

1030 103 103

835 110 107 102 125 102 925 105 105 104 107 893 105 104

1580 109 869 106

1020 103 103

37812 Lab Batch ID: Matrix: S

BLANK /BLANK SPIKE / BLANK SPIKE DUPLICATE RECOVERY STUDY mg/kg Units:


900 100 100 100 100 100 900 100 100 100 100 900 100 100

1800 100 900 100

1000 100 100

Spike Added

[E]

Blank Sample Result

[A] Analytes

BS / BSD Recoveries

12740 Region 4 ERRS


Project ID:


Work Order #:


1.043 Version:

Report Date



<0.50 <0.10 <0.10 <0.10 <0.10 <0.10 <0.50 <0.10 <0.10 <0.10 <0.10 <0.50 <0.10 <0.10 <0.50 <0.10 <0.50 <0.10 <0.10 <0.10

0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

103 120 118 117 146 120 106 108 109 110 115 113 110 107 100 101 96 112 101 444

15 5 3 7 5 4

15 3 3 7 4

14 3 4 5 0

11 4 3 5

25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25

Z

Z Z

Z

Z

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

120 126 122 126 153 125 123 111 112 118 120 130 113 111 105 101 107 117 104 469

Blank Spike

%R [D]

RPD

%

Control Limits %RPD

Flag

Control Limits

%R

Blank Spike

Result [C]


Blank Spike


1.08 0.126 0.122 0.126 0.153 0.125 1.11

0.111 0.112 0.118 0.120 1.17

0.113 0.111 1.89

0.101 0.961 0.117 0.104 0.469

0.930 0.120 0.118 0.117 0.146 0.120 0.954 0.108 0.109 0.110 0.115 1.02

0.110 0.107 1.80

0.101 0.865 0.112 0.101 0.444

37810 Lab Batch ID: Matrix: W

BLANK /BLANK SPIKE / BLANK SPIKE DUPLICATE RECOVERY STUDY mg/L Units:


0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

Spike Added

[E]

Blank Sample Result

[A] Analytes

Form 3 - MS / MSD Recoveries

Matrix Spike Percent Recovery [D] = 100*(C-A)/B Matrix Spike Duplicate Percent Recovery [G] = 100*(F-A)/ERelative Percent Difference RPD = 200*(D-G)/(D+G)


12740 Region 4 ERRS


Project ID:Work Order # :

10/18/07 13:35Report Date:

Chloride

Fluoride

Nitrate

Sulfate

Reactive Sulfide

Cyanide, Reactive

Reactive Sulfide

19

<0.10

0.61

8.7

<100

<1.0

<100

10

0.50

5.0

10

3100

5.0

3100

100

78

100

103

84

90

97

0

8

0

10

11

2

3

20

20

20

20

30

30

30

70-130

70-130

70-130

70-130

30-171

53-129

30-171

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]

SpikedDup.%R[G]

DuplicateSpiked Sample

Result [F]


Result [F]


Result [F]

100

72

100

93

94

92

94

29

0.36

5.6

18

2900

4.6

2900

29

0.39

5.6

19

2600

4.5

3000

Anions by SW9056



12800-001 MS

12740-001 MS

12740-004 MS

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

Lab Batch ID:

37656

37605

37611

Matrix:

Matrix:

Matrix:

W

L

S

MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDY



mg/L

mg/L

mg/kg

Reporting Units:

Reporting Units:

Reporting Units:

10

0.50

5.0

10

3100

5.0

3100

SpikeAdded

[E]

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Flag

Analytes

Analytes

Analytes

1

1

1

Batch #:

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

Reactive Cyanide

Mercury

Mercury

<1.0

<0.0020

<0.049

5.0

0.0030

0.49

90

103

100

2

0

15

30

20

20

53-129

85-115

85-115

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]

SpikedDup.%R[G]


Result [F]


Result [F]


Result [F]

88

103

86

4.4

0.0031

0.42

4.5

0.0031

0.50




12740-003 MS

12752-002 MS

12740-003 MS

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

Lab Batch ID:

37616

37608

37653

Matrix:

Matrix:

Matrix:

S

W

S




mg/kg

mg/L

mg/kg

Reporting Units:

Reporting Units:

Reporting Units:

5.0

0.0030

0.50

SpikeAdded

[E]

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Flag

Analytes

Analytes

Analytes

1

1

1

Batch #:

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,2,4-Trichlorobenzene

1,4-Dichlorobenzene

2,4-Dinitrotoluene

2-Chlorophenol

4-Chloro-3-methylphenol

4-Nitrophenol

Acenaphthene

N-Nitroso-di-n-propylamine

Pentachlorophenol

Phenol

Pyrene

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

<10000000

<10000000

<10000000

<10000000

<10000000

<20000000

<10000000

<10000000

<20000000

<10000000

<10000000

<5000

<5000

<9900

<5000

<5000

500000

500000

500000

1000000

1000000

1000000

500000

500000

1000000

1000000

500000

50000

50000

50000

50000

50000

0

0

0

0

0

0

0

0

0

0

0

116

96

102

112

92

NC

NC

NC

NC

NC

NC

NC

NC

NC

NC

NC

2

2

4

2

2

30

30

30

30

30

30

30

30

30

30

30

20

20

20

20

20

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

Z

27-102

29-91

37-113

29-95

28-115

15-113

12-124

21-119

29-108

26-90

24-132

35-170

38-158

47-153

32-170

50-148

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]


Result [F]


Result [F]

0

0

0

0

0

0

0

0

0

0

0

118

98

106

114

94

<10000000

<10000000

<10000000

<10000000

<10000000

<20000000

<10000000

<10000000

<20000000

<10000000

<10000000

59000

49000

53000

57000

47000

<10000000

<10000000

<10000000

<10000000

<10000000

<20000000

<10000000

<10000000

<20000000

<10000000

<10000000

58000

48000

51000

56000

46000


TCL VOCs by 8260B

12740-004 MS

12740-003 MS

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

37606

37631

Matrix:

Matrix:

S

S



ug/kg

ug/kg

Reporting Units:

Reporting Units:

500000

500000

500000

1000000

1000000

1000000

500000

500000

1000000

1000000

500000

50000

50000

50000

50000

50000

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Analytes

Analytes

1

1

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene

Toluene

Trichloroethene

<4500

<4500

<9000

<4500

<4500

<2500

<2500

<5000

20000

<2500

45000

45000

45000

45000

45000

500000

500000

500000

500000

500000

93

84

91

96

80

100

86

94

102

96

5

0

0

0

2

2

5

2

4

2

20

20

20

20

20

20

20

20

20

20

35-170

38-158

47-153

32-170

50-148

35-170

38-158

47-153

32-170

50-148

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]


Result [F]


Result [F]

98

84

91

96

82

102

90

96

106

98

44000

38000

41000

43000

37000

510000

450000

480000

550000

490000

42000

38000

41000

43000

36000

500000

430000

470000

530000

480000

TCL VOCs by 8260B

TCL VOCs by 8260B

12740-005 MS

12740-007 MS

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

37633

37646

Matrix:

Matrix:

S

S



ug/kg

ug/kg

Reporting Units:

Reporting Units:

45000

45000

45000

45000

45000

500000

500000

500000

500000

500000

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Analytes

Analytes

1

1

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,1-Dichloroethene

Benzene

Chlorobenzene


Toluene

Trichloroethene

1,1-Dichloroethene

Benzene

Chlorobenzene


Toluene

Trichloroethene

<2500

<2500

<2500

<2500

<2500

<2500

<5.0

<5.0

<5.0

<5.0

<5.0

<5.0

50000

50000

50000

100000

50000

50000

50

50

50

100

50

50

96

88

90

110

96

90

94

92

100

80

96

96

2

4

4

0

2

2

6

4

2

0

2

2

20

20

20

20

20

20

20

20

20

20

20

20

70-135

72-128

77-121

50-150

76-124

68-125

70-135

72-128

77-121

50-150

76-124

68-125

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]


Result [F]


Result [F]

98

92

94

110

98

92

100

96

102

80

98

94

49000

46000

47000

110000

49000

46000

50

48

51

80

49

47

48000

44000

45000

110000

48000

45000

47

46

50

80

48

48

TCL VOCs by 8260B

TCL VOCs by 8260B

12740-010 MS

12780-013 MS

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

37654

37655

Matrix:

Matrix:

W

W



ug/L

ug/L

Reporting Units:

Reporting Units:

50000

50000

50000

100000

50000

50000

50

50

50

100

50

50

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Analytes

Analytes

1

1

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

2,4,5-TP (Silvex)

2,4-D

Mercury

Endrin

Gamma-BHC (Lindane)

Heptachlor

Heptachlor Epoxide

Methoxychlor

<0.0050

<0.0050

<0.0200

<0.0010

<0.00050

<0.00050

<0.00050

<0.0050

0.050

0.050

0.0250

0.0050

0.0050

0.0050

0.0050

0.015

194

108

101

142

142

136

134

147

11

0

0

4

4

8

6

4

20

20

20

20

20

20

20

20

Z

Z

Z

Z

Z

Z

30-150

30-150

85-115

34-140

36-122

33-120

63-111

43-136

SpikeAdded

[B]

SpikeAdded

[B]

SpikeAdded

[B]

SpikedSample

%R[D]

SpikedSample

%R[D]

SpikedSample

%R[D]

RPD%

RPD%

RPD%

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits %R

ControlLimits %R

ControlLimits %R

Spiked SampleResult

[C]

Spiked SampleResult

[C]

Spiked SampleResult

[C]

SpikedDup.%R[G]

SpikedDup.%R[G]

SpikedDup.%R[G]


Result [F]


Result [F]


Result [F]

174

108

101

148

136

148

142

153

0.087

0.054

0.0253

0.0074

0.0068

0.0074

0.0071

0.023

0.097

0.054

0.0252

0.0071

0.0071

0.0068

0.0067

0.022




12740-003 MS

12740-003 MS

12740-012 MS

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch ID:

Lab Batch ID:

Lab Batch ID:

37640

37610

37603

Matrix:

Matrix:

Matrix:

S

S

S




mg/L

mg/L

mg/L

Reporting Units:

Reporting Units:

Reporting Units:

0.050

0.050

0.0250

0.0050

0.0050

0.0050

0.0050

0.015

SpikeAdded

[E]

SpikeAdded

[E]

SpikeAdded

[E]

ParentSampleResult

[A]

ParentSampleResult

[A]

ParentSampleResult

[A]

Flag

Flag

Flag

Analytes

Analytes

Analytes

1

1

1

Batch #:

Batch #:

Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,4-Dichlorobenzene



2,4-Dinitrotoluene

2-Methylphenol

3 & 4-Methylphenol

Hexachlorobenzene

Hexachlorobutadiene

Hexachloroethane

Nitrobenzene

Pentachlorophenol

Pyridine

<0.10

<0.10

<0.10

<0.10

<0.10

<0.20

<0.10

<0.10

<0.10

<0.10

<0.20

<0.10

1.0

1.0

1.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

52

56

61

61

58

60

44

53

53

54

54

24

2

13

6

11

5

8

9

6

2

7

2

23

30

30

30

30

30

30

30

30

30

30

30

30

21-97

37-103

39-102

28-103

28-113

35-106

44-114

23-97

22-91

36-101

30-121

4-92

SpikeAdded

[B]

SpikedSample

%R[D]

RPD%

ControlLimits%RPD

ControlLimits %R

Spiked SampleResult

[C]

SpikedDup.%R[G]


Result [F]

53

64

65

68

61

65

48

56

52

58

55

19

0.53

0.64

0.65

0.68

0.61

1.3

0.48

0.56

0.52

0.58

0.55

0.19

0.52

0.56

0.61

0.61

0.58

1.2

0.44

0.53

0.53

0.54

0.54

0.24


12721-001 MSQC- Sample ID:Lab Batch ID: 37594 Matrix: S

MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDYmg/LReporting Units:

1.0

1.0

1.0

1.0

1.0

2.0

1.0

1.0

1.0

1.0

1.0

1.0

SpikeAdded

[E]

ParentSampleResult

[A]

Flag

Analytes

1Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,1-Dichloroethene

1,2-Dichloroethane

2-Butanone

Benzene


Chlorobenzene

Chloroform

Tetrachloroethylene

Trichloroethene

Vinyl Chloride

<0.050

<0.050

<0.45

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.020

0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

90

78

110

86

90

96

84

72

86

86

6

3

9

7

4

2

2

5

7

9

20

20

20

20

20

20

20

20

20

20

Z

70-130

70-131

64-136

76-121

72-125

70-130

75-124

78-127

70-130

57-135

SpikeAdded

[B]

SpikedSample

%R[D]

RPD%

ControlLimits%RPD

ControlLimits %R

Spiked SampleResult

[C]

SpikedDup.%R[G]


Result [F]

96

80

120

92

94

98

86

76

92

94

0.48

0.40

1.2

0.46

0.47

0.49

0.43

0.38

0.46

0.47

0.45

0.39

1.1

0.43

0.45

0.48

0.42

0.36

0.43

0.43




0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

SpikeAdded

[E]

ParentSampleResult

[A]

Flag

Analytes

1Batch #:




12740 Region 4 ERRS



10/18/07 13:35Report Date:

1,1-Dichloroethene

1,2-Dichloroethane

2-Butanone

Benzene


Chlorobenzene

Chloroform

Tetrachloroethylene

Trichloroethene

Vinyl Chloride

<0.050

<0.050

<0.45

<0.050

<0.050

<0.050

<0.050

<0.050

<0.050

<0.020

0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

118

102

87

96

128

102

102

96

90

94

0

4

2

2

2

2

0

2

4

2

20

20

20

20

20

20

20

20

20

20

Z

70-130

70-131

64-136

76-121

72-125

70-130

75-124

78-127

70-130

57-135

SpikeAdded

[B]

SpikedSample

%R[D]

RPD%

ControlLimits%RPD

ControlLimits %R

Spiked SampleResult

[C]

SpikedDup.%R[G]


Result [F]

118

98

89

98

130

104

102

98

94

96

0.59

0.49

0.89

0.49

0.65

0.52

0.51

0.49

0.47

0.48

0.59

0.51

0.87

0.48

0.64

0.51

0.51

0.48

0.45

0.47




0.50

0.50

1.0

0.50

0.50

0.50

0.50

0.50

0.50

0.50

SpikeAdded

[E]

ParentSampleResult

[A]

Flag

Analytes

1Batch #:


Matrix Spike Percent Recovery [D] = 100*(C-A)/B Matrix Spike Duplicate Percent Recovery [G] = 100*(F-A)/E Relative Percent Difference RPD = 200*(D-G)/(D+G) F = RPD exceeded the laboratory control limits

12740 Region 4 ERRS



Report Date:

1.043 Version:


<0.25 <0.05 <0.05 0.10

<0.05 <0.05 3.53

<0.05 <0.05 0.12

<0.05 1.46 0.32 0.06 7.24

<0.05 38.9

<0.05 <0.05 0.49

0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

96 100 120 100 130 100 40

120 110 110 120 86 90

100 107 100 56

110 110 -130

0 11 0

33 0 0

169 0 9 9 8

23 67 0 3

11 66 0 0

850

25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25

ZF Z

ZF

Z

ZF

ZF

ZF

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

Spiked Sample

%R [D]

RPD

%

Control Limits %RPD

Control Limits

%R

Spiked SampleResult

[C]

Spiked Dup. %R [G]

Duplicate Spiked Sample

Result [F]

96 90

120 140 130 100 472 120 120 120 130 108 180 100 110 90

111 110 110 210

0.86 0.09 0.12 0.24 0.13 0.10 7.78 0.12 0.12 0.24 0.13 2.43 0.50 0.16 9.22 0.09 39.9 0.11 0.11 0.70

0.86 0.10 0.12 0.20 0.13 0.10 3.89 0.12 0.11 0.23 0.12 2.23 0.41 0.16 9.17 0.10 39.4 0.11 0.11 0.36


12740-010 MS QC- Sample ID:Lab Batch ID: 37810 Matrix: W

MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDY mg/L Reporting Units:

0.90 0.10 0.10 0.10 0.10 0.10 0.90 0.10 0.10 0.10 0.10 0.90 0.10 0.10 1.80 0.10 0.90 0.10 0.10 0.10

Spike Added

[E]

Parent Sample Result

[A]

Flag

Analytes

1 Batch #:



12740 Region 4 ERRS



Report Date:

1.044 Version:


625 120

<4.99 3040 <1.50 <2.49 1800 7.58

<4.99 5.98

<4.99 <499 17.0

<4.99 <499 <4.99 <499 <4.99 39.5

<4.99 70.1

882 98.0 98.0 98.0 98.0 98.0 882 98.0 98.0 98.0 98.0 882 98.0 98.0 1760 98.0 882 98.0 980 98.0 98.0

184 96

109 -1976 131 104 126 112 114 111 103 113 120 108 99 99

140 94

102 107 253

12 33 2

-16 0 2

52 2 3 1 2

14 7 1 0 7 1 2 4 1

45

20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20

Z ZF

Z Z

ZF

Z

Z

ZF

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

Spiked Sample

%R [D]

RPD

%

Control Limits %RPD

Control Limits

%R

Spiked SampleResult

[C]

Spiked Dup. %R [G]


Result [F]

163 69

111 -1684 131 102 215 110 117 110 101 130 112 109 99

106 142 92 98

108 402

2060 188 109

1390 128 100

3700 115 115 114 99.3 1150 127 107

1750 104

1250 89.7 1000 106 464

2160 209 101

1210 121 96.6 2850 111 106 109 95.1 939 128 100

1650 91.9 1170 87.1 981 99.2 304


12740-003 MS QC- Sample ID:Lab Batch ID: 37811 Matrix: S

MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDY mg/kg Reporting Units:

833 92.6 92.6 92.6 92.6 92.6 833 92.6 92.6 92.6 92.6 833 92.6 92.6 1670 92.6 833 92.6 926 92.6 92.6

Spike Added

[E]


[A]

Flag

Analytes

1 Batch #:



12740 Region 4 ERRS



Report Date:

1.045 Version:


<472 <4.72 <4.72 10.8

<1.42 <2.36 <472 7.17

<4.72 49.6

<4.72 <472 9.95

<4.72 <472 <4.72 <472 <4.72 <4.72 181

874 97.1 97.1 97.1 97.1 97.1 874 97.1 97.1 97.1 97.1 874 97.1 97.1 1750 97.1 874 97.1 97.1 97.1

103 111 109 100 127 102 160 106 108 88

114 105 106 127 93

111 126 108 107 65

36 3 4 7 2 2

81 4 0

32 3

24 2

135 2 3

105 5 0

35

20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20

ZF

Z

ZF

F

ZF

ZF

ZF

ZF

75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125 75-125

Spike Added

[B]

Spiked Sample

%R [D]

RPD

%

Control Limits %RPD

Control Limits

%R

Spiked SampleResult

[C]

Spiked Dup. %R [G]


Result [F]

148 108 105 93

124 104 376 110 108 122 111 134 108 653 95

108 402 103 107 93

1290 105 102 101 120 101

3290 114 105 168 108

1170 115 634

1670 105

3510 99.7 104 271

904 108 106 108 123 98.7 1400 110 105 135 111 921 113 123

1620 108

1100 105 104 244


12740-001 MS QC- Sample ID:Lab Batch ID: 37812 Matrix: S

MATRIX SPIKE / MATRIX SPIKE DUPLICATE RECOVERY STUDY mg/kg Reporting Units:

874 97.1 97.1 97.1 97.1 97.1 874 97.1 97.1 97.1 97.1 874 97.1 97.1 1750 97.1 874 97.1 97.1 97.1

Spike Added

[E]


[A]

Flag

Analytes

1 Batch #:

Sample Duplicate Recovery

Region 4 ERRS

Circle Environmental I

Project ID:

Spike Relative Difference RPD 200 * | (B-A)/(B+A) |All Results are based on MDL and validated for QC purposes.

12740Work Order #:


Project Name:Report Date: 10/18/07 13:35

1.%Version:

Page 1 of 3

Anions by SW9056





12800-001 MD

12740-001 MD

12740-003 MD

12740-001 MD

12740-004 MD

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37656

37620

37623

37605

37611

Chloride

Fluoride

Nitrate

Sulfate

Flash Point

Flash Point

Reactive Sulfide

Cyanide, Reactive

Reactive Sulfide

19

<0.10

0.61

8.7

>140

126

<100

<1.0

<100

RPD

RPD

RPD

RPD

RPD

20

20

20

20

30

20

30

30

30

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

0

NC

11

0

0

2

NC

NC

NC

19

<0.10

0.68

8.7

>140

124

<100

<1.0

<100

SAMPLE / SAMPLE DUPLICATE RECOVERY





Matrix:

Matrix:

Matrix:

Matrix:

Matrix:

W

L

Sd

L

S

mg/L

Deg F

Deg F

mg/L

mg/kg

Reporting Units:

Reporting Units:

Reporting Units:

Reporting Units:

Reporting Units:

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Flag

Flag

Flag

Flag

Flag

Analyte

Analyte

Analyte

Analyte

Analyte

1

1

1

1

1

Batch #:

Batch #:

Batch #:

Batch #:

Batch #:


Region 4 ERRS


Project ID:


12740Work Order #:



1.%Version:

Page 2 of 3





12740-003 MD

12752-002 MD

12740-003 MD

12740-003 MD

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch #:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37616

37608

37653

37610

Reactive Cyanide

Mercury

Mercury

Mercury

<1.0

<0.0020

<0.049

<0.0200

RPD

RPD

RPD

RPD

30

20

20

20

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

NC

NC

NC

NC

<1.0

<0.0020

<0.050

<0.0200





Matrix:

Matrix:

Matrix:

Matrix:

S

W

S

S

mg/kg

mg/L

mg/kg

mg/L

Reporting Units:

Reporting Units:

Reporting Units:

Reporting Units:

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Flag

Flag

Flag

Flag

Analyte

Analyte

Analyte

Analyte

1

1

1

1

Batch #:

Batch #:

Batch #:

Batch #:


Region 4 ERRS


Project ID:


12740Work Order #:



1.%Version:

Page 3 of 3


pH by SW9040B

pH by SW9045C

12699-001 MD

12740-001 MD

12740-006 MD

QC- Sample ID:

QC- Sample ID:

QC- Sample ID:

Lab Batch #:

Lab Batch #:

Lab Batch #:

37592

37628

37627

Arsenic

Barium

Cadmium

Chromium

Lead

Selenium

Silver

pH

pH

<1.00

<1.00

<1.00

<1.00

<1.00

<1.00

<1.00

5.8

5.43

RPD

RPD

RPD

30

30

30

30

25

30

30

20

30

ControlLimits%RPD

ControlLimits%RPD

ControlLimits%RPD

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

SampleDuplicate

Result[B]

NC

NC

NC

NC

NC

NC

NC

2

2

<1.00

<1.00

<1.00

<1.00

<1.00

<1.00

<1.00

5.9

5.55




Matrix:

Matrix:

Matrix:

S

W

S

mg/L

pH

pH

Reporting Units:

Reporting Units:

Reporting Units:

Parent SampleResult

[A]

Parent SampleResult

[A]

Parent SampleResult

[A]

Flag

Flag

Flag

Analyte

Analyte

Analyte

1

1

1

Batch #:

Batch #:

Batch #:


Region 4 ERRS


Project ID:

Spike Relative Difference RPD 200 * | (B-A)/(B+A) | All Results are based on MDL and validated for QC purposes.

12740 Work Order #:


Project Name:Report Date:

1.043 Version:

Page 1 of 1


12740-010 MD QC- Sample ID:

Lab Batch #: 37810


<0.25 <0.05 <0.05 0.10

<0.05 <0.05 3.53

<0.05 <0.05 0.12

<0.05 1.46 0.32 0.24 0.06 7.24

<0.05 38.9

<0.05 <0.05 0.49

RPD

25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25

Control Limits %RPD

F

Sample Duplicate

Result [B]

NC NC NC

22 NC NC

33 NC NC

0 NC

6 13 0 NC

0 NC

1 NC NC

13

<0.25 <0.05 <0.05 0.08

<0.05 <0.05 2.54

<0.05 <0.05 0.12

<0.05 1.38 0.28 0.24

<0.05 7.26

<0.05 39.2

<0.05 <0.05 0.43


Matrix: W mg/L Reporting Units:


[A]

Flag

Analyte

1 Batch #:


Region 4 ERRS


Project ID:


12740 Work Order #:



1.044 Version:

Page 1 of 1



Lab Batch #: 37811


625 120

<4.99 3040 <1.50 <2.49 1800 7.58

<4.99 5.98

<4.99 <499 17.0

<4.99 <499 <4.99 <499 <4.99 39.5

<4.99 70.1

RPD

20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20

Control Limits %RPD

F

F

F

F

F

Sample Duplicate

Result [B]

45 20 NC

40 NC NC

99 14 NC NC NC NC

38 NC NC NC NC NC NC NC

80

988 98.4

<4.95 2020 <1.49 <2.48 609 8.71

<4.95 <4.95 <4.95 <495 25.0

<4.95 <495 <4.95 <495 <4.95 <24.8 <4.95 163


Matrix: S mg/kg Reporting Units:


[A]

Flag

Analyte

1 Batch #:


Region 4 ERRS


Project ID:


12740 Work Order #:



1.045 Version:

Page 1 of 1



Lab Batch #: 37812


<472 <4.72 <4.72 10.8

<1.42 <2.36 <472 7.17

<4.72 49.6

<4.72 <472 9.95

<4.72 <472 <4.72 <472 <4.72 <23.6 <4.72 181

RPD

20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20

Control Limits %RPD

F

F

F

F

Sample Duplicate

Result [B]

NC NC NC

22 NC NC NC

27 NC

44 NC NC

37 NC NC NC NC NC NC NC

13

<485 <4.85 <4.85 8.64 4.37 6.41 1330 9.37

<4.85 77.8 9.71 <485 14.4 98.1 <485 <4.85 1710 <4.85 <24.3 <4.85 206


Matrix: S mg/kg Reporting Units:


[A]

Flag

Analyte

1 Batch #:

XENCO LABORATORIES

KEVIN FERNANDER

6017 FINANCIAL DRIVE

NORCROSS GA 30071-2925

ISO 9001 REGISTERED 3075 CORNERS NORTH COURT

NORCROSS, GA 30071 {770)448-5235 {800)241-6315

FAX: {770)448-5918

STATUS WAS AI ~--------. ~-------.

ON I 25-SEP-07

UNIT 1.0.: 12740-009

COMPONENT: USED OIL

COMP. REF. NO.: 8819747

P.O. I REF. NO.: 12740

OIL TYPE -UNKNOWN

COMPONENT TYPE USED OIL

COMPONENT MANUFACTURER AND MODEL COMPONENT SERIAL NUMBER

MAINTENANCE RECOMMENDATIONS FOR LAB NO. 5827 Received on 02-0CT -07

Condition I Evaluation statements not applicable to this sample. Report issued to provide test results only. Instrument

I est .Jim its exceeded.

5827

LAB NO.

5827

Mi!Hr Unit

Mi/Hr Oil

Oil Fllr Oil WATER AckiChg Chg PPM

>25000

UNDERLINED FIGURES INDICATE SIGNIFICANT VALUES. MAINTENANCE THAT MAY BE REQUIRED IS INDICATED ABOVE UNDER MAINTENANCE RECOMMENDATIONS AND SHOULD BE PERFORMED BY A QUALIFIED MECHANIC PLEASE ADVISE US OF ANY MAINTENANCE PERFORMED ON THIS UNIT.

I

25-SEP-07

FOR LEGEND AND EXPLANATION OF PROPERTIES TESTS PLEASE SEE REVERSE N/R = TEST NOT PERFORMED

COPYRIGHT© INC. FORM NO. 6001·A 12/05

XENCO LABORATORIES

KEVIN FERNANDER

6017 FINANCIAL DRIVE

NORCROSS GA 30071·2925

WORKSITE

ISO 9001 REGISTERED 3075 CORNERS NORTH COURT

NORCROSS. GA 30071 (770) 448·5235 (800) 241-6315

FAX: (770) 448-5918

UNIT MANUFACTURER

ASM i<'lL STATUS WAS

UNIT I. D.: 12740-010

COMPONENT: USED OIL

COMP. REF. NO.: 8819750

P.O. I REF. NO.: 12740

OIL TYPE

-UNKNOWN

AI

J

TYPE USED OIL

COMPONENT MANUFACTURER AND MODEL COMPONENT SERIAL NUMBER

MAINTENANCE RECOMMENDATIONS FOR LAB NO. 5828 Received on 02-0CT-07

LAB No.

5828

Condition I Evaluation statements not applicable to this sample. Report issued to provide test results only. UNABLE to

PERFORM·all tests due to sample condition. Sample appears to be 99.9 percent water with a trace of debris.

Mi/Hr Unit

Mi!Hr 01!

Oil Fl\r Oil WATER AddChg Chg PPM

NIR

I I

BE REQUIRED IS INDICATED ABOVE BY A QUALIFIED MECHANIC. PLEASE

Sample Dale

25·SEP·07

FOR LEGEND AND EXPLANATION OF PHYSICAL PROPERTIES TESTS PLEASE SEE REVERSE SIDE N/R =TEST NOT PERFORMED

COPYRIGHT© 1990 INC. FOAM NO. 6001-A 12f05

Accura Analytical Laboratory _____________________________________________________________

Page 1 of 1

Abbreviations and EPA Qualifier Codes used by AAL

Rep Limit: This abbreviation on our analytical reports is for: Reporting Limit (RL).

BRL: This abbreviation indicates that the analytical results were Below the Reporting Limit (BRL). MDL: The Method Detection Limit (MDL), as defined by 40 CFR Part 136, Appendix B, is the

minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is greater than zero.

U: The compound was analyzed for, but not detected above the specified MDL. J: This indicates an estimated value. The target analyte is positively identified, but the reported

numerical result (analyte concentration) is an estimated value and the direction of the bias is unknown. The result is above the MDL, but below the RL.

B: This is used when the analyte is found in the associated method blank as well as in the sample. It

indicates probable blank contamination and warns the data user to take appropriate action. The flag shall be used for a tentatively identified compound as well as for a positively identified target compound.

D: This flag indicates that the identified analyte is reported from the dilution analysis. E: This identifies compounds whose concentrations exceed the upper level of the linear calibration

range of the instrument for that specific analysis. If one or more compounds have a response greater than the upper level of the calibration range, the sample or extract should be diluted and re-analyzed.

Note: For Xylenes,Total, where three isomers are quantified as two peaks, the calibration range of

each peak is considered separately. F: The Relative Percent Difference (RPD) between recoveries of either analytes or QC spikes were

outside the laboratory or method control limits. Supporting QC data was reviewed by the Department Supervisor and/or QA Officer. Results were determined to be valid for reporting.

X: This qualifier is defined by the laboratory in written case narrative. Z: QC Surrogates/ QC Lab Spikes results are outside the laboratory or method quality control limits.

Supporting QC data was reviewed by the Department Supervisor and/or QA Officer. Results were determined to be valid for reporting.

ZZ: QC Surrogates/ QC Lab Spikes results are outside the laboratory or method quality control limits

in multiple QC samples. Supporting QC data was reviewed by the Department Supervisor and/or QA Officer. Results were determined to be valid for reporting.

***: Surrogate recoveries were diluted out.

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