' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park,...

53
' ' ' CENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET CLIENT Roy F. Weston, Inc._________ ANALYSIS DATE 4/2/84 LAB SAMPLE I.D. NO. A3207/Sample Blank CASE NO. _________ PART I. (Elements to be Identified and Measured) mg/1 mg/1 1. ANTIMONY ••__________<0.005_____ 8. MERCURY___________<.OQQ2 2. ARSENIC_________ <0.002_____ 9. NICKEL____________<0.05 3. BERYLLIUM__________<0.05_______ 10. SELENIUM__________<0.005 4. CADMIUM____________<0.01_____ 11. SILVER____________<Q.Q1 5. CHROMIUM (Total)______<O.Q1______ 12. THALLIUM__________<0.1 6. COPPER_____________<0.01_______ 13. ZINC________________0.03 7. LEAD______________<Q.Q5________ PART II. (Elements to be Identified and Measured) mg/1 1. PHENOLS, (Total)____0.100 2. 3. PART III..(Additional Parameters Requested) 1. 6. CYANIDE ASBESTOS Not Requested Not Requested 2. ______________________________ 7. 3. _________i_______________ 8. 4. _________________________ 9. 5. 10. COMMENTS:

Transcript of ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park,...

Page 1: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

' ' '

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086.Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc._________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3207/Sample Blank CASE NO. _________

PART I. (Elements to be Identified and Measured)mg/1 mg/1

1. ANTIMONY ••__________<0.005_____ 8. MERCURY___________<.OQQ22. ARSENIC_________ <0.002_____ 9. NICKEL____________<0.053. BERYLLIUM__________<0.05_______ 10. SELENIUM__________<0.0054. CADMIUM____________<0.01_____ 11. SILVER____________<Q.Q15. CHROMIUM (Total)______<O.Q1______ 12. THALLIUM__________<0.16. COPPER_____________<0.01_______ 13. ZINC________________0.037. LEAD______________<Q.Q5________

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total)____0.1002.3.

PART III.. (Additional Parameters Requested)

1. 6.

CYANIDEASBESTOS

Not RequestedNot Requested

2. ______________________________ 7.3. _________i_______________ 8.4. _________________________ 9.5. 10.

COMMENTS:

Page 2: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

' I0CLIENT: ROY F. WESTON. INC. ______ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3207_________ CHART NO.: FRN: 20248

62B63B

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSERA * EPA *(21A) 2.4,6-Trichlorophenol _____ N.D. ____ (73B) Benzo(a)pyrene _______ N.D.(22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)f]uoranthene N.1J(24A) 2-Chlorophenol N.D. (75B) Benzo(k)fluoranthene N."D(31A) 2,4-Dichlorophenol M p (76B) Chrysene

2,4-DimethylphenDl N.D. (77B) Acenaphthylene n(57A) 2-Nitrophenol . N.D. (78B) Anthracene N.D.(58A) 4-Nitrophenol un (79B) Benzotghi )pery1ene N.D.(59A) 2,4-Dinitrophenol N.D. (BOB) Fluorene N.D.(60A) 4.6-Dinitro-2-methy1pheno1 N.D. (81B) Phenanthrene N.D.(64A) Pentochlorophenol MO. (82B) Dibenzo(a.h)anthracene N.J65A) Phenol N.D. (83B) Indeno(l,2,3-cd)pyrene ^i^

(B4B) Pyrene NTo

BASE/NEUTRAL COMPOUNDS VOLATILESEPA I EPA I

Acenaphthene___________N.D.____ (2V) Acrolein__________Benzidine_____________N.D.____ (3V) Acrylonitrile

/ - } 1,2,4-Trichlorobenzene_____N.D.____ (4V) Benzene ________(- >J Hexachlorobenzene________N.D.____ (6V) Carbon tetrachloride(12B) Hexachloroethane N n (7V) Chlorobenzene ____^^

bis(2-Ch1oroethy1 )ether N.D. UOV) 1,2-Dichloroethane jjjn!2-Chloronaphthalene_______N p____ (11V) 1,1,1-Trichloroethane N p^~1,2-Di Chlorobenzene_______N.D.____ (13V) 1,1-Dichloroethane______N.D^"1,3-Dichlorobenzene_______N.D.____ (14V) 1,1,2-Trichloroethane____^ p1,4-Di Chlorobenzene_______N.D.____ (15V) 1,1,2,2-Tetrachloroethane N.PT3,3'-Dich1probenzidine N.D. J16V) Chlorethane N.rJT2,4-Dinitrotoluene________N.D.____ (19V) 2-Chloroethylvinyl etFer N n2,6-Dinitrotoluene_______N.D.____ (23V) Chloroform N.D.

(37B) 1,2-Di phenyl hydrazine K n (29V) 1,1-Dlchloroethene______N.D.(39B) Fluoranthene N.D. (30V) trans-l,2-DichToroethene N.D.

4-Chlorophenyl phenyl ether N.D. (32V) 1,2-Dichloropropane N.'bT4-Bromophenyl phenyl ether N.D.____ (33V) trans-l,3-Dich1oropropene N.D.bls(2-Chloroisopropyl )ether ^ p cis-l,3-Dich1oropropene N.D.bl s(2-Chl oroethoxy )methane N.D. (38V) Ethyl benzene N nHexachlorobutadiene______N.D.___ (44V) Methylene chloride______Hexachlorocyclopentadlene N.n.____ (45V) Chl oromethane No.Isophorone_____________N n____ (46V) Bromomethane N.D.Naphthalene____________' N.D.____ (47V) BromoformNitrobenzene____________N n____ (48V) Bromodichloromethane N DN-Nitrosodimethylaniine_____N.D.____ (49V) FT uorotrichl oromethane N.rTTN-Nitrosodipheny]amine_____N.D.____ (50V) DichlorodifluoromethaneN-Nitrosodipropylatnine N n____ (51V) Chlorodibromomethanebis(2-Ethy1hexy1)phtha1ate N.D. (85V Tetrachloroethene"

talcBenzyl butyl phthalate N.n. (86V Toluene 30 mg/k;Di-n-butyl phthalate______N n_____ TBTV" Tn'chloroethene_______N nDi-n-octyl phthalate______N.D. (88V) Vinyl chlorideD1 ethyl phthalate________N n____ a D i n 0 Q C QDimethyl phthalate________N.D. * NOT SfJALVzED- J D 0Benzof a )nnt.hrnrpne N~n

Page 3: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

y~ / ni,,. *«.,!,. ..-. •- »—.-.., ..,-. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3207 CHART NO.: FRN: 20248

PESTICIDES PESTICIDESEPA i EPA i(89P(90P91P

Aldrin _____N.D. (103P) _0 -BHC____________N.D.Dieldrin ___________N.D. (104PT £ -BHC____________N.D.Chlordane_____________N.D. (105P) y -BHC____________N.D.

(96P)(97P(98P)(99P)(100P)(101P)(102P)

G -Endosulfantndosulfan sulfateEndrinEndn'n aldehydeHeptachlorHeptachlor epoxideec -BHC

N.D.N.D.N.D.N.D.N.n.N.D.N.D.

(92P) 4,4'-DDT N.D. (106P) PCB-1242____________N.D.(93P) 4,4'-DDE N n (107P) PCB-1254 " N.D.(94P) 4,4'-DDD N _n, (108P) PCB-1221 N.D!(95P) ex - E n d o s u l f a n Q ; (109P) PCB-1232 N.D~

(110P) PCB-1248 N.D(HIP) PCB-1260 N.D.~(112P) PCB-1016_____________N.D.(113P) Toxaphene___________N.D.

DIOXINSEPA f(129B) 2>3,7,8-TCDD (Screen Only) *

i AND COMMENTS:

PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. Ctwlen, Jr. \\Laboratory Director/Organics Division

LAB CERTIFICATION #: 08153ftR10236ii

Page 4: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3207 WESTOH+I .S. C5+10UL:i ,E = 2600,fl''B = 3,T=10 113!! 16249. IBsHI 36CLC,040384,1830,SP1000 2193 SCflNS (2193 SCflHS, 49.97 MINS)>x 2.0 MRSS RRNGE: 44.0, 281.3 TOTRL RBUND= 2070797.

i& 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52

ORIGINted)

MINS

* 288 RET. TIME: 10.65 TOT RBUNB= 3041. ERSE PK-'flEUND: 49.1/ 1221.

100-1

80-

49*METHYLENE CHLORIDE

60-84

40-

28-52 55 78 88

40.2

50 60 70 80

P3207 WESTON+I.S.(5+10ULJ ,E=2600,fi^D = 3,T = 10 laaii 10249.IBsCT 36CLC,040384,1830,SP1000 _ 2193 SCflNS (2193 SCONS, 49'.97 MINS)

MflSS RfiNGE:. 44.0, 281.3 TOTflL RBUND= 2070797.

r—i—r—r ~r~ ^r \ i r i i i i i i i i i i i i i i i6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52

MINS

*1272 RET. TIME: 33.05 TOT RBUND= 3726. BflSE PK/flBUND: 91.2/ 1221.

100-

50-

0-

100-

50-

9

45 51 65 7i

i *TOLUENE

165 135 149

60 80 100 120 140

180 197 219 259

•32.8

•32.8

10-. ——— r . , • , . , . , , , ^ - ,- -^ ——— , ——— . ——— , ——— , ——— , ——— , ———160 180 200 220 240

•SRI02365

Page 5: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURY ?•'•

LABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Rpu F. Wes'ton. Inc. ________ ANALYSIS DATELAB SAMPLE I.D. NO. A3208/Drum 1 ______ CASE NO.

PART I. (Elements to be Identified and Measured)m9/k9 mg/kq

1. ANTIMONY • 0.2 8. MERCURY <0.12. ARSENIC <0.2 9. NICKEL 11.93. BERYLLIUM <0.4 10. SELENIUM <0.24. CADMIUM 0.4 11. SILVER 0.85. CHROMIUM (Total)_______4^0_____ 12. THALLIUM___________<4.06. COPPER____________1570_______ 13. ZINC____________1397. LEAD 30.2

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total)CYANIDEASBESTOS Not

1.1Requested

PART III. (Additional Parameters Requested)

1. 6.2,, ___________________________ 7.3. ______;____________ s.4. ____________________________ 9.5. 10.

COFWENTS:

HRIQ2366

Page 6: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. INC. ______ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3208

ACID COMPOUNDSEPA 1(21A) 2,4,6-Trichlorophenol(22A) p-Chloro-m-cresolT24A(31A

) 2-Chlorophenol) 2,4-Dichlorophenol

(34A) 2,4-Dimethylphenol(57A) 2-Nitrophenol(58A ) 4-Nitrophenol(59A) 2,4-Dinitroohenol60A(b4A(bbA

EPA(IB)(SB)'°B)JY

) 4,6-Dinitro-2-methylphenol) Pentachlorophenol) Phenol

BASE/NEUTRAL COMPOUNDS

AcenaphtheneBenzidine1,2, 4-Tri chl orobenzeneHexachlorobenzene

fl2B Hexachloroethane(18B) bis(2-Chloroethyl)ether(20BJ 2-Chloronaphthalene(25B) 1,2-Dichlorobenzene^26B) 1,3-Dichlorobenzene(27B) 1,4-Dichlorobenzene(28BUbB(JbB(j/B

3,3'-Dichlorobenzidine1 2,4-Dinitrotoluene1 2,6-Dinitrotoluene1 1,2-Diphenylhydrazine

(39B) Fluoranthene(40B) 4-Chlorophenyl phenyl ether(41B42B43B52B

4-Bromophenyl phenyl etherbis(2-Chloroisopropyl )etherbis(2-Chloroethoxy)methaneHexachl orobutadiene

53B) Hexachlorocyclopentadiene54BbbB56BblB^b2B

t"B]

b8B69BJ(/OBJ71B1'72BJ

JsophoroneNaphthaleneNitrobenzeneN-NitrosodimethylamineN-Nitrosodi phenyl amineN-Nitrosodipropylaminebis(2-Ethylhexyl )phthalateBenzyl butyl phthalateDi-n-butyl phthalateDi-n-octyl phthalateDiethyl phthalateDimethyl phthalateBenzo(a)anthracene

n ,P . _ . * CHART NO.: FRN: 20249 1

N.D.N.D.N.D.N.n.N.D.N.D.N.D.N.D.N.D.N nN.D.

N.D.N.n.-JUJ, ——N.D.N.D.N.D.N.D.N.n.N.D.N.D.N.D.N.n.N.D.N n,

-N D-, ——N.D.N.n.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N n-&UX, ——N.n.N.D. ——N.nN.D.N.D.N.D.

(red)EPA(73B)(74B;(75BJ(76BJ(77B;(78B;(79B

BASE/NEUTRAL COMPOUNDS*

Benzo(a)pyreneBenzo(b)fluorantheneBenzo(k)fluorantheneChryseneAcenaphthyleneAnthraceneBenzo(qhi)perylene

(80B) Fluorene(BIB;(82Bi

PhenanthreneDibenzo(a,h)anthracene

(83B) Indeno(l,2,3-cd)pyrene(84B) Pyrene

EPA(2V)(3V)(4V)(6V)(7V)

VOLATILESf

AcroleinAcrylonitrileBenzeneCarbon tetrachlorideChlorobenzene

(10V) 1,2-Dichloroethane(11V) 1,1,1-Trichloroethane(13V) 1,1-Dichloroethane(14V) 1,1,2-Trichloroethane

A 1

N.D.N.D.N.D.N.D. 1N.n 1N.D.N.D.N-D.N DN.D.N nN.D.

**N.D. 9N.D.N DN.D.N.D.N.D.N,D.

(15V) 1,1,2,2-TetrachloroethaneN n(16V) Chlorethane(19V) 2-Chloroethyl vinyl ether(23V) Chloroform(29V) 1,1-Dichloroethene(30V) trans-l,2-Dichloroethene(32V 1,2-Dichloropropane

N.D.N.D.N.D.N.D.N.D.N.n

(33V) trans-l,3-Dichloropropeng\|.D.ci s- 1 , 3-Di chl oropropene

(38V) Ethyl benzene(44V) Methyl ene chloride(45V) Chloromethane(46V) Bromomethane(47V) Bromoform(48V) Bromodi chloromethane(49V) Fluorotri chloromethane(50V) Dichlorodifluoromethane(51V i Chlorodibromomethane(85V) Tetrachloroethene(86V(87V(88V

fl

N.D.N.D.290 my/kgN.D.N DN.D.N DN.D.N DN D ^N D A

Toluene i^n mn/i^TTTrichloroetheneVinyl chloride

i / Nifll 'S U*T HT T / r I!"S f f jiT\J jf ajb' IF * »*"L/

N.D. *" "N.D.

Page 7: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. INC._________ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3208 CHART NO.: FRN: 20249

PESTICIDESEPA t(89?) Aldrin(90P(91P)

DieldrinChlordane

(92P) 4,4'-DDT(93P 4,4'-DDE(94P) 4,4'-DDD(95P(96P97P(98P

<x -EndosulfanB -EndosulfanEndosulfan sulfateEndrin

(99P) Endrin aldehyde

NNNNNNNNNNN

.D.

.D.

.D.

.D.

.D.

.D.

.D.

.D.

.D.

.n.n

(red)EPA f(103P)(104P)(105P)(106P)(107P)(108P)(109P)(HOP)(HIP)(112P)(113P)

PESTICIDES

/? -BHCS -BHCr -BHCPCB-1242PCB-1254PCB-1221PCB-1232PCB-1248PCB-1260PCB-1016Toxaphene

N.N.N.N.NN.N.NN.N.N.

D.D.D.D.pD.D.nD.D.D.

(100P) Heptachlor ___________ N.D.(101P) Heptachlor epoxide N.D7(102P) c< -BHC N.D. DIOXINS

EPA f(129B) 2.3,7,8-TCDD (Screen Only) *

AND COMMENTS:

*NOT PRESENT

N.D. = <0.10 mg/kg For Base/Neutrals, Acid Extractables and Pesticides/PCB'sN.D. = <0.010 mg/kg For Volatile Fraction

Thomas F. CulS^n, Jr.Laboratory Director/Organics"Division

LAB CERTIFICATION #: 08153

Page 8: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

fl32S8 WESTOH+I .S. (2+10) ,E = 2660 ,fl-Ti = 3,T=10 ,3.58g/10ML iaaii 10251 . IgSni 36CLC, 040384, 2030, SP1000 2272" SCflHS (2272 SCONS, 5l'.95 MINS)

"2.0 MOSS RONGd: 44.0, 281.2 TOTfiL OEUHD= 2035736.

i i—r i ^\ i i i i i i i i i i i i i6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

MINS

* 282 RET. TIME: 10.52 TOT fiBUND= 1930. BflSE PK/flBUND: 49. I/ 783.

100-

80-

60-

20-

0-

49 *METHYLENE CHLORIDE fl f) I t\ IUniuii(red)

ft £ _

8440-

52 58 88_I

40.6

50 60 70 80

03208 UESTON+I .S. (2+10) ,E = 2600 ,0/D = 3 ,T=10 ,3 .58g/10ML H3JI 1 0 2 5 1 ,CLC, 040384, 2030, SP1000 ' 2272" SCONS (2272 SCONS, Si'. 95 MINS)

" MOSS RONG^: 44.0, 281.2 TOTOL flBUND- 2035736.2.0

T ^—r i—r —i—i ^ i i i i i i i i i i i i i6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

MINS

*1273 RET. TIME: 33.07 TOT OBUND= 2186. BflSE PK/OBUND: 91.1/ 627.

100-

58-

0-

100-1

50-

0-

9

45 61 6S 71 77. . 1. ........ . , 1 . 1 . . ... ...... . ..,,,

! *TOLUENE

97 105 120 149i , . | ^ , . , i . , , | . •, • i-- •-, , — ! ———

69 80 100 120 140

180 197 219 259

160 180 200 226 240

28.7

•28.7

1flRI02369

Page 9: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

- / b -^fl n I

CENTURY CLABORATORIES, INCP.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086.Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3209-A/Drum #2 CASE NO.

PART I. (Elements to be Identified and Measured)mq/kq mg/kg

1. ANTIMONY ; 8.2 8. MERCURY <0.12. ARSENIC 10.6 9. NICKEL 27903. BERYLLIUM <0.4 10. SELENIUM <0.34. CADMIUM_______ _ 3.3 11. SILVER____________30.45. CHROMIUM (Total)______68.3_______ 12. THALLIUM___________<4.06. COPPER__________313000_________ 13. ZINC____________358007. LEAD 14800

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS. (Total) 3.25CYANIDE <.10ASBESTOS Not Requested

1. Corrosiveness (ph) 52.3.4.5.

PART III. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS:

HRI0237Q

Page 10: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3209 CHART NO.: FRN: 20250

ORIOINAACID COMPOUNDS (fed) BASE/NEUTRAL COMPOUNDS

EPA t EPA f(21A) 2.4,6-Trichlorophenol_____N.D.____ (73B) Benzo(a)pyrene ________N.D.(22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)fluoranthene N.D.(24A) 2-Chlorophenol N.D. (75B) Benzo(k)fluoranthene N.D.(31A) 2,4-Dichlorophenol N.D. (76B) Chrysene N.D.(34A) 2,4-Dimethylphenol N.D. (77B) Acenaphthylene N.D.

'IS/M; 2-Nitrophenol__________ M.p____ (78B) Anthracene ____________N p.(58A) 4-Nitrophenol N.D. (79B) Benzo(ghiJperylene N.'pj(59A) 2,4-Dinitrophenol N.P. (80B) Fluorene N.D~(60A) 4,6-Dim'tro-2-methylphenol N.D. (81B) Phenanthrene N.D.|64A) Pentachlorophenol N.p. (82B)D i b e n z o ( a , h ) a n t h r a c e n e N D'(65A) Phenol N n' (83B) Indeno(l,2,3-cd)pyrene N!D.'

(84B) Pyrene N.D.

BASE/NEUTRAL COMPOUNDS VOLATILESEPA f EPA I(IB) Acenaphthene___________N.D.____ (2V) Acrolein_____________*(SB BenzidTne______________N.D. (3V) AcrylonitrTle3) 1,2,4-Trichlorobenzene____N.D.____ (4V) Benzene3) Hexachlorobenzene________N.D._____ (6V) Carbon tetrachloride ..._.

(12B) Hexachloroethane N.D. (7V) Chlorobenzene N.D7(18B) bis(2-Chloroethyl)ether j 'n' (10V) 1,2-Di chl oroethane N.~P(20B) 2-Chloronaphthalene N.D.____ (11V) fTHl-Tn' chl oroethane N.D.''(25B) 1,2-Dichlorobenzene N n (13V) 1,1-Dichloroethane_______N.D."(26B) 1,3-Dichlorobenzene N.D. (14V) 1,1,2-Trichloroethane N."D~(27B) 1,4-Dichlorobenzene N.D. (15V) 1,1,2,2-Tetrachloroethane N.D^(28B) 3,3'-Dichlorobenzidine N.D. (16V) Chlorethane "07(35BJ 2,4-Dinitrotoluene N.D. (19V) 2-Chloroethylvinyrether N.D.(36B) 2,6-Dinitrotoluene N.D. (23V) Chloroform N n(37B) 1,2-Diphenylhydrazine M n (29V) 1,1-Di chl oroethene______N_._D.(39B) Fluoranthene N.D. (3DV) trans-1.2-Dichloroethene T.n(40B(41B42B43Bb2Bb3Bb4BbbBb6B

T61B

(63B

4-Chlorophenyl phenyl ether N n (32V) 1,2-Dichloropropane N.D.4-Bromophenyl phenyl ether Np____ (33V) trans-l,3-Dichloropropene N.D.bis(2-ChloroisopropylJether N.D.____ cis-l,3-Dichloropropene N.D.bis(2-Chloroethoxy)methane N n (38V) Ethyl benzene N.D.Hexachlorobutadiene ____N n____ (44V) Methylene chloride________42 mg/kgHexachlorocyclopentadiene N n____ (45V) Chloromethane N"D.Isoohorone____________N.H.____ (46V) Bromomethane N.P.Naphthalene______________N n____ (47V) BromoformQ________ \t/y; promoTorm__________________N pNitrobenzene_____________N p____ (48V) Bromodichloromethane N p.'N-Nitrosodimethylamine____N.D.____ (49V) Fluorotrichloromethane N nN-Nitrosodi phenyl ami ne____M.H____ (50V) Dichlorodifluoromethane fTDN-Nitrosodipropylamine N.P. (51V)Chlorodibromomethane^bis(2-Ethylhexyl)pfBenzyl butyl phthale

hthalate w n (85V)Tetrachloroethene4Wi,____ , r....._late_____N.D. T86V) Toluene(68BT Di-n-fautyl phthalate______N.D.____ (87V) Trichloroethene N.D.(69BJ Di-n-octyl phthalate N.D. (88V) Vinyl chloride N.D.

* NOT ANALYZED(70B)(71B(

Diethyl phthalate N.D.Dimethyl phthalate 3^

(72BJ Benzo(a)anthracene "N .D.-OZ3-/

Page 11: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

r D^ ' O ICLIENT: ROY F. WESTON, INC.______-^ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3209__________ CHART NO.: FRN: 20250

PESTICIDES PESTICIDESEPA * EPA I(89P) Aldrin _______________ N.D. (103P) 0 -BHC ___________ N.D.(90P) Dieldrin N.D. (104P) f -BHC ________ N.D.(91PJ Chlordane N.D. (105P) r -BHC N.D.(92P) 4.4'-DDT N.D. (106P) PCB-1242 _________ N.D.(93P) 4,4'-DDE jj n (107P) PCB-1254 N.D.

"(94P) 4,4'-DDD N p_ " (108P) PCB-1221(95P) ex -Endosulfan Nib; (109P) PCB-1232(96P(97P(98P

-Endosulfan_________N.D. (HOP) PCB-1248 N.D.bndosulfan sulfate N.D. (HIP) PCB-1260Endrin_________________N.D. (112P) PCB-1016____________N.D.

(100P(101P(102P

HeptachlorHeptachlor epoxidee< -BHC

N.D.N.D.N.D.

(99P) Endrin aldehyde__________N.D.____ (113P) Toxaphene___________N.D.

DIOXINSEPA *(129B) 2.3.7,8-TCDD (Screen Only) *

AND COMMENTS:ITl PR*NOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

ORIGINAL(red)

Vt£&><*Zv)p. VThomas F. Sullen, Jr.Laboratory Director/Organic^ Division

.AB CERTIFICATION #: 08153«RI02372

Page 12: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3209CUESTON 10G/18ML 5.0UL INJ +5.0UL I .S .) CE = 2600 ,flxD = 3 ,T= H3JI 10253 , ESH 33ULD 040484 SP-1000 PflCKEB COLUMN 1482 SCflHS (1482 SCflNS, 34'.38 MINS)

1fi3S RflNGE: 44.0, 259.3 TOTflL flBUND= 4459619.>x 20.0

—i—i—r-i-i—i—i—i-i—r . . . . . . . .B 6 7 8 9 1011121314151617181920212223242526272829303132333435363738MINS

« 166 RET. TIME: 7.95 TOT flBUND= 766. BflSE PK/fiBUND : 49.1/ 311.

109 -i

80-

60-

40-

20-

0-K-

49*METHYLENE CHLORIDE ORIGIN/I

(red)84

57

56 60 70 80

88

40.6

R3209CWESTQN 10G/10ML 5.0UL INJ +5.0UL I .S .) (E = 2600 ,fl/B=3 , T = H3JI 10253 , JS331 33WLD 040484 SP-1008 PflCKED COLUMN 1482 SCflNS U482 SCflHS, 34.38 MINS)>x 20.0 SS RflNGE: 44.0, 259.3 TOTflL fiBUND= 4459619.

I t ^ | t , -,^ , , ,VVji , Y-r—T—T- - J—/\5 6 7 8 9 10 11 12 13 14 15 16 17 18 192021 22 23242526272829303'! 32333435 363738

MINS

*1247 RET. TIME: 33.03 TOT RBUND= 1275. BflSE PK/flBUND: 91.1/- 234.

100-

50-

0-

100-

50-

0-

9

45 57 ,,-65 71 7? 83

i lli ,, III i. .1 1,1 ii . l i l , i . , i , , ,i,

I *TOLUENE

97 105 119 135 149i , .1 , . . i

60 83 100 120 140

180 197 219 259I. \ 1 , i

160 180 200 220 240

-18.4

•18.4

1

BRI02373

Page 13: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc._______ ANALYSIS DATE 4/?/R4LAB SAMPLE I.D. NO. A3209-B/Drum #2 CASE NO.

PART I. (Elements to be Identified and Measured)mg/1

1. ANTIMONY ••______ Not Requested 8. MERCURY____________.00032. ARSENIC__________<0.002_____ 9. NICKEL_________Not RpgiiPst.pH3. BERYLLIUM________Not Requested 10. SELENIUM__________<Q.Q054. CADMIUM________ ___<0.01_____ .. 11. SILVER____________<Q.QI5. CHROMIUM (Total)______<0.01_____ 12. THALLIUM_______Not Requested6. COPPER__________Not Requested 13. ZINC_________Not Requested7. LEAD________________<0.05______

PART II. (Elements to be Identified and Measured) II |\ § |j | si

(red)r.

1. PHENOLS, (Total) Not Requested2. CYANIDE3. ASBESTOS

Not RequestedNot Requested

1. Barium <Q.l mo/12.3.4.5.

PART III.. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS:

Richard W. LynchLab Director

Page 14: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

•y

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086.Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Heston. Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3210/Drum #3 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kg mg/kg

1. ANTIMONY •_________2J______ 8. MERCURY___________<Q.l2. ARSENIC_____________10.9_______ 9. NICKEL____________24.53. BERYLLIUM___________<0.5_______ 10. SELENIUM________4.34. CADMIUM 1.6 11. SILVER 0.5

ANTIMONY •ARSENICBERYLLIUMCADMIUMCHROMIUM (Total)COPPERLEAD

2.310.9<0.51.6

12404516100

5. CHROMIUM (Total) 1240 12. THALLIUM 5.46. COPPER 451 13. ZINC 1027.

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total) 0.69

A r»l P ! &30 R I li 11*CYANIDEASBESTOS

140Not Requested

1.HCn <5mg/l

Reactivity H£S <5mq/l2.3.4.5.

PART III. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS:

RRI02375

Page 15: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3210______________ CHART NO.: FRN: 20251

(41B(42B

(52B(53B(54B

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA I EPA #(21A) 2,4,6-Trichlorophenol________N.D. (73B) Benzo(a)pyrene_________N D(22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)fTuoranthene N!D!(24A) 2-Chlorophenol N.D. (75B) Benzo(k)f1uoranthene N.D.(31A) 2,4-Dichlorophenol M n (76B) Chrysene N.D.(34A) 2,4-Dimethylphenol N.D. (77B) Acenaphthylene N!D.'(57A) 2-Nitrophenol . N.D. (78B) Anthracene N.D.(58A) 4-N1tropheno1 N.D. (79B) Benzo(qh1)pery1ene N'n'(59A) 2,4-Dinitrophenol___________N.D. (80B) Fluorene NJD.(60A) 4,6-Dinitro-2-methy1pheno1 N.D. (81B) Phenanthrene N.D.(64A) Pentachlorophenol N.D. (82B) Dibenzo(e,h)anthracene N.D.(65A) Phenol N.D. (83B) Indeno( 1,2,3-cd )pyrene N.'

(84B) Pyrene N.D.

BASE/NEUTRAL COMPOUNDS VOLATILES U K I U I !i [\ *•

EPA* EPAI (red)(IB) Acenaphthene______________N.D. (2V) Acrolein_______v ' *(5B) Benzidine N.D. (3V) Acrylonitrlle *

1,2,4-Tri chl oro benzene_____N.n. (4V) Benzene_____________...„.Hexachlorobenzene________N.D. (6V) Carbon tetrachloride fj'n'

(12B) Hexachloroethane N.D. (7V) Chlorobenzene N.D.~~~(18B) bis(2-Ch1oroethy1)ether N.D. (10V) 1,2-Dichloroethane N.D.(20B) 2-Ch1oronaphtha1ene~_______N.D. (11V) iTTTl-Trichloroethane____M n(25B) 1,2-Dichlorobenzene N n (13V) J.l-Dichloroethane______N D(26B) 1,3-Dichlorobenzene N.D. (14V) 1,1,2-TrichToroethane M'n'——(27B) l74 Di Chlorobenzene_______N.D. (15V) 1.1,2,2-Tetrachloroethane N.D. —(28B) 3,3'-Dich1orobenzidine N.D. (16V) Chlorethane N.D.(35B) 2,4-Dinitrotoluene N.D. (19V) 2-Chloroethylvinyl ether N.D._{36_BTH12,6- D initrotoluene___________________________..._. (23V) Chloroform____________N.D.(37B) 1,2-Di'phenylhydrazine N.D. (29V) 1,1-Dichloroethene______N.D.(39B) Fluoranthene N.D. (30V) trans-l,2-D1ch1oroethene N.D.(40B) 4-Chlorophenyl phenyl ether N.D. (32V) 1,2-Dlchloropropane N n

4-Bromophenyl phenyl ether N.D.___ (33V) trans-l,3-Dich1oropropene N.D.fais(2-Ch1oroisopropy1)ether N.D. c1s-l,3-Dich1oropropene _bi s(2-Chloroethoxy )methane N.D. (38V) Ethyl benzene ___N.D.1436^______________________________ . _________________..._.Hexachlorobutadiene _____N P____ (44V) MethyleTte chloride_______120 mg/kiHexachlorocyclopentadiene N.n____ (45V) Chloromethane_____ N.D.Isophorone________________N.D.____ (46V) Bromomethane___________N.D.

(55BJ~ Naphthalene_____________N.n.___ (47V) Bromoform NJ5!(56B) Nitrobenzene N.D. (48V) Bromodichloromethane N.D.(61B) N-Nitrosodimethylamine N.D. (49V) Fluorotrichloromethane N.D.(62B) N-Nitrosodiphenylamine______N n____ (50V) Dichlorodif 1 uoromethane Nto!(63B) N-Nitrosodipropylamine ^ p (51V) Chl orodi bromomethane N.D.(j|! bis(2-Ethy1hexy1)phtha1ate N'p' (85V) Tetrachloroethene _____N!D.l f, Benzyl butyl phthalate______N.D.____ (86V) Toluene 11 ma/kg(68B Di-n-butyl phthalate______N.D. (87V) TrichToroethene N.D.(69B) Di-n-octyl phthalate N.D. (88V) Vinyl chloride N.D.(70B DI ethyl phthalate_________N.D.______TTTB" Dimethyl phthalate________N.D. *fl fWOfTf|NADir2EI3 . D , A 0 0 _ _772B" Ben2o(a)anthracene N.D.———— H n I U-. O 7T) A It I 0 2 3 7 6

Page 16: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3210_____________ CHART NO.: FRN: 20251

PESTICIDES PESTICIDESEPA f EPA i(89P) Aldrin_______________N-p- (103P) 0 -BHC_______________N.D.(90P Dieldrin N.D. (104P) S -BHC ________N.D.(91Pi Chlordane______________N.D. (105P) V -BHC NTo!(92P 4.4--DDT N.D. (106P) PCB-1242_________N.D.(93P) 4.4'-DDE N n (107P) PCB-1254 N.n.(94P) A.n'-DDD M _ p _ (108P) PCB-1221 N.D.(95P) ex -Endosulfan N Jp; (109P) PCB-1232 N.D.(96P) & -Endosulfan N.D. (HOP) PCB-1248 N.D.97P(98P[99P

tndosulfan sulfate N'!D.' (lllPJ PCB-1260

100P101P102P

_____________________N.D. (112P) PCB^TOie____________N.D.Endn'n aldehyde__________N.D. (113P) Toxaphene NTihHeptachlor__________________N.n.Heptachlor epoxide______________N.D.

N.D. DIOXINSEPA t(129B) 2.3,7,8-TCDD (Screen Only) *

AND COMMENTS:

VNOT PRESENT , .,(red)N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. "Sullen, Jr. jLaboratory Director/Organics Division

.AB CERTIFICATION #: 08153 ^R 1 02377

Page 17: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3210CWESTON 20G/5ML 2.0UL IHJJ+4.0UL I .£ . tE = 2200 ,fl/D=2 ,T=10 O33 28251 , E£&| 126WLB 840284 SE-54 COP COL 1326 SCRHS (1326 SCRNS, 46.97 MI MS)

2.0 IJUIinifJl fl I MflSS RflNGE: 44.0, 422.8 TOTRL RBUND= 4796021.

\ , rj'r"~••

I I I I I I I I I I I I I I I I I I I I I I I4 6 8 10 12 14 16 18 20 22 24 26 28 36 32 34 36 38 40 42 44 46 48

MIHS

* 277 RET. TIME: 12.83 TOT fiBUNH= 6705. ERSE PK/RBUND: 128.1/ 787.

100-1.

80-

66-

40-•

20-

0-

*NRPHTHRLENE

c

III

7 6'

lljlll60|

a

83

l.inlilJ ii.i

97

In . l l l l . l l L l l h l l

128

|'i.i 1

fl R 1 P I r*j •(red)

I-.-. 162139 151 1971 ii 111 i.i.i .. , ii i, . 1. 1 1

•11 .7

80 100 120 140 160 180 200 220 '-

R3210(WESTON 20G/EML 2.0UL INJ)+4.0UL I . S . (E = 2200 ,fl^D = 2 , T=l 0 BSJI 20251 , E3H 1 26I..JLH 040284 SE-54 CRP COL 1326 SCRNS (1326 SCRNS, 46'. 97 MINS)

MRSS RRHGE: 44.0, 422.8 TOTRL RBUND= 4796021.

4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48

RVERRGED SPECTRUM * ERSE PK/RBUND: 128.1/ 32000. + 277 -272

100-1.

80-

60-

40--

20-

0-

*NRPHTHRLENE128

55 69 83

i- U i J l i l1 '60

1 1i ' |

102. ,.. ,,i. .1. ,i . ,,. .IllL1 1 ' 1 ' 1 ' 1 1

|'

80 100 120

•27.7

143 197. . . . . . 1. . ,1 ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 '

140 160 180 200 220

flRI02378

Page 18: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

2.6UL INJ +4.0UL i .s.)£=2600,0/0=3,1=1 pisBl 10255. Igjljl 33ULD 04S4844 SP-1000 PflCKED COLUMN 1568 SCflNS (1568 SCflNS, 36'. 63 MINS)^X 20.0

*

lllSS RflNGE: 44.0, 282.2 T

IA xsA . S s~J *"• —— —— ——— -* " -~- —— - —— •"""i—i—i—i—i T—i—i—r T~"T—i i i i i i i i i i i i i i i i i i i i i i i i

5 6 7 8 9 10111213141516171819202122232425262728293031323334353637383940MINS

* 274 RET. TIME: 10.35 TOT flBUND= 2139. BfiSE PK/fiBUND: 49.lx 844.

100-

80-

60-

40-

20-

0-

49

*METHYLENE CHLORIDE f% Ffc 1 g"& [5 *

84 (red)

180 197• • i • i — i — i — i — rj"*'~hi — ' — i — ' — i — ' — i — ' — i — ' — i — ' — i — ' — i — ' — i — ' — i — ' — i — rJ

60 80 100 120 140 160 180

39.5

R3210CUIESTON 10G/10ML 2.0UL INJ +4.0UL I . S .) E = 2600 ,fl-Ti = 3 , T=l •*'«• 10255. Ig371 33UILD 0404844 SP-1000 PflCKED COLUMN 1568 SCflNS (1568 SCfiNS, 36.63 MINS)*x 20.0

,_ A ..A . S*~J

11 SS RflNGE: 44.0, 282.2 TOTflL flBUND= 3480516

1 r, II *

5 6 7 8 9 1011121314151617181920212223242526 27 28 29 30 3'l 32 33 34 35 36 37 38 39 40MINS

«1242 RET. TIME: 33.02 TOT flBUND= 2313. BflSE PK/flBUND: 91.I/ 200.

100 -]

50-

0-

100-

50-

0-

45

i, , , | l , l .

57

1

91 *TOLUENE71

85

l i i . i l . l i l i60

- l i h , l l i i , l l 1 1 1 i i l l ,

80

r8.65

97 105 m 119 135 149l . l i l i , , l , i , i , i , ,i • i • i ' i • i

100 120

180 157157 165 219,160

1 1,180

1200 228 240

' l -1 ' 1

140

2B9

————

•8.65

260

BRI02379

Page 19: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

OPS i 1*9 i V;-i11 I *rt 1 2'3CENTURYLABORATORIES, INC. (e }P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086.Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3211-B/Drum #4 CASE NO.

PART I. (Elements to be Identified and Measured)mg/1 mg/1

1. ANTIMONY •__________N/R_________" ' 8. MERCURY___________<.QQQ22. ARSENIC_________ <0.002_____ 9. NICKEL___________N/R3. BERYLLIUM___________N/R____________10. SELENIUM_________<0.0054. CADMIUM <0.01 11. SILVER <0.015. CHROMIUM (Total)_____<0.01______ 12. THALLIUM_________N/R6. COPPER_____________N/R_______ 13. ZINC____________N/R7. LEAD______________4.79______

PART II. (Elements to be Identified and Measured)

PHENOLS, (Total)CYANIDEASBESTOS

N/RN/RN/R

1. Barium 0.4 mg/12.3.4.5.

PART III. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS:N/R = Not Requested

Richard W. LynchLaboratory Directo

ARI02380

Page 20: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

t V Cf

I JHC CENTURY OR|Gi\ LABORATORIES, INC. (red)7 \ P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086

J Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3212/Drum #5 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kg mg/kg

1. ANTIMONY :__________25.5_______ 8. MERCURY__________<Q.l2. ARSENIC____________86.0_______ 9. NICKEL_________154003. BERYLLIUM___________<0.5________ 10. SELENIUM__________<0.44. CADMIUM 9.9 11. SILVER 21.95. CHROMIUM (Total)_____148________ 12. THALLIUM_________16.56. COPPER___________89600___________ 13. ZINC___________41207. LEAD 2170

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total)________0.41CYANIDEASBESTOS

.42Not Requested

PART III. (Additional Parameters Requested)

1. __________________________ 6. ________2. ________________________________ 7. ________3. _______________________ 8. ________4. __________________________ 9. ________5. ___________________ 10. ________

COMMENTS:

AR102381

Page 21: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. INC. -^_____ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3212_____ ______ CHART NO.: FRN: 20252

ACID COMPOUNDS f BASE/NEUTRAL COMPOUNDSEPA § \f£U) EPA #21A) 2,4,6-Trichlorophenol ______ N.D. (73B) Benzo(a)pyrene ___________ N.D.22A) p-Chloro-m-cresol . N.D. (74B) Benzo(b)f1uoranthene N.D.~24A) 2-Chlorophenol N.D. (75B) Benzo(k)f1uoranthene N'H'31A) 2,4-Dichlorophenol N.D. (76B) Chrysene N.D.34A) 2,4-Dimethylphenol N.D. (77B) Acenaphthylene N p'

'57A) 2-Nitrophenol _________ N n ____ (78B) Anthracene58A) 4-Nitrophenol __________________ N.D. ___ (79B) Benzo(qhi )pery1ene'59A) 2,4-Dinitrophenol N.n. (80B) Fluorene60A) 4, 6-Dim'tro-2-methy1 phenol n (81B) Phenanthrene

5B) Benzidine_______________N.D. (3V) Acrylonitrlle1,2,4-Trichlorobenzene________N.D. (4V) Benzene

35BJ 2,4-Dinitrotoluene ___________ N n (19V) 2-Chloroethyl vinyl ether36B) 2,6-Dinltrotoluene N.D. (23V) Chloroform

yl

42B43B52B53B54B55B

u n

64A) Pentachlorophenol_______________^_g____ (82B) Dibenzo(a,h)anthracene ^^p,65A) Phenol |j'p' (83B) Indeno(l,2,3-cd)pyrene N'D'

(84B) Pyrene N.D.

BASE/NEUTRAL COMPOUNDS VOLATILESEPA i EPA fIB) Acenaphthene___________________N.D. (2V) Acrolein___________' *

Hexachlorobenzene____________i\|,p____ (6V) Carbon tetrachloride N.D.12B) Hexachloroethane N'T). (7V) . Chlorobenzene__________N.D.18B) bis(2-Ch1oroethy1)ether N.'p; (10V) 1,2-Dichloroethane______N_._D_._20B) 2-Ch1oronaphtha1ene~______N n (11V) iTni-Trichloroethane____tLD^25B) 1,2-Dichlorobenzene N.D. (13V) 1,1-Dichloroethane________N.n.26B) 1,3-Dichlorobenzene N.D. (14V) 1,1,2-Trichloroethane_____N.P.27B) 1,4-Dichlorobenzene N.D. (15V) 1,1,2,2-Tetrachloroethane N..D.28B) 3,3'-Dich1orobenzidine N.D. ~ (16V) Chlorethane 1,'n

37B) 1,2-Diphenylh.ydrazine N,n (29V) 1,1-Dichloroethene ______ N.D.39B) Fluoranthene ^D_ (30V) trans-l,2-Dich1oroethene N.D.40B) 4-Chlorophenyl phenyl ether N]Q' (32V) 1,2-Dichloropropane M p.41B) 4-Bromophenyl phenyl ether N.D (33V) trans-l,3-Dich1oropropene N.D.

bis(2-Cn1oroisopropy1 )ether N.P. cis-l,3-Dich1oropropene_ N.D.bis(2-Ch1oroethoxy)methane , j p.' (38V) Ethyl benzene N.D.Hexachlorobutadlene_______N.n____ (44V) Methylene chloride_______150 mg/k<Hexachlorocyclopentadiene N.D. (45V) Chloromethane________ N.DIsophorone_____________N.D.___ (46V) Bromome thane__________________N.DNaphthalene____________ N.D. (47V) Bromoform

56B) Nitrobenzene_______________N.D. (48V) Bromodi Chloromethane_____N.D.61B) N-Nitrosodimethylamine N.D. ( 9V) FT uorotri Chloromethane N.D.62B) N-Nitrosodi phenyl amine N.D. (50V) Dichlorodifluoromethane N.D.63BJ N-Nitrosodipropylamine______fj-jJ- ~ (51V) Chlorodibromomethane N.D.rA bis(2-Ethy1hexy1)phtha1ate N.D. (85V) Tetrachloroethene ____NJL_^^m Benzyl butyl phthalate N.D. (86V) Toluene N.D.68B? Di-n-butyTiphthalate N.D. (87V) Trichloroethene N.D.69B) Di-n-octyl phthalate N.D. (88V) Vinyl chloride N.D.70B) Diethyl phthalate_____________N.D. * wnil71B Dimethvlphthalate JTTT NOI72B) Benzo(a)anthracene N.P.

Page 22: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. V_____ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: _A3212__ ___ CHART NO.: FRN: 20252

PESTICIDES PESTICIDESERA I EPA ,

(89P90P91P

(92P

Aldrin________________N-P- (103P) /? -BHC______.______N.D.Dieldrin N.D. (104P) j -BHC ________N.D.Chlordane _____________ N.D. (105P) r -BHC_____________4.4'-DDT N.D. (106P) PCB-1242 _________ N.D.

(93P) 4.4'-DDE N n (1Q7P) PCB-1254 N.n.(94P) 4,4'-DDD N p (108P) PCB-1221 N.D.(95P) o< -Endosulfan NiDi (109P) PCB-1232 N.D.(96P) p -Endosulfan N.D. (110P) PCB-1248 N.D7(97P) Endosulfan sulfate N.5! (HIP) PCB-1260 N.D7T98F Endrin ________________ N.D. (112P) PCB-1016 ____________ N.D.(99P; Endn'n aldehyde _________ N.D. (113P) Toxaphene N7o7(100P) Heptachlor N.D. A H I /> I(101P) Heptachlorepoxide H.D. U it I I'l I(102P) ex -BHC N.D. DIOXINSW •••«ll

EPA i (red)(129B) 2,3.7.8-TCDD (Screen Only)

AND COMMENTS:

NOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. Cu^len, Jr. )Laboratory Director/Organics" Division

LAB CERTIFICATION #: 08153 ^nnoRRI02383 I

Page 23: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

" rj " ' • '

R3212(WESTON 20G/1ML 2.8UL INJJ;4.0UL I .S . CE = 2200 ,fl/D=2 ,T=1 8 EQQj 20252 , fSJSi 127WLD 040284 SE-54 CflP COL 1378 SCflNS (1378 SCflNS, 48.97 MINS3r>x 3.0 MflSS RfifcGE: 44.0, 417.5 TOTflL flBUND.= 1845891

Xv*

I I I I I I I I I I I I I I I I I I I I I I I I4 6 8 IB 12 14 16 18 20 22 24 26 28 38 32 34 36 38 48 42 44 46 48 50

MINS

* 766 RET. TIME: 27.72 TOT flBUND= 4041. EflSE P K.-'fi E LI N D : 149. 1 x 1557.*niEUTYLPHTHflLRTE

100-1f

88-

60 -

48-.

20-

0-

1149

57

76 104 121 132.... ,. .1\ . .. ._!._,. 1,1 ll .luJi ——— ,-"'•!"•. .1) ——— r —— . . 1..., ——— ..!..,. ... —— , ——

I ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 ' 1 ' I '

O R I G I N A L(red)

223167 191 285

, . — . i. . . (. 1.. i . i . i . | . i i | t | i

•38.5

68 8@ 180 120 148 168 188 200 228

fi3212(WESTON 28G.--1ML 2.0UL INJ3;4.8UL I .S. (E = 228S .flxp = 2.T=16 JgSRl 28252 . 18 127WLD 040284 SE-54 CflP COL 1378 SCflNS (1378 SCONS, 48.97 MINS)

rj

V-w.

3.8 MRSS RfifcGE: 44.8, 417.5 TOTRL OEUND= 1845891*

I I I I I I I I I I I I I I I I I I I I I I I I4 6 8 16 12 14 16 18 28 22 24 26 28 38 32 34 36 38 40 42 44 46 48 58

MINS

RVERRCED SPECTRUM * EflSE PK/flBUNB: 149.1/ 32088. + 788 -685*DIEUTYLPHTHRLRTE

180-..

88-

60-

48-•

28-

0-

1'

5776 93 I04 121 132

... 1. , ..,!.. ... ..,.,.. .1, ,...., ,..,. .• 1 ' I • I ' I ' 1 ' 1 ' 1 ' 1 1 ' I '

t9

223167 191 285

. . . 1 . . 1 .

•46.5

60 80 100 120 140 160 180 200 228

Page 24: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

03212 (UIESTON 10G/10ML 2.0UL INJ +5.0UL I.S. f£ = 2668,0/H=3,T= GEEI18256 , O33 33ULD 048484 SP-100© POCKED COLUMN 1524 SCONS (1524 SCONS, 34.7? MINS)*x 20.0 M

*

. , , , , , A , . . . ,_A_. 'J

TSS RONGE: 44.0, 259.3 TOTOL OBUND= 2309744.

1

H A A5 6 7 8 9 1 0 11 12 l¥ 14 15 16 17 18 19 20 2*1 22 23 24 25 26 27 28 29 30 3'l 32 33 34 35 36 37 38

MINS

* 272 RET. TIME: 10.30 TOT OBUHD= 2827. EflSE PK/RBUND : 49.1/ 1078.

100-

50-

0-

100 -

50-

0-

rSS.l49 *METHYLEHE CHLORIDE

4l

84

.1 ^1 1 ' 1 ' i * I

60 86

180i —— , —— , —— i —— , —— r — , —— i —160 180

,91 149

I1 ' 1 ' 1 ' 1 ' ) ' 1 * 1

100 120 148

197 2591 " i ' t ' l ' l ' l '

•38.1

200 220 240

ORIGIM.;(red)

ftRl02385

Page 25: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Heston. Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3213/Drum #6 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kq mg/kq

1. ANTIMONY •'__________31.1_______ 8. MERCURY___________Q.22. ARSENIC 16.6 9. NICKEL 1823. BERYLLIUM <0.5 10. SELENIUM <0.44. CADMIUM 3.3 11. SILVER 12.05. CHROMIUM (Total)_____84.8_______ 12. THALLIUM_________<5.46. COPPER___________47800_________ 13. ZINC___________51107. LEAD 2750

PART II. (Elements to be Identified and Measured)

1. PHENOLS, (Total) 0.45CYANIDEASBESTOS

.51Not Requested

PART III. (Additional Parameters Requested)

1. - 6.2. ___________________________ 7.3. _______'_____________________ : 8.4. ____________________________ ^ 9.5. 10.

COMMENTS:

1R102386

(red)

Page 26: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

11/23/99 TOE 14:08 FAX 814 833 8336mm: "or F. KESTON. INC.

ANALYSIS NO.: A3213

0ACID COMPOUNDS

-:PA t .?IA) 2,4,6-THehlorophenol?ZA p-cnloro-m-cresoi?4JT ?-Chloroph*nolTIA) Z.4- )1chlorophenol34A) 2.4-Dimethylphenol577T z-NitroonenoiS8A t 4-N1trophenolC.QA) 2.4~D1nitroDhenol60A) 4, 6-D1nitro-?-methyl phenolf.i£ PentzchloroDfienol^5t Pnenoi

KILLCREEK TOWNSHIP 0003DATE OF ANMYSTt- |/5/fljl

ORIGINA(red)

EPA iN.D. 73B)N.D. ]"yjB»N.D. ( 75B)H.P. ?6B)N.D. U/B)N_D T76BJ "N_J. I'9B)N.D. tOB)N n ' BIB)N.D. 'B2B1N.D. fcj£*

jB4B)

CHART NO.: FRN: 202 3 _^ —^ _~ _____ __ __

BASE/NEUTRAL COHPQUNQS

Benzo(a)pyrene N DBenzol b)fluoramhene " — R~ir ———B«nzo( k )f )uoranthene ' JJ-TT- ———Chrysene — Tpfi — "~~~Acenaphthylene —— iir1" — fc -Anihracene "jnj ———Benzoiqhi Jperyiene ——— N ' n ' " ———Fluorene —— j}-g ———Phenanthrene — 7f"fi —— —UiDen^ole «ri)ar.ip!*B££enf — jfp" —— •"Inaenol i ,<,3-cc ipvrene ~p~n ————Pyrene N;g_

BASE/NEUTRAL COMPOUNDS VOLATILESEPA f EPA fIB) Acenaphthene____________N.D. (?V) Acrolein"5BT Benzldine '

18B

75B

77BEBB35B

37B39B

41B42B43B52B53B

56G6162

66B

T7T?

1.2.4-Trich1probBnJ«ntp.p.N.D.

Hexachorobenzene_____ N.D.oroe thane

2-ChlorQnaohthalgnfi1.2- Die

Dieorobenzeneorobenzcne__ N.O.

^uT cnl orobenzene ___N_n3,3 «-Dicnlorobenrioine2,4-Dlnltrotolueng2 , 6 - D i n l t r o t o l u e n e N . D .T,?'D1phenyTnyorazlneFluoranthene ______N.D.4-Chloro >henyl phgn/1 ether4-Bromop pnenybi5(2'CnToroisopropyi)ethcr

K.D.

OTBenzeneCarbon tetrachlorldg

Jl.D,

TW

4V

T57

75710733V

Chlorobenzenel,2*Dlchloroethane••••••WHIH BArfH ^ IHIIHIIBlBfHflklH lV b

,j-Trichloroethane-Dlchloroethane

Chlorethaneg-CMoroethyl vinyl eth«r

N.D.

tran5*T«3-D1chloroDropene H!bls(2-cmoroetfioxy)niethaneHexachlorobutadieneHexachlorocvclopgntgdiene JLJL

N7D7Isoohorone _______N.D.NaphthaleneJfTtrp benzene_______ N.O.N-N1trosod1methylainine_____MILN-N1tro$odiphenyumlne____N.n

lenzvl butyl phth*litt N.P~htheletc w n

Di-n-butvjj-n-octy

chthal •tc ______N.D.

DJ«thylphth»ute••

phthaUte p.p.h a l a t * R 7 D ,

35V44V7?

fetnylbenzeneN.

Hethyltne chloride *" N.D.CnioromethaneBroffiomethane OT

50785VBbV67VBBV

SromoTonn' iromodjchlororncthaneFluorotHchloromethang"PIchlorodlf1uoromethanTChlorodlbromomethaneTgtracnioroetftene N.D.Toluene N nT Hcnloroethene N.D.Vinyl chlontie

* NOT ANALYZED AR 102387

Page 27: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3214/Drum #8 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kg mg/kq

1. ANTIMONY_____________5^0_____ 8. MERCURY__________<p.i2. ARSENIC____________2Q.2_______ 9. NICKEL__________SE2Q__3. BERYLLIUM____________<0.2______ 10. SELENIUM__________<Q.2_4. CADMIUM____________84.6______ __ 11. SILVER___________39.9_5. CHROMIUM (Total)_______95.1______ 12. THALLIUM___________5^_6. COPPER__________86600_______ 13. ZINC___________5120__7. LEAD_____________2300________

PART II. (Elements to be Identified and Measured) f I f* * ',"•'"'•mg/1

CYANIDEASBESTOS

.55Not Requested

PART III. (Additional Parameters Requested)

1. 6.2. ___________________________ - 7.3. ___________________________ 8.4. __________________________ _ 9.5. 10.

COMMENTS:

1. PHENOLS, (Total)_______0.13 (red)

SRI02388

Page 28: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

rCLIENT: ROY F. WESTON, INC. ______ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3214 ______ CHART NO. : FRN: 20254

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA * EPA #21A) 2,4.6-Trichlorophenol______N.D. (73B) Benzo(a)pyrene________N.D.22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)f1uoranthene N.D.24A) 2-Chlorophenol N.5! (75B) Benzo(k)fluoranthene N.D.31A) 2,4-Dichlorophenol N.D. (76B) Chrysene N.D.34A) 2,4-Dimethylphenol N!D! (77B) Acenaphthylene N7TJ!

2-N'itrophenol_________ N n____ (78B) Anthracene N.D.4-Nitrophenol____________N.D.___ (79B) Benzo(ghi )pery1ene ^ p2,4-Dinl trophenol_________N.D.___ (80B) Fluorene N.D.4,6-Dini tro-2-methyl phenol N.D.___ (81B) Phenanthrene N.D.Pentachlorophenol_________N.D._____ (82B) DibenzoU ,h)anthracene N.p.Phenol__________________N.D.____ (S3B) Indeno(l ,2,3-cd)pyrene ^.p.

(84B) P y r e n e N T o !

Pi ethyl phthalate

BASE/NEUTRAL COMPOUNDS VOLATILES'

EPA * (red)Acenaphthene____________N.D.___ (2V) Acrolein_______________Benzidine_______________N.D. (3V1 Acrylonitrile1,2,4-Tri Chlorobenzene______N.D.___ (4V) Benzene"______________Hexachlorobenzene_________N.D.___ (6V) Carbon tetrachloride_____[i-iyHexachloroethane _________N.D. (7V) Chlorobenzene N\J3bis(2-Ch1oroethy1 )ether NJD. (10V) 1,2-Dichloroethane N.D2-Chloronaphthalene__________N.D. (11V) 1,1,1-Trichloroethane____N._D_1,2-DiChlorobenzene_______N n____ (13V) 1,1-Dichloroethane______N.D1.3-Di Chlorobenzene________N.D. (14V) 1,1,2-Tri'chToroethane____N__D_1,4-Dichlorobenzene_______N.n, (15V) 1,1,2,2-Tetrachloroethane N.D3,3 '-Dichlorobenzi dine_____N.D.___ (16V) Chlorethane N .172,4-Dinitrotoluene__________N.D. (19V) 2-Chloroethylvinyl ether N.D2,6-Dinitrotoluene_________N.D. (23V) Chloroform N.D1,2-Di phenyl hydrazine______N.D. (29V) 1,1-Dichloroethene N.DFluoranthene____________N.D. (30V) trans-l,2-Dichloroethene N.D4-Chlorophenyl phenyl ether N.D. (32V) 1,2-Dichloropropane N.D4-Bromophenyl phenyl ether N.D.___ (33V) trans-l,3-Dich1oropropene N.Dbis(2-Cn1oroisopropyl )ether N.D.___ cis-l,3-Dich1oropropene N.Dbis(2-Ch1oroethoxy)rnethane N.D. (38V) Ethyl benzene N.D____ ..Hexachlorobutadiene _______ N.D. ___ (44V) Methyl ene chloride _______ N.D.Hexachlorocyclopentadiene N.D. ___ (45V) Chloromethane N___ ________ __Isophorone ______________ N.D. (46V) Bromomethane __ O______________ ____________Naphthalene _____________ N.D. (47V) Bromoform N.D.Nitrobenzene ____________ N.D. (48V) Bromodichloromethane____________ .N-Nitrosodimethylamine _____ N.D. (49V) FT uorotri Chloromethane N.D.N-Nitrosodi phenyl anvjne _____ N.D. 150V) Dichlorodifluoromethane N^

'_____ ..

N-Nitrosodipropylamine _____ N p ____ (51V) Chlorodibromome thanebis(2-Ethy1hexy1)htha1ate an (85V) Tetrachloroethene NBenzyl butyl phthalate N.D. (86V) TolueneDi-n-butyl phthalate ______ 0.1 (87V) Trichloroethene

N.n______ .

Di-n-octyl phthalate ______ N.D. (88V) Vinyl chloride 0____________ -- ___ _ ao Q

Dimethyl phthalate ________ N.D. * NOf) /|N|lXZ5lU "RnAnthracene

Page 29: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3214_____________ CHART NO.: FRN: 20254

PESTICIDES PESTICIDESEPA * EPA t(89P) Aldrin_______________________N.D. (103P) 0 -BHC_____________N.D.(90P) Dieldrin N.D. (104P) f -BHC_________N.D.(91PJ Chlordane N.D. (105P) y -BHC N.D(92P) 4,4'-DDT N.D. (106P) PCB-1242 ~__________N!D.'(93P) 4,4'-DDE N n (107P) PCB-1254 " N.D.(94P) 4,4'-DDD N p_ (108P) PCB-1221 ____________N.D.(95P) «x -Endosulfan fo! (109P) PCB-1232 N.o7(96P) B -Endosulfan N.D. ' (HOP) PCB-1248 N-D"!"(97P) hndosulfan sulfate N.D. (HIP) PCB-1260 N.D~(98P) EndrTn________________N.D. (112P PCB^1016____________N.D.(99P) Endrln aldehyde________________N.D. (113P) Toxaphene NT57(100P) Heptachlor N _ n . : ^ m*(101P) Heptachlor epoxide N^D fl P.(102P) oc -BHC N.D. DIOXINSU II

EpA * (red)(129B) 2.3.7,8-TCDD (Screen Only)

AND COMMENTS:

*NOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. Cu^len, Jr.Laboratory Director/Orgam'cs Division

LAB CERTIFICATION #: 08153 RR102390

Page 30: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

'V03214 WESTOH+I .S. (2.0 + 4 ,0'J ,E = 2200 ,fi/'Ii = 2 ,T=1@ 133!! 20254 . KHagp 127CLC , 640284 , 1700 1 6 1 3 SCRHS C1 6 1 3 SCRHS . 56'. 98 MI N£ )r»x 1.0 MRSS RRHGE: 44.6 ,\A2S\.Q TOTRL REUHD= 3628765.

iUJLAluuw '

I I I I I I I I I I I I I I I I I I I I6 9 12 15 18 21 24 27 30 33 36 39 42 45 48 51 54 57

MINS

RVERRGED SPECTRUM * ERSE PK-'REUHD: 149.0," 32080. + 753 -744

100-

.

80-

60 -

40-

20-

0-

55

l l l l l* t

1149

69 8296

ill 1 i

120

60 80i II 1100

|, l l i l l' 1 ' 1

fi i ii s , ,(red)

•13.3

163 187 *** 223

ill II 1 .1 1 ' 1 ' 1 '

120 140 160 180ll 1

200 220 240

B'-'N 1+2 2.0UL ERCH +4.0UL I .S . (E = 2200 ,fl/D=2 ,T=16 latrJil 20246 . WSSfli 125UILD SE-54 CRP.COL. 3231 SCRNS (3231 SCRNS, 41.82 MINS)

MRSS RRNGE: 44.0, £99.9 TOTRL REUND= 4595977.

4 6 8 10 12 14 16 18 20 22 24 26 28 30 34 36 38 40 42 44MINS

*205S RET. TIME: 29.63 TOT REUNB= 2358. ERSE PK/REUNB: 149.0/ 1063.

100-1

80-

60-

40-

20-

0-57 76 93 104 122 132

60 80 100 120 140

t9

1 7 O ^ R I"! ^*» 163 1?8 205 ^^:

160 180 200 220

45.1

5

RRI0239I

Page 31: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3216/Drum #10 CASE NO. ____

PART I. (Elements to be Identified and Measured)mg/kg mg/kg

1. ANTIMONY 23.7 8. MERCURY <0.12. ARSENIC 83.2 9. NICKEL 1153. BERYLLIUM <0.5 10. SELENIUM <0.5

ANTIMONYARSENICBERYLLIUMCADMIUMCHROMIUM (Total)COPPERLEAD

23.783.2<0.52.6

137159082.1

4. CADMIUM 2.6 11. SILVER 3.65. CHROMIUM (Total) 137 12. THALLIUM 15.36. COPPER 1590 13. ZINC 2047. __________

PART II. (Elements to be Identified and Measured)M/I . .

1. PHENOLS. (Total) ______ <.OQ1 v •» * V? 8 S *CYANIDEASBESTOS Not Re<

<.10guested

PART III. (Additional Parameters Requested)

1. 6.2. __________________________ 7.3. ___________________________ 8.4. ___________________________ 9V5. 10.

COMMENTS:

Page 32: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. INC.___________ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3216 CHART NO.: FRN: 20256

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA * EPA I(21A) 2.4,6-Trichlorophenol__________N.D. (73B) Benzo(a)pyrene_______N.D.(22A) p-ChToro-m-cresol N.D. J74B) Benzo(b)f1uoranthene N.D.(24A) 2-Chlorophenol N.D. (75B) Benzo(k)fluoranthene N.D.(31A) 2,4-Dichlorophenol N.D. ( 7 6 B ) C h r y s e n e N . D ~(34A) 2,4-Dimethylphenol N.D. (77B) Acenaphthylene N."D~!(57A) 2-Nitrophenol N n' (78B) Anthracene N.D.("58A) 4-N1tropheno1 N.D. (79B) Benzo(ghi )pery1ene N.n.("59A) 2,4-Dim'trophenol N.D. (80B) Fluorene N.D.(60A) 4,6-Dim'tro-2-methy1 phenol N.D. (8"1B~) Phenanthrene N.D.

Pentechlorophenol_________N.D. (82B) Dibenzo(a ,h)anthracene N.D.Phenol__________________________N.p. (S3B) Indeno( l,2.3-cd)pyrene N.D.

TF4B) Pyrene N.D.'

62B63B

68B

BASE/NEUTRAL COMPOUNDS VOLATILESf I W | I' |IP iI O \EPA * EPA t - - * * • • » • *

[IB) Acenaphthene____________N.D. (2V) Acrolein________________Benzidlne__________________N.D. (3V) Acrylom'trile

P"x 1,2,4-Trichlorobenzene ______ N.D. (4Vj Benzene ______________ N.D. Hexachlorobenzene ______________ N.D. ___ (6V) Carbon tetrachlon'de _____ N.D12B) Hexachloroethane N.D^ (7V) Chlorobenzene __________ N.D.18B) bis(2-Ch1oroethy1 )ether N.D. (10V) 1,2-Dichloroethane "T.D.TOB) 2-Chloronaphthalene _________ N.p. (11V) 1,1,1-Trichloroethane ____ N j>.25B) 1,2-Dichlorobenzene N n (13V) 1,1-Dlchloroethane ______ N.D.26E) 1,3-DI Chlorobenzene N.p. (14V) 1,1,2-Trichloroethane ____ NJL27B) 1,4-Dichlorobenzene ___________ N.n. (15V) 1,1,2,2-Tetrachloroethane N.D.28B) S^'-Dichlorobenzidine N\D. (16V) ChTorethane N.P.35B) 2,4-Dinitrotoluene N.P. (19V) 2-Chloroethyl vinyl ether N.D.36B) 2,6-Dinitrotoluene N.D. (23V) Chloroform ____________ N.D.37B) 1,2-Diphenylhydrazine N.D. (29V) I.l-Di'chloroethene ______ N.D."39B) Fluoranthene N.D. (30V) trans-l,2-D1ch1oroethene N.D.40B) 4-Chlorophenyl phenyl ether N.D. (32V) 1.2-Dich1oroproj>ane N.~DT4 IB) 4-Bromophenyl phenyl ether N.D. ~~ (33V) trans-l.S-Dlchloropropene N.D.42B) bis(2-Ch1oro1sopropy1)ether N.Dt ___ cis-l,3-Dich1oropropene N.D.43B) bis(2-Ch1oroethoxy)methane N.DJ (38V) Ethyl benzene ___ N.D.^2B) Hexachlorobutadiene N.D. (44V) Methyl ene chloride _______ N.D.~53B) Hexachlorocyclopentadiene N.D. (45V) Chloromethane ______________ N . D .54B) Isophorone N.D. (46V) Bromome thane N.D^""55B) Naphthalene N.D. (47V) Bromoform N.D.6B) Nitrobenzene N.D. (48V) Bromodichloromethane N.D.61B) N-Nitrosodimethylamine N.D. (49V) FT uorotri chl oromethane N.D.

N-Nltrosodi phenyl ami ne________N.p,______ (50V) Dichlorodifluoromethane N.D.N-Nitrosodipropyiamine_____u n________ (51V) Chlorodibromomethane___ N.D.bis(2-Ethy1hexy1)phtha1ate N n (85VBenzyl butyl phthalate______N.D. (86VDi-n-butyl phthalate ________0.22 mg/kg (87V

TetrachloroetheneTolueneTrichloroethene__ N.D.

69B) Di-n-octyl phthalate_______N.D. (88V) Vinyl chloride_____________N.D.70B) Diethyl phthalate____________N-D-___71B) Dimethyl phthalate O. * NOT ANALYZ^EL Q Q72B) Benzo(a)anthracene N.D. $ R 1 U L 0 ? 3

Page 33: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. **_____ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3216

EPA i(89P)(90P)(91P)(92P)(93P)(94P)(95P)(96P)(97P)(9SP)(?9F)UOOF )(101P)(102P)

PESTICIDES

.AldrinDieldrinChlordane4,4'-DDT4,4'-DDEM'-DDDex -EndosulfanJ5 -Endosulfantndosulfan sulfateEndrinEndrin el dehydeHeptechlorHeptachlor epoxidec< -BHC

N.D.N.D.N.D.N.D.N.n

N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.

EPA *(103P)(104P)(105P)(106P)(107P)(108P)(109P)(HOP)(HIP)(112P)(113P)

CHART NO.:

PESTICIDEsfl

ff -BHC£ -BHCr -BHC

PCB-1242PCB-1254PCB-122]PCB-1232PCB-1248PCB-1260PCB-1016Toxephene

DIOXINS

FRN: 20256

^ i ,>: ^ ,

it I ll 1 i i , . :..(red)N.o.

N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.

EPA 1(129B) 2,3,7,8-TCDD (Screen Only)

AND COMMENTS:

kNOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's,N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. TDullen, Jr. JLaboratory Director/Organlcs Division

LAB CERTIFICATION #: 08153 flR I

Page 34: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3216 UESTON+I.S.(2.0UL+4.0UL) ,E = 2200 , fl/H = 2,T=10 DEEI20256 , 1333 128CLC,040284,1930 1605 SCflNS (1605 SCflNS, 57.00 MINS)

•1RSS RRNGE: 44.0, 417.7 TOTfiL RBUND= 2397127.

ORIG! ,6 9 12 15 IS 21 24 27 30 33 36 39 42 45 48 51 54 57

-737

755 RET. TIME: 29.40 TOT flBUND= 1649. ERSE PK/flBUND: 149.I/' 221.

100-1

56-

0-

100-

50-

1— +lj

165

1 1

5

|

771 S3

. , 1,1 hi ,, i nL60 80

*HIBUTYLPHTHRLfiTE

91 „ 109 12S

i i < 1 1 1 I t 1 1 i 1 , 1 1 1 1 1 1 1 I i 1 r

100 120

188 20E 231

186 280 220 240

149

133 141i i pi i,l , I

140 160

253 278

r 1 3 . 4

'13.4

260

032 16 UESTON+I .S. (2.0UL + 4 .BUD ,E = 22B@ ,fl/T = 2 , T=10 iJJ!l 20256 , Mblii 128CLC,040284,1930 1605 SCRNS (1605 SCflNS, 57'.00 MINS)

1RSS RflNGE: 44.0, 417.7 TOTRL REUND= 2397127.

I I I I I I I I I I I I I I I I I I I9 12 15 18 21 24 27 36 33 36 39 42 45 48 51 54 57

RVERRGED SPECTRUM * BRSE PK/REUNH; 148.9^ 32000. + 728 -714 + 755 -737

*DIBUTYLPHTHRLRTE100-

50-

0-100-1

56-

0 J

1<

45 54 67 78 86 93 113 122 12g 138p . l|l, .1 , i .1. | 1 . i . . j i .1. i . , . . . .., i. ,11 | i III ,i.n.... , 1 . 1 , , ,1

•9

1.,,60 80 100 120 140 160

169 178 205 223 231 239 253 278I I i l l< i < i > I * t ' i • i ' I > 1 ' I i 1 • i r

-21 .7

-21 .7

180 200 220 240 260

Page 35: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc.________ ANALYSIS DATELAB SAMPLE I.D. NO.fA) A3217/Drum #11 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kq

1. ANTIMONY 35.1 8. MERCURY <0.12. ARSENIC 172 9. NICKEL 106003. BERYLLIUM <0.5 10. SELENIUM <0.34. CADMIUM 12.9 11. SILVER 44.85. CHROMIUM (Total)______159_______ 12, THALLIUM__________20.66. COPPER 153000 13. ZINC 149007. LEAD 4430

PART II. (Elements to be Identified and Measured)

PHENOLS, (TcCYANIDEASBESTOS

>tal) <0.10.18

Not Requested

PART III. (Additional Parameters Requested)

1. 6.2. ______________________ 7.3. __________________________ 8.4. ________________________ 9.5. 10.

COMMENTS:

Richard W. LynchLaboratory Directo

Page 36: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC. (red)P.O. Box 248/1501 Grandview Avenue/Mid Atlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. H0.(rj A3217/Drum #11 CASE NO.

PART I. (Elements to be Identified and Measured)

1. ANTIMONY N/R 8. MERCURY <.00022. ARSENIC______________<0.002 9. NICKEL____________N/R3. BERYLLIUM____________N/R_______ 10. SELENIUM_________<Q.QQ54. CADMIUM___________<n.m_____ 11. SILVER__________<0.0055. CHROMIUM (Total)_______<Q.Q1_____ 12. THALLIUM__________N/R6. COPPER______________N/R_______ 13. ZINC7. LEAD________________<Q.Q5_____

PART II. (Elements to be Identified and Measured)

PHENOLS, (Total)CYANIDEASBESTOS

N/RN/RN/R

1. Eiarium 0.2 mg/12.3.4.5.

PART III. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS: N/R = Not Requested

Page 37: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

' L>CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

EPA #(21A)(22A)(24A)(31A)(34A)(57A)(58A)(59A)(60A)( 64A )(65A)

EPA f(IB)(5B)

(12B)(18B)(20B)(25B)(26B)(27B)(28B)(35B)(36B)(37B)(39B)(40B)(41B)(42B)(43B)(52B)(53B)(54B)(55B)(56B)(61B)(62B)(63B)«"" "")

ANALYSIS NO.: A3217

ACID COMPOUNDS (red)EPA f

2,4,6-Trichlorophenol N.D. (73B)p-Chloro-m-cresol |\I.D. (74B)2-Chlorophenol N.D. (75B)2,4-Dichlorophenol N.D. (76B)2,4-Dimethylphenol N.D. (77B)2-Nitrophenol N n (78B)4-Nitrophenol N.D. (79B)2,4-Dinitrophenol N.D. (80B)4,6-Dinitro-2-methylphenol |VJL_ (81B)Pentachlorophenol N.D. (82B)Phenol 1y|.D. (83B)

(84B)

BASE/NEUTRAL COMPOUNDSEPA 1

Acenaphthene N.D. (2V)Benzidine N.D. (3V)1,2,4-Trichlorobenzene N.D. (4V)Hexachlorobenzene |Y.D. (6V)Hexachloroethane N D (7V)bis(2-Chloroethyl)ether N.D. (10V)2-Chloronaphthalene N.D. (HV)1,2-Dichlorobenzene r« n (13V)1,3-Dichlorobenzene N.D. (14V)1,4-Dichlorobenzene N D (15V)3,3'-Dichlorobenzidine N.D. (16V)2,4-Dinitrotoluene N D (19V)2,6-Dinitrotoluene N.D. (23V)1,2-Diphenylhydrazine N D (29V)Fluoranthene N.D. (30V)4-Chlorophenyl phenyl ether N.D. (32V)4-Bromophenyl phenyl ether N.D. (33V)bis(2-Chloroisopropyl )ether fii n.bis(2-Chloroethoxy)methane N.D. (38V)Hexachlorobutadiene N.D. (44V)Hexachlorocyclopentadiene N.D. (45V)Isophorone N.D. (46V)Naphthalene N.D. (47V)Nitrobenzene N.D. (48V)N-Nitrosodimethylamine N.D. (49V)N-Nitrosodiphenylamine N.D. (50V)N-Nitrosodipropylamine fbis(2-Ethylhexyl)phthalate r

< n (5iv)j n (85V)

) Benzyl butyl phthalate N.D. (86V)(68B)(69B)(70B)(71B)(72B)

Di-n-butyl phthalate 0.46 ma/ka (87V)Di-n-octyl phthalate N.D. (88V)Diethyl phthalate N.D.Dimethyl phthalateBenzo(a )anthracene

.D. *J.D.

CHART NO.: FRN: 20257

BASE/NEUTRAL COMPOUNDS

Benzo(a)pyreneBenzo(b)fluorantheneBenzo( k )f 1 uorantheneChryseneAcenaphthyleneAnthraceneBenzo(ghi )pery1eneFluorenePhenanthreneDibenzo( a, h) anthracenelndeno( 1 ,2,3-cd)pyrenePyrene

VOLATILES

AcroleinAc ryl on it rileBenzeneCarbon tetrachlorideChlorobenzene1,2-Dichloroethane1,1,1-Trichloroethane1,1-Dichloroethane1,1,2-Trichloroethane1,1,2,2-TetrachloroethaneChlorethane2-Chloroethyl vinyl etherChloroform1,1-Dichloroethenetrans-l,2-Dichloroethenel,2-Dichlorop_ropanetrans-l,3-Dichloroprqpenecis-l,3-Dichloroproj>eneEthyl benzeneMethyl ene chlorideChl oromethaneBromomethaneBromoformBromodi chl oromethaneFl uorotri chl oromethaneDi chl orodi f 1 uoromethaneChlorodibromomethaneTetrachl oroetheneTolueneTri chl oroetheneVinyl chloride

NOT ANALY||f| | Q 2 3 9 8

N.D.N.D.N.D.N.D.N.D.N.D.N.n.N.D.N.D.N.D.N.D.N.D.

**N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.N.D.

Page 38: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, I N C . _ _ _ _ _ " D A T E OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3217 CHART NO.: FRN: 20257

PESTICIDES PESTICIDESEPA 1 EPA I(89P) -Aldrin _________________ N.D. (103P) /? -BHC _____________ N.D.(90P) Dieldrin N.D. (104P) f -BHC ________ N.D.(91P Chlordane N.D. (105P) r -BHC N.D(92P) 4,4'-DDT N.D. (106P) PCB-124Z ~ __________ N.D.(93P) 4,4'-DDE M n (107P) PCB-1254 N.D" (108P) PCB-1221 N.D._T95P') ex -Endosulfan Nip; (1Q9P) PCB-1232 N.D.(96P) ft -Endosulfan N.D. (HOP) PCB-1248 N.D(97P) Endosulfan sulfate N!D'. (111P) PCB-1260 N.o(9£F-) Endrin N.D. (112P) P'cTTOle ____________ N.D.

(101P)(102P)

Heptachlor epoxidee< -BHC

N.D.N.D.

(99P-) Er.drln aldehyde_____-______N D.____ (113P) Toxaphene___________N.D.' ]QOF) Heptachlor ____________________

epoxide N.D.DIOXINS

EPA i(129B) 2,3,7,8-TCDD (Screen Only) *

NP""S AND COMMENTS:

*NOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. CiHlen, Jr.Laboratory Director/Organics Division

LAB CERTIFICATION #: 08153 ,AH I 02399

Page 39: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3217 WESTQN+I .£. C2.0UL + 4.0UL) , E = 228@,fi/D = 2,T=18 133TC1£625? . 133711gaCLC,040284,2040 ' 1596 SCflNS (1596 SCflNS, E7'.80 MINS)x 1.0 MflSS RflHGE: 44.0, 42*.2 TOTflL flBUND? 3789665.

———vi i i i i i i i i i i i i i i i i i i i

6 9 12 IE 18 21 24 27 30 33 36 39 42 45 48 51 54 57MINS

* 682 RET. TIME: 27.25 TOT flBUND= 3849. BflSE PK^flBUND i 149.1.-' 343.

100-

50-

0 -

100-

50-

0-

... - *DIBUT0VL PHTHflLfiTE

57 , _ 1'b" k"' 95

111 i-r45 ' 132 139

. . . 1 1 . 1 1,1 1 ... ll Ml 1 . ll II 1 ll . , 1 1 ,1 1 , 1 . . , , , l l ,,, ,1, , , , , 1 , , ,

c.

| ,. | 1 . 1 1 | 1 | | I..J.I 1 1 1 , 1 1 .1.) j I.J.T ,U-L,I |_l-.l+LJ..J-[-U,.lJ l i l j l l l l l 1 1 l| 1 M , | 1 1 1 1 | 1 1 | 1 Ij ————— , ————— j ——————

60 80 100 . 120 140 160

ORIGH1165 188 197 285 £23 231 254 / r\\|n,i i ,i ,i. , . ,. i . . I . . U CU )

180 200 220 240 268

•8.91

r 8 . 9 1l

, u

03217 WESTON + I.S. (2. 0UL + 4.0UL) ,E = 2200 ,fl.''H = 2 , T=l 0 IJdil 20257 . Ijirlij 128CLC,040284,2040 1596 SCONS (1596 SCflNS, 57.00 MINS)

1.0 MflSS RONGE: 44.0, 424.2 TOTflL OBUND= 3789065.

I I I I I I I I I I I I I I I I I I I I6 9 12 15 18 21 24 27 30 33 36 39 42 45 48 51 54 57

MINS

ftVERflGED SPECTRUM * BflSE PK/flBUND : 149.1/ 32000. + 682 -661

100-1

50-

0-

100-

50-

e-

"

1691 1 . 1

1 1 '

*BIBUT*YL PHTHflLflTE

1-

? 69 83 95 104 Jn 12B 136

i ,,..h . ., ii i I.I | ii. . ..., i . i i i.. . i. ,. ., ... . . . . . . . .60 80

183 197 205.1 . , . .1 ___,_, (

180 200

•9

157

100 120 140 160

223 231 2541

220 240 260

-20.3

•20.3

flRIQ2l*00

Page 40: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

o-/

I CENTURY•\ LABORATORIES, INC.7 \ P.O. Box 248/1501 Grandview Avenue/MidAIAvenue/MidAtlantic Park, Thorofare, NJ 08086

Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3218/Drum #12 CASE NO.

PART I. (Elements to be Identified and Measured)ma/1 mg/1

1. ANTIMONY _____________ N/R _______ 8. MERCURY ___________ <O.QQ022. ARSENIC ____________ <0.002 ______ 9. NICKEL ___________ N/R3. BERYLLIUM ____________ N/R _______ 10. SELENIUM __________ <0.0054. CADMIUM ____________ <Q.Q1 _______ 11. SILVER ___________ <Q.Q15. CHROMIUM (Total) _____ <0.01 _______ 12. THALLIUM __________ N/R6. COPPER _____________ N/R ______ 13. ZINC ____________ N/R ___7. LEAD K

PART II. (Elements to be Identified and Measured)

noy ilPHENOLS, (Total)CYANIDEASBESTOS

N/RN/RN/R

PART III. (Additional Parameters Requested)

6.7.8.9.10.

1. Barium <0.1 mg/12.3.4.5.

COMMENTS:

N/R = Not Requested

Richard W. LynchLaboratory Director

Page 41: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston, Inc._________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3219/Drum #14 CASE NO. _____

PART I. (Elements to be Identified and Measured)nig/kg mg/kg

1. ANTIMONY 13.1 8. MERCURY <0.12.3.4.5.6.7.

ARSENICBERYLLIUMCADMIUMCHROMIUM (Total)COPPERLEAD

15.3<0.41.8

1060170040.0

9. NICKEL 110010. SELENIUM <0-411. SILVER 4.612., THALLIUM___________7.113. ZINC 464

PART II. (Elements to be Identified and Measured^ f^ \ I '..mg/1

1. PHENOLS. (Total)_______0.014 (fed)CYANIDE <.10ASBESTOS N/R

PART III. (Additional Parameters Requested)

1. 6.2. ____________________________________ 7.3. ___________________________________ ~ 8.4. ___________________________________ :-9..5. 10.

COMMENTS:

N/R = Not Requested

Page 42: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

» JCLIENT: ROY F. WESTON, INC.______ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3219 CHART NO.: FRN: 20258

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA i EPA *(21A) 2,4.6-Trichlorophenol________N.D. (73B) Benzo(a)pyrene ________N.D.(22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)fluoranthene N7CL

2-Chlorophenol_____________N.D. (75B) Benzo(k)f1uoranthene N.D.2,4-Dichlorophenol___________N.D. (76B) Chrysene M n

42B43B

34A) 2. 4-Dimethyl phenol __________ N.D. (77B) Acenaphthylene Q.,57A) 2-Nitrophenol N.D, (78B) Anthracene j \ ' '|58A) 4-Nitrophenol p (79B) Benzo(qhi )peryTene 'p'J59A) 2,4-Dinitrophenol N'n (80B) Fluorene j\i'n;|60A) 4,6-Dim'tro-2-methy1pheno1 N.p. (81B) Phenanthrene fj.p.|64A) Pentachlorophenol N.D. (82B) Dibenzo(a,h)anthracene N.D.f65A) Phenol N.tL (83B) Indeno( l,2,3-cd)pyrene N.p.

1MB) Pyrene N.p'

H 1

BASE/NEUTRAL COMPOUNDS VOLATILESU l\ I U I IVJ I'iEPA f EPA I

O R I G i(red)

Acenaphthene_____________N.D. (2V) Acrolein___________Benzidlne________________N.D. (3V) Acrylom'trile1,2,4-Trichlorobenzene _______ N.D. (4V) BenzeneHexachlorobenzene__________N.D. (6V) Carbon tetrachloride___________Hexachloroethane __________^ p (7V) Chlorobenzene_______________N.p.

,18B) bis(2-Ch1oroethy1)ether N.D. (10V) 1,2-Dichloroethane N.D.|20B) 2-Chloronaphthalene ________N.D. (11V) 1,1,1-Trichloroethane_____N.p.^25B) 1,2-Dichlorobenzene N 'n' (13V) 1,1-Dlchloroethane______N.D.!26B) 1,3-DichVorobenzene N^D. (14V) 1,1,2-Trichloroethane____N_n

1,4-Dfchlorobenzene N-D- (15V) 1,1,2,2-Tetrachloroethane3,3'-D1ch1orobenzidine V (16V) Chlorethane

M n,N.D._

;35B) 2,4-Dinitrotoluene Nip; (19V) 2-Chloroethyl vinyl ether N.D.|36B) 2,6-Dinitrotoluene N.D. (23V) Chloroform __________ N.p.[37B) 1,2-Diphenylhydrazine N.D. (29V) fj^DichToroethene ______ N.D.[39B) Fluoranthene N.D. (30V) trans-l,2-Dich1oroethene N.D.(40B) 4-Chlorophenyl phenyl ether N.D. (32V) 1.2-Di'chloropropane N.D.

4-Bromophenyl phenyl ether_____N.D. (33V) trans-l,3-Dich1oropropene N.D.bis(2-Ch1oroisopropyT7ether N.D. _____cis-l,3-Dich1oropropene N.D.bi s (2-Chl oroethoxy )methane____N^D. (38V) Ethyl benzeneHexachlorobutadiene________N.D. (44V) Methylene chloride________N.D.Hexachlorocyclopentadiene____N.D. (45V) Chloromethane__________N.D.Isophorone_______________N n, (46V) Bromomethane N.D_.Naphthalene______________N.D. (47V) Bromoform N.D.Nitrobenzene_______________N.p. (48V) Bromodi Chloromethane N.p.N-Ni trosodimethyl ami ne______N.D. (49V) Fluorotri Chloromethane Nj).N-Ni trosodi phenyl ami ne______N.D. (50V) Dichlorodifluoromethane N.p]N-Ni trosodipropyl ami ne_________N n (51V) Chlorodibromomethanebi s (2-Ethyl hexyl )phtha1 ate___12.0 (85V) TetrachloroetheneBenzyl butyl phthalate_________N.D. (86VT TolueneDi-n-butyl phthalate________n.l.? (87V) Trichloroethene________N n

'ftl2i?03——NOT AN?

(69B)(70B)(71B)(72B)

Di-n-octyl phthalateDiethyl phthalateDimethyl phthalateBenzo(a anthracene

N.D.N nN DN.n.

Page 43: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3219__________ CHART NO.: FRN: 20258

PESTICIDES PESTICIDESEPA * EPA *(89P) Aldrin_________________N.D. (103P) 0 -BHC____________N.D.(90P Dieldrin N.D. (104P) «f -BHC _______N.D.(91P Chlordane N.D. (105P) Y -BHC N.D.(92P 4.4'-DDT N.D (106P) PCB-1242 _________N.D.(93P) 4,4'-DDE N n (107P) PCB-1254 N.D.(94P) 4,^'-DDD , N _ p _ (108P) PCB-1221 N.D.(95P) ex -Endosulfan Nip; (109P) PCB-1232 N.D.(96P) ft -Endosulfan N.D. (HOP) PCB-1248 NJDT"(97P) Endosulfan sulfate N.5! ~ (111P) PCB-126Q N.P7~(98PJ Endrin N.D. (112P) PCB-1016_____________N.D.(99P) Endrin aldehyde__________N.D_____ (113P) Toxaphene____ N.D.(100P) Heptachlor N.n. fl D I f* 6 '(101P) Heptachlorepoxide N!D! U f\ I U 1 i'1 * <~(102P) * -BHC N.D. DIOXINSW

EPA t (red)(129B) 2,3.7,8-TCDD (Screen Only) *

AND COMMENTS:

PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F. Cupen, Jr. \jLaboratory Director/Organics Division

LAB CERTIFICATION #: 08153

Page 44: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

fl3219 WESTON+I .£ . (2 .0UL + 4 .0UU ,E=2200 , fl.-'H = 2 , T=l 6 laaii 26258 , 13331129CLC,040284,2266 1154 SCONS (1154 SCRNS , 46.26 MINS)^x 2.0 MflSS ROHGE: 44.6, 424.7 TOTflL flBUNIiM 1651636.

I I I II I I I I I I I I I I I4'6 8 16 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42

MINS

* 761 RET. TIME: 29.56 TOT flBUND= 1684. BflSE PK/flBUND : 149. 1/ 101.

100-1.

80-

66-

46 -

20-

0-

55

45

I I 11

76

1 Illl ill ||60

83

I I

*IHBUTYLPHTHfiLflTE149

97

||80||

109

Illl ill100

131

ll| ll II 1

ORIGI.:.,(red)

160 172 188

Illl 1 II

9.32

aa

120 140 160 180 266

03219 WESTON+I .S. (2 .0UL + 4.0UL) ,E=2206,fl/B=2,T=16 paiagi 26258.____CLC,040284,2206 1154 SCflNS (1154 SCONS, 40.26 MINS)#x '2.6 MOSS RONGE: 44.0, 424.7 TOTflL flBllND=' 1051636.

I I I I I I I I I I I I I4 6 8 10 12 14 16 18 20 22 24 26 28 36 32 34 36 38 40 42

MINS

OVERflGED SPECTRUM * BflSE PK/flBUNB : 149. 1/ 32906. + 761 -749*DIBLITYLPHTHflLOTE

100-

80-

60-

40-

20-

0-

Eb

i U83 95

1651

III' I I I 1 ll60 80

|l|l 1

1-

131

IJ| ll II 1

•9

160 1^2 187

I l l l 1 1 1< l ' 1 ' I * 1 !

•15.8

100 120 140 160 180 200

Page 45: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

R3219 WESTON+I .S. (2.0UL+4.0UL) ,E=2280 ,fi/D=2 ,T=10 BEH 262ES , 133!! 129CLC, 040284, 2206 1154 SCflNS (1154 SCflNS , 48'. 28 MINS),* 2.0 MfiSS RflNGE: 44.0, 424.7 TOTflL flBUND=l 1851636.l 1851

I I I I I I I I I I I I I I I I I I I I4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 48 42

MINS ; :-1013

*1813 RET. TIME: 38.27 TOT fiBUMH= 8082. BflSE PK/flBUNB: 149.0/" 2536.

108-

50-

0-

108 -

50-

8-

1<

76 83 QO 113 r-,.-., .. , , ,.,|l ...,....,., .'".... ., .,.,. ... . .""..

60 80 160 120 146

265 279i V

*BIS(2-ETHYLHEXVL)

[9

167

188 207 219' I ' 1 ' 1 ' 1 ' 1 ' 1 ' 1

168 180 200 228

ORIGIfJM(red)

248 260 280 300 326 348 360 380

='UTU

-31.4

-31.4

R3219 WESTON+I .S. (2.0UL+4.0UL) ,E = 2200 ,fl^H = 2 ,T=10 003(28258, IB3R1129CLC,640284,2200 ' 1154 SCfiNS (1154 SCflNS, 48.20 MINS)r»x 2.8 MRSS RflNGE: 44.8, 424.7 TOTflL flEUND=\ 1851636.

I I I I I I I I I I I I I I I I I I I I4 6 8 18 12 14 16 18 28 22 24 26 28 38 32 34 36 38 48 42

MINS

flVERRGED SPECTRUM * ERSE PK/flEUND: 149.0.-' 32000. +1013 -998

*BIS (2-ETHYLHEXYU PLJTU100-]

50-

1-

57 70 ,10• 83 93 H3 132

,.l ,11...... .., ...... , „ ... ....

t9

1671 188 219

i. . .. 1.

•34.8

W • i • i • i • i • i • i • i • i • i • i * i • i • i • i • i • i • i • i

100-

50-

0-

60 80 100 120 140 160 180 200 220

265 2791

• | ' | • 1 • 1 * 1 ' 1 '1 '1 ' 1 ' 1 ' 1 ' 1 * 1 * 1 ' 1 ' 1 'I

34.0

240 260 280 300 320 340 360 380

Page 46: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3220-A/Drum #15 CASE NO. ___

PART I. (Elements to be Identified and Measured)mg/kg mg/kg

1. ANTIMONY ___________25.2_____ 8. MERCURY___________<Q.l2. ARSENIC 12.6 9. NICKEL 37903. BERYLLIUM_____________<0.3_____ 10. SELENIUM__________<0.34. CADMIUM 5.1 11. SILVER 9.65. CHROMIUM (Total)______264_______ 12. THALLIUM_______14.06. COPPER____________129000_______ 13. ZINC___________1Q1QQ7. LEAD______________6990______

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total)CYANIDE <.lASBESTOS N/R

PART III. (Additional Parameters Requested)

1. __________________________ 6. ________2. ____________________________ 7. ________3. ____________________________ 8. ________4. __________________________ 9. ________5. 10.

COMMENTS:

N/R = Not Requested

RR102U07

Page 47: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. I N C . _ _ _ _ _ D A T E OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3220 CHART NO.: FRN: 20259

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA * EPA f(21A) 2.4,6-Trichlorophenol_______N.D. (73B) Benzo(a)pyrene ________N.D.(22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)f1tioranthene N.D.(24A) 2-Chlorophenol N.5! (75B) Benzo(k)fluorantheneN7b~!(31A 2,4-Dichlorophenol __________ N.p. ___ (76B) Chrysene

' ~~_ _ _ _ _ ___

(34A) 2. 4-Dimethyl phenol N.D ~~ (77B) Acenaphthylene N.'o(57A) 2-Nitrophenol . M n (78B) Anthracene N.D.(58A) 4-Nitrophenol N.D. (79B) Benzo(ghi )perylene N.¥(59A) 2.4-Dim'trophenol N.D. (80B) Fluorene N!D.(60A) 4>6-D1nitro-2-methy1phenol N.Q. (81B) Phenanthrene N.D.(64A) Pentachlorophenol N.D. (82B) D1benzo(a,h)anthracene N."b(65A) Phenol N.D. (83B) Indeno(l,2,3-cd)pyrene N.D.

T84B) Pyrene NJDJ

BASE/NEUTRAL COMPOUNDS VOLATILESEPA f EPA f(IB) Acenaphthene ____________ N.D. (2V) Acrolein(5B) Benz i dine______________N.D. (3V) Acrylom'trile

1,2,4-Trichlorobenzene _____ N.D. (4V) Benzene __________ N.D.lj| Hexachlorobenzene ________ N.D. ___ (6V) Carbon tetrachloride _____ N.D.Tl?B) Hexachloroethane N.D. (7V) Chlorobenzene _________ N.D.(18B) bis(2-Ch1oroethy1)ether N.D. (10V) 1,2-Dlchloroethane ~N.D.(20B) 2-Chloronaphthalene _______ N.D. (11V) 1,1,1-Trichloroethane ____ N_._D_.(25B) 1,2-Dichlorobenzene M n (13V) 1.1-Dichloroethane ______ N.D.(26B) 1,3-Dichlorobenzene N]D] (14V) 1,1,2-Trichloroethane ____ N_._D_.(27B) 1.4-Dlchlorobenzene _______ N.n. (15V) 1,1,2,2-Tetrachloroethane N.D.(28B) S^'-Dichlorobenzi'dlne H.D. (16V) Chlorethane N.n.(35B) 2,4-Dim'trotoluene N.D. (19V) 2-Chloroethyl vinyl ether N.D.(36B) 2,6-Dinitrotoliiene N.D. (23V) Chloroform ____________ N.D.(37B) 1,2-Diphenylhydrazine N.D. (29V) iTFDichloroethene ______ N.D.(39B) Fluoranthene N.D. (30V) trans-1.2-Dich1oroethene N.D.(40B) 4-Chlorophenyl phenyl ether N.D. (32V) 1,2-Dichloropropane N.'D(41B) 4-Bromopnenyl phenyl ether N.D. (33V) trans-l,3-D1ch1oropropene N.D.(42B) bis(2-Ch1oroisopropy1 )ether N.D. ___ cis-l^-Dichloropropene N.D.(43B) bis(2-Ch1oroethoxy)methane N.D! (38V) Ethyl benzene ___ N.D.(52B) Hexachlorobutadiene N.D. (44V) Me thylerie chloride ________ N.D.(53B) Hexachlorocyclopentadiene N.D. ___ (45V) Chloromethane __________ N.D___(54B) Isophorone N.D. (46V) Bromomethane

~(55B) Naphthalene N.D.~ (47V) Bromoform ________ N.D.(56B) Nitrobenzene N.D. (48V) Bromodi Chloromethane N.D.(61B) N-Nitrosodimethylamine N.D. (49V) Fluorotri Chloromethane ~N.D.(62B(63B

N-Ni trosodi phenyl ami ne_____N.D. (50V) Dichlorodifluoromethane N.D.N-Ni trosodi propyl ami ne_____wn____ (51V) Chlorodibromomethane____ N.D.

TWT'bis(2-Ethy1hexy1)phtha1ate N n (85VBenzyl butyl phthalate______N.D. (86VDi-n-butyl phthalate_______N.D. (87V

(69B) Di-n-octyl phthalate NTo. (88V

Tetrachloroethene_______N.D.Toluene N.D.Trichloroethene ______N.D.V i ny 1 chloride________N.D.

(70B[TIB72B

Diethyl phthalate_________N-D-_____Dimethyl phthalate________\ JL___ * NOT ANALYZED, i Q O Q 8Don^n/ a 9 n-l-h v<a <-ana R H H l\ * *** *-Benzo(a)anthracene

Page 48: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3220 CHART NO.: FRN: 20259

96P97P98P99P100P) H e p t a c h l o r N D101P) Heptachlorepoxide_______N.D.(102P) oc -BHC N.D. DIOXINS

NOTES AND COMMENTS:

*NOT PRESENT

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB s.N.D. = <0.010 mg/kg for Volatile fraction.

PESTICIDES PESTICIDESEPA t EPA *(89P) Aldrin__________________N.D. (103P) /y -BHC_____________N.D.(90P) Dieldrin N.D. (104P) f -BHC _______N.D.J91P1 Chlordane N.D. (105P) r -BHC N.D.(92P 4.4'-DDT N.D. (106P) PCB-1242 ~_________N.D.]93P) 4,4'-DDE N n (107P) PCB-1254 " N.n."94P) 4>4'-DDD ,j'p' (108P) PCB-1221 H.D,;95P) ex -Endosulfan Nip] (109P) PCB-1232 N."bT

-Endosulfan__________N.p. (HOP) PCB-1248 N.D."Endosulfan sulfate N.5! (HIP) PCB-1260 N.D."Endrin_______________N.D. (112P) PCB-1016 N.D.Endn'n aldehyde___________N.D._____ (113P) Toxaphene N.D.

EPA t(129B) 2,3.7,8-TCDD (Screen Only) *

_ _ _ _ _ >Thomas F. Cyllen, Jr.Laboratory Director/Orgerfiics Division

LAB CERTIFICATION #: 08153

Page 49: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURY •j ^

LABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Rov G. Weston. Inc.________ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3220-B/Drum #15 CASE NO.

PART I. (Elements to be Identified and Measured)mg/1 mg/1

1. ANTIMONY N/R 8. MERCURY <.00022. ARSENIC <0.002 9. NICKEL N/R3. B E R Y L L I U M N / R 10. SELENIUM <0.0054. CADMIUM <0.01 11. SILVER <0.015. CHROMIUM (Total)_______<0.01____ 12. THALLIUM_________N/R6. COPPER______________N/R______ 13. ZINC_____________N/R7. LEAD______________0.94_____

PART II. (Elements to be Identified and Measured)

PHENOLS, (Total)CYANIDEASBESTOS

N/RN/RN/R

1. Barium <0.1 mg/12.3.4.5.

PART III. (Additional Parameters Requested)

6.7.8.9.10.

COMMENTS:

N/R = Not Requested

Richard W.LynchLab Director

; Kf->H

ARI02MO

Page 50: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

rpCENTURYLABORATORIES, INC. (red>P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

f»1 *•a ~.

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc._______ ANALYSIS DATE 4/2/84LAB SAMPLE I.D. NO. A3221-A/Drum #16 CASE NO.

PART I. (Elements to be Identified and Measured)mg/kg mg/kg

1. ANTIMONY 3.0 8. MERCURY <0.12. ARSENIC__________379_________ 9. NICKEL_______51903. BERYLLIUM <0.4 10. SELENIUM <0.44. CADMIUM 2.7 11. SILVER 18.35. CHROMIUM (Total) 17900__________ 12. THALLIUM_______H-46. COPPER_________469000_________ 13. ZINC_________8787. LEAD 52.3

PART II. (Elements to be Identified and Measured)mg/1

1. PHENOLS, (Total)______0.23CYANIDEASBESTOS

.17Not Requested

PART III. (Additional Parameters Requested)

1. ____________________________ 6. ________2. _________________________ 7. ________3. ________________________ 8. ________4. _________________________ 9. ________5. ____________________________________ 10. ________

COMMENTS:

RR102UU

Page 51: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON. I N C . _ _ _ _ _ D A T E OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3221____________ CHART NO.: FRN; 20260

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA * ERA *21A) 2,4,6-Trichlorophenol_______N.D. (73B) Benzo(a)pyrene________N.D.22A) p-Chloro-m-cresol N.D. (74B) Benzo(b)f]uoranthene N.D.24A) 2-Chlorophenol N.D. (75B) Ben2o(k)f1uoranthene N.D.31A) 2.4-Dichlorophenol N.D. (76B) Chrysene N.D~34A 2,4-Dimethylphenol________N.p. (77B) Acenaphthylene 70757A) 2-Nitrophenol N n (78B) Anthracene N.D758A) 4-Nitrophenol N.D. (79B) Benzo(qh1 )per.y1ene N n.59A) 2,4-Dlnitrophenol N.D. (BOB) Fluorene N.p.60A) 4,6-Dinitro-2-Tnethy1pheno1 N.n. (BIB) Phenanthrene N.D.64A) Pentachlorophenol N.D. (82B) D1ben2o(a ,h)Bnthracene N.p.65A) Phenol N.D. (83B) Indeno(l,2,3-cd)pyrene N.D.

(84B) P y r e n e N ! D !

BASE/NEUTRAL COMPOUNDS VOLATILESEPA i EPA *IB) Acenaphthene_______________N.D. (2V) Acrolein5B) Benzidine ___________N.D. (3V) Acrylonitrile

9«i12B)

1,2,4-Trichlorobenzene _____ N.D. T4V) Benzene ______ N.D.Hexachlorobenzene ________ N.D. (6V) Carbon tetrachloride n.p.~Hexachloroethane ________ N.D. (7V) Chlorobenzene NJoT

"18B) bis(2-ChToroethy1)ether N.D. (10V) 1,2-Dichloroethane N".D.20B) 2-Chloronaphthalene _______ N.D. (11V) 1,1, 1-Tri chl oroethane ____ N.D.25B) 1,2-Di chlorobenzene _______ N n ___ (13V) 1,1-Di chl oroethane ______ N.D.26B) 1,3-Dichlorobenzene N.D. U4V) I,l»2-Tr1 chl oroethane ____ N.D.27B) 1,4-Di chlorobenzene rg'p' (15V) 1 , 1 , 2,2-Tetrachl oroethane N.D.28B) 3,3'-D1ch1orobenzidine N.D. (16V) Chlorethane N.D~35B) 2»4-Din1troto1uene N.n. (19V) 2-Chloroethyl vinyl ether N.D.36B) 2,6-Dinitrotoluene N.D. _ (23V) Chloroform N.D.37B) 1,2-Diphenylhydrazine N.D. (29V) 1,1-DI chl oroethene _______ N.D.39BJ Fluoranthene ______ N.D. (30V) trans-l,2-Dich1oroethene NTDT40B) 4-Chlorophenyl phenyl ether N.D. (32V) 1,2-Dlchloropropane N.D.J41B) A-Bromophenyl pnenyl ether N.D. ~ (33V) trans-lt3-Dich1oropropene N.D.J42B) ~bis(2-Cn1oro1sopropy1)ether N n. cis-l,3-D1ch1oropropene N.D.43B) "~bis(2-Ch1oroethoxy)methane N .V. (38V) Ethyl benzene N.D.;52B!53B;54B[55B[56B[61B[62B

Hexachlorobutadiene_______N.D. (44V) Methylene chloride_______N.D.Hexachlorocyclopentadiene N.D. (45V) Chl oromethane_________N.D.Isophorone______________N.D.___ (46V| Bromomethane___________N.D.Naphthalene __________N.D. (47V)N i trobenzene _________ N.D. (48V)

Bromoform_____________N.D.Bromodlchloromethane N.D.

N-Nitrosodimethyiatnine_____N.n. (49V) Fluorotri chl oromethane N.DN-Nitrosodi phenyl ami ne_____N.D. (50V) Dichlorodifluoromethane N.D"

|conn " "~

N-Nitrosodipropylamine_____^ p____ (51V) Chlorodibromomethane_____N.D.bis(2-Ethylhexy1)phthalate an (85V) Tetrachloroethene ____wnBenzyl butyl phthalate_____N.D. (86V

68B(69B(70B

(Tie

Di-n-butyl phthalate ____N.D. (87VTol uene_____________N.D.Trlchloroethene_______N.D.

Di-n-octyl phthalate______N.D. (88V) Vinyl chloride ______N.D.Pi ethyl phthalate________N.D.Dimethyl phthalate N. I___ * NOT ANALYZED flR 1 Q2k 1 2Ben2o(a)anthracene N.

Page 52: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CLIENT: ROY F. WESTON, INC.._____ DATE OF ANALYSIS: 4/5/84

ANALYSIS NO.: A3221 CHART NO.: FRN: 20260

PESTICIDES PESTICIDESEPA f EPA i(89P) Aldrin_________________N.D._____ (103P) 0 -BHC_____________N.D.(90P Dieldrin N.D. (104P) 'f -BHC _________N.D.91P Chlordane N.D. (105P) r -BHC N.D.(92P) 4,4'-DDT ~ N r> (106P) PCB-1242 __________N.D.93P) 4.4 -DDE_____;________N.D. (107P) PCB-125494P95P96P(97P(98P(99P

4,4'-DDD N n, (108P) PCB-1221 N.D.-Endosulfan________N.n.____ (109P) PCB-1232

6 . -Endosulfan__________N D ____ (110P) PCB-1248 N.D.Endosulfan sulfate ~ j rL (HIP) PCB-1260 N.p]Endrin______ N.D. (112P) PCB-1016____________N.D.Endrin aldehyde M n (113P) Toxaphene___________N.n.

(lOOP) Heptachlor _____________ N.D. ______(101P) Heptachlor epoxide N n,(102P) ex -BHC N.D. DIOXINS

ERA f(129B) 2,3.7.8-TCDD (Screen Only)

AND COMMENTS: fl R I fl -i*NOT PRESENT , ,,(red)

N.D. = <0.10 mg/kg for Base/Neutrals, Acid Extractables and Pesticides/PCB's.N.D. = <0.010 mg/kg for Volatile fraction.

Thomas F.^Cullen, Jr.Laboratory Director/Orgam'cs Division

LAB CERTIFICATION #: 08153

Page 53: ' ' ' CENTURYCENTURY LABORATORIES, INC. P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086. Phone: (609) 848-3939 NJ 800-222-0589 INORGANICS ANALYSIS DATA SHEET

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

INORGANICS ANALYSIS DATA SHEET

CLIENT Roy F. Weston. Inc.________ ANALYSIS DATE ____4/2/84LAB SAMPLE I.D. NO. A3221-B/Drum #16 CASE NO.

PART I. (Elements to be Identified and Measured)mg/1 rng/1

1. ANTIMONY_____________N/R______ 8. MERCURY_______<.QQQ22. ARSENIC____________<0.002_____ 9. NICKEL_______N/R3. BERYLLIUM___________N/R______ 10. SELENIUM_____<O.QQ54. CADMIUM <0.01 11. SILVER <0.015. CHROMIUM (Total)_______<0.01_____ 12. THALLIUM_____N/R6. COPPER______________N/R______ 13. ZINC________N/R7. LEAD 0.08

PART II. (Elements to be Identified and Measured) » *» B -•» "ORIGIN1. PHENOLS. (Total)________N/R , j^2. CYANIDE_______________N/R \Te°J3. ASBESTOS______________N/R

PART III. (Additional Parameters Requested)

6.7.8.9.10.

1. Barium <0.1 mg/12.3.4.5.

COMMENTS:

N/R = Not Requested

Richard W, LynchLab Director

ARI02MI*