Post on 09-Jul-2020
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No.: A671-S_____ Site: ______ Location: ______ Group:
Instrument ID: VOA1______ Calibration Date(s): 12/1/95. 12/1/95
Heated Purge: (Y/N) _ ' Calibration Times: 0917 1249
GC Column DB624 ID: 0.53 (mm)
Lab File ID: RRF10 = L1385.D . RRF20 = L1384.DRRF50 = L1383.D RRFIOO = L1386.D . RRF200 = L1387.D
COMPOUNDDichlorodifluorometbaneChloromethaneBromomethaue *Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dicliloroethene *1 , 1 -Dicliloroethaue *trans- 1 .2-Dichloroethenecis- 1 ,2-DichioroetheneChloroform *1,2-Dichloroechane *2-Butaiione1.1.1 -Trichloroethane *Carbon Tetrachloride *Btomodichloromethane '*1 ,2-Dicliloropropanecis-l,3-Dichloropropene *Irichloroethene *Dibromochloromethane *1,1,2-Trichloroethane *Benzene *trans- 1,3-Dichloropropene *Bromoform *4-Methyl-2-Pentanone2-HexanoneTetrachloroetbene *1,1,2,2-Tetrachloroethane *Toluene *Chlorobenzene *Ethylbenzene - *Styrene *m+ prXylenes *o-xylene *
RRFIO1.8460.5760.8260.7450.5941.7420.5253.2582.0082.7192.0671.7763.3071.6540.1240.4400.4280.5230.3830:4850.3360.4700.3410.8170.3990.2970.4390.2520.4600.7171.2700.9171.4140.8330.4830.979
RRF201.8630.5750.9000.8770.5811.7910.6263.6962.2582.9732.4152.0803.6701.8930.1650.4660.4850.5720.4140.5130.3630.5220.3700.8720.4490.3680.5210.3150.5070.8261.3360.9791.5650.9730.5431.129
RRF501.9100.6080.9330.9390.6181.8770.4733.9812.3523.2642.4622.3273.9251.9690.1360.4690.4600.5690.3970.5040.3810.5270.3530.8750.4350.3600.4170.2670.4880.6961.2480.9281.424
L0.9180.4841.015
RRFIOO1.6950.5230.8430.8300.4621.6510.3483.5082.1042.9992.1612.0053.5031.8190.1240.4540.4480.5490.3870.4860.3500.4880.3400.8210.4330.3200.3990.2700.4600.6681.2040.9061.4160.9060.5171.048
RRF2001.6780.4940.7530.8010.3811.5920.3233.3181.9902.7992.1431.9643.3661.6920.1180.428 _0.4210.5190.3610.4660.3290.4580.3210.7630.4090.3110.3610.2420.4200.6111.0840.8511.3180.8580.4770.983
RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1432.9512.2502.0303.5541.805•0.1340.4510.4480.5470.3880-4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031
%RSD5.88.28.28.819.26.527.48.37.47.17.9 '9.97.07.314.13.85.74.55.03.76.06.35.25.64.89.513.910.47.011.37.65.06.26.15.66.0
*Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. . .» t\ A * Q A.«eiof2 AR3I8H3 OOOU*H M O | O H 4 J FQRM VQA 3/90
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH_________ Contract: EPA REGION-III
Project No.: A671-S_____ Site: • Location: ________ Group:
Instrument ID: VOA1 Calibration Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) _ Calibration Times: 0917 1249
GC Column DB624 ID: 0.53 (mm)
Lab File ID: " RRF10 = L1385.D RRF20 - L1384.DRRF50 = L1383.D RRFIOO = L1386.D RRF200 = L1387.D
COMPOUND
'
Toluene-d8Bromofluorobenzene *1 ,2-DichIoroethane-d4
RRF10
1.2620.6981.544
RRF20
1.1690.6841.525
RRF50
1.1390.6421.560
RRFIOO
1.0530.5801.382
RRF200
• 1.0410.5911.502
RRF
""-
1.1330.6391.503
%RSD
•
8.08.34.7
* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimufn RRF of 0.010.
Page2of2 000135FORMVIVOA
7AVOLATILE CONTINUING CALIBRATION CHECK _ w so
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No. A671-S_____ Site: _____ Location: ______ Group:
Instrument ID: VOA1 Calibration Date: 12/6/95 Time: 1425
Lab File ID: L1395.D Init. Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 0917 1249
GC Column: DB624 ID: 0.53 (mm)
COMPOUNDDichlorodifluoromethane
. ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethyleue ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetliene1,1-Dichloroe thanetrans- 1 ,2-Dichloroedienecis- 1 ,2-DichloroetlieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroediene'Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeueBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene
RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.830 .0.4250.3310.427 '0.2690.4670.7041.2280.9161.4270.8970.5011.031
RRF501.3810.4130.7310.6730.3721.5420.4322.8631.8122.6762.0551.8163.2501.7150.1640.4070.4170.5120.3630.4650.3280.4820.3420.7880.4260.3570.5010.3310.4380.7801.1430.8721.3830.8840.4881.028
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D23.2
r25.6j>14.119.7
C29.4310.95.919.415.49.38.710.5-8.65.0-22.49.86.96.46.45.36.82.20.95.1-0.2-7.9-17.3-23.06.2-10.86.94.83.11.42.60.3
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0'
25.025.025.025.025.025.025.025.0
SAMPLE NO.VSTDOSOVBLK0118I1128W341811128W411811128W421811128W1318H128W46181112834A1811129W47I18H129W48181112948A1811127W201811127W20MS181H27W20MS18H12918B
Page I of2
All other compounds must meet a minimum RRF of 0.010.
AR3
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No. A671-S_____ Site: _____ Location: ______ Group:
Instrument ID: VOA1 . Calibration Date: 12/6/95 Time: 1425
Lab File ID: L1395.D Init. Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ____ Init. Calib. Times: 0917 1249
GC Column: DB624 ID: 0.53 (mm)
COMPOUND
Toiuene-d8Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
1.1330.6391.503
RRF50
1.1250.6811.521
MINRRF
<
-
•
0.200
%D
*
_
0.7-6.6-1.2
MAX%D
'
25.0
All other compounds must meet a minimum RRF of 0.010.
Page 2 of 2 /» R 3 I 8 !* l» 6
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No. A671-S _____ Site: _____ Location: _ _____ Group:
Instrument ID: VOA1 Calibration Date: 12/9/95 Tune: 0858
Lab File ID: L1456.D . Init. Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ___ Init. Calib. Times: 0917 1249
GC Column: DB624 ID: 0.53 (mm)
COMPOUNDDichlorodifiuoromedianeChloromethaneBrbmomethaneVinyl ChlorideChloroethane 'Methyleue ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-DichIoroe thanetrans- 1 , 2-DichIoroethenecis-1 ,2-DichloroedieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachiorideBromodichloromediane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroedieneDibromochlororaediaiie1 , 1 ,2-TrichloroedianeBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroediene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene
•<
RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031
RRF502.1610.6911.0681.150 •0.5081.4270.3713.1051.8702.3581.8641.5942.9231.4300.1510.4470.4200.5530.3500.4790.3210.4570.3200.8170.4020.2890.4560.3020.447
. 0.6901.1940.8401.3770.8620.4921.017
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D-20.2-24.525.5C-37.23.617.619.212.612.720.117.121.517.820.8-12.75:96.3-1.19.82.48.87.37.21.65.412.7-6.8-12.34.32.02.88.33.53.91.81.4
MAX%D
25.025.0
25.025.0
25.0 •25.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.025.025.025.025.025.0
SAMPLE NO.VSTD050VBLK02181112947B1811129W18181H30W061811130WS1181113006A1811204W531811204W541811204W55181 120453 B
All orner compounds must meet a minimum RRF of 0.010. .
000155
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH . Contract: EPA REGION-in
Project No. A671-S _____ Site: Location: ______ , Group:
Instrument ID: VOAI Calibration Date: 12/9/95 Time: . 0858
Lab File ID: L1456.D Init. Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ____ Init. Calib. Times: 0917 1249
GC Column: DB624 ID: 0.53 (mm) "
COMPOUND
^
Toluene -d8BromoQuorobenzenel,2-Dichlorocdiane-d4
RRF
1.1330.6391.503.
RRF50
•
1.3870.7631.564
MINRRF
t
0.200
%D
•~.
-22.4-19.4-4.1
MAX%D
25.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2FORM VH VOA 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION III
Project No. A674-S _____ Site: _____ Location: ______ Group:
Instrument ID: VOA1 ' Calibration Date: 12/17/95 Time: 1419
Lab File ID: L1499.D Init. Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ____ Init. Calib. Times: 0917 1249
GC Column: DB624 ID: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetliene1,1-Dichloroedianetrans- 1 .2-DichIoroedienecis-1 ,2-DichloroedieneChloroform1 ,2-Dichloroethane2-Butanone1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroedieneDibromochloromediane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem+ p-Xyleneso-xylene
RRF1.7980.5550.8510.8380.5271.7310.4593.5522.1422.9512.2502.0303.5541.8050.1340.4510.4480.5470.3880.4910.3520.4930.3450.8300.4250.3310.4270.2690.4670.7041.2280.9161.4270.8970.5011.031
RRF501.3630.4450.8070.6610.4601.4920.3892.5481.6502.7361.9512.1903.4311.6860.1590.3690.4630.4650.4140.4030.3980.5470.3930.6780.3410.3680.4410.3020.5000.7511.0140.9111.1160.8150.4150.86S
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.100 '0.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D24.219.85.221.112.713.815.36a.3323.07.313.3-7.93.56.6-18.713.2-3.315.0-6.717.9-13.1-11.0-13.918.319.8-11.2-3.3-12.3-7.1-6.717.40.521.89.117.216.1
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.0.25.025.025.025.025.0
1SAMPLE NO.VSTD050VBLK031811206P2B1811206W641811206W62181 1206 W651811206W661811207W041811213B011811213B02
•
All odier compounds must meet a minimum RRF of 0.010.AR3 I 81*1*9 000173
Page I of2
7AVOLATILE CONTINUING CALIBRATION CHECK
~ 3 .3 r*Lab Name: CHEMTECH________ Contract: EPA REGION IE
Project No. A674-S___ Site: Location: Group:
Instrument ID: VOA1 Calibration Date: 12/17/95 Tune: 1419
Lab File ID: L1499.D____________ Init- Calib. Date(s): 12/1/95 12/1/95
Heated Purge: (Y/N) ____ luit. Calib. Times: . 0917 1249
GC Column: DB624 ED: 0.53 (mm)
COMPOUND
'
V
Tolueoe-dSBromofluorobenzenc1 ,2-Dichloroethane-d4
RRF
1.1330.6391.503
RRF50
1.1100.6251.411
MINRRF
0.200
%D
""••
2.02.26.1
MAX%D
25.0
All other compounds must meet a minimm^ RRF of 0.010.
Page2of2 A R 3 I 8 k 5 0FORM VH VOA 3/90
6A • " / ' . . " . VVOLATILE ORGANICS INITIAL CALIBRATION DATA
• •• •_Lab Name: CHEMTECH Contract: US EPA REGION PI
Project No.: A689-S _____ Site: _______ Location: _ Group:
Instrument ID: HP5971A Calibration Date(s): 12/20/95 12/20/95
Heated Purge: (Y/N) t__ ' Calibration Times: 0934 1221
GC Column DB624 _______ ID: 0.53 (mm)
Lab File ID: RRF1Q = L1516.D , RRF20 = L1515.DRRF50 = L1514.D RRFIOO - L1517.D RRF200 = L1518.D
COMPOUNDDichlorodifluoromethaneChloromethaneBromomethane •*.Vinyl Chloride *ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1,1-Dichloroethane •*1,2-Dichloroediene (total)Chloroform *1,2-Dichloroethane *2-Butanone1,1,1-Trichloroethane *Carbon Tetrachloride *Bromodichlbromethane *1,2-Dichloropropanecis-1, 3-Dichloropropene *Trichloroethene *Dibromochloromethane *1,1,2-Trichloroethane *Benzene . *trans-1, 3-Dichloropropene *'Bromoform " *4-Methyl-2-Pentanooe2-HexanoneTetrachloroethene *1,1,2,2-Terrachloroethane *Toluene *Chlorobenzene *Ethylbenzene '*Styrene . » *01+ p-Xylenes *o-xylene *
RRF10L4671.3671.440.1.5620.7021.822.:;'0.561 I..3.8502.H33.3805.2095.3602.9570.1870.4960.4580.6120.409-0.5220.3510.4810.3550.8890.448.,0.2950.5260.341 .0.4330.7731.2790.9441.5580.9390.5681.204
RRF201.5421.2091.2151.5110.6101.799 >:•0.5563.7422.170 -3.9495.6075.3992.892.0.1720.4910.4700.6140.4040.5190.356 i •0.490,0.337 •0.8720.4440.304 r0.4770.32510.4490.7221.2700.9381.560,0.952?0.5701.192
RRF501.5061.2851.2021.709.0.530U8260.5873.8742.0913.6585.6295.701 '3.2410.1640.4930.475 ,0.6460.4140.5420.35L0.5270.3560.8790.480. :0.34$0.483, '0.3170.4490.7521.2480.9231.531.0.9510.564'-1.180
RRF.1001.4750.9431.2091.5230.443117820.460 >.3.9141.9723.1534.6104.9573.1140.1250.4630.4460.5880.3810.5010.32T10.4850.3190.8090.436;0.307,0.3870:2600.4190.6221.1370.856-L400,0.882-0.507Nvl.085
1 -
RRF200^ 0.9070.7590:7260.9500.4461.243"0.3092.7561.4542.3373.4133.6242.1270.0950.3590.360 ~0.4690.294013890.2680.3830.2440.629
V0.341-0.2410.2880.1900.3430.4690.9280.6891.124: 0:7100.4130.851
RRF1.3801.1131.1581.4510.5461.694 :
0.4953.6271.9603.2954.8945.0082.8660.1480.4600.4420.5860.3800.4940.3320.4730.3220.8160.4300.2990.4320.2860.4190.6671.172'0.8701.4350.887.0.5241.102
RSD19.322.822.620.120.314.923.213.514.918.618.916.315.225.512.610.711,713.112.311.011.414.513.312.212.622.021.710.618.812.612.312.911.6J2.913.4
* Compounds with required minimum RRF and maximum 56RSD values. ^00054All other compounds must meet a minimum RRF of 0.010. ~
Page 1 of 2 'FORM VI VGA AR3I8U5I 3/9°
6A .* :VOLATILE ORGANICS INITIAL CALIBRATION DATA — S 6-3
Lab Name: CHEMTECH_________ Contract: US EPA REGION m
Project No.: A689-S_____ Site: _____ Location: ______ Group:
Instrument ID: HP5971A Calibration Date(s): 12/20/95 12/20/95
Heated Purge: (Y/N) _N_ ' Calibration Times: 0934 1221
GC Column DB624_____ ID: 0153 (mm)
Lab File ID: RRF10 = L1516.D RRF20 = L1515.DRRF50 - L1514.D RRFIOO = L1517.D RRF200 = L1518.D
COMPOUND
.
. . . .
. ' - ' • " '
- <.- - - . /''Vi''.
Toluene-dS. • . - -"fBromofluorobenzene *l,2-Dichloroethane-d4
RRF10
-..-
- - •
••*'*<%&&£112840.8743.052
RRF20
-
i
:;-;,•:.<•".•:-
1.1140.7442.524
RRF50
-
\ - . ' - - •
•u-C H1.073*0.7202.718
RRFIOO
•,
" •' -
.
•« ^ 4-1.014 >0.6512.667
RRF200
t'ff ' '
. •
• - ,
' •--»'/' -,• _— i.- •]-
-• " •
••••&%>$&&0.859-•0.5351.887
RRF, V; '.
• - .-
'-":• • *".'»•*•,*"•
• •;,.•
,
».
,. - - • -, ,• ''• -' T %* *~ *~ • * *•*;
, .
:>.:i'!1.069,0.705 •:2.570
%RSD.r-
1 t
'- . ,
., •
. -..
• '
," ': '.-'<14.417.716.7
f,.
*
* Compounds with required minimum RRF and maTimum %RSD values. . 'All other compounds must meet a minimum RRF of 0.010. f
Page 2 of2FORM VI VOA AR 3 I 8U52 3/9°
, • 7A 'VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH . Contract: US EPA REGION ffl
Project No. A689-S_____ Site: _____ Location: ______ Group:
Instrument ID: HP5971A Calibration Date: 12/20/95 time: 1445
Lab File ID: L1520.D Init. Calib. Date(s): 12/20/95 12/20/95
Heated Purge: (Y/N) N Init. Calib. Times: 0934 1221
GC Column: DB624 ID: 0.53 (mm)
COMPOUND• DichlorodifluorometnaneChloromethaneBromomethaneVinyl ChlorideChloroetnaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1 ,2-Dichloroethene (total)Chloroform1 ,2-Dichloroe thane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromediane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroethene"Dibromochloromediane1,1,2-TrichloroedianeBenzenetrans-1, 3-DichloropropeneBromoform ,4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzeneStyrenem+ p-Xyleneso-xylene -
RRF1.3801.1121.1581.4510.5461.6940.4953.6271.9603.2954.8945.0082.8660.1480.4600.4420.5860.3800.4940.3320.4730.3220.8160.4300.2990.432-0.2860.4190.6671.1720.8701.4350.8870.5241.102
RRF501.4200.9861.3081.5580.6621.6590.5063.8421.9112.9984.5884.7613.1340.1810.4840,4230.6330.4010.5290.3030.4740.3330.861
• 0.4720.2880.5170.3400.3510.7521.1900.8201.4800.9360.5171.139
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.10001100
0.2000.5000.4000.5000.1000.3000.3000.300
%D-2.911.3-13.0
- -7.4-21.22.1-2.2-5.92.59.06.64.9-9.4-22.3-5.2~ 3-8.0-5.5-7.18.7-0.2-3.4-5.5-9.83.7-19.7-18.916.2-12.7-1.55.7-3.1-5.51.3-3.4
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.025.025.025.025.025.0
SAMPLE NO.VSTD050VBLK011811213B031811214B041811214T031811214W671811218W221811218W681811218T681811218T68MS1811218T68MSD
-
All other compounds must meet a minimum RRF of 0.010. ''00073
AR3I8U53FORM VH VOA 3/90
7A 'VOLATILE CONTINUING CALIBRATION CHECK
. .Lab Name: CHEMTECH Contract: US EPA REGION m
Project No. A689-S ____ Site: Location: ____ Group:
Instrument ID: HP5971A Calibration Date: 12/20/95 Tune: 1445
Lab File ID: L1520.D____________ Init. Calib. Date(s): 12/20/95 12/20/95
Heated Purge: (Y/N) N Init. Calib. Times: 0934 1221
GC Column: DB624 ID: 0.53 (mm)
COMPOUND
-.
-
. . «
- • - • - .
*'
- -' - . ----- -"'---Toluene-d8Bromofiuorobenzenel,2-Dichloroethane-d4
RRF
. •-•- • ,-
1.0690.7052.570
RRF50
. , \
,\
0.9650.6432.398
MENRRF
•
. .
'
.- ...-•..•
.
.
0.200
%D
•
, •9.78.86.7
MAX%D
25.0
All other compounds must meet a miniming RRF of 0.010. * ^ U U f 4
Page2of2 . A R 3 I 8 »* 51*FORM VH VOA 3/90
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH . Contract: EPA REGION m
Project No.: A672-S_____ Site: ______ Location: ______ Group:
Instrument ID: VOA1_____ Calibration Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) _Y_ ' Calibration Times: 0738 1038
GC Column DB624 ID: 0.53 (mm)
Lab File ID: RRF10 = L1391.D RRF20 = L1390.DRRF50 = L1389.D RRFIOO = L1392.D RRF200 = L1393.D
COMPOUNDDichlorodifluoromethaneChtoromethaneBroraomethaue *Vinyl Chloride *Chloroethahe • •Methyiene ChlorideAcetone - .Carbon Disulfide .1,1-Dichloroethene *1,1-Dichloroethane / *trans-1, 2-dichloroetbenecis-1 ,2-DichloroetheneChloroform - *1,2-Dichloroediane *2-Butanone1,1,1-Trichloroethane , *Carbon Terrachloride *Bromodkhlaromethane *1,2-Dichloropropane .- 'cis-1, 3-Dichloropropene *Frichloroethene , • -*Dibromochloromethane *1,1,2-Trichloroethane +•Benzene; ... .,' . . - ;*trans-1, 3-Dichloropropene • *iromoform . *4-Memyl-2-Pentanone2-Hexanone -retrachloroethene *1,1,2,2-Tetrachloroethane >Toluene ..*Chlorobenzene . • ,- > , *Ethylbenzene " ffc "'""'.SfeAStyrene '- • .. "r ••<'•--' >.*ta+ p-Xylenes , . • "; *o-xylene. *
RRF100.2410.4100.6950.6150.4571.664.0.736.'3.1171.886?2.8072.1721.9203.5071,7830.2750.4520.4180.531s0.4080.487
. 0.3580.4730.3800.846,'0.438- -0:3480.7630.4740.47,10.9361.2430.947,
:M34iI*?jJO.8701 .0.5311.043
. RRg20 :0,249;-0.454 , -0.770.-0.701 J
0.618."•'. IJS6S&:0:908£?3.219*1.965;3.2052.1612.0663.486.2.0510.3420.492f0.48370.609K0.435 K0.554-f;0;408f;0.552 c0.434.0.922,rOJ505l"0.4210.8350.617,0.4760.967.1.256.0.984;VtiS&K.-0.9390.5401.066
'
vRRFSO0.3000.453,0.7030,768-a5371 668';0.707 '3:3172.0983.1542.3222.1403.6851.9170.2830.4640.4740.5800.415 v.5160.380.0.531 :0.396;0.859SO.4770.4080.765.0.554-0.4770.9111.213:0.9603 456T0.919 r0,5141.046
RRFIOO.0.2120.4020.6950.6460.426.1.652-0.5522.9491.974 -2.8992.1512.0003.5541.9340.2410.4340.4200.5340.3810.4800.3580.5000.3660.8000.4480.378
> 0.6000.448
' 0.4250.7851.1250.865n.329 ;0.863.0.4820.981
"
RRF200.0.2100.4310.578 .0.6690.3561.4950.4962.5571.6862.7061.9381.9173.1431.8200.2500.395 .0.3920.4880.336
. 0.4330.3060.4730.3560.7230.421 '0.3660.6170.4580.405"0.7981.0610.837>1.140 -.0.8320.5050.932
RRF0.2420.4300.6880.6800.4791.6300.6803:0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.4940.3620.5060.387018300.4580.3840.7160.5100.4510.8791.1790.9191.3680.885 .0.514L014
%RSD15.05.610.18.621.24.623.99.87.97.46.44.85.85.514.28.19.08.69.69.110.37.07.98.97.37.714.314.37.49.47.16.910.54.94'.45.5
* Compounds with required minimnni RRF and maximum %RSD values. . H A H 1 /( OAll other compounds must meet a minimum RRF of 0.010. U U U J. 4 O
Pagelof2. . AR3I81*55FORM VI VOA 3/90
6A , .' VOLATILE ORGAlNICS INITIAL CALIBRATION DATA ___ -^ g Q
- Lab Name: CHEMTECH _____ Contract: EPA REGION ffl
Project No.: A672-S Site: _____ Location: ______ Group: ___
Instrument ID: VOA1______ Calibration Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) _Y_ Calibration Tunes: 0738 1038
GC Column DB624 ID: 0.53 (mm)
Lab File ID: ' RRF10 = LI39I.D RRF20 - L1390JDRRF50 = . LI389.D RRFIOO = L1392.D RRF200 - L1393.D
COMPOUND
,
-
-
•
, ,
' ,: " . • ' - • - •
Toluene-dSBromofluorobenzene ,. *1 ,2-Dichloroethane-d4
RRF10
1.2780.7271.802
RRF20
1
1.1360.6601.825
RRF50
,
1.0510.5951,728
RRFIOO
_
0.9940.5651.711
RRF200
'
^
. ••,0.9620.5391.587
RRF
•
— ••».,
'; , '/ _-,.
1.084O.6171.731
J£D.,'
,
• ,- ..
*
••:v'.11.712.45.4
-
*.
* Compounds with required minimum RRF and maTJmtmi %RSD values.All odier compounds must meet a minimum RRF of 0.010.
Page 2 of 2FORM VI VGA A R 3 j 8 k 5 6 3/90
000144
. , 7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION in
Project No. A672-S Site: • Location: Group:
Instrument ID: VOA1 Calibration Date: 12/7/95 Tune: 0928
Lab File ID: L1411.D ______ Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Init. Calib. Tunes: 0738 1038
GC Column: DB624 - ID: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneBromometbaneVinyl ChlorideChloroethane .Methylene ChlorideAcetone ;Carbon Disulfide1,1-Dichloroethene1 , 1 -Dichloroethanetrans- 1 ,2-dichloroedienecis-1 ,2-DichloroetheneChloroform1 ,2-Dichloroediane2-Butanone1,1,1-TrichloroedianeCarbon TerrachldrideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroedieneDibromochioromediane1 , 1 ,2-TrichloroedianeBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanbneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzene . . • ;- .Ethylbenzene. ' •Styrenem-l- p-Xylenes \ .o-xylene
-
RRF0.2420.4300.6880.6800.4791.6300.680 J3:0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.4940.362 *0.5060.387"0.830:0.4580.3840.7160.5100.4510.8791.1790:9191.3680.8850.5141.013
RRF500.252 '0.4740.7500.7260.4211.9460.4413.5382.0462.9402.3422.0243.6161.8400.1860.5090.5080.6210.4400.5570.4030.5960.425
; 0:9070.4870.4500.522014590.5330.8781.240
•4 1.0261.5131.0400.5731.156
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.100*0.5000.1000.100
0.2000.5000.4000.5000.100:0.3000.3000.300
%D-4.1-10.2-9.0-6.812.1-19.4O5-O
-16.7-6.50.5-9.0>0.84.13.2
03.0-i3:&--16.2
. -13.1-11.4-12.8-11.3-17.8-9.8-9.3-6.3-17.2r27.G?10.0-18.20.1-5.2 .rll.6
-10.6* -17.5-11.5-14.1
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.025.025.025.025.025.0
I
SAMPLE NO.VSTD050VBLK011811127PD51811128D411811128D421811128D461811129D471811129D48 .I811127D201181I127D20MS1811127D20MSD
.
All other compounds must meet a mininmtn RRF of 0.010.flR3!8li57 Q00162
Page I of 2
, 7 AVOLATILE CONTINUING CALIBRATION CHECK _ N o
Lab Name: CHEMTECH -_____ , Contract: EPA REGION HI
Project No. A672-S Site: Location: Group: __
Instrument ID: VOA1 Calibration Date: 12/7/95 Tune: 0928
Lab File ID: L1411.D Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Init. Calib. Times': 0738 1038
GC Column: DB624 ID: 0.53 (mm)
COMPOUND-
*¥
-
:
Toluene-d8; Bromofluorobenzene1 ,2-Dichloroethane-d4
RRF
-
1.0840.6171.731
RRF50
1.3330.8061.676
MINRRF
0.200
%D
~"--
,
-23.0C30.63.2
MAX%D
--
1)25.0
All other compounds must meet a minimum RRF of 0.010. n A n « n n000163Page2of2 AR3 181*58
FORM VH VOA 3/90
VOLATILE CONTINUING CALIBRATION CHECK-. .. ' . -
Lab Name: CHEMTECH_______ Contract: EPA REGION m
Project No. • A672-S Site: Location: ____ Group:
Instrument ID: VOA1 Calibration Date: 12/7/95 Tune: 2203
Lab File ID: L1427.D _______ Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Init. Calib. Times: 0738 1038
GC Column: DB624 ID: 0.53 (mm)
All other compounds must meet a minimum RRF of 0.010.AR3I81*59 000164
Page I of2
COMPOUNDDichlorodiiluoromedianeChloromethaneBromomethaneVinyl ChlorideChlbroethane . .
. Methylene Chloride .Acetone .Carbon Disulfide1 , l-Dichloroernene1 ; 1-Dichloroethane
. trans- 1.2-dichloroethenecis- 1 ,2-DichloroetheneChloroform1,2-Dichloroethane
• 2-Butanone1,1,1 -TrichloroethaneCarbon TetrachlorideBrbmodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromediane1 , 1 ,2-TrichloroethaneBenzene -trans-1 ,3-DichloropropeneBromoform4-Memyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneToluene -Chtorooenzene : •EthylbenzeneStyrenem-l- p-Xylenes • ,.o-xylene
RRF0.2420.4300.688 :0.6800.479 -: 1,630 '*•0,6803.0321.9222.9542.1492.0083.4751.9010.278,0.4480.4370.5490,3950:4940.362 .0.5060.387
~01S30~0.4580.384
- 0.716 -0.5100.4510:8791.179rO#19'•*!li368-.~:0.885015141.013
RRF500.212.0.4535o.83r-0.5080*415**la$?5 •• 0.751,:2:9241:8%2.7822.207
' 2.0893.5751.837 .0.3340.519'0.5430.688."0.465-0.572-0.4320.6280.427O.'SSS'0.4790.3970.7750.5560.5260.8361.250
~*QM1 -i sr0.9610.5131.053
MINRRF
-
0.-1000.100. :.;,
- -.,..,.-.....-...-- 1 .-.,
011000.200
0.2000.100
0.1000.1000.200
v .
0.2000.3000.1000.100•X):500-0.1000.100
0.2000.5000.4000.500.1000.3000.3000.300'
%D12.4-5.3-20.8 -.(25.3J13.4-2.8-10,43.61.45.8-2.7-4.0-2.93.4-20.1-isra--24.3C-25.&-17.7-15.8-19.3-24.1-10.3-7.0. --4.6 --3.4-8.2-9.0-16.64.9-6.0-3.0 --1.08.60.2-3.9
.MAX%D
25.025.0
25.025.0
•
25.025.0
25.0, 25:025.0
25.025.025.025.0-25.025.025.0
25.025.025.025.0.25.0.25.0-25.025.0
SAMPLE NO.VSTD050VBLK021811128D341811128D131811129D181811130D061811130D501811130D49181H30D511811204D531811204D541811204D551811204D561811204D57
-
' • • • • - " - • - . . - • T----7A .VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION ffl
Project No. A672-S_____ Site: Location: ___ Group:
Instrument ID: VOA1 Calibration Date: 12/7/95 Time: 2203
Lab File ID: L1427.D __________ Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Ink. Calib. Times: 0738 1038
GC Column: DB624 ID: 0.53 (mm)
COMPOUND
.•
• ' ' , . • • - - . ». • • ' - - - .' • . .
• • •. - - •
,
.•
-
;.
i ~ . .*
' • • • • • • , • • ' ' • .•••" • • -: •_•„;*":• -
"
' V" '- " ' f
'•''-.-X? -.-:,>".'----v**-4-.>-<*»' J r?.• '• -•- . • .v- ,-..-;, -: <:: -SLxz-Toluene-d8 . ,>•••• •'••Bromofluorobenzene
. l,2-Dichloroethane-d4
RRF
•
•«-;. v- • •/• •-••
4e fes .'t. • , ff,. .*•-»•"*?**, '-'
- 1.084. 0.6171.731
RRF50,
,.-- •• -' •
•
.. .'. '. .-'--' -••'
V- •.-"..,r* • •' ' •
.1.2400.7361.721
MINRRF
1 ' '. --
-
..;• ' ''
....„_.
. •"•--'
0.200
%D
• > ' ,
~*~
v;'>' . "
,.,'i--.-. _ . ,
-14.4. -19.30.6
MAX%D
\
25.0.
All other compounds, must meet a minimum RRF of 0.010.
Page2of2 A R 3 I 8 1* 6 0FORM Vn VOA 3/90
. • " ' . 6A ' . ' ' '' .VOLATILE ORGANICS INITIAL-CALIBRATION DATA 33)6-
Lab Name: CHEMTECH _____ Contract: EPA REGION IIIf . . •
Project No.: A673-S_____ Site: _____ Location: ______ Group:
Instrument ID: VOA1 _____ Calibration Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) _Y_ ' Calibration Times: 0738 1038GC Column DB624 ID: 0.53 (mm)
Lab File ID: RRF10 = L1391.D RRF20 = L1390.DRRF50 = L1389.D RRFIOO = L1392.D RRF200 = L1393.D
COMPOUNDDichlorodifluoromethaneChloromethaneBromomediane *Vinyl Chloride *ChloroethaneMemylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1,1-Dicliloroethane *trans- 1 ,2-dichloroethenecis-1, 2-Dichloroethene "Chloroform *1,2-Dichloroethane, *2-Butanone1,1,1 -Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1 ,2-Dichloropropanecis-1, 3-Dichloropropene *Trichloroethene *Dibrbmochloromediane *1,1,2-Trichloroethane *Benzene *trans-1, 3-Dichloropropene •*Bromoform *4-Methyl-2-Pentanone2-Hexanoneretrachloroethene *1 , 1 ,2,2-Tetrachloroethane *Toluene *Chlorobenzene , *Ethylbenzene *Styrene *nr+ p-Xylenes - *o-xylene *
• • •
RRFIO0.2410.4100.6950.6150.4571.6640.7363.1171.8862.8072.1721.9203.5071.7830.2750.4520.4180.5310.4080;4870.3580.4730.3800.8460.4380.3480.7630.4740.4710.9361.2430.9471.411,0.8700.5311.043
RRF200.2490.4540.7700.701:0.618.1.6690.9083.2191.965'3.2052.1612.0663.4862.0510.3420.4920.4830.6090.4350.5540.4080.5520.4340.9220.505 =0.4210.8350.6170.4760.9671.2560.9841.505 '«0.9390.5401.066
RRF500.3000.4530.7030.768V0.5371.6680.7073.3172.0983.1542.3222.1403.6851.9170.2830.4640.4740.5800.4150.5160.3800.5310.3%0.8590.4770.4080.7650.5540.4770.9111.2130.9601.4560.9190.5141.046
RRFIOO0.2120.4020.6950.6460.426.1.6520.5522.9491.9742.8992.1512.0003.5541.9340.241.0.4340.4200.5340.3810.4800.3580.5000.3660.8000.4480.3780.6000.4480.4250.7851.1250.8651.3290.8630.4820.981
RRF2000.2100.4310.5780.6690.3561.4950.4962.5571.6862.7061.9381.9173.1431.820
. 0.2500.395 _0.3920.4880.3360.4330.3060.4730.3560.7230.4210.3660.6170.4580.4050.7981.0610.8371.1400.8320.5050.932
RRF0.2420.4300.6880.6800.4791.630.0.6803.0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.5490.3950.494013620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.9191.3680.8850.514'
_ 1.014
%RSD15.05.610.18.621.24.623.99.87.97.46.44.85.85.514.28.19.08/69.69.110.37.07.98.97.37.714.314.37.49.47.16.910.54.94.4515
**
**
**
4>
*
*
4>
4>
*
*
*
*
4i
*
*
*
*
*
*
4>
*
Compounds with required minimum RRF and mariiniiin %RSD values. U U U1 4All other compounds must meet a minimum RRF of 0.010. /} D o I o / r I
Page 1 of2 Hn •? i 0*40 IFORM VI VGA 3/90
. 6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH_________ Contract: EPA REGION m — ]>* — — ——• — —--—— _—-i-- ^ V_____BB____________________________.M^_^__MH_
Project No.: A673-S_____ Site: _____ Location: _____ Group:
Instrument ID: VOA1________ Calibration Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) _Y_ ' Calibration Tunes: 0738 1038
GC Column DB624 ID: 0.53 (mm)
Lab File ID: RRF10 = L1391.D RRF20 = L1390.DRRF50 •=* L1389.D RRFIOO = L1392.D RRF200 = L1393.D
COMPOUND
•
t
•
•
•
1• - - • • - '
roiuene-dS 'Bromofluorobenzene *l,2-Dichloroethane-d4
RRF10
-
.1.2780.7271.802
RRF20
-
,.
1.1360.6601.825
RRF50
•»,
,'
1.0510.5951.728
RRFIOO
\
0.9940.5651.711
RRF200
^
-
0.9620.5391.587
RRF
•_
,
1.0840.6171.731
%RSD
x
11.712.45.4
* Compounds with required minimum RRF and maximmn %RSD values. A Q() 1 AAll Other compounds must meet a minimum RRF nf Q.Q1Q, •'-I**
Page 2 of2AR3I8l*62 3/9°
7A ..VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: EPA REGION III
Project No. A673-S _____ Site: ' Location: _____ Group:
Instrument ID: VOA1 Calibration Date: 12/8/95 Tune: 1700
Lab File ID: L1442.D _________ Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y hiit. Calib. Times: 0738 1038
GC Column: DB624 ID: 0.53 (nun)
COMPOUND• Dichlorodifluorouietl mi ieCnloromediarieBromomedianeVinyl ChlorideChjorocthane
. Medrylene ChlorideAcetoneCarbon Disul fide1,1-DicbJorpeiheiic1 , 1 -Dichlorocdiauc:trans-l,2-Dichlon)ctliciiccis-l,2-Dichkm>ctliciicChloroform1 ,2-Dichloroethanc2-Butanonel,l,l-Trichlonx:tlianeCarbon.TetrachlorkleBromodichloromethaiic1,2-Dichloropropaiic
. cis-1 ,3-DichloropropciicTrichloroetlieiieDibrbmoclilontmetliane1,1,2-TrichlonKJthaiic-
•iBenzene: 1'* • 'trans-1.3-DichloropropcticBromofbrm4-Methyl-2-Pentaiu)iie2-HexanoneTerrachloroetliene1 , 1 ,2,2-TetrachloroethaneToluene .ChlorbbenzeueEmylbenzeneStyrenem+ p-Xyleheso-xylene
RRF0.2420.4300.6880.6800.4791.6300.6803.0321.9222.9542.1492.0083.475 .1.901'0.278•0.4480.437
[ 0.549.0.3950.4940.3620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.9191.3680.8850.5141.013
' •
.
RRF500.1220.2770.7530.4240.256!1.7130.7392.8562.0042.8972.2281.9483.5501.8640.3620.5380.4800.7480.4980.6150.3920.5780.4460.9750.5110.3840.7260.5730.459 .0.7501.2991.0081.4020.9680.5381.121
MINRRF
0.1000.100.
0.1000.200
. 0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000,5000.100 •0.3000.3000.300
•
*bC49C35J2
-9.4(37.6:)C46.6J)-5.1-8.7 . '5.8-4.31.9-3.73.0-2.21.9
C-30.2-20.T-9.8
<r36.23>
G?eX>-24.5-8.3
•-14.2-15.2-17.5-11.60.0-1.4-12.4-1.814.7-10.2-9.7-2.5'-9.4-4.7-10.7
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.025,025.025.025.025.0
j SAMPLE NO.VSTD050VBLK011811205D581811205DS91811205D601811205D63181 1205 DOS18112P5D03 1811206P02 '«.1811206D611811204D521811204D52MS1811204D52MSD
•
,
'
All other compounds must meet a minimum RRF of 0.010. 000166A n 3 I 8 k 6 3
Page I of2
7AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH________ Contract: EPA REGION III . —j> S 2—
Project No. A673-S Site: Location: ___ Group:
Instrument ID: VOA1 Calibration Date: 12/8/95 Tune: 1700
Lab File ID: L1442.D Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Init. Calih. Times: 0738 1038
GC Column: DB624 ID: 0.53 (nun)
COMPOUND
.
-
•
-
. '
t^
. . . .«
Toluene-d8Bromofluorobenzeuel,2-Diculoroedianc:-d4 .
RRF
1
•1.0840.6171.731
RRF50
,
-
,
:
1.4290.7061.980
MINRRF
1
'"
0.200
%D,
-. •
~ ~-
•
-
C3y_-14.4-14.4
MAX%D
1
"
25.0
All other compounds must meet a minimum RRF of 0.010.
Page2of2 'fl R 3 1 8 k 6 I*FORM VH VGA 3/90 II
• '• 7A• .VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH - Contract: EPA REGION III
Project No. A673-S' Site: Location: Group:
Instrument ID: VOA1 Calibration Date: 12/16/95 Time: 0847
Lab File ID: L148S.D___________ I''"- Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y , Init. Calih. Times: 0738 1038
GC Column: DB624 ID: U53 (mm)
COMPOUNDDichlorodifluorometlunc .Chloromethaue ' 'BromomedianeVinyl ChlorideChloroediane • .Methylene Chloride •AcetoneCarbon Disuitide1,1-Dichloroethcnc1,1-Dichloroethanctrans- L2-Dichloroetlicnccis-1 ,2-DichloroedieiicChloroform1,2-Dichioroethahe2-Butanone1,1, 1-TrichloroethaiicCarbon TetrachlorideBromodichloroinetliaiic1,2-Dichloropropanecis-1 ,3-DichloropnipeneTrichloroediene ' 'Dibromochloronietliane1 , 1 »2-Trichlon>etliaiie
"-'•Benzene '.• • '*r •• , •trans-1, 3-DichloropropciieBromofbrm4-Memyl-2-PentaiK)iie24iexanoneTerrachloroedieueIrli2,2-Tetrachicm>etliaiicTolueneChlorobenzeneEthylbenzene <-.••'.'Styrenem+ p-Xylenes. •o-xylene
RRF0.2420.4300.6880.6800.4791.6300.6803.0321.9222.9542.1492.0083.4751.9010.2780.4480.4370.549U3950.4940.3620.5060.3870.8300.4580.3840.7160.5100.4510.8791.1790.919113680.8850.5141.013
RRF500.1060.4430.8010.4660.2741.6170.9012.8291.5872.7352.1172.3743.8541.9840.3560.4270.5270.5770.4690.4870.4570.6230.4390.7910.4230.4160.8040.590Q.5520.8391.1050.9841.2130.9400.4690/909
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
%D-_C56.2-3.0-16.4f3_1.5j)C42.8>>O.g.
C-32.5J6.717.47.41.5-18.2-10.9-4.4
C-28.J >4.7---20.6-5.1-18.71.4
&6.£>-23.1-13.44.77.6-8.3-12.3-15.7-22.44.66.3-7.111.3-6.28.810.3
MAX%D
25.025.0
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025.025.025.025.025.025.025.0
1SAMPLE NO.VSTD050VBLK021811206P02RE181I206D6418112060621811206D6S1811206D661811207D041811213G011811213G021811213G031811214G041811214D67
All other compounds must meet a minimum RRF of 0.010.AR3!8i*65
Page 1 of 2
7 AVOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH . Contract: EPA REGION III
Project No. A673-S _____ Site: __ Location: __ Group:
Instrument ID: VOA1 Calibration Date: 12/16/95 Time: 0847
Lab File ID: L1485.D Init. Calib. Date(s): 12/3/95 12/3/95
Heated Purge: (Y/N) Y Iiiit. Calib. Times: 0738 1038
GC Column: DB624 ID: 0!5? (nun) .
COMPOUND
Toluene-d8Bromofiuorobenzene1 ,2-Dichloroethane-d4
-RRF
•*
1.0840.6171.731
RRF50
- /
•
1.2290.7001.582
MINRRF
0.200
%D
B
""" "
'
'
-13.4-13.58.6
MAX%D
•
25.0
All odier compounds must meet a minimum RRF of 0 010. U U U 1 D O
Page2of2 A R 3 I 8 'I* 6 6FORM VH VOA 3/90
' . ' ; . " • - • ' . • . - - • . 6 AVOLATILE ORGANICS INITIAL CALIBRATION BATA '
Lab Name: CHEMTECH_____. Contract: US EPA REGION ffl .
Project No.: A695-S_____ Site: Location: ______ Group:
Instrument ID: HP5971A Calibration Date(s): 12/21/95 12/21/95
Heated Purge: (Y/N) _Y_ " Calibration Times: 1034 1401
GC Column DB624 ID: 0.53 (mm) -
Lab File ID: RRF10 = L1534.D RRF20 - L1533.DRRF50 = L1532.D RRFIOO = L1535.D RRF200 = L1536.D
COMPOUNDDicMorodiflaoromethaneChloromethaneBromomethane . *Vinyl Chloride • *ChloroethaneMethylene Chloride 'AcetoneCarbon Disulfide '1,1-Dichloroethene *1,1-Dichloroethane *1,2-Dichloroethene (total)Chloroform. . *1,2-Dichloroethane *2-Butanone1,1, 1-Trichloroethane *Carbon Tetrachloride *Bromodichloromethane *1,2-Dichldropropanecis-113-DichIoropropene" *rrichloroediene - . *Dibromochloromethane • *1,1,2-Trichloroethane *Benzene *trans-1, 3-Dichloropropene ,. *Bromoform ' - ' - *4-Methyl-2-Pentanone2-HexanoneTetrachloroethene *1,1,2,2-Tetrachloroethane *Toluene *Chlorobenzene , *Ethylbenzene *Styrerie ,'•' ::-^--: • -';/&$*m+ p-Xylenes . o- *o-xylene ' • ' • . - ' *
RRF101.0600.9420.9511.2150.3511.757 ,0.9403.8662.0303.1974.7075.9563.1380.3090.5090.4750.6720.4300.540 '0.4150.5250.3930.909
, 0.480 ;0:344;0.7600.5210.4360.7241.2080.9211.5090.9250.5491.200
RRF201.2461.3071.0231.2600.3381.7640.8823.7552.097,311614.8245.4633.0630.2810.4870.4710.6470.4110.5190.3980.5270.3710.862.0.467.;0.3610.763 -t0.554
i 0.4580.7271.2320.9301.5290.938 h0.5571.178
RRFSO^0.9831.1220.760.1.0000.301,Iv372 :.0.683 ..-,.3.0321.576 :2.4033.7473.8262.4780.2180.4000.3790,5030.3160.4110.3320.4340.291.0.6810.3670.315*:0.5700.3900.3660.571 v0.951 .0.7111.134,0.723$0.412 '-ft.0.876• . . ' -- >','
RRFIOO'0 8571.0080.781a%20.28113810:6 73.084 -r1.6482.3413.512-3.4292.6520.2640.477'0.45501621 :D1402 ;0.520"013930.509-
.0.3650.830 r-
0.473;}.••*O361$i*0.6760.4%0.4050.641 .1,108. 0.845.1.340 „*&&$&*•vOi494f,1.056
RRF2000.7250.9360.784
_• 1.0000.260
v:l:l%-U'582;;2.8021.343
, 1.9963.7723.5532.2330.2100.372.0.355-,0.478>0 3110.4070.3110.400.0.2860.644
;fc0.373E?o:290'0.5380.3950.321 •0.5050.8620.668
- 1;0330:674 •-,"
* 0.388 '0.798i
RRF0.9741.0630.8601.0870.3061.4940.7573.3081.7392.6204,1194.4452.7130.2560.4490.4270.5840.3740.4790.3700,4790.3410.7850.4320.3340.6620.4710.3970.6331.0720.8151.3090.8220.480 *1.022
• •• '>
.%RSD20,314.613.912.812.517.019.714.318.320.414.626.414.216.513.313.1-15.015.013.512.312.214.514.813.19.315.815.913.815.315.114.816.914.516.117.6
**
**
**
**4>
4>
*
41
*
*
*
*
*
41
4r.
*
*
*
*
4>
* Compounds with required minimum RRF and maximum %RSD values.All other compounds must meet a minimum RRF of 0.010. . .. • 000044
Page 1 of 2 • '/I R Q f O/. C 7FORM VI VGA '^ H 0 j 0 4 b / 3/90
6AVOLATILE ORGANICS INITIAL CALIBRATION DATA
Lab Name: CHEMTECH Contract: US EPA REGION m
Project No.: A695-S_____ Site: _____ Location: ______ Group:
Instrument ID: HP5971A Calibration Date(s): 12/21/95 12/21/95
Heated Purge: (Y/N) _Y_ " Calibration Times: 1034 1401
GC Column DB624 ID: 0.53 (mm)
Lab File ID: RRF10 = L1534.D RRF20 = L1533.DRRF50 = L1532.D RRFIOO = L1535.D RRF200 = L1536.D
COMPOUND
X
• - • -; V'-V '?'<#**•' " • *::* •?;-
**'• '•- " ,r
." - ••-,:.•
' . '. "V
.
• •- --.v . '.-••.• • ,',.'.:„,-: - z~, ''*': .--V"
. - ,
. - ••• . iij$ c**?'9S -%*-$&
ToIuene-dS ^ ' '*• ' ;f- r* '~Bromofluorobenzene . *l,2TDichloroetnane-d4
RRFIO
;
I/
..--
• -\ '
' X - >•
..*•'• • : •'-
,-
.• r ;--*-1.423.1.0023.727
RRF20
•
. • ••
i
••".?:• 3$?%;
1.117 r0.7612.649
RRF50
,
.;.^ J-1.0160.651
' 2.388
RRFIOO
_
1.0130.6502.253
RRF200
.
0.8170.5082.131
RRF
1.0770.7142.629
%RSD
•
20.625.724.5
* Compounds with required minimum RRF arid mflyiimnn %RSD values. . 000045All other compounds must meet a miniminn RRF of 0.010.
Page 2 of 2 • ' - - A D O I O I C oFORM VI VOA H (1 O I O «4 D O 3/90
• • ' ' : ' • ' '' 7A • •' ' ,VOLATILE CONTINUING CALIBRATION CHECK
Lab Name: CHEMTECH Contract: US EPA REGION m
Project No, A695-S _____ Site: Location: _____ Group:
Instrument ID: HP5971A Calibration Date: 12/22/95 Tune: 1034
Lab File ID: L1538.D________ Init. Calib. Date(s): 12/21/95 12/21/95
Heated Purge: (Y/N) Y Init. Calib. Times: 1034 1401
GC Column: DB624 ID: 0.53 (mm)
COMPOUNDDichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethane . -Methylene ChlorideAcetone , •Carbon Disulfide1,1-Dichloroethenc1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane -2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzene ;trans-1 ,3-DichloropropeneBromofbrm '4~Methyl-2-Pentanone .
. 2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEmylbenzene • ; , .Styrene .m+ p-Xyleneso-xylene
^RRF0.9741.0630.8601.0870.3061.4940.7573.3081.7392.6204.1194.4452.7130.2560.4490.4270.5840.3740.4790.3700.4790.3410.7850.4320.3340.6620.4710.3970.633L0720.815,1.3090.8220.4801.022
RRF501.0360.8890.8661.0690.2841.580 -0.7713.3481.8652.8614.3854.4082.9470.2530.4800.4470.6250.3940.5210.3930.4970.3570.8480.4690.3460.6490.4760.4140.6231.1490.8561.4000.8220.5081.104
MINRRF
0.1000.100
0.1000.200
0.2000.100
0.1000.1000.200
0.2000.3000.1000.1000.5000.1000.100
0.2000.5000.4000.5000.1000.3000.3000.300
•
%D-6.416.4-0.71.77.2-5.8 .-1.8-1.2-7.2-9.2-7.40.8-8.61.2-6.9-4.?-7.0-5.3-8.8-6.2.-3.8-4.7-8.0-8.6 -•„••-3.62.0-LI-4.31.6-7.2-5.0-7:00.0-5.8 '•-8.0 -
MAX%D
25.0 ,25.0
.-'
25.025.0
25.025.0
25.025.025.0
25.025.025.025.025.025.025.0
25.025,025.025.0.,25.0,25.025.025.0
All odier compounds must meet a minimum RRF of 0.010. '•
SAMPLE NO.VSTD050VBLK011811218D691811218D22 -1811218D681811218D68MS1811218D68MSD1811218D69RE1811218D68RE
10062
Pagelof2 ' AR3l&l»69FORM VH VOA 3/90
7AVOLATILE CONTINUING CALIBRATION CHECK
' 'LabName: CHEMTECH Contract: US EPA REGION ffl
'
Project No. A69S-S _____ Site: Location: _____ Group:
Instrument ID: HP5971A Calibration Date: 12/22/95 Tune: 1034
Lab File ID: L1538.D___________ Init. Calib. Date(s): 12/21/95 12/21/95
Heated Purge: (Y/N) Y Init. Calib. Times: 1034 1401
GC Column: DB624 • ID: 0.53 (mm)
COMPOUND
.
1
•*
• • " ' • - ' . , (-''•..". *"• .
' ., " "
Toluene-d8Bromofluorobenzene . .l,2-DicbloroethaiK-d4
RRF
-. ' !'•-? < '• ''
•,'••.'.;,•%'•"•-'
1.0770.7142.629
RRF50
r~
- •
0.9870.6552.4%
MIN.RRF
T.
0.200
%D
,
---.
•
8.48.35.1
MAX%D
V
.,
25.0
All other compounds must meet a minimum RRF of 0.010. 000063
Page2of2 A R 3 I 8 k 7 0FORM VH VGA 3/90
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Report Number: A671-S Dase Number: R3181
a. Number of Samples and Date of Sample Receipt:
20 water samples were received intact on November 29.30, and December 1.1995. .
b. Parameters:
These samples were analyzed for TCL Volatile + Dichlorodifluoromethahe.t • - -
c. Analytical Techniques:
Samples were purged and analyzed by EPA GLP SOW OLM03.0 Method.
d. QA/QC's:
The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eaSample is found on Form VIII-A, and Initial Calibration results are. found on Form VI-A. Both ContinuiCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatsamples are reported on Form "IV-A". The 1811127W20 is reported on Form HI A and all %R's are within tcontrol limits.
I certify that the data package is in compliance with the terms and conditions of the contract, both technically and icompleteness, for other/than the conditions detailed above. Release of the data contained in this hard copy data packahas been authorized by thejaboratory manager or his designed, as verified by the following signature.
Name: Divyajit Mehta
Tide: Lab Manager
AR3I8488.
Gannett Fleming GANNETT FLEMING, INC.Suite 200
ENGINEERS AND PLANNERS ow KeysBaltimore. MD 21210
. . Fax: (410) 433-6520Office: (410) 433-8832
December 19, 1995
Mr. Emmanuel HedvatChemtech Consulting Group1 1 0 Route 4Englewood, New Jersey 07631
Re: EPA Contract No.: 68-W8-0037EPA Work Assignment: 37-34-3JZZEPA Region III DAS Case Number R3181Shipping Dates: November 28, November 29, and December 4, 1995Federal Express Airbill Nos.: 4405012183, 4405012113, and 4405011800,
Dear Mr. Hedvat:
The purpose of this letter is to correct errors in the Station Number column on the EPA Chain ofCustody Forms (COCs) for the referenced shipments of samples to Chemtech Consulting Group.
The following table provides the correct Sample Numbers. The Station Location column on theCOCs and the EPA Sample #s were correct:
coc#3-16043
3-16049
3-16049
3-16049
3-16058
3-16058
ShippingDate11/28/95
1 1 /29/95
1 1 /29/95
11/29/95
12/04/95
12/04/95 .
IncorrectStationNumber
SW-34
SW-18
SW-47
SW-48
SW-53
SW-53
CorrectStationNumberSW-34A
SW-18B
SW-47B
SW-48A
SW-53B
SW-53A .
FedExAirbillNumber
4405012183
4405012113
4405012113
4405012113
4405011800
4405011800
•CommentsSample was a trip blank.Sample location and EPASample # were correct.
Sample was a field blank.Sample location and EPASample # were correct.Sample was a field blank.Sample location and EPASample # were correct.Sample was a trip blank.Sample location and EPASample # were correct.
Sample was a field blank.Sample location and EPASample # were cprrect.Sample was a trip blank.Sample location and EPASampfe i were correct.
A Tradition of Excellence Since 1915 A R 3 | 8 l| 8 9
Corrected copies of the COCs referenced above are enclosed.
We apologize for any inconvenience these discrepancies may have caused.
Sincerely,GANNETT FLEMING, INC.
Sidney J. Curran
Enclosures
cc: Annette Lage (CRL) >Christopher Corbert (EPA Region III) (w/o enclosures)Rayo Bhumgara (GF (w/o enclosures)William Wentworth (HNUSI .
File: 9529.001/4.0.
flR3l8l»90
1A >'. SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811127W20MSLab Name: CHEMTECH . Contract: EPA REGION-HI
Project No.: A671-S Site: _____ Location: •_______ Group:
Matrix: (soil/water) WATER Lab Sample ID: t)48162
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1407.D
Level: (low/med) Date Received: 11/29/95
% Moisture: not dec. ______ Date Analyzed: 12/6/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Page Iof2
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:-CAS No. Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-3- '71-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571 -43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChlorometiiaueBromoniethaneVinyl ChlorideChloroetlianeMethylene ChlorideAcetoneCarbon Disulfide1 , i -Dichloroethene1, 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 , 3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachioroethene1 , 1,2,2-TetrachloroethaneTolueneChJorobenzeneEthylbenzeneStyrene
10.10101010
- 10r2.6}1064101010 ^101010101010-10511010581010
. 1010
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H R 3 j 8 k 9 I FORM IVOA 3/90ooo
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No.: A671-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/voi: 5.0 ' (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
>
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1811127W20MS
Group:
048162
L1407.D
11/29/95'
12/6/95
1.0
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Page 2 of 2 . .
AR3I8I»92 FORMIVOA 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION-IE1811127W20MSD
Project No.: A671-S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O48163
Sample wt/vol: 5.Q (g/mL) ML Lab File ID L1408.D
Level: (low/med) Date Received: 11/29/95
% Moisture: not dec. ______ Date Analyzed: 12/7/95
GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ____' (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) . ug/L Q
75-71-874-87-3 •74-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478 87-510061-01-579-01-6124-48-179-00-57M3-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5-108-88-3108-90-7100-41-4100-42-5
DichlorodifluorometnaneCWoromethaneBromometlianeVinyl ChlorideChloroe thaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetheue1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroediane2-Butanone1,1,1 -TrichloroethaneCarbon TetrachJorideBromodichloromethane1 ,2-Dtchloropropanecis- 1 ,3-DichloropropeneTrichloroetheneTDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroetfaene1 ,1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
101010101010$*J1060101010101010101010105310106110101010e**j1058511010
UUuuuuJu
uuuuuu
, uuuuuu
uuuu •Ju
uu
Page 1 of 2FORM I VGA ft4\(!>199 3/90
LA " . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No.: A671-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
1811127W20MSD
Group:
048163
Lab File ID: L1408.D
Date Received:v
Date Analyzed:
GC Column: DB624 ID:' 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L -
1
0 m+ p-Xylenes :1330-20-7 o-xylene
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. •. •- •
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11/29/95
12/7/95
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Page 2 of23/90
Lab Name: CHEMTECH Contract: EPA REGION-IH
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01
Project No.: A671-S Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER . Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) ML . Lab File ID: L1396.D
Level: (low/med) • -Date Received: ____
% Moisture: not dec. ______' Date Analyzed: 12/6/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L • Q
75-71-874-87-374-83-975-OM »75-00-375-09-2 .67-64-175-15-075-35 475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-5 -75-27-478-87-510061-01-5
DichlorodifluoromethaneChloromethaneBromomedianeVinyl ChlorideChloroedianeMemylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichlotoethene1,1-Dichloroethane -1,2-Dichlproethene (total)Chloroform • -,'-1 ,2-Dich!6roethane2-Butanone1,111-Trichloroediane '.Carbon TetrachlorideBromodichloromethane1,2-Dichloropropanccis- 1, 3-Dichloropropene ,
79-01--6 ''r-'* • TnchlotoeaieiS? -'' •-*'>—•124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-
Dibromochloromethane1 , 1 ,2-TrichlbroethaneBenzene - ,nans-l ,"3-DicnloropropeneBromoform4-Memyl-2-Pentanone. 2-Hexanone p ; r
127fl8 ^ «$*<Didi tgt iaafc <f-~ ••*••*#**••79-34-5 ! *Lfl , Tca cnlotocthane108-88-3108-90-7100-41-4 .100-42-5
TolueneChlorobenzeneEthylbenzeneStyrene
10 .101010101010101010101010101010101010
,1010101010101010
..,._,,, .:• |Q> . „ _v. ,.,
1010101010
uuuuuuu
. uuu.u,uuuuuuuuuuuuuuuuuU 'uuuu
Page Iof2 R i Q i ntr84^5 FORMIVOA v. ^__ 3/90
' 1A 'VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION-IE
Project No.: A671-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
SAMPLE NO.
VBLK01
Group:
PBLK01
Lab File ID: L1396.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L Or ug/Kg) ug/L
. •.
0 " m^- p-Xylenes1330-20-7 o-xyiene
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Page 2 of 2' 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01TENTATIVELY'IDENTIFIED COMPOUNDSLab Name: CHEMTECH Contract: EPA REGION-III
Project No. A671 Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER • Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) ML Lab File II): L1396.D
Level: (low/med) Date Received:
% Moisture: not dec. ________ . Date Analyzed; 12/6/95
GC Column: DB624 ID: 0.53 (mm) Dilution Facton 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0 (ug/Lorug/Kg) .ug/L
|£A£ Number1.2.3.4.5.6.7.8.9.10.H.
•12.13.14.15. -'16.17.18..19.20.21.22.23.24.25.26.27.28.29.30.
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1A .. SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK02Lab Name: CHEMTECH Contract: EPA, REGION-HI
Project No.: A671-S Site: _____ Location: ________' Group:
Matrix: (soil/water) WATER Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L14S7.D
Level: (low/med) Date Received:
% Moisture: not dec. ______ Date Analyzed: 12/9/95.
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. -Compound (ug/Lorug/Kg) . ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-1 .75-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-5-10061-01-579-01-6124-18-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-710CW1-4100-42-5
Dichlorodi fluoromethaneChloromethaneBroraometlianeVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfidel.i-Dichloroethene1 , 1 -Dichloroethane1,2-Dicbloroethene (total)Chloroform1,2-DichJoroethane .2-Butanone1 , 1 , 1 -TrichloroedianeCarbon Tetrachloride
, Bromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroetnaneBenzenetrans-1 ,3-DichloropropeneBromoform .4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1, 1.2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
101010101010101010to10101016 x1010101010101010101010101010 : •1010101010
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Page 1 of 2FORM IVOA ' 3/90
M3I8498 OOOltS •
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION-III
Project No.: A671-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 , ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) . ug/L
0 m+ p-Xy4enes1330-20-7 o-xyiene
.
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12/9/95.
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Page 2 of 2HH 3 18*49 9 FORMIVOA Y 3/9°
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH Contract: EPA REGION-HI
VBLK02
Project No. A671 Site: _____ Location: ____________ Group:
Matrix: (soil/water) WATER Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1457.D
Level: (low/med) . Date Received:
% Moisture: not dec. ________ Date Analyzed: 12/9/95
GC Column: DB624_____ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ._____'(uL) Soil Aliquot Volume: _____ (uL)
Concentration Units:Number TICs found: ___0___ (ug/L or ug/Kg) ug/L
CAS Number1.2- •3.4.5.6.7.8.9.10.11.12.13.14.15. -16.17.18.19.20.21.22.23.24. ^25.26.27.28.29.30.
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ChEmiECH7'.'jSiJLTING GSOUP iNC
Report Number: \674-S . Dase Number: R3181/ * . . _ - • -
a. Number ef Samples and Date of Sample Receipt:
20 water samples were received intact on December 5, 6, 8, and 15, 1995.
b. Parameters:
These samples were analyzed for TCL Volatile + Dichlorodifluoromethane.
c. Analytical Techniques:
Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.
d. QA/QC's:"--—. *
The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eacSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuirCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associat<samples are reported on Form "IV-A". The. 1811204W52 is reported on Form HI A and all %R'sare within t!control limits. •
I certify that the data package is in compliance with the terms and conditions of the contract, both technically and fcompleteness, for othe than the conditions detailed above. Release of the data contained in this hard copy data packajhas been authorized! y thejabojatory manager or his designed, as verified by the following signature.
: Divyajit Mehta
Title: Lab Manager ,
AR3I8502 00000?
3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY
Lab Name: CHEMTECH ___________ Contract: EPA REGION III
Project No. A674-S Site: _______ Location: ________ Group: _
Matrix Spike - Sample No.: 1811204W52
COMPOUND1,1-DichloroethcneTrichloroetheneBenzene •TolueneChlorobenzene
SPIKEADDED(ug/L)
5050505050
SAMPLECONCENTRATION
(ug/L)00000
MSCONCENTRATION
(ug/L)5752634743
MS%
REC #1141041269486
QC. 'LIMITSREC.
(61-145)(71-120)(76-127)(76-125)(75-130)
COMPOUND1 , 1-DichioroetheneTrichloroetheneBenzeneTolueneChlorobenzene
SPIKEADDED(ug/L)
5050505050
MSDCONCENTRATION
(ug/L).67SO655545
MS%
REC #134100130 *no •90
%RPD #
16 *4316 *5
QC LRPD1414111313
IMITSREC.
(61-145)(71-120)(76-127)(76-125)(75-130)
# Column to be used to flag recovery and RPD values with an asterisk
* Values outside of QC limits
RPD: 2 out of 5 outside limitsSpike Recovery: 1 out of 10 outside limits
Comments:
FORMin. VOA-I AR3I8503
1A __SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811204W52MSLab Name: CHEMTECH Contract: EPA REGION
Project No.: A674-S , Site: _____ .' Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: O48324
Sample wt/vol: 5.0 (g/mL) ML Lab File ID:L1481.D
Level: (low/med) Date Received: 12/5/95
Page 1 of2 FORMIVOA AR3I850I*
% Moisture:. not dec. ,,___. . Date Analyzed: 12/10/95
GC Column: DB624,________ ID: 0.53 (mm) , Dilution Factor: . 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No, Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87,374-83-9,75-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethane •BromomethaneVinyl ChlorideChloroedianeMediylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetlieue1,1-Dichloroetbane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1 , 1 , 1 -TrichloroethaneCarbon TetrachlonW
- Bromodichloronietbane1 ,2-Dichloropropanccis- 1 ,3-DichloropropeneTrichloroetheneDibromochlorometbane1,1,2-TrichloroethaneBenzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene ._. .1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
. 1010
' 1010
. 1010 '10105710101010101010101010
•• ••--•• •- - -52 •10106310101010
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Lab Name: CHEMTECH - . Contract: EPA REGION HI .1811204W52MS
Project No.: A674-S Site: Location: Group:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID: 048324
Lab File ID: L1481.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ' ug/L
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Page 2 of2FORMIVOA AR3I8505 00 22
1A 'SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION III1811204W52MSD
Project No.: A674-S Site: • Location: ___________ Group:
Matrix: (soil/water) WATER . Lab Sample ID: 048325
Sample \yt/vol: 5.0 (g/mL) ML Lab File ID: L1482.D
Level: (low/med) Date Received: 12/5/95
% Moisture: not dec. ' Date Analyzed: 12/10/95.
GC Column: DB624 ID: 0-.53 (mm) Dilution Factor IJO
Soil Extract Volume:. ______-(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18?*79-34-5 .108-88-3108-90-7100-41-4100-42-5
Dichlorodifluorumethane 'ChlorotnethaneBrbmomethane •.Vinyl ChlorideChloroethaneMediylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene *1 , 1 -Dichloroethane1,2-Dichloroediene (total)Chloroform1 ,2-Dichloroethane2-Butanone1,1,1-Trichloroediane .Carbon TctrachloridcBromodicbJoromeoiane1,2-Dichloropropanecis-1, 3-DichloropropeneTrichloroethene •Dibromochloromethane1 , 1 ,2-TrichloroetbaneBenzenetrans-l,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-Hexanone :.Tetrachlproethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEtfaylbenzeneStyrene
1010101010no 310106710101010
- 1010101010105010106510101010101055451010
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Page 1 of 2 ftooiocnrFORMIVOA ARvl I 8506
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION m
Project No.: A674-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
Lab File ID:
Date Received:t
Date Analyzed:
GC Column: DB624 ID: 0.53. .(mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
/
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1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01Lab Name: CHEMTECH " Contract: EPA REGION ffl
Project No.: A674-S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER . Lab Sample ID: PBLK01
Sample wt/vol: , 5.0 (g/mL) ML Lab File ID: L1457.D
Level: (low/med) • Date Received:
% Moisture: not dec. ___. Date Analyzed: 12/9/95
GC Column: DB624______ ID: 0.53 (mm) Dilution Facton 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)'i
Concentration Units:CASNo. . Compound (ug/L Or ug/Kg) ug/L Q
75-71-8 Dichlorodifluoromethane74-57-3 Chloromediane •74-83-975-0.1-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-3 ..'71-55-6 .56-23-575-27-478-87-510061.-01-579-01*124-48-179-00-371-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
BroniomediaheVinyl ChlorideCfaJoroethaneMediylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1,1 -Dichloroethane1.2-Dichloroediene (total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanecis-1, 3-Dichloropropene
-TrichloroetheneDibromocbJoromethane1, 1 ,2-Tn'chloroethane
• Benzenetrans-1 ,3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone
'v Tetrachloroethehe '.'•-•1,1,2,2-TetrachlbroethaneTolueneChlorobenzeneEthylbenzeneStyrene
101010101010101010101010101010101010101010101010101010101010101010
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Page 1 of 2 •FORMIVOA AR3I8508 000 &3
1A .VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH - Contract: EPA REGION ffi
SAMPLE NO.
VBLK01
Project No.: A674-S Site: Location: Group: VH
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/L
Page 2 ol
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IE ' SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH * Contract: EPA REGION IH
VBLK01
Project No. A674 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER " Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1457.D
Level: (low/med) , Date Received:
% Moisture: not dec. ______ Date Analyzed: 12/9/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _____ (uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:'Number TICs found: 0 (ug/L or ug/Kg) ug/L
CAS Number1.2. .3.4.5.6.7.8.9.10.11.12.13.14.15. .16.17.18. ' <. •19.20.21.22.23. .24.25.36.O?A-& .-'.-v27. '.;.'•..; •:•:28. "•'29.30.
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1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK02Lab Name: CHEMTECH Contract: EPA REGION ffl
Project No.: A674-S Site: _____ Location: __________ Group:
Matrix: (soil/water) WATER Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) ML Lab File ID:L1471.D
Level: (low/med) Date Received:
% Moisture: not dec. ______ Date Analyzed: 12/9/95
GC Column: DB624 - ID: 0.53 (mm) Dilution Factor: 1.0
Page 1 of 2FORM I VGA
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66 3107-06-2 •78-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
Dichlorodi fluoromedianeChloromedianeBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroediane2-Butanone1,1,1-Trichloroethane -Carbon TetrachlorideBromodichloromethane1,2-Dichloropropane .cis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroetnaneBenzenetrans-1 ,3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1,1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
101010101010101010101010 "--101010101010101010101010101010101010101010
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Lab Name: CHEMTECH Contract: EPA REGION IH
Project No.: A674-S Site: ' Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: .not dec.
Lab Sample ID:
SAMPLE NO.
VBLK02
Group:
PBLK02
LabFileID:L1471.D
Date Received:
Date Analyzed:
GC Column: DB624 , ID: 0.53 (mm) . Dilution Factor
Soil Extract Volume: (uL)' Soil Aliquot Volume:
Concentration Units:CAS No. Compound . (ug/L or ug/Kg) ug/L
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IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS VBLK02
Lab Name: CHEMTECH___________' Contract: EPA REGION. HI
Project No. A674 Site: _______ Location: '_______ Group:
Matrix: (soil/water) WATER Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) ML Lab File ID:L1471.D
Level: (low/med) . Date Received:
% Moisture: not dec. ________ Date Analyzed: 12/9/95
GC Column: DB624_______ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) • Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found; .0 v (ug/L or ug/Kg) ug/L
CAS Number•1. , ' ' . •2.3.4.5.6.7.8.9.10.11.12. .13.14. .15.16.17.18.19.20.21.22. ,23.24.25. ,>&&**?+.:;--. •; -27..28.29.30.
: Compound Name
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1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK03Lab Name: CHEMTECH , Contract: EPA REGION ffl
Project No.: A674-S Site: _____ Location: ._______ Group:
Matrix: (soil/water) WATER . Lab Sample ID: PBLK03
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1500.D
Level: (low/med) Date Received:
% Moisture: not dec. ______ . Date Analyzed: 12/17/95
GC Column: DB624______ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) . Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06r278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloronietnane 'Bromomethane-Vinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetbene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform • • - • • •1.2-Dichloroethane2-Butanone '1.1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroethene - •Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-L3-DichloropropeneBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene ••••v«f--.1,1,2,2-TetrachloroedianeTolueneChlorobenzeneEthylbenzeneStyrene
1010101010101010101010101010
- 101010101010101010101Q1010
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Page 1 of 2 'FORMIVOA AR3I85U 00021R
IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION in
1
VBLK03
Project No.: A674-S Site: Location: Group:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec.
Lab Sample ID: PBLK03
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:\
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
0 m+ p-Xylenes1330-20-7 o-xylene
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IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH Contract: EPA REGION III
VBLK03
Project No. A674 Site: _____ Location: •______ Group:
Matrix: (soil/water) WATER Lab Sample ID: PBLK03
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1500.D
Level: (low/med) Date Received:
% Moisture: • not dec. ____' Date Analyzed: 12/17/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) " Soil Aliquot Volume: ____' (uL)
Concentration Units:Number TICs found: 0 ' (ug/L or ug/Kg) ug/L
CAS Number1. • '2.3.4.5. •6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28. .29.30.
Compound Name
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FORMI VOA-TICAR3 I 85 I 6 000 1?
GPO 605-924
ANALYSESQ
Preservative:Yes 0 No D
BOD. AnionsSolids (TSS) (TOS) (SS)
COD. TOC, NutrientsPhenolicsMercuryMetalsCyanideOil and GreaseOrganics GC/MSPriority PollutantsVolatile OrganicsPesticidesMutagenicityBacteriology
TagNa UbSamptoNa
3-1.Oft51.T5
A R 3 I 8 5 I 7
AfOEmiECH
NSULTING GROUPS,
Report Number: A689-S Dase Number: R3181
a. Number of Samples and Date of Sample Receipt: ]•
. /7 water samples were received intact on December IS and 19.1995.
v " '• ' ' * ' ' ' • ' ' " . * * ' *
b. Parameters:
These samples were analyzed for TCL Volatile + Dichlorodifluoromethane.
c. Analytical Techniques: , , , '
Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.
QA/QC's:
The surrogate recoveries of each sample is found on Form II-A. ,The Internal Standard Area counts for eacSample is found on Form VTJI-A, and Initial Calibration results are'found on Form VI-A. Both ContinuinCalibrations and Instrument Tuning Information are located onForm V-A: Data for the Blank and associatesamples are reported on Form "IV-A". The 1811218T68 is reported oh Form HI A and all %R's are within thcontrol limits. ' ' . ' ,, •' . : .
I certify that the data package is in compliance with the terms and conditions of the contract, both technically and fccompleteness, for other than the conditions detailed above. Release of the data, contained in this hard copy data packaghas been authorizedjjby the laboratory manager or his designed, as verified by the following signature.
. Name: Dryyajfr Mehta r.-_ . .,'...:' .;
Tnie: Lab Manaeer
AR3I85I9-
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1S11218T68MSLab Name: CHEMTECH - Contract: US EPA REGION H
Project No.: A689-S Site: _____ Location: _________ Group: ___
Matrix: (soil/water) WATER . Lab Sample ID: O48948MS
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1529.D
Level: (low/med) _________ Date Received: 12/19/95
% Moisture: not dec. 100 Date Analyzed: 12/20/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ____ • (liL)
Concentration Units:CAS No. Compound . . (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-2.67-64-175-15-075-35-475-34-4540-39-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-5
DichlorodifiuoromemaneChloromethane •BromomethaneVinyl ChlorideChloroetfaancMethylenc ChlorideAcetoneCarbon Disulfide1 , 1-DichloFoethene1 , 1-Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichioroethane,2-Butanonc ~ . • - - . - -• - -1,1,1-TrichloroethaneCarbon-TetrachlorideBromodichloromethane1,2-Dichloropropanecis-l,3-DichloroprDpcne
79-01-6 ' Tricoldrjbeaiene~* '*& r* ' ' •124-48-179-00-571-43-2.10061-02-675-25-2108-10-1591-78-6127-18-4 ^79-34-5108-88-3108-90-7100-41-4KXM2-5 '
DibFomochldromethane1,1,2-TrichlotoethaoeBenzene ,,trans-1 , j-uicuioropropene
' Bromofbrm4-Methyl-2-Pentanone24iexanone. .•,.-->•
* -'-•"f_'t ...nl.'f.-i'^jl.a.. a..-'.' - • ' ff- ......,.- >ueinciuoiucuicQC ';*'•'.; - ..14,2 -TettachloroethaneToluene "ChlorobenzeneEmylbenzeneStyrene
10101010101010
. 1054101010 ^1010101010101053 "10104810101010101048481010
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Lab Nam
Project N
Matrix:
Sample \v
Level:
% Moisti
GCColui
SoilExtrj
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH , Contract: US EPA REGION H
o.: A689-S Site: Location:
(soil/water) WATER
t/vol: 5.0 (g/mL) ML
(low/med)
ire: not dec. 100
Lab Sample ID:
SAMPLE NO.
181L218T68MS
Group:
O48948MS
Lab File ID: L1529.D
Date Received:
Date Analyzed:
nn: DB624 ID: 0.53 (mm) Dilution Factor
act Volume: ' . (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/L
/
Page 2 of
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1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION H1811218T68MSD
Project No.: A689-S Site: _____ Location: ____________ Group:
Matrix: (soil/water) WATER . Lab Sample ID: O48948MD
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1530.D
Level: (low/med) ______ Date Received: 12/19/95
% Moisture: not dec. 100 Date Analyzed: 12/20/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-0 -75-35-475-34-4540-59-067-66-3107-06-278-93-3 '71-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1 , LJDichloroethane1,2-Dichloroethene (total)Chloroform •• .1,2-Dichloroe thane
. 2-Butanone .1,1,1-TrichloroethaneCarbon Tetrachloride
• Bromodichloromethane' 1,2-Dichloropropane<&•! ,3-DichloropropeneTrichloroethene .Dibromochloromethane1,1,2-TrichloroethaneBenzene . 'trans-1, 3-DichloropropeneBromofotm4-Methyl-2-Pentanone,2-Hexanone .. . -: ,
127™Io"i4 * , -0*"' _-j nTctlTKinlOrOCtlvrPiff- .»**", '79-34-5 .108-88-3108-90-710O41-4100-42-5
1,1,2,2-TetrachloroethaneToluene .ChlorobenzeneEthylbenzene
• Styrenc
101010101010101052101010101010101010105710105310101010101051521010
UuuuuuU t
• u
uuuuuuuuuu
uuuuuuuu
uU . f
Page 1 of2 FORMIVOA AR3I8522 3/90
1A .SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION H
Project No.: A689-S Site: Location:
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/mL) ML
Level: (low/med)
% Moisture: not dec. 100
Lab Sample ID:
1811218T68MSD
Group:
O48948MD
Lab File ID: L1530.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor.
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
•
0 m+ p-Xylenes1330-20-7 o-xylene
.
' • i
,. ' • • . • •
vlO,10
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.
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.
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12/20/95
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CM09!Page 2 of2
FORMIVOA AR3 18523 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
"•• VBLK01Lab Name: CHEMTECH Contract: US EPA REGION IT
Project No.: A689-S Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER . Lab Sample ID: VBLK01
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1521.D
Level: (low/med) Date Received:
% Moisture:, not dec. 100 Date Analyzed: 12/20/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-4M100-42-5
Dichlorodifluoromethane .. .Chloromethane ' • - ' :BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-DichlOroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform •1 ,2-Dichloroethane2-Butanone ' ' •1,1, 1-TrichloroethaneCarbon TetrachlorideBromodichloromcthanc .1 ,2-Dichloropropanetis-l,3-DichloropropeneTrichloroemene ' '- "Dibromochloromethane ,1,1,2-TrichloroethaneBenzene ,trans-1, 3-DichloropropeneBromoform4-Methyl-2-Pentanone2-Hexanone
"•' Tetrachloroethene .1,1,2,2-TetrachlorocthaneTolueneChlorobenzeneEthylbenzeneStyrene
1010
. 1 010101010101010
. 101010101010101010 .10101010 '1010101010 .1010101010
.uuu .uU'uuuu .uuuuuu-uuuu
, uuu .
-'• U- u
- uuu
•?: :U ' ' • ,•:uuU '
-. uu
Page 1 of 2 • • ' .FORMIVOA AR3I8521* OOW84.
1A .VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab-Name: CHEMTECH . . Contract: US EPA REGION IE
Project N
Matrix:
Sample v
Level:i
% Moisti
fo.: A689-S Site: Location:
(soil/water) WATER
rt/vol: 5.0 (g/mL) ML
(low/med)
are: not dec. 100
Lab Sample ID:
SAMPLE NO.
VBLK01
Group:
VBLK01
LabFileID:L1521.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: ___ (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/L
Page 2 of
0 m-f p-Xylenes1330-20-7 o-xylene
/- - ' '
-
1010 ,
-
• , '•
,
12/20/95
1.0
QUU
FORM I VOA fl R 3 1 8 5 2 5
(uL)
»
>000853/90
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS VBLK01
Lab Name: CHEMTECH_____________________1 Contract: US EPA REGION ffl
Project No. A689 Site: _____ Location: _________ Group:
Matrix: (soil/water) WATER " " Lab Sample ID: VBLK01
Sample wt/vol: 5.0 (g/mL) ML Lab File ID: L1521.Dk
Level: (low/med) ________ Date Received:
% Moisture: not dec. 100 Date Analyzed: 12/20/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: __ 0 ___ (ug/L or ug/Kg) ug/L
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
.
1
RT Est. Cone.
~~~ —
,
Q
•
nft
(
• '<HHQR
FORM I VOA-TIC A R 3 ! 8 5 2 6 3/9°
OEimECH
Report Number: A672-S Dase Number: '_ R3181
a. Number of Samples and Date of Sample Receipt:
19 soil samples were received intact on November 29,30, December 1, and S, 1995.
b. Parameters:f
These samples were analyzed for TCL Volatile + Dichlorodifluoromethane.
c. Analytical Techniques:
Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.
d. QA/QC's:
The surrogate recoveries of each sample is found^on Form II-A. The Internal Standard Area counts for eachSample is found oh Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuingCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatedsamples are reported on Form "IV-A". The 1811127D20 is reported on Form HI A and all %R's are within thecontrol limits. , ,
I certify that the data pcompleteness, for otherhas been authorized bj
~ \<Signature: \
Date:
ickage is in compliance with the terms and conditions of the contract, both technically and forthan the conditions detailed above. Release of the data contained in this hard copy data packagethe laboratory manager or his designed, as verified by the following signatureT~~~ ~^^ ' . ...C )r / ^ - ^ OJame: Diwaiit Mehta
J#& &*Y. Title: LakManager/
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811127D20MSLab Name: CHEMTECH Contract: EPA REGION III
Project No. :• A672-S Site: _______ Location: '_____ Group: ___
Matrix: (soil/water) SOIL Lab Sample ID: O48177
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1424.D
Level: (low/med) LOW Date Received: 11/29/95
% Moisture: not dec. 27 ' Date Analyzed: 12/7/95
GC Column: DB624 ______ ID: 0.53 .(mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64- 1'75-15-075-35-4 -75-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-57941-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-S108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBroniomethaneVinyl ChlorideChloroetliaiieMethyiene ChlorideAcetoneCarbon Disulfide1 . 1 -Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethane2-Butahone1.1,1 -TrichloroethaueCarbon Tetrachloridc .Bromodichloromethane1,2-Dichloropropanecis- 1 ,3-Dichloropropene
. TrichloroetheneDibromochloromethaoe1,1,2-Trichloroediane "Benzenetrans- 1 ,3-DichloropropeneBromofbnn4-Methyl-2-Pentanone2-HcxanoncTetrachloroetnene1,1,2,2-TctrachIoroethane .TolueneChlorobenzeneEthylbenzeneStyrcnc
141414141414
r™j>~~~1489141414141414141414145914147114141414141468531414
UUUuuu
u
uuuuuuuuuu
uu
uuuuuu
uu
Page 1 of 2FORMIVOA 000194 3/90
AR3I8529
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION, HI
Project No.: A672-S Site: Location:
Matrix: (soil/water) SOILi *
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not deq. 27
•Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 6.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. . Compound (ug/L or ug/Kg) ug/Kg
0 m-f- p-Xylenes1330-20-7 o-xylene
'
; l
-'
.
• . ' • ' ' -• • ,
'
1414
•'
-
~~->-
- •:
--
SAMPLE NO. T
1811127D20MS
Group:
048177
L1424.D
11/29/95
12/7/95
1.0
Quu
- •
•
(uL)
Page2of2 ««*»-*»—FORMIVOA 000195 3/90
AR3I8530
1A " SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811127D20MSDLab Name: -CHEMTECH . Contract: EPA REGION III
Project No.: A672-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O48178•
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1425.D
Level: (low/med) LOW . Date Received: 11/29/95
% Moisture: not dec. 27 Date Analyzed: 12/7/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound . (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-3 .74-83-975-0 1-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-579-01-6 :124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41r4100-42-5
DichlorodifluommethaneChloromethaneBromomethaneVinyl ChlorideChloroediane .Metbylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethane2-Butanone . • .'1,1,1 -TrichloroedianeCarbon TetrachlorideBromodichloromcthaue1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetbeneDibromochloromethanc1 , 1 ,2-TrichloroethaneBenzene
. trans-1 ,3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-Hexanone , -
"Tetrachloroethene- . -...• .*-_£1,1,2,2-TetrachloroethaneToluene. > -ChlorobenzeneEthylbenzeneStyrene
1414
: . 14141414
S*4?~1485141414141414 .141414145714146714141414
.:,,..-,,-; ,;l- -t14«- •;,<:,.
1468531414
UU •Uuuu
u-uu
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uu
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Page 1 of 2 _*_».,.-_«FORM I VGA 000198 3/90
AR3I853I
1A .- SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH . , Contract: EPA REGION HI.
Project No.: A672-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 27
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: • (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
1
0 • m+ p-Xylenes1330-20-7 o-xylene
-
•'' ... " • . '
.
1414
•
.
.
1811127D20MSD
Group:
048178
L1425.D
11/29/95
12/7/95
1.0
Quu
--
x
-
(uL)
Page 2 of 2FORMIVOA 3/90
AR3J8532
4 IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01Lab Name: CHEMTECH * Contract: EPA REGION HI
Project No.: A672-S Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL - Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1412.D
Level: (lo\v/med) LOW Date Received:
% Moisture: not dec. 0 Date Analyzed: 12/7/95
GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ___ (uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-2 .67-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-2778-87-510061-01-5 .79-01-6124-48-179-00-571-43-2 '10061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichiorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 , 1 -Dichloroethane1,2-Dichlorocthenc (total)Chloroform1 ,2-Dichlorocthane2-Butanone1,1,1-TrichJoroethane .Carbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans-1, 3-DichloropropeneBromoform4-MethyI-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
101010101010101010101010101010101010101010101010101010101010101010
uuuuuu
. uuuuuuuuuuuuuuuuu
- uuuuuuuuuu
Page 1 of2FORM IVOA 3/90
AR.3I8533 00018?
Lab Narn
Project N
Matrix:
Sample w
Level:
% Moisti
GCColui
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH " <• Contract: " EPA REGlbN ffl
o.: A672-S Site: Location:
(soil/water) SOIL - -
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 0 . , • ' '
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
Tin: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
/
Page 2 of
0 m+ p-Xytenes t •-. .:.,; '.„. ..1330-20-7 o-xylene : ., •' \'-A?
. .. = •' ;
\
- ' •• • , ;*
' - ' '' -i' '">- * . , - - . . -.;..'.--7
*
** " " ' " ""' " . » , , . J", .- 'r,S<-~ ', ' ' "- -* "
• 1 ""',"' ". "•-•- ' * •'"* ' " ' ~* -,"
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'
• . . , .- . . ' . . , - . . -. -* •"' --•-«! V\-J, i;..*"1*". •ji i-t '-V.i '-i ••-• V,.r-r': «~'-V. / t*1 •.. %*.*'**.'
,. '• •: "• «. ,.'•'•'? : •" " .'
: -
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•. , . . • • • • ' '
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~
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:
SAMPLE NO.
VBLK01
Group: .
PBLK01
L1412.D
12/7/95
1,0
QUU
\
(uL)
'2FORM I VGA , 3/90
AR3,I8531* 000183
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH Contract: EPA REGION HI
Project No. A672 Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL ' Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) G_____ Lab File ID: L1412.D
Level: (low/med) LOW Date Received: _____
% Moisture: not dec. ___0____ . Date Analyzed: 12/7/95
GC Column: DB624_______ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: 0____ (ug/L or ug/Kg) ug/Kg
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29.30.
Compound Name
•
- .
RT
.
-
Est. Cone.
~"~-
.
Q
FORM I VOA-TIC 3/90
AR3I8535 000184
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK02Lab Name: CHEMTECH Contract: EPA REGION ffl
Project No.: A672-S Site: _____ Location: _______'' Group:
Matrix: (soil/water) SOIL . Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1428.D
Level: (low/med) LOW Date Received:
% Moisture: not dec. 0 . Date Analyzed: 12/7/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units: •CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-2 .67-64-175-15-075-35-475-344540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061r01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78r6127:18-4.79-34-5108-88-3 .108-90-7100-41-4100-42-5
• Dichlorodi fluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene Chloride
. AcetoneCarbon Disulfide1,1-Dichloroethene1,1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloroprqpanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene •trans-l',3-DichloropropcneBromoform4-Methyl-2-Pcntanone2-HexanoneTettachloroethene v r '1,1,2,2-TetrachloroedianeTolueneChlorobenzene.EmylbenzeneStyrene
101010101010101010101010 '101010101010101010101010101010101010101010
. uuuuuuuu
- uuuuuuuuuuu
• uuuuuuuuuuuuuu
/1R3I8536
Page 1 o f 2 . . .FORM I VGA 3/9°
Lab Nam
Project N
Matrix:
Sample v,
Level:
% Moisti
GCColui
Soil Extr
IAVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH ' Contract: EPA REGION IH
o.: A672-S Site: Location:
(soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 0
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
:nn: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
/
0 m+ p-Xylenes1330-20-7 o-xylene
^
»
" . \
*
f
*
1010
SAMPLE NO.
VBLK02
Group:
PBLK02
L1428.D
12/7/95
1.0
QuU
"~~-
(uL)
Page2of2 FORMIVOA lOj 3/90
AR3I8537
.
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH " Contract: EPA REGION HI
VBLK02
Project No. A672 . Site: • Location: __________ Group:
Matrix: (soil/water) SOIL ' Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1428.D
Level: (low/med) LOW . Date Received:
% Moisture: not dec. ___0___ Date Analyzed: 12/7/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: .______ (uL)
Concentration Units:Number TICs found: 0 (ug/L or ug/Kg) ug/Kg
CAS Number1.2.3.4.5.6.7. '8.9.10.11.12.13. .14.15. •16.17.18.19.20.21.22.23.24.25.26.27.28.29. '30.
Compound Name
,
••
••
.'' '
,
RT
-
Est.Conc.
"~- -
Q
-
FORM I VOA-TIC 000190 3/90
AR3I8538
ctEimECH•4S--L* NGGSGL'P -NC
Report Number: A673-S Dase Number: R3181\
a. Number of Samples and Date of Sample Receipt:_r
19 soil samples were received intact on December 5. 6. 8, and 15. 1995.
b . Parameters: ' - . ' . . . -
These samples were analyzed for TCL Volatile.* Dichlorodifluoromethane.
c. Analytical Techniques: .
Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.
"3. QA/QC's:
The surrogate recoveries of each sample is found on Form II-A. The Internal Standard Area counts for eachSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A, Both ContinuingCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatedsamples are reported on Form "IV-A". The 1811204D52 is reported on Form III A and all %R's are within thecontrol limits.'
I certify that the data package is in compliance with the terms and conditions of the contract, both technically and forcompleteness, for other than the conditions detailed above. Release of the data contained in this hard copy data packagehas been authorized by fhe laboratory manager or his designed, as verified by the following signature.
Name: Pivyaiit Mehta
Title: Lab Manager
000001AR3I85UO
8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: CHEMTECH Contract: EPA REGION III
Project No.: A673-S_____ Site: ______ Location: ______ Group:
Lab File ID (Standard): L1442.D_____ Date Analyzed: 12/8/95
Instrument ID: VQA1____ Time Analyzed: L700
GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N). Y
010203040506070809101112131415161718192021•22
12 HOUR STDUPPER LIMITLOWER LIMIT, SAMPLE
NO.VBLK01181I205D581811205D591811205D601811205D631811205D08 .181 1205D03- I3lfca4 Dfl31811206P021811206D611811204D5218H204D52MS1811204D52MSD
.
ISI (BCM)AREA tt42301:846024211506
373607252697277X3S2750442358762442 IS .2327 vX1 7659S *
RT #9.67
.10/179.17
9.719.800.889.92' • .9.95 "l>.9710.02 .10.05
260056 i 111.03276477 • 10.04IOS5S") » | 10.09230325 • 10.10
1
IS2 (DFB) .AREA #,16550123310024827506
/
1366457,.11)68825,1145151 .1307885108856311940359042416620% *10643621129319810083 *900395
RT M13.8314.3313.33
13.8413,9414.0214.0814.0914.1014.1514.1714.1614.1714.2014.23
IS3 (CBZ)AREA #10921202184240546060
809550667599716112819922685438785056601440408806 *712519
. 752369483455 *5(56126 •*
v
RT '#24.0924.5923.59
24.0724.2024.2724.3124.3024.3324.3724.3924.3724.4024.4324.43
ISI (BCM) - Bromochlorome?haiicIS2 (DFB) - 1,4-DifluorobenzeiieIS3 (CBZ) = Chlorobenzeiie-d5
AREA UPPER LIMIT = +1005? of internal standard area . .AREA LOWER LIMIT =-50% of internal standard areaRT UPPER LIMIT = 4-0.50 minutes of internal standard RTRT LOWER LIMIT = -0.50 minutes of internal standard RT
# Column used to flag values outside QC limits with an asterisk- * Values outside of QC limits. . 0 fl fl f Q ft
Page lofl RD o l o C I 1FORM VIH VGA H n O I O J H I 3/90
' . . . - . 8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: CHEMTECH Contract: EPA REGION IH
Project No.: A673-S_____ Site: ______ Location: _______ Group:
Lab File ID (Standard): L1485.D____ Date Analyzed: 12/16/95
Instrument ID: VOA1 Time Analyzed: 0847
GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N) Y
01020304050607080910111213141516171819202122
12 HOUR STDUPPER LIMITLOWER LIMITSAMPLE
NO.VBLK021811206P02RE1811206D641811206D62181 1206D651811206D661811207D041811213G011811213G021811213G031811214G04 .18U214D67
,
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ISI (BCM)AREA #427211854422213606
- 396408 ,223364 . '3i3i2f.- •.;.351734 .
. 269036249065327359353304242971302404.273829382659 •
."'. • - ' '
" * . ..- - .... -1. +ff •„ .
RT #9.8610.369.36
9.93,,,-IQ.QO .10.0110.02 .10.0710.0910.1110.1110.1310.1610.1310.13 •
IS2 (DFB)AREA #19355453871090967773
1186239791568 *1329994127176112615791364497136551417566721153952120253916430441824922
RT #14.0314.5313.53
14.0514.1314. 1414.17-14.2014.2114.2014.2214.2514.2714.26.14.26
IS3 (CBZ)AREA #13320172664034666009
828539539651 *73519868971774557167980080284011606707004627104381103462U35971
RT #24.2824.7823.78
24.31. 24.3524.3724.3924.4224.4224.4324.4424.4524.4724.4724.47
ISI (BCM) = Bromochloromethaiie . 'IS2 (DFB) - 1,4-DifluorobenzeneIS3 (CBZ) — Chlorobenzeue-dS
AREA UPPER LIMIT. +100$^ofimenial standard areaAREA LOWER LIMTf5= 50% ofimeniai standard areaRT UPPER LIMIT = +0.50 minutes of internal standard RTRT LOWER UMTT = -0.50 minutes of internal standard RT
. i' , . • ~ - - '# Column used to Sag values, outside QC limits with an asterisk* Values outside of QC limits. - '" ftftft T fl *
Page 1 of 1FORMVffl VOA 3/90
1A __ SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION III181L204D52MSD_____ 4.
Project No.: A673-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL - Lab Sample ID: O48322
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1454.D
Level: (low/med) LOW . . Date Received: 12/5/95
% Moisture: not dec. 49 Date Analyzed: 12/9/95
GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: t.O
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-8 ,74-87-374-83-975-01 -475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
Dichlorodi fluorometlianeChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1 -Dichloroetheue1 , 1 -Dichloroethanc1,2-Dichloroethene (total)Chloroform1 ,2-Dichloroethanc2-Butanone '1,1.1 -TrichloroethaneCarbon TetrachloridcBromodichloromethane1 ,2-Dichloropropanecis-1. 3-DichloropropeneTrichloroetheneDibromochloromcthanc1 , 1 ,2-TrichloroethaneBenzene
, trans-1, 3-DichloropropeneBromofonn4-MethyI-2-Pentanone2-HexanoneTetrachloroetnene1,1,2,2-TetrachIoroetbaneTolueneChlorobenzeneEthylbenzeoeStyrene
202020202020202012020202020202020202020%2020110202020202020120842020
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FORM I VGA 3/90AR3I851*3
. • SAMPLEVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION HI18H204D52MSD
Project No.: A673-S Site: ____ Location: ___________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O48322
Sample wt/vol: 5.0 (g/mL) G , Lab File ID: L1454.D
Level: (low/med) . LOW Date Received: 12/5/95
% Moisture: not dec. 49 . Date Analyzed: 12/9/95
GC Column: DB624 ' ID: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: . (uL) Soil Aliquot Volume: (uL)
Concentration Units:CAS No. Compound > (ug/L or ug/Kg) ug/Kg
0 v m+ p-Xylenes1330-20-7'. o-xylene
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FORM I VGA 3/90
1A , SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811204D52MSLab Name: CHEMTECH - Contract: EPA REGION III
Project No.: A673-S Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O48321
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1453.D
Level: (low/med) LOW. Date Received: 12/5/95
% Moisture: not dec. 49 Date Analyzed: 12/9/95
GC Column: DB624___________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: " ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-7 ITS74-87-374-83-975-OM75-00-375-09-267-64-175-15-075-35-475-34-4 -540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-5 ,10061-01r5
79-016.,.124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6
. DichiorodifluoromeuianeChloromethane :BromomethaneVinyl Chloride .ChloroetiianeMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1 . 1 -Dichloroethane1 .2-Dichloroethene (total)Chloroform1,2-Dichlorocihane2-Butanone. 1 . 1 , 1 -TrichloroeihaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanc
. cis-1, 3-Dichloropropene: - TrichloroedieneV;? • ;Dibromochloromethane1 , 1 ,2-TrichloroethaneBenzenetrans- 1 ,3-DichloropropeneBromoform4-Methyl-2-Pentahone2-Hexanone ... '
127-18-4 i e*t oroedie:ne -: :f .-£x. £'.79-34-5 i ....108-88-3108-90-7100-41-4100-42-5
. ! iri,l;2 TetrachjoroedianeTolueneChlorobenzeneEthylbenzeneStyrene
20-20 >
, 20202020202010020202020202020202020
. 90 .202011020202020202011078 <2020
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Page 1 of 2FORM I VOA 3/90
AR3i85l*5
" 1A. VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: EPA REGION HI
Project No.: A673-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 49
Lab Sample ID:
Lab File ID:
Date' Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
>
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12/5/95
12/9/95
1.0
QUU
' f- '
(uL)
0001Page 2 of 2
FORMIVOA 3/90
AR3l.85if6
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01Lab Name: CHEMTECH Contract: EPA REGION III
Project No.: A673-S Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL • Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) G Lab File ID:L1443.D
Level: (low/med) LOW Date Received: _____
% Moisture: not dec. 0 Date Analyzed: • 12/8/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Page 1 of 2
F°RMIVOA AR3I85U7
Soil Extract Volume: ______(uL) Soil Aliquot Volume: _______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-4.79-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoroniedianeChloromethaneBromoniethaneVinyl ChlorideChloroetltaneMethylene ChlorideAcetoneCarbon Disulfide1 . 1 -Dichldroethene1 . 1 -Dichloroethanc1,2-Dichloroethene (total)Chloroform1.2-Dichloroethane2-Butanone-1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1 ,2-DichIoropropanecis- 1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-Trichloroethane -Benzenetrans-1, 3-DichloropropeneBromofbrm4-Methyl-2-Pentanone
. 2-Hexanone- - Tetrachloroethene . * .'
1,1,2,2-Tetrachlorocthane'- Toluene
ChlorobenzeneEmylbenzeneStyrene
101010,1010 •10101010101010101010101010101010101010101010
,101010101010
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Lab Nam
Project N
Matrix:
Sample w
Level:
% Moisn
GCColui
Soil Extr
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: EPA REGION IH
o.: A673-S Site: Location:
(soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 0
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed:
mn: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: (uL)f
Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
0 m+ p'Xylenes1330-20-7 o-xylene
10 - ,10
~~~~-
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: SAMPLE NO. '
VBLK01-%i
Group:
PBLK01
L1443.D
12/8/95
1.0
Q
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Page 2 of 2FORM I VGA - 3/90
AR3I85U8
IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: CHEMTECH * Contract: EPA REGION UI
Project No. A673 Site: _____ Location: _______, Group:
Matrix: (soil/water) SOIL ' Lab Sample ID: PBLK01
Sample wt/vol: 5.0 (g/mL) G____ Lab File ID: L1443.D
Level: (low/med) LOW Date Received: _____
% Moisture: not dec. 0 Date Analyzed: 12/8/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: __ 0 .(ug/L or ug/Kg) ug/Kg
CAS Number1. c2.'3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26. ' .27.28.29.30.
Compound Name.• „.
'
RT Est. Cone.
- ~\
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Q
FORMIVOA-TIC
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK02Lab Name: CHEMTECH Contract: EPA REGION III
Project No.: A673-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL - Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1486.O
Level: (low/med) LOW Date Received: ___
% Moisture: not dec. 0 , Date Analyzed: 12/16/95
. GC Column; DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: _____(uL) Soil Aliquot Volume: ______ (uL)~
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-9 .75-01-475-00-3 .75-09-267-64-175-15-075-35-475.34-4540-59-067-66-3107-06-2 .78 93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48rl79-00-571-43-210061-02-675-25-2108-10-1591r78-6
' DichlorodifluoromethaneChloromethaneBromomedianeViayl Chloride
. ChloroethaneMethylene ChlorideAcetoneCarbon Disulfide '1,1-Dichloroediene1 , 1 -Dichloroethane1,2-Dichloroethene (total).Chloroform1,2-Dichldroethane2-Butanone1 , 1 . 1 -TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropane -
, cis-1, 3-DichloropropeneTricntoroetheneDibromochloromethane1,1,2-TrichloroediancBenzenetrans-1, 3-DichloropropeneBromoform. 4-Methyl-2-Pentanone24Iexanone
l2/T*o*"4 • * ~ * "T "TCtTftCnloroCincnff - • *79-34-5108-88-3108-90-7100-41-4100-42-5
.. 1,1,2,2-TetnichloroethaneToluene. ..ChlorobenzeneEthylbenzeneStyrene
1010 '10101010101010101010101010101010101010101010101010101010101010
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Lab Name
Project N
Matrix: (
Sample w
Level:
% Moistu
GCColur
Soil Extn
Page 2 of
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
j: CHEMTECH Contract: EP A» REGION in
o.: A673-S Site: Location:
soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 0
Lab Sample ID:
Lab File ID:
Date Received:
Date Analyzed: .
un: DB624 ID: 0.53 (mm) Dilution Factor
ict Volume: (uL) . Soil Aliquot Volume:
Concentration Units:CAS No. Compound ~ (ug/L.or ug/Kg) ug/Kg
0 m+ p-Xylenes1330-20-7 o-xylene
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12/16/95
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Lab Name: CHEMTECH Contract: EPA REGION III
VBLK02
Project No. A673___ Site: ' Location: __________ Group:
Matrix: (soil/water) SOIL ; Lab Sample ID: PBLK02
Sample wt/vol: 5.0 (g/mL) G Lab File ID: LI486.D
Level: (low/med) LOW Date Received:
% Moisture: . not dec. 0___ Date Analyzed: 12/16/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ________(uL) ' Soil Aliquot Volume: _____ (uL)
Number TICs found:d: 0
CAS Number1.2.3.4.5.6.7.8.9.10.11.12.13.14. ~15. '.16.17.18.19.20.21.22.23.24.25.26;h "\ •'• ', •27,.28.29.30.
Concentration Units:(ug/L or ug/Kg)
Compound Name.
,
1 • •
V
RT
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Est. Cone.
"
.
Q
000194FORM I VOA-TIC 3/90
AR3I8552
IA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
U8H20SD03"Lab Name: CHEMTECH Contract: EPA REGION III
Project No.: A673-S Site: _____ Location: _________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O48349
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1449.D
Level: (tow/med) LOW Date Received: 12/6/95
% Moisture: not dec. 54 Date Analyzed: 12/8/95
GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CASNo. Compound , (ug/L or ug/Kg) ug/Kg Q
MD03 'J""«-*" • |
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-S10061-01-579-01-6124-48-t79-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethancChloromethaneBromomethane
' Vinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1,1-Dichloroetbene1 , 1-Dichlorocdune
' 1,2-Dichloroethene (total)Chlorofonn1 ,2-Dichloroethane2-Butanone1,1,1-TrichloroethaneCarbon Tetrachioride •Bromodichloromethane1 ,2-Dichloropropane. cis-1, 3-DichloropropeneTrichloroetheneDibromochloromcdutne1 , 1 ,2-TrichloroethaneBenzenetnns- 1. 3-DichloropropeneBromofonn4-Methyl-2-Pentanone2-HexanoneTetnchkHoethene1, 1,2,2-TetnchIoroetittneTolueneChlorobeozeneBthylbenzeneStyrene
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Page 1 of2FORMIVOA 3/90
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*-• • i
a. Number of Samples and Date or Sample Receipt:
3 soil samples were received intact on December 19. 1995.
b. Parameters:
These samples were analyzed for TCL Volatile + Dichlorodifluoromethane.
c. Analytical Techniques:
Samples were purged and analyzed by EPA CLP SOW OLM03.0 Method.
d. QA/QC's:
The surrogate recoveries of each sample is found on Form H-A. The Internal Standard Area counts for eacSample is found on Form VIII-A, and Initial Calibration results are found on Form VI-A. Both ContinuinCalibrations and Instrument Tuning Information are located on Form V-A. Data for the Blank and associatesamples are reported on Form "IV-A". The 1811218D68 is reported on Form HI A and all %R's are within tl' control limits. '
I certify that the data package is in compliance with the terms and conditions of the contract, both technically, and ftcompleteness, for other than the conditions detailed above. Release of the data contained in this hard copy data packaghas been authorized b the laboratory manager or his designed, as verified by the following signature.
Name; Divyajit Mehta
Title* Lab Manacer
0 0001V-.,
flR3!8559 *'"J
8AVOLATILE INTERNAL STANDARD AREA AND RT SUMMARY
Lab Name: CHEMTECH Contract: US EPA REGION
Project No.: A695-S_____ Site: _______ Location: ______ Group:
Lab File ID (Standard): L1538.D_____ Date Analyzed: 12/22/95
Instrument ID: HPS971A . Time Analyzed: 1034
GC Column: DB624 ID: 0.53 (mm) Heated Purge (Y/N) Y
01020304050607080910111213141516171819202122
. .'. .12 HOUR STDUPPER LIMITLOWER LIMITSAMPLE .NO.
VBLK01 ' '••1811218D691811218D221811218D681811218D68MS1811218D68MSD1811218D69RE1811218D68RE'
ISI (BCM)AREA #14585329170672927
128896 ::.v,- 67543'*,8174739794 *51070 *49954 *51685 *32973 *
'•
RT #8.488.987.98
8.508.5,18.488.478.518.48 .8.498.52
IS2(DFB) .AREA' #11990732398146599537
1100764 :563445 ' *:656093357948 *471954 *469587 *454387 .*302625 *
L. •- w * - ,.
RT #12.6713.1712;17
.•-.«12367S3£gS-w.;32a»rr:>.- 12.168 "'12.6812.6812.6712.67
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IS3(CBZ)AREA #930524
' 1861048465262
' 894891•* 403223 •:•:*489752 ,258238 *343078 *361770 *316248 *198248 *
~^ -
RT' #23.0823.5822.58
23.0823.0823.0823.0923.0723.0823.0823.08
ISI (BCM) « Bromocfaloromethane 'IS2 (DFB) = 1,4-DifluorobenzeneIS3 (CBZ) = Chlorobenzene-dS
AREA UPPER LIMIT =? +10056 of internal standard ana. .v .-i, :*:5v7 =v" ,AREA LOWER UMTT•«* -30% of imemal stiidaid area: ; * ' V;"-'-". '* ,RT UPPER LIMIT = +0.50 minuteslof internal standard RTRT LOWER LtMTT = -0.50 minutes of internal standard RT ,
# Column used to flag values outside QC limits with an asterisk -* Values outside of QC limits. 0 00069
Page 1 o f 1 - . - . ' -FORMvmvoA I1R3J8560 3/9°
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
1811218D68MSLab Name: CHEMTECH - Contract: US EPA REGION H
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-5 .71-43-210061-02-675-25-2108-10-1591-78-6
DichlorodifluotomcthancChloromethane; -•• ; - '•.BromomethaneVinyl Chloride ~ChloroethaneMethytene ChlorideAcetoneCarbon Disulfide1,1-Dichloroethene1,1-Dichloroethane1,2-Dichloroethene (total)Chloroform ;1,2-Dichloroethane2-Butanone .'•1,1,1-TrichloroethaneCarbon TetrachlorideBromodichloromethane1,2-Dichloropropanetis-l,3-DichioropropeneTiicWcooethene t:J: 'DibromochloromethaiH. 1,1,2-TrichloroethaneBenzene ,trans-l,3-Dichloropropene
. Bromoform4-Methyl-2-Pentanone2-Hexanone" ..v;
127-184, T«ti3»i ilbnje11iene : ,' ".:- ~.79-34-5108-88-3108-90-7100-41-4100-42-5
1,1,2,2-TetrichloroethaneToluene* .-'ChlorobenzeneEthylbenzeneStyrene
2020
. 2 020202020,2015020202020.20202020202086202011020202020
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UUUUUUUU
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Project No.: A695-S ' Site: _____ Location: __________ Group: ___
Matrix: (soil/water) SOIL . Lab Sample ID: O48951MS
Sample wt/vol: 5.0 (g/mL) G Lab File ID: LJ543.D
Level: (low/med) LOW . ' Date Received: 12/19/95 •
% Moisture: not dec. 51 Date Analyzed: 12/22/95
GC Column: DB624 ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: ______(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q.
00007?Page 1 of2
v FORMIVOA 3/90AR3I856I
Lab Nam
Project N
Matrix:
Sample w
Level:
% Moisti
GCColui
Soil Extr
1A .VOLATILE ORGANICS ANALYSIS DATA SHEET
e: CHEMTECH Contract: US EPA REGION H
o.: A695-S Site: Location: .
(soil/water) SOIL
t/vol: 5.0 (g/mL) G
(low/med) LOW
ire: not dec. 51
Lab Sample ID:
SAMPLE NO.
1811218D68MS
Group:
O48951MS
Lab File ID: L1543.D
Date Received:
Date Analyzed:
inn: DB624 ID: 0.53 (mm) Dilution Factor:
act Volume: • (uL) Soil. Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
0 m-Kp-Xylenes1330-20-7 . o-xylene
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Page 2 of 2FORMIVOA
AR3I8562
1A . SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH Contract: US EPA REGION H1811218D68MSD
Project No.: A695-S Site: _____ Location: __________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: O48951MD
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1544.D
Level: (low/med) LOW Date Received: 12/19/95
% Moisture: not dec. 51 Date Analyzed: 12/22/95
GC Column: DB624_________ ID: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: (uL) Soil Aliquot Volume: ___________ (uL)
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg Q
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067r66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41-4100-42-5
DichlorodifluoromethaneChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Disulfide1 , 1-Dichloroethene1,1-Dichloroethane
. 1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-TrichioroethaneCarbon TetrachlorideBromodichloromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzene
Bromoform4-Methyl-2-Pentanonc2-Hexanone
•» - Tetrachloroethenc1,1,2,2-TetrachloroethaneToluene .ChlorobenzeneEthylbenzencStyrene
20202020202020201602020202020202020202011020201302020202020201301002020
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FORMIVOA 3/90
flR3!8563
1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH - Contract: US EPA REGION H
Project No.: A695-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 51
Lab Sample ID:
1811218D68MSD
Group:
O48951MD
Lab File ID: L1544.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CASNo. Compound (ug/L or ug/Kg) ug/Kg
-0 m+ pOCylenes
1330-20-7 q-xylenc
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12/22/95
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FORM I VGA 3/90
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1A SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET
VBLK01Lab Name: CHEMTECH , ... Contract: US EPA REGION tti
Project No.: A695-S Site: _____ Location: ____________ Group:
Matrix: (soil/water) SOIL . Lab Sample ID: VBLK01
Sample wt/vol: 5.0 (g/mL) G Lab File ID: L1S39.D
Level: (low/med) LJDW_ Date Received: ______
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg Q
% Moisture: not dec. 0 Date Analyzed: 12/22/95
GC Column: DB624 _________ ID: 0.53 (mm) Dilution Factor: 1.0
Soil Extract Volume: __________ ("*-) Soil Aliquot Volume: _______ (uL)
75-71-874-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-4540-59-067-66-3107-06-278-93-371-55-656-23-575-27-478-87-510061-01-579-01-6124-48-179-00-571-43-210061-02-675-25-2 .108-10-1591-78-6127-18-479-34-5108-88-3108-90-7100-41 *100-42-5
DichlorodifluoromethaneChloromethane "BromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetbneCarbon Disulfide1 , 1-Dichloroethene1 , 1 -Dichloroethane1,2-Dichloroethene (total)Chloroform1,2-Dichloroethane2-Butanone1,1, 1-Trichloroe thaneCarbon TetrachlorideBromodichlbromethane1 ,2-Dichloropropanecis-1 ,3-DichloropropeneTrichloroetheneDibromochloromcthane1 , 1 ,2-TrichloroethaneBenzene ,trans-1 ,3-DichloropropeneBromoform4-Methyi-2-Pentanone2-HexanoneTetrachloroethene .1, 1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrene
10101010101010101010101010101010101010io10101010101010101010101010
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Page 1 of 2FORMIVOA H D O I O C C C 3/9°AnJ I 8565
1AVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: CHEMTECH - Contract: US EPA REGION H
Project No.: A695-S Site: Location:
Matrix: (soil/water) SOIL
Sample wt/vol: . 5.0 (g/mL) G
Level: (low/med) LOW
% Moisture: not dec. 0
Lab Sample ID:
SAMPLE NO.t
VBLK01
Group:
VBLK01
Lab File ID: L1539.D
Date Received:
Date Analyzed:
GC Column: DB624 ID: 0.53 (mm) Dilution Factor:
Soil Extract Volume: (uL) Soil Aliquot Volume:
Concentration Units:CAS No. Compound (ug/L or ug/Kg) ug/Kg
Page 2 of
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IE SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS VBLK01
Lab Name: CHEMTECH________________ Contract: US EPA REGION ffl -
Project No. A695 Site: _____ Location: ______________ Group:
Matrix: (soil/water) SOIL Lab Sample ID: VBLK01
Sample wt/vol: 5.0 (g/mL) G____ Lab File ID: L1539.D
Level: (low/med) LOW Date Received: __
% Moisture: not dec. ___0___ Date Analyzed: 12/22/95
GC Column: DB624________ ID: 0.53 (mm) Dilution Factor 1.0
Soil Extract Volume: ________(uL) Soil Aliquot Volume: ______ (uL)
Concentration Units:Number TICs found: ._______ (ug/L or ug/Kg) ug/Kg
CAS Number1.2.3..4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.21.22.23.24.25.26.27.28.29. .30.
Compound Name
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