APPENDIX 3 - California Institute of Technology · Appendix 3 – Spectra Related to Chapter 3 220...

Appendix 3 – Spectra Related to Chapter 3

APPENDIX 3

Spectra Related to Chapter 3:

Construction of Vicinal Tertiary and All-Carbon Quaternary

Stereocenters via Ir-Catalyzed Regio-, Diastereo-, and Enantioselective

Allylic Alkylation and Applications in Sequential Pd-Catalysis

��

l 3) o

d 100a

OPh CO

��

Figure A3.2 Infrared spectrum (thin film/NaCl) of compound 100a.

Figure A3.3 13C NMR (125 MHz, CDCl3) of compound 100a.

��

l 3) o

d 100b

��

Figure A3.6 Infrared spectrum (thin film/NaCl) of compound 100b.

Figure A3.6 13C NMR (125 MHz, CDCl3) of compound 100b.

��

l 3) o

d 100c

��

Figure A3.8 Infrared spectrum (thin film/NaCl) of compound 100c.

Figure A3.9 13C NMR (125 MHz, CDCl3) of compound 100c.

��

l 3) o

d 100d

��

Figure A3.11 Infrared spectrum (thin film/NaCl) of compound 100d.

Figure A3.12 13C NMR (125 MHz, CDCl3) of compound 100d.

��

l 3) o

d 100e

��

Figure A3.14 Infrared spectrum (thin film/NaCl) of compound 100e.

Figure A3.15 13C NMR (125 MHz, CDCl3) of compound 100e.

��

l 3) o

d 100f

��

Figure A3.17 Infrared spectrum (thin film/NaCl) of compound 100f.

Figure A3.18 13C NMR (125 MHz, CDCl3) of compound 100f.

��

l 3) o

d 100g

020406080100120140160180200ppm

Figure A3.20 Infrared spectrum (thin film/NaCl) of compound 100g.

Figure A3.21 13C NMR (125 MHz, CDCl3) of compound 100g.

��

l 3) o

d 100h

��

Figure A3.23 Infrared spectrum (thin film/NaCl) of compound 100h.

Figure A3.24 13C NMR (125 MHz, CDCl3) of compound 100h.

��

l 3) o

d 100i

OPh CO

��

Figure A3.26 Infrared spectrum (thin film/NaCl) of compound 100i.

Figure A3.27 13C NMR (125 MHz, CDCl3) of compound 100i.

��

l 3) o

d 103a

��

Figure A3.29 Infrared spectrum (thin film/NaCl) of compound 103a.

Figure A3.30 13C NMR (125 MHz, CDCl3) of compound 103a.

��

l 3) o

d 103b

OPh CO

��

l 3) o

d 103c

OPh CO

2CH2CH2TMS

020406080100120140160180200220ppm

��

l 3) o

d 103d

OPh CO

��

Figure A3.38 Infrared spectrum (thin film/NaCl) of compound 103d.

Figure A3.39 13C NMR (125 MHz, CDCl3) of compound 103d.

��

l 3) o

d 103e

OOPh CO

��

Figure A3.41 Infrared spectrum (thin film/NaCl) of compound 103e.

Figure A3.42 13C NMR (125 MHz, CDCl3) of compound 103e.

��

l 3) o

d 103f

N BnOPh CO

��

Figure A3.44 Infrared spectrum (thin film/NaCl) of compound 103f.

Figure A3.44 13C NMR (125 MHz, CDCl3) of compound 103f.

l 3) o

020406080100120140160180200220ppm

Figure A3.47 Infrared spectrum (thin film/NaCl) of compound 106a and 107a.

Figure A3.48 13C NMR (125 MHz, CDCl3) of compound 106a and 107a.

l 3) o

d 106b

020406080100120140160180200220ppm

l 3) o

d 106c

020406080100120140160180200220ppm

0 1 2 3 4 5 6 7 8

f1 (ppm)

-245-all2

l 3) o

d 108.

020406080100120140160180200220ppm

Figure A3.56 Infrared spectrum (thin film/NaCl) of compound 108.

Figure A3.57 13C NMR (125 MHz, CDCl3) of compound 108.

und L14.

PhF 3C

020406080100120140160180200220ppm

126128130132134136138140142144146148ppm

Figure A3.59 Infrared spectrum (thin film/NaCl) of compound L14.

Figure A3.60 13C NMR (125 MHz, C6D6) of compound L14.

und L14.

PhF 3C

d L14.

PhF 3C

und L15.

020406080100120140160180200220ppm

Figure A3.64 Infrared spectrum (thin film/NaCl) of compound L15.

Figure A3.65 13C NMR (125 MHz, C6D6) of compound L15.

d L15.

APPENDIX 3 - California Institute of Technology · Appendix 3 – Spectra Related to Chapter 3 220...

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